CN110141524A - A kind of production method of complex biological fiber face mask substrate material - Google Patents
A kind of production method of complex biological fiber face mask substrate material Download PDFInfo
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- CN110141524A CN110141524A CN201910584969.0A CN201910584969A CN110141524A CN 110141524 A CN110141524 A CN 110141524A CN 201910584969 A CN201910584969 A CN 201910584969A CN 110141524 A CN110141524 A CN 110141524A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/325—Amines
- D06M13/342—Amino-carboxylic acids; Betaines; Aminosulfonic acids; Sulfo-betaines
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/05—Cellulose or derivatives thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/05—Cellulose or derivatives thereof
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/11—Starch or derivatives thereof
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/18—Synthetic fibres consisting of macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/20—Polyalkenes, polymers or copolymers of compounds with alkenyl groups bonded to aromatic groups
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Abstract
The present invention relates to a kind of production methods of complex biological fiber face mask substrate material, comprising the following steps: the preparation of S1, culture solution；S2, filling fermentation disk；S3, acetobacter xylinum inoculation；S4, harvest chankings；S5, cleaning bleaching rinse；S6, mashing is crushed；S7, it sizes mixing: biological fiber slurry, sodium carboxymethylcellulose, hydroxypropul starch, carragheen, sodium alginate, Sodium Polyacrylate, disodium ethylene diamine tetraacetate is mixed in a certain ratio, it is heated to 80~85 DEG C, it stirs evenly, homogeneous, is then cooled to 60~65 DEG C；S8, whitewashing coating；S9, sizing is flattened；S10, drying；S11, shape of face is cut.The present invention has the advantages that the process for saving fragment, the blocky sheet material of biological fiber is first crushed mashing, slurry is sparged on successional coiled material using high-pressure nozzle, then efficient production is realized by the production model of coiled material, increase drying process, make the membrane material generated convenient for storage and transport, is also beneficial to the filling production of downstream Cosmetics Plant.
Description
Technical field
The present invention relates to facial mask production technical field, especially a kind of producer of complex biological fiber face mask substrate material
Method.
Background technique
The biological fiber substrate that skin care item use, the bacteria cellulose generated from acetobacter xylinum fermentation are production lifes
One of fibres facial mask, carrier of eye mask class product.Different from other types of facial mask substrate, base used in Biofibre facial mask
Material is that fermentation comes out in fixed-size plate, so this raw material is blocky sheet material, rather than synthetic fibers or nothing
The coiled material of woven fabric type.Biofibre facial mask substrate traditional processing technology are as follows: culture solution-fermentation disk-chankings-cleaning-fragment-sanction
The shape of face is cut, 1 is had the following deficiencies:, is the static fermentation in fermentation disk due to fermenting, obtained primary raw materials is block-like
Sheet material lacks continuity, so that all production processes of biological fiber membrane material later, cannot be implemented by transmission belt, to make
Big at the amount of labour used, production efficiency is low；2, due to 2-3 centimetres of thickness of this blocky sheet material, the 0.2-0.3 needed greater than facial mask
Millimeter, also wants lateral fragment, which increase production procedures, and cause a large amount of loss in actual use；3, facial mask is selected
Chankings it is very strict, cannot have any flaw, crack, folding line, cavity, stain, uniformity etc. causes to may be used as facial mask raw
The chankings starving of production, price increase.
Summary of the invention
The purpose of the present invention is to overcome the shortcomings of the existing technology, provides a kind of life of complex biological fiber face mask substrate material
Production method.
