CN110095321A - A kind of on-line automatic sampler of environment-friendly high-temperature pitch - Google Patents

A kind of on-line automatic sampler of environment-friendly high-temperature pitch Download PDF

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Publication number
CN110095321A
CN110095321A CN201910392195.1A CN201910392195A CN110095321A CN 110095321 A CN110095321 A CN 110095321A CN 201910392195 A CN201910392195 A CN 201910392195A CN 110095321 A CN110095321 A CN 110095321A
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CN
China
Prior art keywords
sampling
valve
pneumatic
gas fume
bench
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Granted
Application number
CN201910392195.1A
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Chinese (zh)
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CN110095321B (en
Inventor
孙宝平
马克任
谢玉林
付进
徐孝廉
张小宝
管远力
高学频
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Masteel Oseia Chemical Co Ltd
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Masteel Oseia Chemical Co Ltd
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Priority to CN201910392195.1A priority Critical patent/CN110095321B/en
Publication of CN110095321A publication Critical patent/CN110095321A/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N1/20Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials
    • G01N1/2035Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials by deviating part of a fluid stream, e.g. by drawing-off or tapping
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N2001/1006Dispersed solids
    • G01N2001/1012Suspensions
    • G01N2001/1025Liquid suspensions; Slurries; Mud; Sludge
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N2001/1031Sampling from special places
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N1/20Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials
    • G01N1/2035Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials by deviating part of a fluid stream, e.g. by drawing-off or tapping
    • G01N2001/205Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials by deviating part of a fluid stream, e.g. by drawing-off or tapping using a valve

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  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The invention discloses a kind of on-line automatic samplers of environment-friendly high-temperature pitch, belong to coal tar processing production equipment field, including online sampling mechanism and automatic control system, the on-line period mechanism includes pedestal, sampling bench, raffinate box, thief rod, sampling cup, dust cover, heat tracing pipe, insulating layer, explosion-proof spot;The automatic control system includes PLC rack, cylinder, three-position four-way electromagnetic directional valve, pneumatic sample cock, pneumatic gas fume valve;The PLC rack is connected by controlling route with three-position four-way electromagnetic directional valve, pneumatic sample cock, pneumatic gas fume valve;Cylinder is then installed on thief rod.The present invention is achieved the purpose that automatic sampling and is effectively prevent generating pollution of a large amount of glance coals to environment in hard pitch sampling process using the method for PLC sequential control three position four-way electromagnetic valve, pneumatic sample cock, pneumatic gas fume valve.

