CN110146594A - A kind of device and measuring method of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate - Google Patents
A kind of device and measuring method of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate Download PDFInfo
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- CN110146594A CN110146594A CN201910489818.7A CN201910489818A CN110146594A CN 110146594 A CN110146594 A CN 110146594A CN 201910489818 A CN201910489818 A CN 201910489818A CN 110146594 A CN110146594 A CN 110146594A
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- coaming plate
- probe
- fixed block
- receiving transducer
- pedestal
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N29/00—Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
- G01N29/02—Analysing fluids
- G01N29/024—Analysing fluids by measuring propagation velocity or propagation time of acoustic waves
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- Acoustics & Sound (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analyzing Materials By The Use Of Ultrasonic Waves (AREA)
Abstract
The present invention relates to a kind of devices of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate, including the accommodating chamber for accommodating cement slurry;For fixing the fixed block of ultrasonic probe;Accommodating chamber includes pedestal and coaming plate, and notch is provided on pedestal, and coaming plate is inserted in the notch of pedestal, the cavity body structure of pedestal and coaming plate formation upper end opening;Ultrasonic probe includes transmitting probe and receiving transducer, there are two fixed block is set, respectively correspond fixed transmission probe and receiving transducer, two fixed blocks are relatively arranged on the outside of coaming plate, fixed block is equipped with the through-hole passed through for transmitting probe or receiving transducer, through-hole internal diameter is suitable with transmitting probe or receiving transducer outer diameter, and transmitting probe and receiving transducer are supported to coaming plate after through-hole and contacted with coaming plate.The device is a kind of cement setting hardening rate detection device continuous, efficient, convenient, repeatability is high.
Description
Technical field
The present invention relates to a kind of hardening of cement rate determination device more particularly to a kind of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening speed
The device and measuring method of rate.
Background technique
Cement is one of the construction material being most widely used, and condensation hardening rate is that investigation cement slurry early hydration is anti-
The important indicator of degree is answered, commonly uses coagulation time tester at present to survey the setting time of cement.However it is only capable of surveying with the method
Whether examination cement slurry reaches in a flash initial set, final set at certain, for some high-early (strength) cements, condenses hardening rate quickly, difficult
To evaluate this process by single initial set, final setting time.Such as when studying cement based patching material, often select early strong
Cement, quick-hardening cement etc. are used as raw material, and cement-based material needs are pumped to repairing position.If at this time cannot METHOD FOR CONTINUOUS DETERMINATION cement
Condensation hardening rate just not can know that its early hydration response situation, just be unable to control pump time, cement-based material has very much yet
It may be hardened in pumping line or not become hardenite for a long time after reaching repairing position.
Summary of the invention
The purpose of the present invention is to provide a kind of device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate, which can not only connect
Continuous measurement hardening of cement situation, and avoid probe positions and be not fixed caused error.
The technical solution used in the present invention are as follows: a kind of device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate, including
For accommodating the accommodating chamber of cement slurry;
For fixing the fixed block of ultrasonic probe;
The accommodating chamber includes pedestal and coaming plate, and notch is provided on the pedestal, and the coaming plate is inserted in the slot of the pedestal
In mouthful, the cavity body structure of the pedestal and coaming plate formation upper end opening;
The ultrasonic probe includes transmitting probe and receiving transducer, there are two the fixed block is set, respectively corresponds the fixed hair
Probe and the receiving transducer are penetrated, two fixed blocks are relatively arranged on the outside of the coaming plate, and the fixed block is equipped with for described
The through-hole that transmitting probe or the receiving transducer pass through, the through-hole internal diameter and the transmitting probe or the receiving transducer outer diameter
Quite, the transmitting probe and the receiving transducer are supported to the coaming plate after passing through the through-hole and are contacted with the coaming plate.
Further, the coaming plate includes the first horizontal coaming plate and the second horizontal coaming plate being oppositely arranged, and further includes being oppositely arranged
The first vertical coaming plate and the second vertical coaming plate, the first horizontal coaming plate, the second horizontal coaming plate, the first vertical coaming plate and the second vertical coaming plate with it is described
The cube cavity body structure of pedestal formation upper end opening.
Further, the fixed block is fixedly connected with the coaming plate, and the fixed block is opened up by the side back to coaming plate
Through-hole leads to the coaming plate, and the transmitting probe and the receiving transducer include probe body and fixing seat, and the probe is originally
Body is fixedly connected with the fixing seat, and the fixing seat is placed in side of the probe body far from transmitting terminal or receiving end, the spy
After head ontology is inserted into the through-hole, the fixing seat assembly is installed on the fixed block.
Further, the side of the coaming plate towards through-hole offers and groove, and the groove is built-in with vaseline, described
Ultrasonic probe is contacted by the vaseline with the groove after passing through the through-hole.
