CN110100877A - A kind of Halogen boils the preservation method of Spiced beef - Google Patents

A kind of Halogen boils the preservation method of Spiced beef Download PDF

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Publication number
CN110100877A
CN110100877A CN201910522962.6A CN201910522962A CN110100877A CN 110100877 A CN110100877 A CN 110100877A CN 201910522962 A CN201910522962 A CN 201910522962A CN 110100877 A CN110100877 A CN 110100877A
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China
Prior art keywords
halogen
spiced beef
antistaling agent
boils
thick gravy
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
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CN201910522962.6A
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Chinese (zh)
Inventor
蔡华珍
孙红引
陈梦南
李文超
杜庆飞
邢明言
周頔
龙门
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Chuzhou University
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Chuzhou University
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Priority to CN201910522962.6A priority Critical patent/CN110100877A/en
Publication of CN110100877A publication Critical patent/CN110100877A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
    • A23B4/00General methods for preserving meat, sausages, fish or fish products
    • A23B4/005Preserving by heating
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
    • A23B4/00General methods for preserving meat, sausages, fish or fish products
    • A23B4/015Preserving by irradiation or electric treatment without heating effect
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
    • A23B4/00General methods for preserving meat, sausages, fish or fish products
    • A23B4/14Preserving with chemicals not covered by groups A23B4/02 or A23B4/12
    • A23B4/18Preserving with chemicals not covered by groups A23B4/02 or A23B4/12 in the form of liquids or solids
    • A23B4/20Organic compounds; Microorganisms; Enzymes
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L13/00Meat products; Meat meal; Preparation or treatment thereof
    • A23L13/70Tenderised or flavoured meat pieces; Macerating or marinating solutions specially adapted therefor
    • A23L13/72Tenderised or flavoured meat pieces; Macerating or marinating solutions specially adapted therefor using additives, e.g. by injection of solutions
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/125Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives containing carbohydrate syrups; containing sugars; containing sugar alcohols; containing starch hydrolysates
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/90Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in food processing or handling, e.g. food conservation

Abstract

The invention discloses the preservation method that a kind of Halogen boils Spiced beef, preservation methods are as follows: will first prepare the spice that thick gravy uses and uses microwave disinfection, then prepares concentration thick gravy;The preparation flow of Spiced beef being boiled according to Halogen: pretreatment of raw material, → either shallow is dry → pickle → steams → cools down → packaging → ultrasonic sterilization → finished product, natural composite antistaling agent is added in marinated link, in conjunction with the secondary cold sterilization of ultrasonic wave, reaches and extend fresh-keeping purpose.Natural composite antistaling agent is made of chitosan oligosaccharide, epsilon-polylysine and tea polyphenols, the Halogen handled through the synthetical preservation technology of natural composite antistaling agent combination microwave disinfection spice and the secondary cold sterilization of ultrasonic wave boils Spiced beef, shelf life is up to 130-136d at 25 DEG C, Halogen boils Spiced beef after fresh-keeping, the aromatic strongly fragrant, color stability of halogen, due to using cold sterilization, product nutrition is preferably retained, quality and in good taste, the addition of chitosan oligosaccharide, not only there is preservation, also there is certain health care effect.