Description

A kind of on-line automatic sampler of environment-friendly high-temperature pitch
Technical field
The present invention relates to a kind of coal tar processing production equipment fields, online more particularly, to a kind of environment-friendly high-temperature pitch Automatic sampling device.
Background technique
Hard pitch on-line period is the indispensable link that asphaltic products quality adjustment is carried out in coal tar processing production process, It is that hard pitch > 300 DEG C in production pipeline are directly taken in sampling cup, then by the asphalt sample in sampling cup Lab analysis is carried out, production operation personnel carry out intervention adjusting to scene by resulting analysis data, to reach raising The purpose of asphaltic products quality.
The on-line period of hard pitch mainly passes through artificial scene and completes at present, and site operation personnel passes through in opening conduits Manual sample cock carry out on-line period, the splashing of sampling process high temperature pitch is easily to the person of site operation personnel It damages, while generating a large amount of glance coals in sampling process, it is a variety of more containing BaP, benzanthracene, carbazole etc. in glance coal Cyclophane hydrocarbons, and be carcinogenic and strong carcinogen mostly, partial size is only 0.01 μm the smallest mostly between 0.1 ~ 1.0 μm, most Big about 10.0 μm are especially a variety of carcinogens of representative with 3,4- BaP.Its main way being detrimental to health Diameter is attached on 8 um floating dust below, by respiratory tract by suction human body.Therefore, on-line automatic take is carried out to hard pitch Glance coal in sample and elimination hard pitch sampling process, is very important.
By retrieval, relevant solution, such as China Patent No.: CN201711005532.4 exists in the prior art, A kind of pitch automatic sampling device, including heating muff, pitch probe tube, temperature sensor, control are disclosed in this application scheme Warm component, negative pressure taking sample bottle and vacuum pump;The heating muff is set in outside the pitch probe tube, the temperature sensing Device is connected with the heating muff, and the negative pressure taking sample bottle is connected with the pitch probe tube, the vacuum pump and the negative pressure Sampling bottle is connected, and the temperature-controlling component is connected with the heating muff and the vacuum pump;The device is formed using vacuum pump The extraction of negative pressure sampling bottle inner air makes its internal subnormal ambient that formed draw asphalt sample, can not eliminate glance coal to environment Pollution.
Summary of the invention
The present invention is directed to the deficiency of existing product, and provides a kind of on-line automatic sampler of environment-friendly high-temperature pitch, energy It is enough automatically to take the hard pitch in production pipeline in sampling cup, and the glance coal in hard pitch sampling process is eliminated, The personal injury in hard pitch sampling process high temperature pitch and its glance coal to operator is avoided, eliminates glance coal to ring The pollution in border.Meanwhile structure of the invention design is reasonable, easy to operate, sampling fast and easy.
A kind of on-line automatic sampler of environment-friendly high-temperature pitch of the invention, including online sampling mechanism and automatic control System, the on-line period mechanism include pedestal, sampling bench, raffinate box, thief rod, sampling cup, dust cover, heat tracing pipe, Insulating layer, explosion-proof spot;Sampling bench, the sampling bench one side setting sampling gate, the sampling are fixedly installed on the pedestal Door is connected by hinge with sampling bench, and tempered glass observation window is equipped on sampling gate, and bolt dress is fixedly welded on sampling gate It sets, its excess-three face of the sampling bench is provided with tempered glass observation window, and sampling bench wherein pacify by a face tempered glass observation panel top Equipped with explosion-proof spot, bottom is placed with raffinate box in sampling bench, and thief rod is equipped with above the raffinate box, and thief rod passes through close Seal is connected with sampling bench, and sampling cup is fixed by the lasso on the thief rod, and the sampling bench is internally located under sample tap Side is equipped with dust cover.The automatic control system includes PLC rack, cylinder, three-position four-way electromagnetic directional valve, pneumatic sampling Valve, pneumatic gas fume valve;Top is equipped with pneumatic sample cock outside the sampling bench, and the pneumatic sample cock side is logical It crosses flange to be connected with sampling bench, the pneumatic sample cock other side is connected by flange with process high-temperature pitch pipeline, pneumatic to sample Valve and its connecting pipe are externally wrapped with heat tracing pipe, pass through insulating layer packet outside the heat tracing pipe of pneumatic sample cock and its winding It wraps up in, top is provided with pneumatic gas fume valve outside the sampling bench, and pneumatic gas fume valve side is connected by flange with sampling bench, The pneumatic gas fume valve other side is connected with factory's negative pressure flue gas system, and the PLC rack passes through control route and three four Electric change valve, pneumatic sample cock, pneumatic gas fume valve are connected;Cylinder is then installed between thief rod and sampling bench.