Further, the pedestal includes bottom plate and position-limit mechanism, and the position-limit mechanism includes limit plate and limited block, institute
It states limit plate and limited block and limits the fixed block in the fixed block side, the bottom plate is equipped with for plugging the coaming plate
With the notch of the limit plate, the limit plate is inserted in the notch, and the limited block is fixed on the bottom plate.
Further, it is equipped between the coaming plate and the notch and is coated with vaseline.
Further, the pedestal, first longitudinal direction coaming plate, second longitudinal direction coaming plate material be high damping alloy damping material
Material.
The invention also discloses a kind of methods using above-mentioned apparatus measurement cement setting hardening rate, include the following steps
Coaming plate is mounted on the base by S01, surrounds the accommodating chamber;
The fixed block is placed in the coaming plate two sides by S02, and the transmitting probe and the receiving transducer are respectively placed in two
It is that probe end is contacted with the coaming plate in the through-hole of the fixed block of side;
S03 is poured concrete mortar in the accommodating chamber, opens ultrasonic wave detector, records the propagation time in real time, until water
Mud becomes hardenite;
When S04 is according to spacing and ultrasonic transmission between the transmitting probe and the coaming plate contacted with the receiving transducer
Between obtain velocity of wave, draw velocity of wave-time graph and simultaneously calculate cement setting hardening rate.
Beneficial effect caused by the present invention include: in the present invention device it is solidifying using Method of Ultrasonic Penetration METHOD FOR CONTINUOUS DETERMINATION cement
Hardening rate is tied, detection accuracy is improved, is a kind of cement setting hardening rate detection continuous, efficient, convenient, repeatability is high
Device.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the invention patent;
Fig. 2 detects fast gravity die sulphate aluminium cement hardening rate result using the device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate
Figure;
In figure, 1, ultrasonic wave detector, 1-1, transmitting probe, 1-2, receiving transducer;2,2-2, fixed block, 2-1, bolt hole lead to
Hole;3, coaming plate, 3-1, longitudinal coaming plate, 3-2, lateral coaming plate, 3-2-1, groove, 4, pedestal, 4-1, notch, 4-2, limited block, 4-
3, spacing edge-cut.
Specific embodiment
Further details of explanation is done to the present invention with reference to the accompanying drawings and detailed description, it should be appreciated that
The protection scope of the present invention is not limited by the specific implementation manner.
Such as Fig. 1, the present invention relates to a kind of devices of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate, including for accommodating cement slurry
The accommodating chamber of body and fixed block 2 for fixing ultrasonic probe;Accommodating chamber includes pedestal 4 and coaming plate 3, is provided with slot on pedestal 4
Mouth 4-1, coaming plate 3 are inserted in the notch 4-1 of pedestal 4, the cavity body structure of pedestal 4 and the formation upper end opening of coaming plate 3, the cavity knot
Structure ensure that cement slurry contacts in wherein molding and hardening process with air.
The instrument that hardening of cement rate is detected in the present invention is ultrasound measuring instrument, and ultrasonic probe includes transmitting probe 1-1
With receiving transducer 1-2, there are two fixed block 2 is set, fixed transmission probe 1-1 and receiving transducer 1-2, two fixed blocks 2 are respectively corresponded
It is relatively arranged on 3 outside of coaming plate, coaming plate 3 includes the first horizontal coaming plate 3 and the second horizontal coaming plate 3 being oppositely arranged in the present invention, is also wrapped
Include the vertical coaming plate 3 of first be oppositely arranged and the second vertical coaming plate 3, the first horizontal coaming plate 3, the second horizontal coaming plate 3, the first vertical coaming plate 3 and
Two vertical coaming plates 3 form the cube cavity body structure of upper end opening with pedestal 4.Two fixed blocks 2 are respectively placed in the first horizontal coaming plate 3 and second
Horizontal coaming plate 3 generates the variation of relative position, or ultrasound back to the side of cavity in order to prevent between ultrasonic probe and concrete
The through-hole 2-2 of perforation is arranged in the variation of detecting location on fixed block 2, and through-hole 2-2 is penetrated through from 2 one side of fixed block to the other side,
And leading to coaming plate 3, through-hole 2-2 internal diameter is suitable with transmitting probe 1-1 or receiving transducer 1-2 outer diameter, and transmitting probe 1-1 and reception are visited
Head 1-2 is supported to coaming plate 3 after passing through through-hole 2-2 and is contacted with coaming plate 3, is emitted ultrasonic wave by transmitting probe 1-1 in the present invention, is surpassed
Sound wave is received after passing through concrete mortar by receiving transducer 1-2, learns concrete hardening degree by detecting velocity of wave, the setting was both
The relative position for securing probe and concrete prevents probe minute movement, guarantees result precision and ensure that the easy of probe
The easy to clean of disassembly property and concrete block.Through-hole 2-2 internal diameter and probe diameter are 30mm in the present invention, ensure that probe can
To be tightly inserted into inside probe cavern.Probe length and through-hole 2-2 length are 52mm, and two probes squeeze into spiral shell with bolt
In keyhole 2-1, so that probe can be placed in fixed block 2 and shift in position does not occur.
