CN107782584A - A kind of pitch automatic sampling device - Google Patents

A kind of pitch automatic sampling device Download PDF

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Publication number
CN107782584A
CN107782584A CN201711005532.4A CN201711005532A CN107782584A CN 107782584 A CN107782584 A CN 107782584A CN 201711005532 A CN201711005532 A CN 201711005532A CN 107782584 A CN107782584 A CN 107782584A
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CN
China
Prior art keywords
sampling
temperature
pitch
probe tube
heating muff
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Granted
Application number
CN201711005532.4A
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Chinese (zh)
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CN107782584B (en
Inventor
时敬涛
李剑新
赵磊
袁野
李玉环
蒋福山
刘瑾潼
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Petrochina Co Ltd
Petrochina Fuel Oil Co Ltd
Original Assignee
RESEARCH INSTITUTE OF CNPC FUEL OIL Co Ltd
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Priority to CN201711005532.4A priority Critical patent/CN107782584B/en
Publication of CN107782584A publication Critical patent/CN107782584A/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N1/14Suction devices, e.g. pumps; Ejector devices
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N1/14Suction devices, e.g. pumps; Ejector devices
    • G01N2001/1418Depression, aspiration

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  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The invention discloses a kind of pitch automatic sampling device, and under a kind of implementation, the device can include heating muff, pitch probe tube, temperature sensor, temperature-controlling component, sampling below atmospheric pressure bottle and vavuum pump;The heating muff is set in outside the pitch probe tube, the temperature sensor is connected with the heating muff, the sampling below atmospheric pressure bottle is connected with the pitch probe tube, the vavuum pump is connected with the sampling below atmospheric pressure bottle, and the temperature-controlling component is connected with the heating muff and the vavuum pump.The device that the application provides, probe tube have the function that design temperature heats, and when solving pitch sampling, need to heat the problem of whole tank pitch samples.Positioning sampling, the mode of fast sampling are provided for pitch sampling.Labor intensity is reduced, improves the efficiency of pitch sampling.Sampling process is automatically performed, easy to operate, and sampling efficiency is high.Device can realize quantitative sampling.In addition, probe tube can be placed in different sample depths, samples' representativeness is improved.