Further, PLC rack is controlled by the control route being connected respectively with pneumatic sample cock, pneumatic gas fume valve The opening and closing of pneumatic sample cock, pneumatic gas fume valve, and the control line by being connected with three-position four-way electromagnetic directional valve Road controls the flexible of cylinder, and the flexible realization that thief rod then passes through cylinder is moved forward and backward.Pneumatic sample cock, pneumatic flue gas simultaneously Valve position signal is sent in PLC system by valve by the control route being connected with PLC rack, and the PLC system in PLC rack is then The control program of the control command and inside that are issued according to sample button on PLC rack panel realizes automatic sampling function.
The beneficial effects of the present invention are: compared with prior art, there is following remarkable result:
(1), a kind of on-line automatic sampler of environment-friendly high-temperature pitch of the invention is born by enclosed sampling platform and its with factory The glance coal that the connected pneumatic gas fume valve of pressure flue gas system generates sampling process all absorbs, so that without drip in sampling process Green cigarette discharge, field sampling are environmental-friendly.
(2), a kind of on-line automatic sampler of environment-friendly high-temperature pitch of the invention, by dust-proof inside sampling bench Cover avoids pitch splashes to sampling bench tempered glass observation panel in sampling process pollution and damage, simultaneously because tempering The explosion-proof spot installed above glass viewing port, so that operator observes sampling process and is more clear.
3, a kind of on-line automatic sampler of environment-friendly high-temperature pitch of the invention has lasso by unique design Thief rod and driving cylinder, can be avoided when operator is directly sampled with hand by sampling cup hard pitch to operation The injury of personnel.
4, a kind of on-line automatic sampler of environment-friendly high-temperature pitch of the invention, the program being arranged by PLC system Carry out a key sampling operation, after sampling cup need to be only put into sampling bench by operator, start the sampling that is arranged on PLC rack by Button, device, which will be automatically performed, first to be put raffinate and is sampled etc. that a whole set of sampling, eliminate smoke operation again, so that sampling operation is simple, side Just quickly.
5, a kind of on-line automatic sampler of environment-friendly high-temperature pitch of the invention, it is few to be directed to equipment, structure is simple, Reliably, manufacturing cost is low.
Detailed description of the invention
Fig. 1 is schematic structural view of the invention;
Fig. 2 is thief rod schematic diagram of the invention;
Fig. 3 is automatic control system composition schematic diagram of the invention;
Fig. 4 is automatic sampling program flow diagram of the invention.
In figure: pedestal 1, raffinate box 3, thief rod 4, sampling cup 5, dust cover 6, heat tracing pipe 7, insulating layer 8, is prevented sampling bench 2 Booster lamp 9, PLC rack 10, cylinder 11, three-position four-way electromagnetic directional valve 12, pneumatic sample cock 13, pneumatic gas fume valve 14, set Circle 15.
Specific embodiment
The present invention will be further described with reference to the examples below.
As shown in figure, a kind of on-line automatic sampler of environment-friendly high-temperature pitch of the invention, including online sampling mechanism And automatic control system, the on-line period mechanism include pedestal 1, sampling bench 2, raffinate box 3, sampling cup 5, dust cover 6, companion Heat pipe 7, insulating layer 8, explosion-proof spot 9;Sampling bench 2 is fixedly installed on the pedestal 1, the one side setting of the sampling bench 2 takes Sample door, the sampling gate are connected by hinge with sampling bench 2, and tempered glass observation window is equipped on sampling gate, is consolidated on sampling gate Surely it is welded with bolt device, its excess-three face of the sampling bench 2 is provided with tempered glass observation window, a sampling bench wherein face tempering glass Explosion-proof spot 9 is installed above glass observation panel, bottom is placed with raffinate box 3 in sampling bench 2, is equipped with above the raffinate box 3 Thief rod 4, thief rod 4 are connected by sealing ring with sampling bench 2, and sampling cup 5 is fixed by the lasso 15 on the thief rod 4, The sampling bench 2 is internally located at below sample tap and is equipped with dust cover 6;
