CN110080030A - A kind of preparation method of fire-retardant anti-forge paper - Google Patents
A kind of preparation method of fire-retardant anti-forge paper Download PDFInfo
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- CN110080030A CN110080030A CN201910314391.7A CN201910314391A CN110080030A CN 110080030 A CN110080030 A CN 110080030A CN 201910314391 A CN201910314391 A CN 201910314391A CN 110080030 A CN110080030 A CN 110080030A
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- parts
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- bone
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- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21F—PAPER-MAKING MACHINES; METHODS OF PRODUCING PAPER THEREON
- D21F11/00—Processes for making continuous lengths of paper, or of cardboard, or of wet web for fibre board production, on paper-making machines
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/34—Ignifugeants
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Abstract
The invention discloses a kind of preparation methods of fire-retardant anti-forge paper, are related to pulp technology for making paper, mainly for solving the problems, such as that existing anti-forge paper flame retardant property is poor；Method includes the following steps: 1) weigh raw material；2) dyestuff is added in basic paper pulp, base sheet of paper is dyed；3) fluorescer is added to dyeing treated in the basic paper pulp in basis, be sufficiently mixed stirring at normal temperature, obtain modified pulp；4) lubricant, fire retardant and fish-bone extract are added in modified pulp, stirring is sufficiently mixed under normal temperature environment, magma is made；5) magma is subjected to cooled and solidified, while carries out removal of impurities processing, obtain raw material to be processed；6) it treats to process raw material and carries out squeezing processing, obtain pulpboard；7) will pulpboard carry out cooling treatment after be sent into paper machine in carry out printing paper delivery, then cut to get.The present invention can effectively improve the flame retardant property of anti-forge paper.
Description
Technical field
The present invention relates to pulp technology for making paper, the preparation method of specifically a kind of fire-retardant anti-forge paper.
Background technique
Anti-counterfeiting paper antifalsification paper, surface have label or hiding secret mark (pattern, decorative pattern, watermark, number
Code etc.), it is not easy to copy, do the general designation of pseudo- or change extraordinary stationery.Anti-fake is to for the purpose of deception and without owner
Permit and carries out the imitated or activity replicated and the Prevention method taken.Typically mainly have safety paper (safety paper) and
Bank-note paper (bank-note paper；currency paper).His tensile strength, wearability, folding strength is very high.With excellent
Good water-resistance and intaglio plate printability.Using cotton, flaxen fiber as raw material, boiling, bleaching, mashing through mitigating (add wet strength agent, such as urea
Urea formaldehyde, melamine resin), on the fourdrinier machine of special designing, after pressing watermark or safety line, copied through sizing
Paper is caused, is then handled through drying, press polish and surface plastic coating and product is made.
Performance of the current anti-counterfeiting paper in flame retardant property is often not satisfactory, easily spontaneous combustion under high temperature environment, and there are one
Fixed security risk, the reason is that raw material proportioning is unreasonable.
Summary of the invention
The purpose of the present invention is to provide a kind of preparation methods of fire-retardant anti-forge paper, to solve the above problems.
To achieve the above object, the invention provides the following technical scheme:
A kind of preparation method of fire-retardant anti-forge paper, comprising the following steps:
1) the following raw material according to weight percent is weighed: basic paper pulp 34-49 parts, 1.2-2.7 parts of lubricant, fire retardant
1.3-2.8 parts, 8-14 parts of fish-bone extracting solution, 2.4-3.9 parts of dyestuff, 0.9-1.7 parts of fluorescer；
2) dyestuff is added in basic paper pulp, base sheet of paper is dyed；
3) fluorescer is added to dyeing treated in the basic paper pulp in basis, be sufficiently mixed stirring at normal temperature, obtain
Modified pulp；
4) lubricant, fire retardant and fish-bone extract are added in modified pulp, stirring is sufficiently mixed under normal temperature environment,
Magma is made；
5) magma is subjected to cooled and solidified, while carries out removal of impurities processing, obtain raw material to be processed；
6) it treats to process raw material and carries out squeezing processing, obtain pulpboard；
7) will pulpboard carry out cooling treatment after be sent into paper machine in carry out printing paper delivery, then cut to get.