Description

A kind of Halogen boils the preservation method of Spiced beef
Technical field
The present invention relates to the preservation methods that a kind of Halogen boils Spiced beef, belong to food preservation technical field.
Background technique
Halogen boils Spiced beef and mainly obtains halogen meat flavor by the way of thick gravy injection, using toast or steam, low temperature etc. Mode processing and fabricating is the improvement to traditional stew in soy sauce technique, has well solved the peace such as heterocycle amine content increase in old halogen stew in soy sauce Full problem, compared with traditional Spiced beef, Halogen boils that Spiced beef full of nutrition, color stability, in good taste, yield rate is higher.But Since Halogen boils, Spiced beef is full of nutrition, moisture content is higher, and microorganism is easy growth and breeding, affects the shelf life of product.
In food preservation research, people use many methods, are summed up and are broadly divided into two major classes, one kind is fresh-keeping Agent is fresh-keeping, and one kind is that technique is fresh-keeping.Fresh-keeping antistaling agent is a kind of common preservation method in food industry, can effective bacteria reducing, Extend shelf life of products, is conducive to keep the original nutrition of product and flavor.Meat industry, 2017 (04):, will in mono- text of 28-34 The spiced beef that preservative is added is compared with vacuum group, controlled atmosphere group, and the bacterium colony that discovery preservative can effectively reduce spiced beef is total Several and TBARS value.The fresh-keeping main method of technique has sterilization fresh-keeping, fresh-keeping, fresh-keeping storing.Wherein sterilization is protected It is fresh and be divided into thermal sterilization and cold sterilization.Food industry science and technology, 2013,34 (17): by two kinds of sterilization modes in mono- text of 354-359. Comparison, although discovery thermal sterilization technology can effectively inhibit microbial reproduction, high temperature can cause the quality of meat product very big It destroys, the soft rotten, nutritive loss of meat, flavor are deteriorated etc..Therefore, single preservation technology remains shortcoming in one aspect or not Foot, according to hurdle theory, it is fresh-keeping that it is fresh-keeping, which to be applied to stewed meat products, for two or more comprehensive preservation mode The trend of technology development.
Summary of the invention
It is an object of that present invention to provide the comprehensive fresh-keeping methods that a kind of Halogen boils Spiced beef, provide a kind of with preferable The natural composite antistaling agent and its preservation method of antibacterial, anti-oxidant and certain shelf effect, meet the actual needs.
To solve the above problems, the technical solution used in the present invention is as follows:
A kind of Halogen boils Spiced beef preservation method, comprising the following steps:
Step 1, spice sterilization;
Step 2 prepares antistaling agent;
Step 3 adds antistaling agent in pickling;
Product after step 4, packaging is using ultrasonic pasteurize.
Preferably, the spice method for disinfection is first to soak spice, killed using power 700W-850W microwave Bacterium 10min-15min.
Preferably, the weight percent composition are as follows: chitosan oligosaccharide 0.30-0.45%, epsilon-polylysine 0.25- 0.35%, tea polyphenols 0.20-0.30%, surplus are concentration thick gravy liquid.
Preferably, it is described it is marinated in addition antistaling agent method are as follows: weigh 4% amount by meat and weigh concentration thick gravy liquid, press than Epsilon-polylysine, tea polyphenols, chitosan oligosaccharide are added in concentration thick gravy liquid by example, after mixing, are injected in beef, then are poured into true Tumbling is all absorbed by meat to thick gravy in empty tumbler, meat piece uniform color, tumbling time 40-60min.
Preferably, it is described ultrasound pasteurize, be will about 8 aged beefs vacuum packaging after, be placed in ultrasonic drilling machine, adopt With 60-80 DEG C of power 2200-2800W, temperature, 20-30min is sterilized, then flowing water is cooled to room temperature.
For the present invention compared with existing other preservation technologies, implementation result of the invention is as follows:
Halogen after the present invention is fresh-keeping, which boils Spiced beef, has the characteristics that the aromatic strongly fragrant, color stability of halogen, and selected antistaling agent ε-is poly- Lysine is native trophism biological preservative, and tea polyphenols are the naturals extracted from tealeaves, and chitosan oligosaccharide belongs to newly Resource raw-food material not only has preservation, also has certain health care effect, further, since killing using low temperature Bacterium, product nutrition are preferably retained, quality and in good taste.
Detailed description of the invention
Fig. 1 is the Arrhenius curve graph that Halogen of the present invention boils the variation of Spiced beef TVB-N value.
Specific embodiment
Illustrate the contents of the present invention below in conjunction with specific embodiments.
Embodiment 1
Halogen boils the preservation method of Spiced beef, comprising the following steps:
(1) spice method for disinfection is first to soak spice, using power 700W microwave disinfection 15min;
(2) antistaling agent weight percent forms are as follows: chitosan oligosaccharide 0.30%, epsilon-polylysine 0.30%, and tea polyphenols 0.25%, Surplus is concentration thick gravy liquid;
(3) method of addition antistaling agent is in pickling, and weighs 4% amount by meat and weighs concentration thick gravy liquid, gathers ε-rely in proportion Propylhomoserin, tea polyphenols, chitosan oligosaccharide are added in concentration thick gravy liquid, after mixing, are injected in beef, then pour into vacuum tumbler Tumbling is all absorbed by meat to thick gravy, meat piece uniform color, about 40min;
(4) Pasteur's ultrasonic sterilization, be will about 8 aged beefs vacuum packaging after, be placed in ultrasonic drilling machine, using power 2200W, temperature 60 C sterilize 20min, and then flowing water is cooled to room temperature.
Embodiment 2
Halogen boils the preservation method of Spiced beef, comprising the following steps:
(1) spice method for disinfection is first to soak spice, using power 750W microwave disinfection 12min;