The purpose of the present invention is achieved through the following technical solutions:
A kind of production method of complex biological fiber face mask substrate material, comprising the following steps:
The preparation of S1, culture solution: in stainless cylinder of steel, it is separately added into water, coconut milk, sucrose, urea, sulphur by a certain percentage
Sour magnesium, stirring are heated to 90 DEG C, keep 20~40min, are cooled to 80 DEG C of heat preservations, spare；
S2, filling fermentation disk: under environment purification, 80 DEG C of culture solution is packed into fermentation disk, sealing, standing is cooled to
40℃；
S3, acetobacter xylinum inoculation: after culture solution is cooled to 40 DEG C in the disk that ferments, the acetobacter xylinum that second incubation is added is female
Then liquid seals, control fermentation temperature between 27~32 DEG C；
S4, harvest chankings: until fermentation disk in liquid be completely absorbed, after 5~7 days, obtain with a thickness of 2~3cm's
Bacteria cellulose chankings；
S5, cleaning bleaching rinse: first being cleaned up bacteria cellulose chankings with water, add chlorine dioxide, and described two
The additional amount of chlorine monoxid is the 4~6% of total amount of liquid, bleaches 48~72h, then by remaining chlorine dioxide rinsed clean, make base
Material reaches edible security level, and meets hygienic standards for cosmetics；
S6, it crushes mashing: the chankings after rinsing being subjected to pelletizing, is then beaten by fiberizer, homogeneous is heated, then exists
In compressed water generation apparatus, the water content in chankings is adjusted to 88~92%, biological fiber slurry is obtained；
S7, it sizes mixing: by biological fiber slurry, sodium carboxymethylcellulose, hydroxypropul starch, carragheen, sodium alginate, poly- third
Olefin(e) acid sodium, disodium ethylene diamine tetraacetate are mixed in a certain ratio, and are heated to 80~85 DEG C, are stirred evenly, then homogeneous is cooled to
60~65 DEG C；
S8, whitewashing coating: being delivered to spray head for the slurry after sizing mixing using metering pump, even spraying be coated on unreel it is poly-
On propylene lining cloth；
S9, flatten sizing: coated coiled material is squeezed by stainless steel rod, flattens sizing, 2.5~3.5m/ of conveying speed
s；
S10, drying: the coiled material of pressing is put into drying unit, is heated to 120~125 DEG C, after 10~15min, coiled material
Moisture be reduced to 30~35% after, winding, sealed with plastic paper；
S11, it cuts shape of face: by cutting machine, the coiled material of winding being cut out into shape of face, the biological fiber face of shape of face will be cut
Film is packed into plastic bag vacuum packing, is protected from light moisture-proof preservation.
Further, in step S1, each raw material of culture solution is made of following parts by weight: 45~55 parts of water, coconut milk 23
Each raw material of culture solution is imported stainless cylinder of steel by~27 parts, 12~18 parts of sucrose, 8~12 parts of urea, 0.1~0.5 part of magnesium sulfate
In after, be stirred with 50~70rpm speed, until uniform.
Further, in step S2, the culture solution of 1600~1700ml is injected into the fermentation having a size of 32cm*23cm*6cm
In disk, preceding preparation of fermenting is carried out.
Further, in step S3, the additional amount of the acetobacter xylinum mother liquor is 70~90ml.
Further, in step S6, when pelletizing, the chankings after rinsing is cut into rectangular of 0.8cm*0.8cm*0.8cm
Grain, is then beaten in stainless steel sander, and in homogenizing process, mixing speed is 1000~2000rpm, stirs 2~4min.
Further, in step S7, each material sized mixing is matched by following parts by weight: biological fiber slurry 80~90
Part, is gathered 0.1~0.2 part of sodium carboxymethylcellulose, 2~5 parts of hydroxypropul starch, 1~3 part of carragheen, 0.3~1 part of sodium alginate
0.3~0.6 part of sodium acrylate, 0.1 part of disodium ethylene diamine tetraacetate；After being heated to 80~85 DEG C, stirred with the speed of 40~80rpm
10~15min is mixed, then rotates 10~20min of homogeneous with the homogeneous head of 2500~3500rpm, then again with the speed of 40~80rpm
Under degree, it is cooled to 60~65 DEG C.
Further, in step S8, the metering pump is stainless steel gear metering pump, and the spray head sprays pressure and is
0.6~1.0MPa.
Further, in step S9, coated coiled material by twice diameter be 600mm and polish after stainless steel rod into
Row squeezes.
Further, in step S10, the drying unit is that tunnel type depressurizes electromagnetic drying device.
Further, in step S11, the cutting machine is four column hydraulic cutters, output pressure 30t/m2。
The invention has the following advantages that
1, the blocky sheet material of biological fiber is first crushed mashing by the process for saving fragment, using high-pressure nozzle by slurry
It sparges on successional coiled material, then realizes efficient production by the production model of coiled material, increase drying process, make
The membrane material of generation is also beneficial to the filling production of downstream Cosmetics Plant convenient for storage and transport.
