CN110080700A - A kind of method of Environment-protecting Drilling Fluids granularity optimization - Google Patents

A kind of method of Environment-protecting Drilling Fluids granularity optimization Download PDF

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Publication number
CN110080700A
CN110080700A CN201810076954.9A CN201810076954A CN110080700A CN 110080700 A CN110080700 A CN 110080700A CN 201810076954 A CN201810076954 A CN 201810076954A CN 110080700 A CN110080700 A CN 110080700A
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CN
China
Prior art keywords
drilling fluid
particle
drilling
granularity
environment
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810076954.9A
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Chinese (zh)
Inventor
李公让
韩来聚
李作会
周延军
刘振东
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sinopec Oilfield Service Corp
Sinopec Shengli Petroleum Engineering Corp
Drilling Technology Research Institute of Sinopec Shengli Petroleum Engineering Corp
Original Assignee
Sinopec Oilfield Service Corp
Sinopec Shengli Petroleum Engineering Corp
Drilling Technology Research Institute of Sinopec Shengli Petroleum Engineering Corp
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Publication date
Application filed by Sinopec Oilfield Service Corp, Sinopec Shengli Petroleum Engineering Corp, Drilling Technology Research Institute of Sinopec Shengli Petroleum Engineering Corp filed Critical Sinopec Oilfield Service Corp
Priority to CN201810076954.9A priority Critical patent/CN110080700A/en
Publication of CN110080700A publication Critical patent/CN110080700A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/02Well-drilling compositions
    • C09K8/04Aqueous well-drilling compositions
    • C09K8/14Clay-containing compositions
    • C09K8/18Clay-containing compositions characterised by the organic compounds
    • C09K8/22Synthetic organic compounds
    • C09K8/24Polymers
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/42Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells
    • C09K8/426Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells for plugging
    • EFIXED CONSTRUCTIONS
    • E21EARTH DRILLING; MINING
    • E21BEARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B21/00Methods or apparatus for flushing boreholes, e.g. by use of exhaust air from motor
    • E21B21/06Arrangements for treating drilling fluids outside the borehole
    • E21B21/062Arrangements for treating drilling fluids outside the borehole by mixing components
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K2208/00Aspects relating to compositions of drilling or well treatment fluids
    • C09K2208/10Nanoparticle-containing well treatment fluids

Abstract

A kind of method of Environment-protecting Drilling Fluids granularity optimization, at room temperature, drilling fluid is added in nano-particle and subparticle, then high-speed stirred 30min ~ 60min, making drilling fluid size distribution after above-mentioned particle is added is in normal distribution within 20 μm, whole is in bimodal distribution, and the optimization of drilling fluid granularity can be realized.The drilling fluid includes 3 ~ 5%wt sodium bentonite, 1 ~ 3%wt sulfonated phenol formaldehyde resin, pH=7 ~ 10.The nano-particle particle size range is 2~5 μm, 0.1 ~ 5%wt of content in drilling fluid;The subparticle particle size range is 5~20 μm, 0.1 ~ 8%wt of content in drilling fluid.This method optimizes drilling fluid size distribution using varigrained nontoxic particle, forms high-quality mud cake in the borehole wall, is conducive to safely and fast drilling well, is suitable for the fields such as the leak stopping of oil drilling leakage type, borehole wall reinforcing.

