CN110146594A - A kind of device and measuring method of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate - Google Patents

A kind of device and measuring method of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate Download PDF

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Publication number
CN110146594A
CN110146594A CN201910489818.7A CN201910489818A CN110146594A CN 110146594 A CN110146594 A CN 110146594A CN 201910489818 A CN201910489818 A CN 201910489818A CN 110146594 A CN110146594 A CN 110146594A
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CN
China
Prior art keywords
coaming plate
probe
fixed block
receiving transducer
pedestal
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Pending
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CN201910489818.7A
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Chinese (zh)
Inventor
李平
范成文
白银
高磊
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Hohai University HHU
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Hohai University HHU
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Priority to CN201910489818.7A priority Critical patent/CN110146594A/en
Publication of CN110146594A publication Critical patent/CN110146594A/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N29/00Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
    • G01N29/02Analysing fluids
    • G01N29/024Analysing fluids by measuring propagation velocity or propagation time of acoustic waves

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  • Physics & Mathematics (AREA)
  • Acoustics & Sound (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Or Analyzing Materials By The Use Of Ultrasonic Waves (AREA)

Abstract

The present invention relates to a kind of devices of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate, including the accommodating chamber for accommodating cement slurry;For fixing the fixed block of ultrasonic probe;Accommodating chamber includes pedestal and coaming plate, and notch is provided on pedestal, and coaming plate is inserted in the notch of pedestal, the cavity body structure of pedestal and coaming plate formation upper end opening;Ultrasonic probe includes transmitting probe and receiving transducer, there are two fixed block is set, respectively correspond fixed transmission probe and receiving transducer, two fixed blocks are relatively arranged on the outside of coaming plate, fixed block is equipped with the through-hole passed through for transmitting probe or receiving transducer, through-hole internal diameter is suitable with transmitting probe or receiving transducer outer diameter, and transmitting probe and receiving transducer are supported to coaming plate after through-hole and contacted with coaming plate.The device is a kind of cement setting hardening rate detection device continuous, efficient, convenient, repeatability is high.