2, the bacteria cellulose chankings to ferment through acetobacter xylinum, after crushing mashing, in the form of Tofu pudding shape, point
It dissipates and without viscosity, subsequent coating process is carried out and must be added to suspending agent and adhesive etc. to be modified, to reach spray
The effect of painting.
Specific embodiment
Below with reference to embodiment, the present invention will be further described, but protection scope of the present invention is not limited to following institute
It states.
[embodiment 1]:
A kind of production method of complex biological fiber face mask substrate material, comprising the following steps:
The preparation of S1, culture solution: in stainless cylinder of steel, it is separately added into water, coconut milk, sucrose, urea, sulphur by a certain percentage
Sour magnesium, wherein each raw material of culture solution is made of following parts by weight: 55 parts of water, 23 parts of coconut milk, 18 parts of sucrose, 8 parts of urea,
It 0.5 part of magnesium sulfate, is stirred with 50rpm speed to uniform, is heated to 90 DEG C, kept 40min, be cooled to 80 DEG C of heat preservations, it is standby
With；
S2, filling fermentation disk: under environment purification, 1600ml, 80 DEG C of culture solution are packed into having a size of 32cm*23cm*
In the fermentation disk of 6cm, sealing, standing is cooled to 40 DEG C；
S3, acetobacter xylinum inoculation: after culture solution is cooled to 40 DEG C in the disk that ferments, the wooden vinegar bar of 90ml second incubation is added
Then mother bacterial liquid seals, control fermentation temperature at 27 DEG C；
S4, harvest chankings: it until the liquid in fermentation disk is completely absorbed, after 7 days, obtains fine with a thickness of the bacterium of 2cm
Tie up plain chankings；
S5, cleaning bleaching rinse: first being cleaned up bacteria cellulose chankings with water, add chlorine dioxide, and described two
The additional amount of chlorine monoxid is the 6% of total amount of liquid, bleaches 48h, then by remaining chlorine dioxide rinsed clean, reaching substrate can
Edible security level, and meet hygienic standards for cosmetics；
S6, it crushes mashing: the chankings after rinsing being subjected to pelletizing, is cut into the rectangular particle of 0.8cm*0.8cm*0.8cm, so
It is beaten afterwards by stainless steel sander, heats homogeneous, in homogenizing process, mixing speed 2000rpm stirs 2min, then
In compressed water generation apparatus, the water content in chankings is adjusted to 92%, biological fiber slurry is obtained；
S7, it sizes mixing: by 80 parts of biological fiber slurry, 0.2 part of sodium carboxymethylcellulose, 2 parts of hydroxypropul starch, carragheen 3
Part, 0.3 part of sodium alginate, 0.6 part of Sodium Polyacrylate, 0.1 part of disodium ethylene diamine tetraacetate mixed, be heated to 80 DEG C, with
The speed of 40rpm stirs 15min, then with the homogeneous head rotation homogeneous 20min of 2500rpm, then again under the speed of 40rpm,
It is cooled to 65 DEG C；
S8, whitewashing coating: the slurry after sizing mixing is delivered to spray head, even spraying coating using stainless steel gear metering pump
On the polypropylene lining cloth unreeled, it is 0.6MPa that the spray head, which sprays pressure,；
S9, flatten sizing: coated coiled material is squeezed by the stainless steel rod after twice diameter is 600mm and polishes
Pressure flattens sizing, conveying speed 3.5m/s；
S10, drying: the coiled material of pressing is put into tunnel type decompression electromagnetic drying device, is heated to 120 DEG C, 15min
Afterwards, after the moisture of coiled material is reduced to 30%, winding is sealed with plastic paper；
S11, it cuts shape of face: by four column hydraulic cutters, the coiled material of winding being cut out into shape of face, output pressure 30t/
m2, the Biofibre facial mask for cutting shape of face is packed into plastic bag vacuum packing, is protected from light moisture-proof preservation.