Description

A kind of pitch automatic sampling device
Technical field
The present invention relates to pitch sampling equipment technical field, it is automatically performed more particularly to a kind of sampling process, operation letter Just, the high pitch automatic sampling device of sampling efficiency.
Background technology
The dark brown mixture that pitch is made up of the hydrocarbon and non metallic derivatives of different molecular weight, under normal temperature Viscosity is very high, solid-state or semisolid is presented, being heated to more than 80 DEG C has mobility.In the production and construction of pitch, to protect The quality and construction quality of pitch are demonstrate,proved, pitch needs inspection by sampling, and it is for future reference to keep sample.Common sampling method is:1st, from pitch The method sampled in tank:Pitch in tank has mobility in the state of heating, opens sample cock sampling;2nd, from the tank that keeps sample Sampling:The tank that will keep sample heats, and is sampled again after asphalt melting in tank.Traditional pitch sampling method is restricted more, works as pitch Tank at normal temperatures, can not sample.For the sample for the tank that keeps sample, whole tank heating, sample time length are needed, samples' representativeness can not protect Card.In addition, to keep sample multiple measurement when, heating cooling asphalt sample repeatedly, the performance to keep sample can change, and influence keeps sample inspection The accuracy of survey.
The content of the invention
The invention provides a kind of pitch automatic sampling device.Sample is heated using probe tube, made at sampling Pitch has mobility, recycles the mode vacuumized, the sampling bottle that is connected with probe tube is formed negative pressure, and pitch is along sampling Pipe flows into sampling bottle.Pitch automatic sampling device is by heating muff, pitch probe tube, temperature sensor, temperature regulating device, negative pressure taking Sample bottle and vacuum pump group into.The device can realize the automatic sampling of pitch, improve the uniformity and sampling efficiency of sampling.
The invention provides following scheme:
A kind of pitch automatic sampling device, including:
Heating muff, pitch probe tube, temperature sensor, temperature-controlling component, sampling below atmospheric pressure bottle and vavuum pump;The heating muff It is set in outside the pitch probe tube, the temperature sensor is connected with the heating muff, the sampling below atmospheric pressure bottle and institute Pitch probe tube is stated to be connected, the vavuum pump is connected with the sampling below atmospheric pressure bottle, the temperature-controlling component and the heating muff with And the vavuum pump is connected;
Wherein, the temperature-controlling component is used for the heating-up temperature for controlling the heating muff, and the heating muff is used for the drip Blue or green probe tube is heated, and the temperature sensor is used for the Current Temperatures for detecting the pitch probe tube, and the vavuum pump is used It is set to be internally formed subnormal ambient in the negative pressure sampling bottle inner air is extracted out.
Preferably:The temperature-controlling component includes prompting device, and the prompting device is used for when the temperature sensor detects institute State when pitch probe tube Current Temperatures reach design temperature and send cue.
Preferably:The prompting device includes drive circuit and buzzer.
Preferably:The prompting device includes drive circuit and LED lamp bead.
Preferably:The temperature-controlling component includes temperature assignment component, and the temperature assignment component is used to set the heating The heating-up temperature of sleeve pipe.
According to specific embodiment provided by the invention, the invention discloses following technique effect:
By the invention it is possible to realize a kind of pitch automatic sampling device, under a kind of implementation, the device can include adding Thermal sleeve, pitch probe tube, temperature sensor, temperature-controlling component, sampling below atmospheric pressure bottle and vavuum pump;The heating muff is set in Outside the pitch probe tube, the temperature sensor is connected with the heating muff, the sampling below atmospheric pressure bottle and the pitch Probe tube is connected, and the vavuum pump is connected with the sampling below atmospheric pressure bottle, the temperature-controlling component and the heating muff and described Vavuum pump is connected;Wherein, the temperature-controlling component is used to controlling the heating-up temperature of the heating muff, and the heating muff is used for pair The pitch probe tube is heated, and the temperature sensor is used for the Current Temperatures for detecting the pitch probe tube, described true Empty pump, which is used to extract out the negative pressure sampling bottle inner air, makes it be internally formed subnormal ambient.The device that the application provides, knot Structure advantages of simple, it is easy to install.Probe tube has the function that design temperature heats, and when solving pitch sampling, need to heat whole The problem of tank pitch samples.Positioning sampling, the mode of fast sampling are provided for pitch sampling.Labor intensity is reduced, improves pitch The efficiency of sampling.Sampling process is automatically performed, easy to operate, and sampling efficiency is high.Device can realize quantitative sampling.In addition, sampling Pipe can be placed in different sample depths, improve samples' representativeness.
Certainly, any product for implementing the present invention it is not absolutely required to reach all the above advantage simultaneously.
Brief description of the drawings
In order to illustrate more clearly about the embodiment of the present invention or technical scheme of the prior art, below will be to institute in embodiment The accompanying drawing needed to use is briefly described, it should be apparent that, drawings in the following description are only some implementations of the present invention Example, for those of ordinary skill in the art, on the premise of not paying creative work, can also be obtained according to these accompanying drawings Obtain other accompanying drawings.
Fig. 1 is a kind of structural representation of pitch automatic sampling device provided in an embodiment of the present invention.
In figure:Heating muff 1, pitch probe tube 2, temperature sensor 3, temperature-controlling component 4, sampling below atmospheric pressure bottle 6, vavuum pump 6.
Embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.It is based on Embodiment in the present invention, the every other embodiment that those of ordinary skill in the art are obtained, belong to what the present invention protected Scope.