In conjunction with attached drawing 1, the on-line period mechanism include pedestal 1, sampling bench 2, raffinate box 3, thief rod 4, sampling cup 5, Dust cover 6, heat tracing pipe 7, insulating layer 8, explosion-proof spot 9;The pedestal 1 of selection is welded using 20# ordinary carbon steel material, and four Lower margin is reserved with M12 hole for the expansion bolt, and surface applies anti-rust paint and finish paint again after processing of rust removing.The sampling bench 2 uses It is welded with a thickness of the 20# steel plate of 6mm, glass viewing port is stepped on 300 DEG C of tempered glass using general and is made, and high temperature resistant and soda acid are invaded Erosion, 2 surface of sampling bench applies anti-rust paint and finish paint again after processing of rust removing.The raffinate box 3 and dust cover 6 are thick using 2mm Stainless steel 304 production, dust cover 6 are connected by the through-hole stainless steel bolt of M6 with sampling bench 2.What the sampling cup 5 was selected It is stainless steel bottom flat conical cup, stainless steel is with a thickness of 2mm.The heat tracing pipe 7 uses R410A copper tube coil, model: 9.52* 0.7 TP2, interior logical 250 DEG C of superheated steams carry out heat tracing.The insulating layer 8 is selected to be wrapped up with a thickness of the ceramic fibre mat of 50mm Two layers, outside is wrapped up in matizhi and 0.5mm aluminium suitcase again.Explosion-proof spot 9 selects anti-explosion LED stick spot SW2180 band magnetic frame.
The automatic control system includes PLC rack 10, cylinder 11, three-position four-way electromagnetic directional valve 12, pneumatic sampling valve Door 13, pneumatic gas fume valve 14;The 2 outside top of sampling bench is equipped with pneumatic gas fume valve 14, the pneumatic gas fume valve 14 sides are connected by flange with sampling bench 2, and pneumatic 14 other side of gas fume valve passes through flange and process high-temperature pitch pipeline phase Even, pneumatic gas fume valve 14 and its connecting pipe are externally wrapped with the heat tracing pipe 7 of heat tracing pipe 7, pneumatic gas fume valve 14 and its winding Outside is wrapped up by insulating layer 8, and the 2 outside top of sampling bench is provided with pneumatic gas fume valve 14, pneumatic gas fume valve 14 1 Side is connected by flange with sampling bench 2, and pneumatic 14 other side of gas fume valve is connected with factory's negative pressure flue gas system, described PLC rack 10 is connected by controlling route with three-position four-way electromagnetic directional valve 12, pneumatic sample cock 13, pneumatic gas fume valve 14; Cylinder 11 is installed between thief rod 4 and sampling bench 2.
In conjunction with attached drawing 1, the automatic control system includes PLC rack 10, cylinder 11, three-position four-way electromagnetic directional valve 12, pneumatic sample cock 13, pneumatic gas fume valve 14;The PLC rack 10 selects Siemens CPU-226, model: 6ES7 216-2BD23-0XB8,10 panel of PLC rack setting sampling starting, failure reset, power supply are normal, sampling is completed four and pressed with lamps Button, button model: LA39-B2-22D/g23.The cylinder 11 selects the model of Wenzhou Dong Te Air Movement Technologies Inc production QGAII 100X350 MF1 double-acting cylinder, the cylinder 11 pass through the through-hole stainless steel spiral shell of four M6 with the one side of sampling bench 2 Bolt is fixed.The three-position four-way electromagnetic directional valve 12 is the universal directional control valve of FESTO, model: VUVG-L10-P53C- 2#, 4# mouth of T-M5-1R8L, the three-position four-way electromagnetic directional valve 12 are connected by stainless steel tracheae with cylinder 11, described The 1# mouth of three-position four-way electromagnetic directional valve 12 be connected with plant instrumentation compressed air cylinder by stainless steel tracheae.Described is pneumatic What sample cock 13 was selected is the jettron butterfly valve of seat diameter 3/4 ".What the pneumatic gas fume valve 14 was selected is valve seat The jettron butterfly valve of bore 4 ".
The PLC rack 10 is controlled by the control route being connected respectively with pneumatic sample cock 13, pneumatic gas fume valve 14 The opening and closing of pneumatic sample cock 13, pneumatic gas fume valve 14 are made, and by being connected with three-position four-way electromagnetic directional valve 12 Control route control cylinder it is flexible, thief rod 4 is then moved forward and backward by the flexible realization of cylinder 11;Pneumatic sampling valve simultaneously Valve position signal is sent in PLC system by door 13, pneumatic gas fume valve 14 by the control route being connected with PLC rack 10, The control program of control command and inside that PLC system in PLC rack 10 is then issued according to sample button on PLC rack panel is real Existing automatic sampling function.
In conjunction with attached drawing 2, the thief rod 4 selects the production of φ 6mm stainless steel 304 round steel, and one end of the thief rod 4 is logical The through-hole stainless steel bolt for crossing M6 is connected with cylinder 11, and has rubber seal to φ 8mm by 2 side two of sampling bench Through-hole moved.
In conjunction with attached drawing 3, the three-position four-way electromagnetic directional valve 12, pneumatic sample cock 13 and pneumatic gas fume valve 14 It is connected by control line with PLC rack 10.
In conjunction with attached drawing 4, by Siemens's programming software work out corresponding control program and under be filled to west gate in PLC rack 10 In sub- CPU-226, operator can carry out on-line automatic sampling work by pressing the button on 10 panel of PLC rack, and in real time Understand the operation conditions of device.
The above description is only an embodiment of the present invention, is not intended to limit the scope of the invention, all to utilize this hair Equivalent structure or equivalent flow shift made by bright description is applied directly or indirectly in other relevant technology necks Domain is included within the scope of the present invention.