(2) antistaling agent weight percent forms are as follows: chitosan oligosaccharide 0.35%, epsilon-polylysine 0.30%, and tea polyphenols 0.25%, Surplus is concentration thick gravy liquid;
(3) method of addition antistaling agent is in pickling, and weighs 4% amount by meat and weighs concentration thick gravy liquid, gathers ε-rely in proportion Propylhomoserin, tea polyphenols, chitosan oligosaccharide are added in concentration thick gravy liquid, after mixing, are injected in beef, then pour into vacuum tumbler Tumbling is all absorbed by meat to thick gravy, meat piece uniform color, about 40-60min;
(4) Pasteur's ultrasonic sterilization, be will about 7 aged beefs vacuum packaging after, be placed in ultrasonic drilling machine, using power 2500W, temperature 70 C sterilize 25min, and then flowing water is cooled to room temperature.
Embodiment 3
Halogen boils the preservation method of Spiced beef, comprising the following steps:
(1) spice method for disinfection is first to soak spice, using power 800W microwave disinfection 14min;
(2) antistaling agent weight percent forms are as follows: chitosan oligosaccharide 0.45%, epsilon-polylysine 0.30%, and tea polyphenols 0.30%, Surplus is concentration thick gravy liquid;
(3) method of addition antistaling agent is in pickling, and weighs 4% amount by meat and weighs concentration thick gravy liquid, gathers ε-rely in proportion Propylhomoserin, tea polyphenols, chitosan oligosaccharide are added in concentration thick gravy liquid, after mixing, are injected in beef, then pour into vacuum tumbler Tumbling is all absorbed by meat to thick gravy, meat piece uniform color, about 40-60min;
(4) Pasteur's ultrasonic sterilization, be will about 7 aged beefs vacuum packaging after, be placed in ultrasonic drilling machine, using power 80 DEG C of 2800W, temperature sterilize 30min, and then flowing water is cooled to room temperature.
Embodiment 4
Halogen boils the preservation method of Spiced beef, comprising the following steps:
(1) spice method for disinfection is first to soak spice, using power 850W microwave disinfection 10min;
(2) antistaling agent weight percent forms are as follows: chitosan oligosaccharide 0.45%, epsilon-polylysine 0.35%, and tea polyphenols 0.30%, Surplus is concentration thick gravy liquid;
(3) method of addition antistaling agent is in pickling, and weighs 4% amount by meat and weighs concentration thick gravy liquid, gathers ε-rely in proportion Propylhomoserin, tea polyphenols, chitosan oligosaccharide are added in concentration thick gravy liquid, after mixing, are injected in beef, then pour into vacuum tumbler Tumbling is all absorbed by meat to thick gravy, meat piece uniform color, about 60min;
(4) Pasteur's ultrasonic sterilization, be will about 7 aged beefs vacuum packaging after, be placed in ultrasonic drilling machine, using power 80 DEG C of 2700W, temperature sterilize 25min, and then flowing water is cooled to room temperature.
Embodiment 5
Halogen boils the preservation method of Spiced beef, comprising the following steps:
(1) spice method for disinfection is first to soak spice, using power 800W microwave disinfection 10min;
(2) antistaling agent weight percent forms are as follows: chitosan oligosaccharide 0.42%, epsilon-polylysine 0.35%, and tea polyphenols 0.20%, Surplus is concentration thick gravy liquid;
(3) method of addition antistaling agent is in pickling, and weighs 4% amount by meat and weighs concentration thick gravy liquid, gathers ε-rely in proportion Propylhomoserin, tea polyphenols, chitosan oligosaccharide are added in concentration thick gravy liquid, after mixing, are injected in beef, then pour into vacuum tumbler Tumbling is all absorbed by meat to thick gravy, meat piece uniform color, about 60min;
(4) Pasteur's ultrasonic sterilization, be will about 8 aged beefs vacuum packaging after, be placed in ultrasonic drilling machine, using power 2200W, temperature 60 C sterilize 30min, and then flowing water is cooled to room temperature.
The product that will be obtained through above-described embodiment, using TVB-N as index, using first order reaction kinetics model combination Ah Lei Ni Wusi (Arrhenius) equation, integrated forecasting Halogen boil the shelf-life of Spiced beef, TVB-N rate of change constant k and storage temperature Degree T meets Arrhenius equation: k=k0exp(-Ea/RT)+lnk.As a result are as follows:
1 Halogen of table boils the variation of TVB-N under Spiced beef different temperatures
2 Halogen of table boils the regression equation that TVB-N changes with storage time under Spiced beef difference reserve temperature
The linear graph (Fig. 1) of lnk and 1000/T, i.e. y=-6.8921x+ are drawn by three slope ks and its storage temperature 18.687(R2=0.972), meet Arrhenius curvilinear equation, as shown in Figure 1;
Therefore, k=1.04*108exp(-6.8921*103/T)————————①
In formula, T is temperature (K)
It is reacted according to first order kinetics, i.e.,
N=N0Exp (kt), is changed into logarithmic form, it may be assumed that
LnN=lnN0+ kt, after transformation:
T=(lnN-lnN0)/k—————————②
In formula,
T is storage time (d);
N0The TVB-N value (mg/100g) when Spiced beef stores initial is boiled for Halogen;
N is TVB-N value (mg/100g);
K is the rate of change constant of TVB-N;
Therefore, 1. formula 2. formula will be substituted into, and will calculate Halogen and boil 4 DEG C of Spiced beef, 10 DEG C, 25 DEG C, 37 DEG C of shelf-lifves, acquires result Such as table 3.
Halogen boils the shelf life of Spiced beef under the different reserve temperatures of table 3
The foregoing is merely presently preferred embodiments of the present invention, it is all according to equivalent change made by scope of the present invention patent with Modification, shall all be covered by the patent of the invention.
Measuring method:
Volatile Base Nitrogen value (TVB-N) measurement:
According to GB/T5009.228-2016 " analysis method of meat and meat hygiene standard: Volatile Base Nitrogen " method Measurement.
The foregoing is a detailed description of the present invention in conjunction with specific embodiments, and it cannot be said that the present invention is specifically real It applies and is only limitted to these explanations.For those skilled in the art to which the present invention belongs, before not departing from present inventive concept It puts, a number of simple deductions or replacements can also be made, all shall be regarded as belonging to the scope of protection of the invention.