Embodiment
It is a kind of pitch automatic sampling device provided in an embodiment of the present invention, as shown in figure 1, the device includes referring to Fig. 1 Heating muff 1, pitch probe tube 2, temperature sensor 3, temperature-controlling component 4, sampling below atmospheric pressure bottle 5 and vavuum pump 6;The heating mantle Pipe 1 is set in outside the pitch probe tube 2, and the temperature sensor 3 is connected with the heating muff 1, the sampling below atmospheric pressure Bottle 5 is connected with the pitch probe tube 2, and the vavuum pump 6 is connected with the sampling below atmospheric pressure bottle 5, the temperature-controlling component 4 with it is described Heating muff 1 and the vavuum pump 6 are connected;
Wherein, the temperature-controlling component 4 is used for the heating-up temperature for controlling the heating muff 1, and the heating muff 1 is used for described Pitch probe tube 2 is heated, and the temperature sensor 3 is used for the Current Temperatures for detecting the pitch probe tube 2, the vacuum Pump 6, which is used to extract out the inner air of negative pressure sampling bottle 5, makes it be internally formed subnormal ambient.Temperature regulating device setting probe tube Temperature(The temperature of asphalt melting flowing), after reaching design temperature, probe tube is positioned over sample position;Temperature regulating device can lead to The measured value of the temperature sensor of over sampling pipe front end judges the temperature at sampling, after temperature stabilization to design temperature, tentatively Judge that sample has mobility around probe tube, can meet the requirement of sampling below atmospheric pressure.Probe tube and sampling bottle are tightly connected, Sampling bottle is sealed, starts sample button, sampling bottle forms negative pressure, and pitch flows along probe tube, into the specimen cup of sampling bottle. Sample sample size and stop sampling to the sampling value of setting, device, complete sampling process.
Further, the temperature-controlling component 4 includes prompting device, and the prompting device is used for when the temperature sensor detects The pitch probe tube Current Temperatures send cue when reaching design temperature.The prompting device includes drive circuit and honeybee Ring device.The prompting device includes drive circuit and LED lamp bead.The temperature-controlling component includes temperature assignment component, the temperature Assignment component is used for the heating-up temperature for setting the heating muff.
The device is by by heating muff, pitch probe tube, temperature sensor, temperature regulating device, sampling below atmospheric pressure bottle and vavuum pump Composition.With temperature automatically controlled function, the heating-up temperature of probe tube according to environment temperature and the kind of pitch, can be set, In sampling process, ensure the mobility of sampling point pitch.Different sample depths can be positioned over, completes the drip of different parts Blue or green sampling.It is convenient that probe tube is changed, and ensures the independence of sampling.The sampling mode of negative pressure, it is simple in construction, sampling bottle volume Flexible design, easy to maintenance, sampling sample size is easily controllable.
It is described in detail below by the application method of the device provided with occupation mode the application:The device is having Body in use, keeping sample from the pitch of 1 liter of volume in take 30g samples, be positioned in sampling bottle, in case pitch examine use.With reference to The explanation of each part in Fig. 1 structural representations, specific embodiment is described, it is as follows:
The first step:It is 120 DEG C to set the temperature of 1 pitch probe tube from 4 temperature regulating devices of Fig. 1 pitch automatic sampling devices, and is opened Dynamic heating function, the heating of pitch probe tube, temperature regulating device read pitch probe tube Current Temperatures by 3 temperature sensors, work as temperature Degree reaches set temperature value, can start to sample;
Second step:Pitch probe tube is positioned over pitch sampling point, and observes the depth of probe tube in the sample.Reach set Sample depth after, fixed probe tube, and connect probe tube and 5 sampling below atmospheric pressure bottles.
3rd step:Probe tube head temperature is observed, after reaching 120 DEG C of design temperature, after device waits 2 minutes, temperature control dress The panel prompting put starts sampling, and after confirming button, device starts 6 vavuum pumps, starts to sample, and asphalt sample is along probe tube stream Enter sampling bottle.
4th step:The pitch for flowing into sampling bottle reaches the sample size of setting, and sampling stops.
5th step:Pitch sampling bottle is taken out, completes sampling process.
In a word, the device that the application provides, it is simple and reasonable, it is easy to install.There is probe tube design temperature to add The function of heat, when solving pitch sampling, the problem of whole tank pitch samples need to be heated.Positioning sampling is provided for pitch sampling, quickly The mode of sampling.Labor intensity is reduced, improves the efficiency of pitch sampling.Sampling process is automatically performed, easy to operate, sampling efficiency It is high.Device can realize quantitative sampling.In addition, probe tube can be placed in different sample depths, samples' representativeness is improved.
It should be noted that herein, such as first and second or the like relational terms are used merely to a reality Body or operation make a distinction with another entity or operation, and not necessarily require or imply and deposited between these entities or operation In any this actual relation or order.Moreover, term " comprising ", "comprising" or its any other variant are intended to Nonexcludability includes, so that process, method, article or equipment including a series of elements not only will including those Element, but also the other element including being not expressly set out, or it is this process, method, article or equipment also to include Intrinsic key element.In the absence of more restrictions, the key element limited by sentence "including a ...", it is not excluded that Other identical element also be present in process, method, article or equipment including the key element.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the scope of the present invention.It is all Any modification, equivalent substitution and improvements made within the spirit and principles in the present invention etc., are all contained in protection scope of the present invention It is interior.