Description

A kind of method of Environment-protecting Drilling Fluids granularity optimization
Technical field
The present invention relates to oil drilling auxiliary chemicals field, in particular to a kind of side of Environment-protecting Drilling Fluids granularity optimization Method.
Background technique
It is analyzed according to statistics, brill Well Completion Engineering of Oil Reservoirs occupies 40 ~ 60% with modern oilfield prospecting developing totle drilling cost, bores The quality of well construction quality directly influences obtainable economic benefit.Wellbore stability, mud cake quality, drilling speed in drilling process Speed, down hole problem prevention and processing all be unable to do without property of drilling fluid control.In drilling process, need at any time Regulate and control the performances such as density, the viscosity of drilling fluid, keeps the stability and greasy property of drilling fluid system, enhance the leak-off of drilling fluid Wave making machine adjusts the performance of drilling fluid when complex situations occurs in underground in time.The properties of drilling fluid are all solid with drilling fluid The distribution situation of phase granularity has direct or indirect relationship, by adjusting mud solid phase granule content, size, distribution Situation and gradation relationship can largely influence the properties of drilling fluid.
The solid particle in drilling fluid is scattered in as the solid phase in drilling fluid, and there are mainly two types of its sources, first is that coming Derived from the landwaste for the rock generation that is broken, second is that be artificially added for drilling technology requirement.In drilling process, in drilling fluid The size distribution of solid phase particles has a very big impact the traditional performance parameter and oil layer protection performance of drilling fluid.It can be with shadow Rheological characteristic, the size of the quality of mud cake quality and filter loss for ringing drilling fluid, to drilling technology challenge (such as mud shale and coal The collapsing of layer, undergauge, bit freezing, pressure excitement etc.) have a significant impact, especially deep-well, as drilling cuttings etc. is ground for a long time, Solid concentration increase inferior, solid phase particles size distribution are unreasonable in drilling fluid, it is easy to the performances such as rheological characteristic and dehydration occur Situation out of hand influences the safety of underground.Solid phase particles size distribution is unreasonable in drilling fluid also very formation damage It is big to influence.Drilling fluid particle size distribution first has a major impact mud cake quality, and adjustment drilling fluid particle size distribution can shape At thin and compact high-quality mud cake.Temporarily stifled being mainly characterized by utilizing in drilling fluid of conventional shielding has solid phase particles and stores up to oil gas Some bridge formation grains to match with pore throat blocking mechanism are artificially added in the laws for plugging of layer into drilling fluid as needed Son, particle filled composite and deformation particle, so that these particles is rapidly formed around the borehole wall, effective, permeability is almost nil Shading ring, prevent subsequent job entry well fluid in solid, liquid phase invaded formation.But currently used technology only only accounts for The relationship between material and formation pore throat is temporarily blocked up in shielding, and there is no consider that already existing solid phase particles are to temporary in drilling fluid The matched influence of blocking agent.By using level Four solid control equipment in drilling process, certain effect, but being directed in measure are achieved Property it is insufficient.
Existing researcher proposes the method for carrying out size distribution adjustment for reservoir.Application No. is 201310453524.1 patent proposes the maximum pore throat diameter D90 according to target reservoir, to drilling fluid and blocks screener The analysis of size distribution curve filters out drilling fluid and blocks the grain diameter proportion of screener.Application No. is The Low Damage grain size distribution that the patent of 201610881250.X proposes high temperature ultradeep well reservoir aggravates water-base drilling fluid, is applicable in In the drilling of the long net horizontal section of shale of microcrack development.Its technical solution is to prepare the raw materials used component of the drilling fluid and contain Amount: bentonite 13.5-15;Sodium carbonate 0.675-0.75;Calcium oxide 4.5-5;Transporting agent 2.7-3;Sulfonated phenol formaldehyde resin 45-50; Sulfonated lignite resin 45-50;Sulfonated lignite 45-50;Sefstromite powder and millimicro barite adjust density to 2.50g/cm3;Profit Lubrication prescription 27-30;Without infiltration borehole wall stabilizer 27-30;Nanometer calcium carbonate 27-30;Anti-sloughing agent 18-20;Tap water 900-1000.First After having configured clay-based slurry, then in 500r/min it is added with stirring calcium oxide, sequentially adds above-mentioned inorganic agent after continuing stirring, then Regulation system density is 2.5g/cm3It finally prepares to form Low Damage grain size distribution exacerbation water-base drilling fluid.These researchs are to brill The adjustment of well liquid size distribution plays important impetus, but fails the optimization that size distribution is carried out for environment-friendly type inorganic agent, Or it need to be further clarified in terms of size distribution form, size, content.
Summary of the invention
In response to the problems existing in the prior art, the purpose of the present invention is to provide a kind of sides of Environment-protecting Drilling Fluids granularity optimization Method, this method optimize drilling fluid size distribution using varigrained nontoxic particle, form high-quality mud cake in the borehole wall, have Conducive to safely and fast drilling well, it is suitable for the fields such as the leak stopping of oil drilling leakage type, borehole wall reinforcing.
In order to reach the purpose of the present invention, the technical scheme is that be achieved:
At room temperature, drilling fluid is added in nano-particle and subparticle, then high-speed stirred 30min ~ 60min, makes to be added above-mentioned Drilling fluid size distribution is in normal distribution within 20 μm after particle, and whole is in bimodal distribution, and it is excellent that drilling fluid granularity can be realized Change.
The drilling fluid includes 3 ~ 5%wt sodium bentonite, 1 ~ 3%wt sulfonated phenol formaldehyde resin (SMP), pH=7 ~ 10.
The nano-particle is the combination of one or more of bentonite, nanometer calcium, nano-silicon, and particle size range is 2~5 μm, 0.1 ~ 5%wt of content in drilling fluid;The subparticle is the combination of one or both of calcium carbonate, bluestone powder, grain Diameter range is 5~20 μm, 0.1 ~ 8%wt of content in drilling fluid.
Bentonite of the bentonite after hydration process in the nano-particle.
The bentonitic hydration process is at room temperature, bentonite to be configured to the bentonite slurry of 8-12%wt, then water Change 20-30h.
The present invention has the advantage that compared with prior art
(1) nano-particle and subparticle that the present invention uses, the materials such as opposite pitch, nanoemulsions, environment friendly is stronger, Asepsis environment-protecting, cost is relatively low, and granularity optimization is easy to execute-in-place;
(2) present invention can be used in the solidification of the oil drilling borehole wall and microcrack leakage stopping technology, improve filter cake intensity.
Detailed description of the invention
Attached drawing 1 is the granularity optimum results figure of an embodiment of the present invention.
Specific embodiment
The present invention is further explained in the light of specific embodiments.
Embodiment 1:
At room temperature, bentonite is configured to the bentonite slurry of 10%wt, aquation takes 100ml and 1000 mesh calcium carbonate 50g mono- afterwards for 24 hours It rises and is added in 1000ml drilling fluid, carry out high-speed stirred 30min, the optimization of drilling fluid granularity can be realized.Wherein drilling fluid includes 4%wt sodium bentonite (hereinafter referred to as sodium soil), 2%wt sulfonated phenol formaldehyde resin (hereinafter referred to as SMP), pH=8.
Embodiment 2:
At room temperature, the bentonite slurry 80ml, nano-silicon 10g that same procedure is prepared in above-described embodiment 1 are taken;800 mesh of subparticle 1000ml drilling fluid (comprising 4.5%wt sodium soil, 2.7%wt SMP, pH=9) is added in calcium carbonate 50g, 1200 mesh calcium carbonate 50g, into The optimization of drilling fluid granularity can be realized in row high-speed stirred 50min.
Embodiment 3:
At room temperature, the bentonite slurry 80ml, nanometer calcium 10g that same procedure is prepared in above-described embodiment are taken;500 mesh of subparticle is green 1000ml drilling fluid (comprising 4.5%wt sodium soil, 1.5%wt SMP, pH=7.8) is added in mountain flour 50g, 1200 mesh calcium carbonate 50g, into The optimization of drilling fluid granularity can be realized in row high-speed stirred 40min.
Embodiment 4:
At room temperature, nano-silicon l0g, nanometer calcium 10g are taken;1000ml drilling well is added in 500 mesh bluestone powder 50g, 800 mesh calcium carbonate 50g In liquid (including 3.5%wt sodium soil, 2%wt SMP, pH=8.8), high-speed stirred 55min is carried out, it is excellent that drilling fluid granularity can be realized Change.
Embodiment 5:
At room temperature, nano-silicon l0g and 800 mesh calcium carbonate 50g is taken, 1000ml drilling fluid (drilling fluid composition are as follows: 5% sodium base is swollen is added Moisten+15% weight of+0.4%+2.5% polymeric alcohol of ammonium salt+1%SMP+ 0.5%LV-CMC of native+0.2% natural polymers Spar, pH=8) in, high-speed stirred 30min, granularity optimum results such as Fig. 1.