Based on the above technical solution, the present invention also provides following optional technical solutions:
In a kind of optinal plan: weighing the following raw material according to weight percent in the step 1): basic paper pulp 39-
44 parts, 1.8-2.1 parts of lubricant, 1.8-2.3 parts of fire retardant, 10-12 parts of fish-bone extracting solution, 2.8-3.5 parts of dyestuff, fluorescer
1.1-1.4 part.
In a kind of optinal plan: weighing the following raw material according to weight percent in the step 1): basic paper pulp 41
Part, 2 parts of lubricant, 2.1 parts of fire retardant, 11 parts of fish-bone extracting solution, 3.3 parts of dyestuff, 1.2 parts of fluorescer.
In a kind of optinal plan: the fish-bone extracting solution the preparation method is as follows: weigh snakeheaded fish fish-bone, clean, be added
Fish-bone is sufficiently softened into acetum, is then drained, in the snakeheaded fish fish-bone after softening plus water and protease, heating carry out
Enzymatic hydrolysis, wait digest after be filtered to get fish-bone extracting solution.
In a kind of optinal plan: the step 2) further include: wash away the unreacted dyestuff after the completion of dyeing.
In a kind of optinal plan: the stirring rate in the step 3) and step 4) is 400-700rpm.
In a kind of optinal plan: the cooling treatment temperature of pulpboard is -10 DEG C in the step 7).
Compared to the prior art, beneficial effects of the present invention are as follows:
The embodiment of the present invention can be mentioned effectively by the way that fish-bone extracting solution is added using fish-bone extracting solution as building component
The flame retardant property of high anti-forge paper, have a vast market foreground with higher application value, be worth of widely use.
Specific embodiment
Each embodiment cited by the present invention is only to illustrate the present invention, is not used to limit the scope of the present invention.To this
Any modification apparent easy to know or change are without departure from spirit and scope of the invention made by invention.
Embodiment 1
In the embodiment of the present invention, a kind of preparation method of fire-retardant anti-forge paper, comprising the following steps:
1) weigh the following raw material according to weight percent: 34 parts of basic paper pulp, 1.2 parts of lubricant, 1.3 parts of fire retardant,
8 parts of fish-bone extracting solution, 2.4 parts of dyestuff, 0.9 part of fluorescer；
2) dyestuff is added in basic paper pulp, base sheet of paper is dyed；
3) fluorescer is added to dyeing treated in the basic paper pulp in basis, be sufficiently mixed stirring at normal temperature, obtain
Modified pulp；
4) lubricant, fire retardant and fish-bone extract are added in modified pulp, stirring is sufficiently mixed under normal temperature environment,
Magma is made；
5) magma is subjected to cooled and solidified, while carries out removal of impurities processing, obtain raw material to be processed；
6) it treats to process raw material and carries out squeezing processing, obtain pulpboard；
7) will pulpboard carry out cooling treatment after be sent into paper machine in carry out printing paper delivery, then cut to get.
The fish-bone extracting solution the preparation method is as follows: weigh snakeheaded fish fish-bone, clean, be added to fish-bone in acetum
Sufficiently softening, then drains, and water and protease is added in the snakeheaded fish fish-bone after softening, heating is digested, after digesting
It is filtered to get fish-bone extracting solution.
The step 2) further include: the unreacted dyestuff is washed away after the completion of dyeing.
Stirring rate in the step 3) and step 4) is 400rpm.
The cooling treatment temperature of pulpboard is -10 DEG C in the step 7).
Embodiment 2
In the embodiment of the present invention, a kind of preparation method of fire-retardant anti-forge paper, comprising the following steps:
1) weigh the following raw material according to weight percent: 39 parts of basic paper pulp, 1.8 parts of lubricant, 1.8 parts of fire retardant,
10 parts of fish-bone extracting solution, 2.8 parts of dyestuff, 1.1 parts of fluorescer；
2) dyestuff is added in basic paper pulp, base sheet of paper is dyed；
3) fluorescer is added to dyeing treated in the basic paper pulp in basis, be sufficiently mixed stirring at normal temperature, obtain
Modified pulp；
4) lubricant, fire retardant and fish-bone extract are added in modified pulp, stirring is sufficiently mixed under normal temperature environment,
Magma is made；
5) magma is subjected to cooled and solidified, while carries out removal of impurities processing, obtain raw material to be processed；
6) it treats to process raw material and carries out squeezing processing, obtain pulpboard；
7) will pulpboard carry out cooling treatment after be sent into paper machine in carry out printing paper delivery, then cut to get.