Fixed block 2 is fixedly connected with coaming plate 3 in the present invention, and assembly installation can be used, and can also will be consolidated using position-limit mechanism
Determine the limit of block 2, fixed block 2 leads to coaming plate 3, transmitting probe 1-1 and receiving transducer by opening up through-hole 2-2 back to the side of coaming plate 3
1-2 includes probe body and fixing seat, and probe body is fixedly connected with fixing seat, and fixing seat is placed in probe body far from transmitting
The side of end or receiving end, after probe body is inserted into through-hole 2-2, fixing seat assembly is installed on fixed block 2, which prevents from visiting
Head is moved along through-hole 2-2 one-dimensional square, is changed the distance between two probes, is influenced measurement accuracy.
In the prior art, vaseline coating thickness is not easy to control, largely effects on ultrasonic detection precision, all in order to be precisely controlled
The coating thickness of intellectual circle, in the horizontal coaming plate 3 of coaming plate 3(i.e. first and the second horizontal coaming plate 3) towards the side of through-hole 2-2 offer with it is recessed
Slot 3-2-1, groove 3-2-1 diameter are the circular groove 3-2-1 of 3mm, depth 10mm, and with a thickness of 3mm, groove 3-2-1 is interior to be applied coaming plate 3
Full medical ventolin is as couplant, so that probe can tightly be fitted on medical ventolin and emit, receive ultrasonic wave, and
Medical ventolin smearing thickness is 1mm, and ultrasonic transmission is relatively sharp accurate.
Pedestal 4 includes bottom plate and position-limit mechanism in the present invention, and fixed block 2 guarantees itself and receiving cavity by position-limit mechanism
Relative position, position-limit mechanism include limit plate and limited block 4-2, and limit plate and limited block 4-2 are limited in 2 side of fixed block to be fixed
Block 2, bottom plate are equipped with the spacing edge-cut 4-3 for plugging the notch 4-1 of coaming plate 3 and for plugging limit plate, and limit plate plugs
In in spacing edge-cut 4-3, limited block 4-2 is fixed on bottom plate, and there are two limited block 4-2 is set, it is remote to be respectively arranged at two fixed blocks 2
Side from receiving cavity, fixed block 2 and coaming plate 3 form the limit of first direction to fixed block 2 relatively, and each fixed block 2 is right
Two limit plates are answered, two limit plates are oppositely arranged the limit that second direction is formed to fixed block 2.
Vaseline is coated between coaming plate 3 and notch 4-1, fixed block 2 prevents from surpassing using damping materials such as high damping alloys
Sound wave propagates at receiving transducer 1-2 around cement/concrete;Longitudinal coaming plate 3-1 is by the characteristic impedances such as organic glass and cement
Material similar in slurries is made, and other materials can be used in transverse direction coaming plate 3-2;4 material of pedestal is that high damping alloy etc. damps material
Material prevents ultrasonic wave from propagating at receiving transducer 1-2 around cement.
A method of cement setting hardening rate is measured using above-mentioned apparatus, is included the following steps
Coaming plate 3 is installed on pedestal 4 by S01, surrounds accommodating chamber;
Fixed block 2 is placed in 3 two sides of coaming plate by S02, and transmitting probe 1-1 and receiving transducer 1-2 are respectively placed in the fixation of two sides
It is that probe end is contacted with coaming plate 3 in the through-hole 2-2 of block 2;
S03 is poured concrete mortar in accommodating chamber, opens ultrasonic wave detector 1, records the propagation time in real time, until cement
As hardenite;
When S04 is according to spacing and ultrasonic transmission between transmitting probe 1-1 and the coaming plate contacted with receiving transducer 1-2 3
Between obtain velocity of wave, draw velocity of wave-time graph and simultaneously calculate cement setting hardening rate.
Coaming plate 3 and hardening of cement body, cleaning plant are unloaded after the completion of detection.
The invention patent is specifically addressed below with reference to measured result shown in Fig. 2.
Test material is fast gravity die sulphate aluminium cement, and result curve is divided into 3 regions: meadow I, rapid growth area
II and approximate meadow III., it is apparent that I area's velocity of wave has almost no change, cement/concrete gradually condenses in this stage
But and the hardenite of not formed densification, so ultrasonic wave spread speed in slurry-semisolid is slower;And certain of arrival and IIth area
Velocity of wave rapid sharp increase when a critical point represents cement with very fast setting rate and develops into hardenite, this critical point
Corresponding abscissa value is final setting time (presetting period can traditionally measure);III area's curve is gradually steady but so slightly increases
Long, this illustrates that cement still carries out slowly reaction after quick-hardening, and reaction speed is slower and slower, that is, represents this rank
Section cement forms intensity in slow hardening.