[embodiment 2]:
A kind of production method of complex biological fiber face mask substrate material, comprising the following steps:
The preparation of S1, culture solution: in stainless cylinder of steel, it is separately added into water, coconut milk, sucrose, urea, sulphur by a certain percentage
Sour magnesium, wherein each raw material of culture solution is made of following parts by weight: 50 parts of water, 25 parts of coconut milk, 15 parts of sucrose, 10 parts of urea,
It 0.3 part of magnesium sulfate, is stirred with 60rpm speed to uniform, is heated to 90 DEG C, kept 30min, be cooled to 80 DEG C of heat preservations, it is standby
With；
S2, filling fermentation disk: under environment purification, 1650ml, 80 DEG C of culture solution are packed into having a size of 32cm*23cm*
In the fermentation disk of 6cm, sealing, standing is cooled to 40 DEG C；
S3, acetobacter xylinum inoculation: after culture solution is cooled to 40 DEG C in the disk that ferments, the wooden vinegar bar of 80ml second incubation is added
Then mother bacterial liquid seals, control fermentation temperature at 30 DEG C；
S4, harvest chankings: until fermentation disk in liquid be completely absorbed, after 6 days, obtain the bacterium with a thickness of 2.5cm
Cellulose chankings；
S5, cleaning bleaching rinse: first being cleaned up bacteria cellulose chankings with water, add chlorine dioxide, and described two
The additional amount of chlorine monoxid is the 5% of total amount of liquid, bleaches 60h, then by remaining chlorine dioxide rinsed clean, reaching substrate can
Edible security level, and meet hygienic standards for cosmetics；
S6, it crushes mashing: the chankings after rinsing being subjected to pelletizing, is cut into the rectangular particle of 0.8cm*0.8cm*0.8cm, so
It is beaten afterwards by stainless steel sander, heats homogeneous, in homogenizing process, mixing speed 1500rpm stirs 3min, then
In compressed water generation apparatus, the water content in chankings is adjusted to 90%, biological fiber slurry is obtained；
S7, it sizes mixing: by 85 parts of biological fiber slurry, 0.15 part of sodium carboxymethylcellulose, 3.5 parts of hydroxypropul starch, OK a karaoke club
2 parts of glue, 0.6 part of sodium alginate, 0.45 part of Sodium Polyacrylate, 0.1 part of disodium ethylene diamine tetraacetate mixed, be heated to 82
DEG C, 12min is stirred with the speed of 60rpm, then rotate homogeneous 15min with the homogeneous head of 3000rpm, then again with the speed of 60rpm
Under degree, it is cooled to 63 DEG C；
S8, whitewashing coating: the slurry after sizing mixing is delivered to spray head, even spraying coating using stainless steel gear metering pump
On the polypropylene lining cloth unreeled, it is 0.8MPa that the spray head, which sprays pressure,；
S9, flatten sizing: coated coiled material is squeezed by the stainless steel rod after twice diameter is 600mm and polishes
Pressure flattens sizing, conveying speed 3m/s；
S10, drying: the coiled material of pressing is put into tunnel type decompression electromagnetic drying device, is heated to 122 DEG C, 13min
Afterwards, after the moisture of coiled material is reduced to 32%, winding is sealed with plastic paper；
S11, it cuts shape of face: by four column hydraulic cutters, the coiled material of winding being cut out into shape of face, output pressure 30t/
m2, the Biofibre facial mask for cutting shape of face is packed into plastic bag vacuum packing, is protected from light moisture-proof preservation.