The fish-bone extracting solution the preparation method is as follows: weigh snakeheaded fish fish-bone, clean, be added to fish-bone in acetum
Sufficiently softening, then drains, and water and protease is added in the snakeheaded fish fish-bone after softening, heating is digested, after digesting
It is filtered to get fish-bone extracting solution.
The step 2) further include: the unreacted dyestuff is washed away after the completion of dyeing.
Stirring rate in the step 3) and step 4) is 600rpm.
The cooling treatment temperature of pulpboard is -10 DEG C in the step 7).
Embodiment 3
In the embodiment of the present invention, a kind of preparation method of fire-retardant anti-forge paper, comprising the following steps:
1) the following raw material according to weight percent is weighed: 41 parts of basic paper pulp, 2 parts of lubricant, 2.1 parts of fire retardant, fish
11 parts of bone extracting solution, 3.3 parts of dyestuff, 1.2 parts of fluorescer；
2) dyestuff is added in basic paper pulp, base sheet of paper is dyed；
3) fluorescer is added to dyeing treated in the basic paper pulp in basis, be sufficiently mixed stirring at normal temperature, obtain
Modified pulp；
4) lubricant, fire retardant and fish-bone extract are added in modified pulp, stirring is sufficiently mixed under normal temperature environment,
Magma is made；
5) magma is subjected to cooled and solidified, while carries out removal of impurities processing, obtain raw material to be processed；
6) it treats to process raw material and carries out squeezing processing, obtain pulpboard；
7) will pulpboard carry out cooling treatment after be sent into paper machine in carry out printing paper delivery, then cut to get.
The fish-bone extracting solution the preparation method is as follows: weigh snakeheaded fish fish-bone, clean, be added to fish-bone in acetum
Sufficiently softening, then drains, and water and protease is added in the snakeheaded fish fish-bone after softening, heating is digested, after digesting
It is filtered to get fish-bone extracting solution.
The step 2) further include: the unreacted dyestuff is washed away after the completion of dyeing.
Stirring rate in the step 3) and step 4) is 500rpm.
The cooling treatment temperature of pulpboard is -10 DEG C in the step 7).
Embodiment 4
In the embodiment of the present invention, a kind of preparation method of fire-retardant anti-forge paper, comprising the following steps:
1) weigh the following raw material according to weight percent: 44 parts of basic paper pulp, 2.1 parts of lubricant, 2.3 parts of fire retardant,
12 parts of fish-bone extracting solution, 3.5 parts of dyestuff, 1.4 parts of fluorescer；
2) dyestuff is added in basic paper pulp, base sheet of paper is dyed；
3) fluorescer is added to dyeing treated in the basic paper pulp in basis, be sufficiently mixed stirring at normal temperature, obtain
Modified pulp；
4) lubricant, fire retardant and fish-bone extract are added in modified pulp, stirring is sufficiently mixed under normal temperature environment,
Magma is made；
5) magma is subjected to cooled and solidified, while carries out removal of impurities processing, obtain raw material to be processed；
6) it treats to process raw material and carries out squeezing processing, obtain pulpboard；
7) will pulpboard carry out cooling treatment after be sent into paper machine in carry out printing paper delivery, then cut to get.
The fish-bone extracting solution the preparation method is as follows: weigh snakeheaded fish fish-bone, clean, be added to fish-bone in acetum
Sufficiently softening, then drains, and water and protease is added in the snakeheaded fish fish-bone after softening, heating is digested, after digesting
It is filtered to get fish-bone extracting solution.
The step 2) further include: the unreacted dyestuff is washed away after the completion of dyeing.