The above is only the preferred embodiment of the invention patent, it should be pointed out that: for the common skill of the art
For art personnel, under the premise of not departing from the invention patent principle, several improvements and modifications can also be made, these improve and
Retouching also should be regarded as the scope of protection of the patent of the present invention.
The above is only a preferred embodiment of the present invention, and the present invention is not limited in the content of embodiment.For in this field
Technical staff for, can have various change and change within the scope of technical solution of the present invention, made any variation and
Change, within that scope of the present invention.
Claims (8)
1. a kind of device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate, it is characterised in that: including
For accommodating the accommodating chamber of cement slurry;
For fixing the fixed block of ultrasonic probe;
The accommodating chamber includes pedestal and coaming plate, and notch is provided on the pedestal, and the coaming plate is inserted in the slot of the pedestal
In mouthful, the cavity body structure of the pedestal and coaming plate formation upper end opening;
The ultrasonic probe includes transmitting probe and receiving transducer, there are two the fixed block is set, respectively corresponds the fixed hair
Probe and the receiving transducer are penetrated, two fixed blocks are relatively arranged on the outside of the coaming plate, and the fixed block is equipped with for described
The through-hole that transmitting probe or the receiving transducer pass through, the through-hole internal diameter and the transmitting probe or the receiving transducer outer diameter
Quite, the transmitting probe and the receiving transducer are supported to the coaming plate after passing through the through-hole and are contacted with the coaming plate.
2. the device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate according to claim 1, it is characterised in that: the coaming plate packet
The horizontal coaming plate of first be oppositely arranged and the second horizontal coaming plate are included, further includes the first vertical coaming plate and the second vertical coaming plate being oppositely arranged, the
One horizontal coaming plate, the second horizontal coaming plate, the first vertical coaming plate and the second vertical coaming plate and the pedestal form the cube cavity knot of upper end opening
Structure.
3. the device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate according to claim 1, it is characterised in that: the fixed block
It is fixedly connected with the coaming plate, the fixed block opens up through-hole by the side back to coaming plate and leads to the coaming plate, and the transmitting is visited
Head and the receiving transducer include probe body and fixing seat, and the probe body is fixedly connected with the fixing seat, described
Fixing seat is placed in side of the probe body far from transmitting terminal or receiving end, described solid after the probe body is inserted into the through-hole
Reservation assembly is installed on the fixed block.
4. the device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate according to claim 1, it is characterised in that: the coaming plate court
It is offered to the side of through-hole and groove, the groove is built-in with vaseline, the ultrasonic probe passes through after passing through the through-hole
The vaseline is contacted with the groove.
5. the device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate according to claim 1, it is characterised in that: the pedestal packet
Bottom plate and position-limit mechanism are included, the position-limit mechanism includes limit plate and limited block, and the limit plate and limited block are in the fixation
Block side limits the fixed block, and the bottom plate is equipped with the notch for plugging the coaming plate and the limit plate, the limit
Position plate is inserted in the notch, and the limited block is fixed on the bottom plate.
6. the device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate according to claim 1, it is characterised in that: the coaming plate with
Vaseline is coated between the notch.
7. the device of METHOD FOR CONTINUOUS DETERMINATION cement setting hardening rate according to claim 2, it is characterised in that: the pedestal,
First longitudinal direction coaming plate, second longitudinal direction coaming plate material be high damping alloy damping material.
8. a kind of method using claim 1 described device measurement cement setting hardening rate, it is characterised in that: including following
Step
Coaming plate is mounted on the base by S01, surrounds the accommodating chamber;
The fixed block is placed in the coaming plate two sides by S02, and the transmitting probe and the receiving transducer are respectively placed in two
It is that probe end is contacted with the coaming plate in the through-hole of the fixed block of side;
S03 is poured concrete mortar in the accommodating chamber, opens ultrasonic wave detector, records the propagation time in real time, until water
Mud becomes hardenite;
When S04 is according to spacing and ultrasonic transmission between the transmitting probe and the coaming plate contacted with the receiving transducer
Between obtain velocity of wave, draw velocity of wave-time graph and simultaneously calculate cement setting hardening rate.
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Cited By (2)
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CN112305074A (en) * | 2020-10-28 | 2021-02-02 | 济南大学 | Piezoelectric ultrasonic device for on-line monitoring cement concrete hydration process |
CN114354763A (en) * | 2021-12-31 | 2022-04-15 | 临沂大学 | Ultrasonic array type cement-based material hydration real-time monitoring device and application thereof |
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