Description

A kind of device and measuring method of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate
Technical field
The present invention relates to a kind of hardening of cement rate determination device more particularly to a kind of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening speed The device and measuring method of rate.
Background technique
Cement is one of the construction material being most widely used, and condensation hardening rate is that investigation cement slurry early hydration is anti- The important indicator of degree is answered, commonly uses coagulation time tester at present to survey the setting time of cement.However it is only capable of surveying with the method Whether examination cement slurry reaches in a flash initial set, final set at certain, for some high-early (strength) cements, condenses hardening rate quickly, difficult To evaluate this process by single initial set, final setting time.Such as when studying cement based patching material, often select early strong Cement, quick-hardening cement etc. are used as raw material, and cement-based material needs are pumped to repairing position.If at this time cannot METHOD FOR CONTINUOUS DETERMINATION cement Condensation hardening rate just not can know that its early hydration response situation, just be unable to control pump time, cement-based material has very much yet It may be hardened in pumping line or not become hardenite for a long time after reaching repairing position.
Summary of the invention
The purpose of the present invention is to provide a kind of device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate, which can not only connect Continuous measurement hardening of cement situation, and avoid probe positions and be not fixed caused error.
The technical solution used in the present invention are as follows: a kind of device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate, including
For accommodating the accommodating chamber of cement slurry;
For fixing the fixed block of ultrasonic probe;
The accommodating chamber includes pedestal and coaming plate, and notch is provided on the pedestal, and the coaming plate is inserted in the slot of the pedestal In mouthful, the cavity body structure of the pedestal and coaming plate formation upper end opening;
The ultrasonic probe includes transmitting probe and receiving transducer, there are two the fixed block is set, respectively corresponds the fixed hair Probe and the receiving transducer are penetrated, two fixed blocks are relatively arranged on the outside of the coaming plate, and the fixed block is equipped with for described The through-hole that transmitting probe or the receiving transducer pass through, the through-hole internal diameter and the transmitting probe or the receiving transducer outer diameter Quite, the transmitting probe and the receiving transducer are supported to the coaming plate after passing through the through-hole and are contacted with the coaming plate.
Further, the coaming plate includes the first horizontal coaming plate and the second horizontal coaming plate being oppositely arranged, and further includes being oppositely arranged The first vertical coaming plate and the second vertical coaming plate, the first horizontal coaming plate, the second horizontal coaming plate, the first vertical coaming plate and the second vertical coaming plate with it is described The cube cavity body structure of pedestal formation upper end opening.
Further, the fixed block is fixedly connected with the coaming plate, and the fixed block is opened up by the side back to coaming plate Through-hole leads to the coaming plate, and the transmitting probe and the receiving transducer include probe body and fixing seat, and the probe is originally Body is fixedly connected with the fixing seat, and the fixing seat is placed in side of the probe body far from transmitting terminal or receiving end, the spy After head ontology is inserted into the through-hole, the fixing seat assembly is installed on the fixed block.
Further, the side of the coaming plate towards through-hole offers and groove, and the groove is built-in with vaseline, described Ultrasonic probe is contacted by the vaseline with the groove after passing through the through-hole.
Further, the pedestal includes bottom plate and position-limit mechanism, and the position-limit mechanism includes limit plate and limited block, institute It states limit plate and limited block and limits the fixed block in the fixed block side, the bottom plate is equipped with for plugging the coaming plate With the notch of the limit plate, the limit plate is inserted in the notch, and the limited block is fixed on the bottom plate.
Further, it is equipped between the coaming plate and the notch and is coated with vaseline.
Further, the pedestal, first longitudinal direction coaming plate, second longitudinal direction coaming plate material be high damping alloy damping material Material.
The invention also discloses a kind of methods using above-mentioned apparatus measurement cement setting hardening rate, include the following steps
Coaming plate is mounted on the base by S01, surrounds the accommodating chamber;
The fixed block is placed in the coaming plate two sides by S02, and the transmitting probe and the receiving transducer are respectively placed in two It is that probe end is contacted with the coaming plate in the through-hole of the fixed block of side;