Stirring rate in the step 3) and step 4) is 600rpm.
The cooling treatment temperature of pulpboard is -10 DEG C in the step 7).
Embodiment 5
In the embodiment of the present invention, a kind of preparation method of fire-retardant anti-forge paper, comprising the following steps:
1) weigh the following raw material according to weight percent: 49 parts of basic paper pulp, 2.7 parts of lubricant, 2.8 parts of fire retardant,
14 parts of fish-bone extracting solution, 3.9 parts of dyestuff, 1.7 parts of fluorescer；
2) dyestuff is added in basic paper pulp, base sheet of paper is dyed；
3) fluorescer is added to dyeing treated in the basic paper pulp in basis, be sufficiently mixed stirring at normal temperature, obtain
Modified pulp；
4) lubricant, fire retardant and fish-bone extract are added in modified pulp, stirring is sufficiently mixed under normal temperature environment,
Magma is made；
5) magma is subjected to cooled and solidified, while carries out removal of impurities processing, obtain raw material to be processed；
6) it treats to process raw material and carries out squeezing processing, obtain pulpboard；
7) will pulpboard carry out cooling treatment after be sent into paper machine in carry out printing paper delivery, then cut to get.
The fish-bone extracting solution the preparation method is as follows: weigh snakeheaded fish fish-bone, clean, be added to fish-bone in acetum
Sufficiently softening, then drains, and water and protease is added in the snakeheaded fish fish-bone after softening, heating is digested, after digesting
It is filtered to get fish-bone extracting solution.
The step 2) further include: the unreacted dyestuff is washed away after the completion of dyeing.
Stirring rate in the step 3) and step 4) is 700rpm.
The cooling treatment temperature of pulpboard is -10 DEG C in the step 7).
The above, the only specific embodiment of the disclosure, but the protection scope of the disclosure is not limited thereto, it is any
Those familiar with the art can easily think of the change or the replacement in the technical scope that the disclosure discloses, and should all contain
It covers within the protection scope of the disclosure.Therefore, the protection scope of the disclosure should be subject to the protection scope in claims.
Claims (7)
1. a kind of preparation method of fire-retardant anti-forge paper, which comprises the following steps:
1) the following raw material according to weight percent is weighed: basic paper pulp 34-49 parts, 1.2-2.7 parts of lubricant, fire retardant 1.3-
2.8 parts, 8-14 parts of fish-bone extracting solution, 2.4-3.9 parts of dyestuff, 0.9-1.7 parts of fluorescer；
2) dyestuff is added in basic paper pulp, base sheet of paper is dyed；
3) fluorescer is added to dyeing treated in the basic paper pulp in basis, be sufficiently mixed stirring at normal temperature, be modified
Paper pulp；
4) lubricant, fire retardant and fish-bone extract are added in modified pulp, stirring is sufficiently mixed under normal temperature environment, is made
Magma；
5) magma is subjected to cooled and solidified, while carries out removal of impurities processing, obtain raw material to be processed；
6) it treats to process raw material and carries out squeezing processing, obtain pulpboard；
7) will pulpboard carry out cooling treatment after be sent into paper machine in carry out printing paper delivery, then cut to get.
2. the preparation method of fire-retardant anti-forge paper according to claim 1, which is characterized in that weighed in the step 1) with
Under according to weight percent raw material: basic paper pulp 39-44 parts, 1.8-2.1 parts of lubricant, 1.8-2.3 parts of fire retardant, fish-bone mention
Take 10-12 parts of liquid, 2.8-3.5 parts of dyestuff, 1.1-1.4 parts of fluorescer.
3. the preparation method of fire-retardant anti-forge paper according to claim 2, which is characterized in that weighed in the step 1) with
Under according to weight percent raw material: 41 parts of basic paper pulp, 2 parts of lubricant, 2.1 parts of fire retardant, 11 parts of fish-bone extracting solution, dyestuff
3.3 parts, 1.2 parts of fluorescer.