Claims (5)

1. a kind of Halogen boils Spiced beef preservation method, it is characterised in that: the following steps are included:
Step 1, spice sterilization;
Step 2 prepares antistaling agent;
Step 3 adds antistaling agent in pickling;
Product after step 4, packaging is using ultrasonic pasteurize.
2. Halogen boils Spiced beef preservation method according to claim 1, it is characterised in that: the spice method for disinfection is, First spice is soaked, using power 700W-850W microwave disinfection 10min-15min.
3. Halogen boils Spiced beef preservation method according to claim 1, it is characterised in that: the weight percent composition are as follows: Chitosan oligosaccharide 0.30-0.45%, epsilon-polylysine 0.25-0.35%, tea polyphenols 0.20-0.30%, surplus are concentration thick gravy liquid.
4. Halogen boils Spiced beef preservation method according to claim 1, it is characterised in that: the marinated middle addition antistaling agent Method are as follows: weigh 4% amount by meat and weigh concentration thick gravy liquid, epsilon-polylysine, tea polyphenols, chitosan oligosaccharide are added to concentration halogen in proportion In juice, after mixing, inject in beef, then pour into tumbling in vacuum tumbler and all absorbed to thick gravy by meat, meat piece color It is damp uniform, time 40-60min.
5. Halogen boils Spiced beef preservation method according to claim 1, it is characterised in that: it is described ultrasound pasteurize, be by It after the vacuum packaging of about 8 aged beefs, is placed in ultrasonic drilling machine, using 60-80 DEG C of power 2200-2800W, temperature, sterilizes 20- 30min, then flowing water is cooled to room temperature.
CN201910522962.6A 2019-06-17 2019-06-17 A kind of Halogen boils the preservation method of Spiced beef Pending CN110100877A (en)

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CN110338358A (en) * 2019-08-27 2019-10-18 香格里拉藏龙生物开发股份有限公司 A kind of Yak Beef Stick and preparation method thereof
CN111034892A (en) * 2019-12-03 2020-04-21 西北农林科技大学 Ultrasonic combined epsilon-polylysine sterilization method for grape juice sterilization

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Publication number Priority date Publication date Assignee Title
CN110338360A (en) * 2019-08-27 2019-10-18 香格里拉藏龙生物开发股份有限公司 A kind of air-dried yak meat and preparation method thereof
CN110338358A (en) * 2019-08-27 2019-10-18 香格里拉藏龙生物开发股份有限公司 A kind of Yak Beef Stick and preparation method thereof
CN111034892A (en) * 2019-12-03 2020-04-21 西北农林科技大学 Ultrasonic combined epsilon-polylysine sterilization method for grape juice sterilization

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