Claims (5)

  1. A kind of 1. pitch automatic sampling device, it is characterised in that including:
    Heating muff, pitch probe tube, temperature sensor, temperature-controlling component, sampling below atmospheric pressure bottle and vavuum pump;The heating muff It is set in outside the pitch probe tube, the temperature sensor is connected with the heating muff, the sampling below atmospheric pressure bottle and institute Pitch probe tube is stated to be connected, the vavuum pump is connected with the sampling below atmospheric pressure bottle, the temperature-controlling component and the heating muff with And the vavuum pump is connected;
    Wherein, the temperature-controlling component is used for the heating-up temperature for controlling the heating muff, and the heating muff is used for the drip Blue or green probe tube is heated, and the temperature sensor is used for the Current Temperatures for detecting the pitch probe tube, and the vavuum pump is used It is set to be internally formed subnormal ambient in the negative pressure sampling bottle inner air is extracted out.
  2. 2. device according to claim 1, it is characterised in that the temperature-controlling component includes prompting device, and the prompting device is used In sending cue when the temperature sensor detects that the pitch probe tube Current Temperatures reach design temperature.
  3. 3. device according to claim 2, it is characterised in that the prompting device includes drive circuit and buzzer.
  4. 4. device according to claim 2, it is characterised in that the prompting device includes drive circuit and LED lamp bead.
  5. 5. device according to claim 1, it is characterised in that the temperature-controlling component includes temperature assignment component, the temperature Degree assignment component is used for the heating-up temperature for setting the heating muff.
CN201711005532.4A 2017-10-25 2017-10-25 Automatic sampling device of pitch Active CN107782584B (en)

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Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
CN201711005532.4A CN107782584B (en) 2017-10-25 2017-10-25 Automatic sampling device of pitch

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CN107782584B CN107782584B (en) 2020-06-16

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110095321A (en) * 2019-05-13 2019-08-06 马钢奥瑟亚化工有限公司 A kind of on-line automatic sampler of environment-friendly high-temperature pitch

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202066715U (en) * 2010-06-25 2011-12-07 上海宝钢工业检测公司 Negative pressure oil liquid sampling device
CN202372371U (en) * 2011-11-30 2012-08-08 河北瑞晶康生物科技有限公司 Insulating and sampling device
CN204964250U (en) * 2015-09-14 2016-01-13 南京电力设备质量性能检验中心 Buggy sampling gun
CN205352767U (en) * 2015-12-30 2016-06-29 浙江龙鑫化工有限公司 Resin sampling device
CN205656030U (en) * 2016-04-05 2016-10-19 中海沥青(四川)有限公司 Pitch sampling device
CN206095711U (en) * 2016-10-13 2017-04-12 山西省交通科学研究院 Heterogeneous body pitch stratified sampling mould

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202066715U (en) * 2010-06-25 2011-12-07 上海宝钢工业检测公司 Negative pressure oil liquid sampling device
CN202372371U (en) * 2011-11-30 2012-08-08 河北瑞晶康生物科技有限公司 Insulating and sampling device
CN204964250U (en) * 2015-09-14 2016-01-13 南京电力设备质量性能检验中心 Buggy sampling gun
CN205352767U (en) * 2015-12-30 2016-06-29 浙江龙鑫化工有限公司 Resin sampling device
CN205656030U (en) * 2016-04-05 2016-10-19 中海沥青(四川)有限公司 Pitch sampling device
CN206095711U (en) * 2016-10-13 2017-04-12 山西省交通科学研究院 Heterogeneous body pitch stratified sampling mould

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110095321A (en) * 2019-05-13 2019-08-06 马钢奥瑟亚化工有限公司 A kind of on-line automatic sampler of environment-friendly high-temperature pitch
CN110095321B (en) * 2019-05-13 2024-02-02 马钢奥瑟亚化工有限公司 Environment-friendly high-temperature asphalt online automatic sampling device

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Effective date of registration: 20201014

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Patentee after: PETROCHINA FUEL OIL Co.,Ltd.

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