4. the preparation method of fire-retardant anti-forge paper according to claim 1, which is characterized in that the system of the fish-bone extracting solution
Preparation Method is as follows: weighing snakeheaded fish fish-bone, cleans, be added in acetum and sufficiently soften fish-bone, then drain, after softening
Snakeheaded fish fish-bone in plus water and protease, heating digested, wait digest after be filtered to get fish-bone extracting solution.
5. the preparation method of fire-retardant anti-forge paper according to claim 1, which is characterized in that the step 2) further include:
The unreacted dyestuff is washed away after the completion of dyeing.
6. the preparation method of fire-retardant anti-forge paper according to claim 1, which is characterized in that the step 3) and step 4)
In stirring rate be 400-700rpm.
7. the preparation method of fire-retardant anti-forge paper according to claim 1, which is characterized in that pulpboard in the step 7)
Cooling treatment temperature is -10 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910314391.7A CN110080030A (en) | 2019-04-18 | 2019-04-18 | A kind of preparation method of fire-retardant anti-forge paper |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910314391.7A CN110080030A (en) | 2019-04-18 | 2019-04-18 | A kind of preparation method of fire-retardant anti-forge paper |
Publications (1)
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| CN110080030A true CN110080030A (en) | 2019-08-02 |
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| CN201910314391.7A Withdrawn CN110080030A (en) | 2019-04-18 | 2019-04-18 | A kind of preparation method of fire-retardant anti-forge paper |
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|---|---|---|---|---|
| US20050263234A1 (en) * | 2003-10-28 | 2005-12-01 | Greener Bags, Llc | Reinforced paper product and method for making same |
| JP2009267010A (en) * | 2008-04-24 | 2009-11-12 | Nanojoin Kk | Electromagnetic wave suppression paper |
| CN104099810A (en) * | 2014-06-30 | 2014-10-15 | 华南理工大学 | Environment-friendly flame retardant paper and preparation method and application thereof |
| CN106480775A (en) * | 2016-08-27 | 2017-03-08 | 安阳华森纸业有限责任公司 | The preparation method of fire-retardant anti-forge paper |
| CN107326746A (en) * | 2017-06-22 | 2017-11-07 | 杭州特种纸业有限公司 | A kind of fire retardant insulating vulcan fibre and preparation method thereof |
| CN108316055A (en) * | 2018-03-28 | 2018-07-24 | 宁波依森纸制品有限公司 | A kind of fire-retardant paper furniture corrugated paper and preparation method thereof |
| CN108589375A (en) * | 2018-03-19 | 2018-09-28 | 宁波亚洲浆纸业有限公司 | The preparation method of cheque paper and anti-false fiber |
| CN109315641A (en) * | 2018-10-25 | 2019-02-12 | 荣延洲 | A kind of collagen juice drinks and preparation method thereof |
-
2019
- 2019-04-18 CN CN201910314391.7A patent/CN110080030A/en not_active Withdrawn
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20050263234A1 (en) * | 2003-10-28 | 2005-12-01 | Greener Bags, Llc | Reinforced paper product and method for making same |
| JP2009267010A (en) * | 2008-04-24 | 2009-11-12 | Nanojoin Kk | Electromagnetic wave suppression paper |
| CN104099810A (en) * | 2014-06-30 | 2014-10-15 | 华南理工大学 | Environment-friendly flame retardant paper and preparation method and application thereof |
| CN106480775A (en) * | 2016-08-27 | 2017-03-08 | 安阳华森纸业有限责任公司 | The preparation method of fire-retardant anti-forge paper |
| CN107326746A (en) * | 2017-06-22 | 2017-11-07 | 杭州特种纸业有限公司 | A kind of fire retardant insulating vulcan fibre and preparation method thereof |
| CN108589375A (en) * | 2018-03-19 | 2018-09-28 | 宁波亚洲浆纸业有限公司 | The preparation method of cheque paper and anti-false fiber |
| CN108316055A (en) * | 2018-03-28 | 2018-07-24 | 宁波依森纸制品有限公司 | A kind of fire-retardant paper furniture corrugated paper and preparation method thereof |
| CN109315641A (en) * | 2018-10-25 | 2019-02-12 | 荣延洲 | A kind of collagen juice drinks and preparation method thereof |
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Application publication date: 20190802 |