[embodiment 3]:
A kind of production method of complex biological fiber face mask substrate material, comprising the following steps:
The preparation of S1, culture solution: in stainless cylinder of steel, it is separately added into water, coconut milk, sucrose, urea, sulphur by a certain percentage
Sour magnesium, wherein each raw material of culture solution is made of following parts by weight: 41 parts of water, 26 parts of coconut milk, 14 parts of sucrose, 11 parts of urea,
It 0.4 part of magnesium sulfate, is stirred with 55rpm speed to uniform, is heated to 90 DEG C, kept 33min, be cooled to 80 DEG C of heat preservations, it is standby
With；
S2, filling fermentation disk: under environment purification, 1700ml, 80 DEG C of culture solution are packed into having a size of 32cm*23cm*
In the fermentation disk of 6cm, sealing, standing is cooled to 40 DEG C；
S3, acetobacter xylinum inoculation: after culture solution is cooled to 40 DEG C in the disk that ferments, the wooden vinegar bar of 85ml second incubation is added
Then mother bacterial liquid seals, control fermentation temperature at 30 DEG C；
S4, harvest chankings: until fermentation disk in liquid be completely absorbed, after 6 days, obtain the bacterium with a thickness of 2.2cm
Cellulose chankings；
S5, cleaning bleaching rinse: first being cleaned up bacteria cellulose chankings with water, add chlorine dioxide, and described two
The additional amount of chlorine monoxid is the 5% of total amount of liquid, bleaches 55h, then by remaining chlorine dioxide rinsed clean, reaching substrate can
Edible security level, and meet hygienic standards for cosmetics；
S6, it crushes mashing: the chankings after rinsing being subjected to pelletizing, is cut into the rectangular particle of 0.8cm*0.8cm*0.8cm, so
It is beaten afterwards by stainless steel sander, heats homogeneous, in homogenizing process, mixing speed 1800rpm stirs 3min, then
In compressed water generation apparatus, the water content in chankings is adjusted to 91%, biological fiber slurry is obtained；
S7, it sizes mixing: by 88 parts of biological fiber slurry, 0.13 part of sodium carboxymethylcellulose, 4 parts of hydroxypropul starch, carragheen 1
Part, 0.7 part of sodium alginate, 0.5 part of Sodium Polyacrylate, 0.1 part of disodium ethylene diamine tetraacetate mixed, be heated to 82 DEG C, with
The speed of 48rpm stirs 13min, then with the homogeneous head rotation homogeneous 14min of 3000rpm, then again under the speed of 70rpm,
It is cooled to 62 DEG C；
S8, whitewashing coating: the slurry after sizing mixing is delivered to spray head, even spraying coating using stainless steel gear metering pump
On the polypropylene lining cloth unreeled, it is 0.9MPa that the spray head, which sprays pressure,；
S9, flatten sizing: coated coiled material is squeezed by the stainless steel rod after twice diameter is 600mm and polishes
Pressure flattens sizing, conveying speed 2.9m/s；
S10, drying: the coiled material of pressing is put into tunnel type decompression electromagnetic drying device, is heated to 120 DEG C, 14min
Afterwards, after the moisture of coiled material is reduced to 34%, winding is sealed with plastic paper；
S11, it cuts shape of face: by four column hydraulic cutters, the coiled material of winding being cut out into shape of face, output pressure 30t/
m2, the Biofibre facial mask for cutting shape of face is packed into plastic bag vacuum packing, is protected from light moisture-proof preservation.
[embodiment 4]:
A kind of production method of complex biological fiber face mask substrate material, comprising the following steps:
The preparation of S1, culture solution: in stainless cylinder of steel, it is separately added into water, coconut milk, sucrose, urea, sulphur by a certain percentage
Sour magnesium, wherein each raw material of culture solution is made of following parts by weight: 45 parts of water, 27 parts of coconut milk, 12 parts of sucrose, 12 parts of urea,
It 0.1 part of magnesium sulfate, is stirred with 70rpm speed to uniform, is heated to 90 DEG C, kept 20min, be cooled to 80 DEG C of heat preservations, it is standby
With；
S2, filling fermentation disk: under environment purification, 1700ml, 80 DEG C of culture solution are packed into having a size of 32cm*23cm*
In the fermentation disk of 6cm, sealing, standing is cooled to 40 DEG C；
S3, acetobacter xylinum inoculation: after culture solution is cooled to 40 DEG C in the disk that ferments, the wooden vinegar bar of 70ml second incubation is added
Then mother bacterial liquid seals, control fermentation temperature between 32 DEG C；
S4, harvest chankings: it until the liquid in fermentation disk is completely absorbed, after 5 days, obtains fine with a thickness of the bacterium of 3cm
Tie up plain chankings；
S5, cleaning bleaching rinse: first being cleaned up bacteria cellulose chankings with water, add chlorine dioxide, and described two