S03 is poured concrete mortar in the accommodating chamber, opens ultrasonic wave detector, records the propagation time in real time, until water Mud becomes hardenite;
When S04 is according to spacing and ultrasonic transmission between the transmitting probe and the coaming plate contacted with the receiving transducer Between obtain velocity of wave, draw velocity of wave-time graph and simultaneously calculate cement setting hardening rate.
Beneficial effect caused by the present invention include: in the present invention device it is solidifying using Method of Ultrasonic Penetration METHOD FOR CONTINUOUS DETERMINATION cement Hardening rate is tied, detection accuracy is improved, is a kind of cement setting hardening rate detection continuous, efficient, convenient, repeatability is high Device.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the invention patent;
Fig. 2 detects fast gravity die sulphate aluminium cement hardening rate result using the device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate Figure;
In figure, 1, ultrasonic wave detector, 1-1, transmitting probe, 1-2, receiving transducer;2,2-2, fixed block, 2-1, bolt hole lead to Hole;3, coaming plate, 3-1, longitudinal coaming plate, 3-2, lateral coaming plate, 3-2-1, groove, 4, pedestal, 4-1, notch, 4-2, limited block, 4- 3, spacing edge-cut.
Specific embodiment
Further details of explanation is done to the present invention with reference to the accompanying drawings and detailed description, it should be appreciated that The protection scope of the present invention is not limited by the specific implementation manner.
Such as Fig. 1, the present invention relates to a kind of devices of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate, including for accommodating cement slurry The accommodating chamber of body and fixed block 2 for fixing ultrasonic probe;Accommodating chamber includes pedestal 4 and coaming plate 3, is provided with slot on pedestal 4 Mouth 4-1, coaming plate 3 are inserted in the notch 4-1 of pedestal 4, the cavity body structure of pedestal 4 and the formation upper end opening of coaming plate 3, the cavity knot Structure ensure that cement slurry contacts in wherein molding and hardening process with air.
The instrument that hardening of cement rate is detected in the present invention is ultrasound measuring instrument, and ultrasonic probe includes transmitting probe 1-1 With receiving transducer 1-2, there are two fixed block 2 is set, fixed transmission probe 1-1 and receiving transducer 1-2, two fixed blocks 2 are respectively corresponded It is relatively arranged on 3 outside of coaming plate, coaming plate 3 includes the first horizontal coaming plate 3 and the second horizontal coaming plate 3 being oppositely arranged in the present invention, is also wrapped Include the vertical coaming plate 3 of first be oppositely arranged and the second vertical coaming plate 3, the first horizontal coaming plate 3, the second horizontal coaming plate 3, the first vertical coaming plate 3 and Two vertical coaming plates 3 form the cube cavity body structure of upper end opening with pedestal 4.Two fixed blocks 2 are respectively placed in the first horizontal coaming plate 3 and second Horizontal coaming plate 3 generates the variation of relative position, or ultrasound back to the side of cavity in order to prevent between ultrasonic probe and concrete The through-hole 2-2 of perforation is arranged in the variation of detecting location on fixed block 2, and through-hole 2-2 is penetrated through from 2 one side of fixed block to the other side, And leading to coaming plate 3, through-hole 2-2 internal diameter is suitable with transmitting probe 1-1 or receiving transducer 1-2 outer diameter, and transmitting probe 1-1 and reception are visited Head 1-2 is supported to coaming plate 3 after passing through through-hole 2-2 and is contacted with coaming plate 3, is emitted ultrasonic wave by transmitting probe 1-1 in the present invention, is surpassed Sound wave is received after passing through concrete mortar by receiving transducer 1-2, learns concrete hardening degree by detecting velocity of wave, the setting was both The relative position for securing probe and concrete prevents probe minute movement, guarantees result precision and ensure that the easy of probe The easy to clean of disassembly property and concrete block.Through-hole 2-2 internal diameter and probe diameter are 30mm in the present invention, ensure that probe can To be tightly inserted into inside probe cavern.Probe length and through-hole 2-2 length are 52mm, and two probes squeeze into spiral shell with bolt In keyhole 2-1, so that probe can be placed in fixed block 2 and shift in position does not occur.
Fixed block 2 is fixedly connected with coaming plate 3 in the present invention, and assembly installation can be used, and can also will be consolidated using position-limit mechanism Determine the limit of block 2, fixed block 2 leads to coaming plate 3, transmitting probe 1-1 and receiving transducer by opening up through-hole 2-2 back to the side of coaming plate 3 1-2 includes probe body and fixing seat, and probe body is fixedly connected with fixing seat, and fixing seat is placed in probe body far from transmitting The side of end or receiving end, after probe body is inserted into through-hole 2-2, fixing seat assembly is installed on fixed block 2, which prevents from visiting Head is moved along through-hole 2-2 one-dimensional square, is changed the distance between two probes, is influenced measurement accuracy.