Claims (3)

1. a kind of on-line automatic sampler of environment-friendly high-temperature pitch, characterized in that the on-line automatic sampler is included in Line sampling mechanism and automatic control system, the on-line period mechanism include pedestal (1), sampling bench (2), raffinate box (3), take Sample cup (5), dust cover (6), heat tracing pipe (7), insulating layer (8), explosion-proof spot (9);Sampling is fixedly installed on the pedestal (1) Sampling gate is arranged in platform (2), the one side of the sampling bench (2), and the sampling gate is connected by hinge with sampling bench (2), sampling gate On tempered glass observation window is installed, bolt device is fixedly welded on sampling gate, described its excess-three face of sampling bench (2) is provided with Tempered glass observation window, wherein a face tempered glass observation panel top is equipped with explosion-proof spot (9) sampling bench, in sampling bench (2) Bottom is placed with raffinate box (3), is equipped with thief rod (4) above the raffinate box (3), and thief rod (4) is by sealing ring and takes Sample platform (2) is connected, and sampling cup (5) is fixed by the lasso (15) on the thief rod (4), and the sampling bench (2) is internally located at Dust cover (6) are installed below sample tap;
The automatic control system includes PLC rack (10), cylinder (11), three-position four-way electromagnetic directional valve (12), pneumatic sampling Valve (13), pneumatic gas fume valve (14);The external top of the sampling bench (2) is equipped with pneumatic gas fume valve (14), the gas Dynamic gas fume valve (14) side is connected by flange with sampling bench (2), and pneumatic gas fume valve (14) other side passes through flange and work Skill hard pitch pipeline is connected, and pneumatic gas fume valve (14) and its connecting pipe are externally wrapped with heat tracing pipe (7), pneumatic gas fume valve (14) and its outside the heat tracing pipe (7) of winding it is wrapped up by insulating layer (8), the external top of the sampling bench (2) is provided with pneumatic Gas fume valve (14), pneumatic gas fume valve (14) side are connected by flange with sampling bench (2), the pneumatic gas fume valve (14) The other side is connected with factory's negative pressure flue gas system, and the PLC rack (10) passes through control route and three-position four-way electromagnetic directional valve (12), pneumatic sample cock (13), pneumatic gas fume valve (14) are connected;Cylinder (11) is installed on thief rod (4) and sampling bench (2) Between.
2. a kind of on-line automatic sampler of environment-friendly high-temperature pitch according to claim 1, characterized in that the PLC Cabinet (10) controls pneumatic sampling by the control route being connected respectively with pneumatic sample cock (13), pneumatic gas fume valve (14) The opening and closing of valve (13), pneumatic gas fume valve (14), and the control by being connected with three-position four-way electromagnetic directional valve (12) Route control cylinder processed stretches, and thief rod (4) is then moved forward and backward by the flexible realization of cylinder (11);Pneumatic sampling valve simultaneously Valve position signal is sent to PLC system by the control route being connected with PLC rack (10) by door (13), pneumatic gas fume valve (14) In system, the control of control command and inside that the PLC system in PLC rack (10) is then issued according to sample button on PLC rack panel Processing procedure sequence realizes automatic sampling function.
3. a kind of on-line automatic sampler of environment-friendly high-temperature pitch according to claim 1, characterized in that the guarantor The ceramic fibre mat that warm layer (8) is thickness 30-100mm wraps up two layers, and outside is wrapped up in matizhi and 0.5mm aluminium suitcase again.
CN201910392195.1A 2019-05-13 2019-05-13 Environment-friendly high-temperature asphalt online automatic sampling device Active CN110095321B (en)

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CN201910392195.1A CN110095321B (en) 2019-05-13 2019-05-13 Environment-friendly high-temperature asphalt online automatic sampling device

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CN201910392195.1A CN110095321B (en) 2019-05-13 2019-05-13 Environment-friendly high-temperature asphalt online automatic sampling device

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CN110095321B CN110095321B (en) 2024-02-02

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007033386A1 (en) * 2007-06-12 2008-12-18 Ritag Ritterhuder Armaturen Gmbh & Co. Armaturenwerk Kg Safety cabinet for safe withdrawal of samples of gaseous or liquid media from pipelines, has housing that is closed by door
CN207036489U (en) * 2017-08-23 2018-02-23 成都知行新材料技术研究有限公司 A kind of asphaltum with high viscosity rapid sampling attachment
CN107782584A (en) * 2017-10-25 2018-03-09 中石油燃料油有限责任公司研究院 A kind of pitch automatic sampling device
CN108120619A (en) * 2016-11-29 2018-06-05 上海宝钢化工有限公司 Closed sampler and high-temperature smokeless sampling method
CN207667689U (en) * 2017-11-29 2018-07-31 安阳师范学院 Solution heats tilting device
CN209979306U (en) * 2019-05-13 2020-01-21 马钢奥瑟亚化工有限公司 Environment-friendly high-temperature asphalt on-line automatic sampling device

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007033386A1 (en) * 2007-06-12 2008-12-18 Ritag Ritterhuder Armaturen Gmbh & Co. Armaturenwerk Kg Safety cabinet for safe withdrawal of samples of gaseous or liquid media from pipelines, has housing that is closed by door
CN108120619A (en) * 2016-11-29 2018-06-05 上海宝钢化工有限公司 Closed sampler and high-temperature smokeless sampling method
CN207036489U (en) * 2017-08-23 2018-02-23 成都知行新材料技术研究有限公司 A kind of asphaltum with high viscosity rapid sampling attachment
CN107782584A (en) * 2017-10-25 2018-03-09 中石油燃料油有限责任公司研究院 A kind of pitch automatic sampling device
CN207667689U (en) * 2017-11-29 2018-07-31 安阳师范学院 Solution heats tilting device
CN209979306U (en) * 2019-05-13 2020-01-21 马钢奥瑟亚化工有限公司 Environment-friendly high-temperature asphalt on-line automatic sampling device

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