The additional amount of chlorine monoxid is the 4% of total amount of liquid, bleaches 72h, then by remaining chlorine dioxide rinsed clean, reaching substrate can
Edible security level, and meet hygienic standards for cosmetics；
S6, it crushes mashing: the chankings after rinsing being subjected to pelletizing, is cut into the rectangular particle of 0.8cm*0.8cm*0.8cm, so
It is beaten afterwards by stainless steel sander, heats homogeneous, in homogenizing process, mixing speed 1000rpm stirs 4min, then
In compressed water generation apparatus, the water content in chankings is adjusted to 88%, biological fiber slurry is obtained；
S7, it sizes mixing: by 90 parts of biological fiber slurry, 0.1 part of sodium carboxymethylcellulose, 5 parts of hydroxypropul starch, carragheen 1
Part, 1 part of sodium alginate, 0.3 part of Sodium Polyacrylate, 0.1 part of disodium ethylene diamine tetraacetate mixed, be heated to 85 DEG C, with
The speed of 40rpm stirs 10min, then with the homogeneous head rotation homogeneous 10min of 3500rpm, then again under the speed of 80rpm,
It is cooled to 60 DEG C；
S8, whitewashing coating: the slurry after sizing mixing is delivered to spray head, even spraying coating using stainless steel gear metering pump
On the polypropylene lining cloth unreeled, it is 1.0MPa that the spray head, which sprays pressure,；
S9, flatten sizing: coated coiled material is squeezed by the stainless steel rod after twice diameter is 600mm and polishes
Pressure flattens sizing, conveying speed 2.5m/s；
S10, drying: the coiled material of pressing is put into tunnel type decompression electromagnetic drying device, is heated to 125 DEG C, 10min
Afterwards, after the moisture of coiled material is reduced to 35%, winding is sealed with plastic paper；
S11, it cuts shape of face: by four column hydraulic cutters, the coiled material of winding being cut out into shape of face, output pressure 30t/
m2, the Biofibre facial mask for cutting shape of face is packed into plastic bag vacuum packing, is protected from light moisture-proof preservation.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (10)
1. a kind of production method of complex biological fiber face mask substrate material, it is characterised in that: the following steps are included:
The preparation of S1, culture solution: in stainless cylinder of steel, it is separately added into water, coconut milk, sucrose, urea, sulfuric acid by a certain percentage
Magnesium, stirring are heated to 90 DEG C, keep 20~40min, are cooled to 80 DEG C of heat preservations, spare；
S2, filling fermentation disk: under environment purification, 80 DEG C of culture solution is packed into fermentation disk, sealing, standing is cooled to 40
℃；
S3, acetobacter xylinum inoculation: after culture solution is cooled to 40 DEG C in the disk that ferments, being added the acetobacter xylinum mother liquor of second incubation,
Then it seals, controls fermentation temperature between 27~32 DEG C；
S4, harvest chankings: until fermentation disk in liquid be completely absorbed, after 5~7 days, obtain the bacterium with a thickness of 2~3cm
Cellulose chankings；
S5, cleaning bleaching rinse: first bacteria cellulose chankings is cleaned up with water, adds chlorine dioxide, the titanium dioxide
The additional amount of chlorine is the 4~6% of total amount of liquid, bleaches 48~72h, then by remaining chlorine dioxide rinsed clean, reach substrate
To edible security level, and meet hygienic standards for cosmetics；
S6, it crushes mashing: the chankings after rinsing being subjected to pelletizing, is then beaten by fiberizer, homogeneous is heated, then in pressure water
In device, the water content in chankings is adjusted to 88~92%, biological fiber slurry is obtained；
S7, it sizes mixing: by biological fiber slurry, sodium carboxymethylcellulose, hydroxypropul starch, carragheen, sodium alginate, polyacrylic acid
Sodium, disodium ethylene diamine tetraacetate are mixed in a certain ratio, and are heated to 80~85 DEG C, are stirred evenly, homogeneous, then it is cooled to 60~
65℃；
S8, whitewashing coating: the slurry after sizing mixing is delivered to spray head using metering pump, even spraying is coated on the polypropylene unreeled
On lining cloth；
S9, flatten sizing: coated coiled material is squeezed by stainless steel rod, flattens sizing, 2.5~3.5m/s of conveying speed；
S10, drying: the coiled material of pressing is put into drying unit, is heated to 120~125 DEG C, after 10~15min, the water of coiled material
Divide after being reduced to 30~35%, winding is sealed with plastic paper；
S11, it cuts shape of face: by cutting machine, the coiled material of winding being cut out into shape of face, the Biofibre facial mask for cutting shape of face is filled
Enter plastic bag vacuum packing, is protected from light moisture-proof preservation.