In the prior art, vaseline coating thickness is not easy to control, largely effects on ultrasonic detection precision, all in order to be precisely controlled The coating thickness of intellectual circle, in the horizontal coaming plate 3 of coaming plate 3(i.e. first and the second horizontal coaming plate 3) towards the side of through-hole 2-2 offer with it is recessed Slot 3-2-1, groove 3-2-1 diameter are the circular groove 3-2-1 of 3mm, depth 10mm, and with a thickness of 3mm, groove 3-2-1 is interior to be applied coaming plate 3 Full medical ventolin is as couplant, so that probe can tightly be fitted on medical ventolin and emit, receive ultrasonic wave, and Medical ventolin smearing thickness is 1mm, and ultrasonic transmission is relatively sharp accurate.
Pedestal 4 includes bottom plate and position-limit mechanism in the present invention, and fixed block 2 guarantees itself and receiving cavity by position-limit mechanism Relative position, position-limit mechanism include limit plate and limited block 4-2, and limit plate and limited block 4-2 are limited in 2 side of fixed block to be fixed Block 2, bottom plate are equipped with the spacing edge-cut 4-3 for plugging the notch 4-1 of coaming plate 3 and for plugging limit plate, and limit plate plugs In in spacing edge-cut 4-3, limited block 4-2 is fixed on bottom plate, and there are two limited block 4-2 is set, it is remote to be respectively arranged at two fixed blocks 2 Side from receiving cavity, fixed block 2 and coaming plate 3 form the limit of first direction to fixed block 2 relatively, and each fixed block 2 is right Two limit plates are answered, two limit plates are oppositely arranged the limit that second direction is formed to fixed block 2.
Vaseline is coated between coaming plate 3 and notch 4-1, fixed block 2 prevents from surpassing using damping materials such as high damping alloys Sound wave propagates at receiving transducer 1-2 around cement/concrete;Longitudinal coaming plate 3-1 is by the characteristic impedances such as organic glass and cement Material similar in slurries is made, and other materials can be used in transverse direction coaming plate 3-2;4 material of pedestal is that high damping alloy etc. damps material Material prevents ultrasonic wave from propagating at receiving transducer 1-2 around cement.
A method of cement setting hardening rate is measured using above-mentioned apparatus, is included the following steps
Coaming plate 3 is installed on pedestal 4 by S01, surrounds accommodating chamber;
Fixed block 2 is placed in 3 two sides of coaming plate by S02, and transmitting probe 1-1 and receiving transducer 1-2 are respectively placed in the fixation of two sides It is that probe end is contacted with coaming plate 3 in the through-hole 2-2 of block 2;
S03 is poured concrete mortar in accommodating chamber, opens ultrasonic wave detector 1, records the propagation time in real time, until cement As hardenite;
When S04 is according to spacing and ultrasonic transmission between transmitting probe 1-1 and the coaming plate contacted with receiving transducer 1-2 3 Between obtain velocity of wave, draw velocity of wave-time graph and simultaneously calculate cement setting hardening rate.
Coaming plate 3 and hardening of cement body, cleaning plant are unloaded after the completion of detection.
The invention patent is specifically addressed below with reference to measured result shown in Fig. 2.
Test material is fast gravity die sulphate aluminium cement, and result curve is divided into 3 regions: meadow I, rapid growth area II and approximate meadow III., it is apparent that I area's velocity of wave has almost no change, cement/concrete gradually condenses in this stage But and the hardenite of not formed densification, so ultrasonic wave spread speed in slurry-semisolid is slower;And certain of arrival and IIth area Velocity of wave rapid sharp increase when a critical point represents cement with very fast setting rate and develops into hardenite, this critical point Corresponding abscissa value is final setting time (presetting period can traditionally measure);III area's curve is gradually steady but so slightly increases Long, this illustrates that cement still carries out slowly reaction after quick-hardening, and reaction speed is slower and slower, that is, represents this rank Section cement forms intensity in slow hardening.
The above is only the preferred embodiment of the invention patent, it should be pointed out that: for the common skill of the art For art personnel, under the premise of not departing from the invention patent principle, several improvements and modifications can also be made, these improve and Retouching also should be regarded as the scope of protection of the patent of the present invention.
The above is only a preferred embodiment of the present invention, and the present invention is not limited in the content of embodiment.For in this field Technical staff for, can have various change and change within the scope of technical solution of the present invention, made any variation and Change, within that scope of the present invention.