Claims (5)

1. a kind of method of Environment-protecting Drilling Fluids granularity optimization, it is characterised in that:
At room temperature, drilling fluid is added in nano-particle and subparticle, then high-speed stirred 30min ~ 60min, makes to be added above-mentioned Drilling fluid size distribution is in normal distribution within 20 μm after particle, and whole is in bimodal distribution.
2. the method for Environment-protecting Drilling Fluids granularity according to claim 1 optimization, it is characterised in that: the drilling fluid includes 3 ~ 5%wt sodium bentonite, 1 ~ 3%wt sulfonated phenol formaldehyde resin, pH=7 ~ 10.
3. the method for Environment-protecting Drilling Fluids granularity according to claim 1 or 2 optimization, it is characterised in that: described to receive micro- Grain is the combination of one or more of bentonite, nanometer calcium, nano-silicon, and particle size range is 2~5 μm, the content in drilling fluid 0.1~5%wt;The subparticle is the combination of one or both of calcium carbonate, bluestone powder, and particle size range is 5~20 μm, 0.1 ~ 8%wt of content in drilling fluid.
4. the method for Environment-protecting Drilling Fluids granularity optimization according to claim 3, it is characterised in that: in the nano-particle Bentonite of the bentonite after hydration process.
5. the method for Environment-protecting Drilling Fluids granularity optimization according to claim 4, it is characterised in that: the bentonitic water Change processing is at room temperature, bentonite to be configured to the bentonite slurry of 8-12%wt, then aquation 20-30h.
CN201810076954.9A 2018-01-26 2018-01-26 A kind of method of Environment-protecting Drilling Fluids granularity optimization Pending CN110080700A (en)

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Application Number Priority Date Filing Date Title
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WO2009106796A1 (en) * 2008-02-29 2009-09-03 Halliburton Energy Services, Inc. Lost circulation material formulation and method of use
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Application publication date: 20190802