2. a kind of production method of complex biological fiber face mask substrate material according to claim 1, it is characterised in that: step S1
In, each raw material of culture solution is made of following parts by weight: 45~55 parts of water, 23~27 parts of coconut milk, 12~18 parts of sucrose, urea
8~12 parts, 0.1~0.5 part of magnesium sulfate, after each raw material of culture solution is imported in stainless cylinder of steel, with the progress of 50~70rpm speed
Stirring, until uniform.
3. a kind of production method of complex biological fiber face mask substrate material according to claim 2, it is characterised in that: step S2
In, by fermentation disk of the culture solution injection having a size of 32cm*23cm*6cm of 1600~1700ml, carry out preceding preparation of fermenting.
4. a kind of production method of complex biological fiber face mask substrate material according to claim 3, it is characterised in that: step S3
In, the additional amount of the acetobacter xylinum mother liquor is 70~90ml.
5. a kind of production method of complex biological fiber face mask substrate material according to claim 4, it is characterised in that: step S6
In, when pelletizing, the chankings after rinsing is cut into the rectangular particle of 0.8cm*0.8cm*0.8cm, then in stainless steel sander
Mashing, in homogenizing process, mixing speed is 1000~2000rpm, stirs 2~4min.
6. a kind of production method of complex biological fiber face mask substrate material according to claim 5, it is characterised in that: step S7
In, each material sized mixing is matched by following parts by weight: 80~90 parts of biological fiber slurry, sodium carboxymethylcellulose 0.1~
0.2 part, 2~5 parts of hydroxypropul starch, 1~3 part of carragheen, 0.3~1 part of sodium alginate, 0.3~0.6 part of Sodium Polyacrylate, second
0.1 part of edetate disodium；After being heated to 80~85 DEG C, 10~15min is stirred with the speed of 40~80rpm, then with 2500
The homogeneous head of~3500rpm rotates 10~20min of homogeneous, then again to be cooled to 60~65 DEG C under the speed of 40~80rpm.
7. a kind of production method of complex biological fiber face mask substrate material according to claim 6, it is characterised in that: step S8
In, the metering pump is stainless steel gear metering pump, and it is 0.6~1.0MPa that the spray head, which sprays pressure,.
8. a kind of production method of complex biological fiber face mask substrate material according to claim 7, it is characterised in that: step S9
In, stainless steel rod of the coated coiled material after twice diameter is 600mm and polishes is squeezed.
9. a kind of production method of complex biological fiber face mask substrate material according to claim 8, it is characterised in that: step
In S10, the drying unit is that tunnel type depressurizes electromagnetic drying device.
10. a kind of production method of complex biological fiber face mask substrate material according to claim 9, it is characterised in that: step
In S11, the cutting machine is four column hydraulic cutters, output pressure 30t/m2。
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| CN106214499A (en) * | 2016-08-26 | 2016-12-14 | 陈雄 | A kind of preparation method of face mask substrate material |
| CN109718193A (en) * | 2017-10-26 | 2019-05-07 | 王金涛 | A kind of biology cellulose facial mask and preparation method thereof |
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| CN101530749A (en) * | 2009-03-05 | 2009-09-16 | 海南大学 | Method for preparing carboxymethyl cellulose and bacterial cellulose composite material |
| CN106214499A (en) * | 2016-08-26 | 2016-12-14 | 陈雄 | A kind of preparation method of face mask substrate material |
| CN109718193A (en) * | 2017-10-26 | 2019-05-07 | 王金涛 | A kind of biology cellulose facial mask and preparation method thereof |
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Application publication date: 20190820 |