Claims (8)

1. a kind of device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate, it is characterised in that: including
For accommodating the accommodating chamber of cement slurry;
For fixing the fixed block of ultrasonic probe;
The accommodating chamber includes pedestal and coaming plate, and notch is provided on the pedestal, and the coaming plate is inserted in the slot of the pedestal In mouthful, the cavity body structure of the pedestal and coaming plate formation upper end opening;
The ultrasonic probe includes transmitting probe and receiving transducer, there are two the fixed block is set, respectively corresponds the fixed hair Probe and the receiving transducer are penetrated, two fixed blocks are relatively arranged on the outside of the coaming plate, and the fixed block is equipped with for described The through-hole that transmitting probe or the receiving transducer pass through, the through-hole internal diameter and the transmitting probe or the receiving transducer outer diameter Quite, the transmitting probe and the receiving transducer are supported to the coaming plate after passing through the through-hole and are contacted with the coaming plate.
2. the device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate according to claim 1, it is characterised in that: the coaming plate packet The horizontal coaming plate of first be oppositely arranged and the second horizontal coaming plate are included, further includes the first vertical coaming plate and the second vertical coaming plate being oppositely arranged, the One horizontal coaming plate, the second horizontal coaming plate, the first vertical coaming plate and the second vertical coaming plate and the pedestal form the cube cavity knot of upper end opening Structure.
3. the device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate according to claim 1, it is characterised in that: the fixed block It is fixedly connected with the coaming plate, the fixed block opens up through-hole by the side back to coaming plate and leads to the coaming plate, and the transmitting is visited Head and the receiving transducer include probe body and fixing seat, and the probe body is fixedly connected with the fixing seat, described Fixing seat is placed in side of the probe body far from transmitting terminal or receiving end, described solid after the probe body is inserted into the through-hole Reservation assembly is installed on the fixed block.
4. the device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate according to claim 1, it is characterised in that: the coaming plate court It is offered to the side of through-hole and groove, the groove is built-in with vaseline, the ultrasonic probe passes through after passing through the through-hole The vaseline is contacted with the groove.
5. the device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate according to claim 1, it is characterised in that: the pedestal packet Bottom plate and position-limit mechanism are included, the position-limit mechanism includes limit plate and limited block, and the limit plate and limited block are in the fixation Block side limits the fixed block, and the bottom plate is equipped with the notch for plugging the coaming plate and the limit plate, the limit Position plate is inserted in the notch, and the limited block is fixed on the bottom plate.
6. the device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate according to claim 1, it is characterised in that: the coaming plate with Vaseline is coated between the notch.
7. the device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate according to claim 2, it is characterised in that: the pedestal, First longitudinal direction coaming plate, second longitudinal direction coaming plate material be high damping alloy damping material.
8. a kind of method using claim 1 described device measurement cement setting hardening rate, it is characterised in that: including following Step
Coaming plate is mounted on the base by S01, surrounds the accommodating chamber;
The fixed block is placed in the coaming plate two sides by S02, and the transmitting probe and the receiving transducer are respectively placed in two It is that probe end is contacted with the coaming plate in the through-hole of the fixed block of side;
S03 is poured concrete mortar in the accommodating chamber, opens ultrasonic wave detector, records the propagation time in real time, until water Mud becomes hardenite;
When S04 is according to spacing and ultrasonic transmission between the transmitting probe and the coaming plate contacted with the receiving transducer Between obtain velocity of wave, draw velocity of wave-time graph and simultaneously calculate cement setting hardening rate.
CN201910489818.7A 2019-06-06 2019-06-06 A kind of device and measuring method of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate Pending CN110146594A (en)

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CN201910489818.7A CN110146594A (en) 2019-06-06 2019-06-06 A kind of device and measuring method of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate

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Application Number Priority Date Filing Date Title
CN201910489818.7A CN110146594A (en) 2019-06-06 2019-06-06 A kind of device and measuring method of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate

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CN112305074A (en) * 2020-10-28 2021-02-02 济南大学 Piezoelectric ultrasonic device for on-line monitoring cement concrete hydration process
CN114354763A (en) * 2021-12-31 2022-04-15 临沂大学 Ultrasonic array type cement-based material hydration real-time monitoring device and application thereof

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Publication number Priority date Publication date Assignee Title
CN112305074A (en) * 2020-10-28 2021-02-02 济南大学 Piezoelectric ultrasonic device for on-line monitoring cement concrete hydration process
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CN114354763A (en) * 2021-12-31 2022-04-15 临沂大学 Ultrasonic array type cement-based material hydration real-time monitoring device and application thereof
CN114354763B (en) * 2021-12-31 2023-11-10 临沂大学 Ultrasonic array type cement-based material hydration real-time monitoring device and application thereof

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Application publication date: 20190820