CN110079238A - A kind of AB glue with the ultra-thin intermediate following layer of high refractive index - Google Patents
A kind of AB glue with the ultra-thin intermediate following layer of high refractive index Download PDFInfo
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- CN110079238A CN110079238A CN201910476760.2A CN201910476760A CN110079238A CN 110079238 A CN110079238 A CN 110079238A CN 201910476760 A CN201910476760 A CN 201910476760A CN 110079238 A CN110079238 A CN 110079238A
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- layer
- refractive index
- high refractive
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- following layer
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J7/00—Adhesives in the form of films or foils
- C09J7/20—Adhesives in the form of films or foils characterised by their carriers
- C09J7/29—Laminated material
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Abstract
A kind of AB glue with the ultra-thin intermediate following layer of high refractive index, including the ultra-thin intermediate following layer of high refractive index, the upper surface of the intermediate following layer is pasted with one layer of low viscous silica gel layer, intermediate following layer lower surface is pasted with one layer of high adhesive-layer, the lower surface of the high adhesive-layer is pasted with one layer of silicone release film, and the upper surface of the low viscous silica gel layer is pasted with one layer of pretreatment PET film;The ultra-thin intermediate following layer of high refractive index is that inorganic nanoparticles with a high refractive index are introduced into organic coating with a high refractive index, and the organic coating is coated on the high adhesive-layer, is had following layer among hardness and high-transmittance simultaneously.High adhesive-layer is bonded tempered glass, and fit closely with glass in use, first tearing silicone release film by the AB glue of the present invention with the ultra-thin intermediate following layer of high refractive index;Pretreatment PET film is torn again; layer of silica gel is affixed on display screen; because of the low viscosity of layer of silica gel, low-surface-energy; it is fast with exhaust; it is good to be bonded effect; tempered glass is posted on the mobile terminal screens such as mobile phone by AB glue, the screen of mobile terminal product is protected not scratched, improves the surface impact energy of mobile terminal product.The present invention compare traditional AB glue have the advantages that high translucency, refractive index height, flexibility it is good, it is good to non-planar display screen adaptability, using simple, good weatherability, easily do over again.
Description
Technical field
The present invention relates to viscose glue technical fields, and in particular to a kind of AB glue with the ultra-thin intermediate following layer of high refractive index.
Background technique
Up to now, what is provided in the market is applied to tempered glass fitting AB glue entirely, mainly poly- to benzene with PET(
Naphthalate) it is substrate, substrate is low viscous organic silica gel on one side, and another side is other high mucilage materials.
The AB glue production technology is mainly: then the first laminating protective film after the coated on one side organic silica gel of PET base material exists
The another side of PET base material is coated with other high mucilage materials and laminating silicone release film.The technique major defect has: substrate is by two
It is secondary to unreel stretcher strain;Secondary coating process will affect the planarization for the glue-line having been coated with for the first time, to influence entirety
Product quality.In addition, certain from haveing the defects that on optical as the intermediate PET using layer, refractive index is low, mist degree compared with
Height, and the trilaminate material index of refraction difference in the above structure is larger, reduces light transmittance, the refractive index of AB glue;PET base material thickness is high
Cause AB glue pliability insufficient, it is poor to be bonded effect entirely to non-planar display screen, causes client's experience on probation bad.
And after directly removing intermediate PET base material, cause the hardness of AB glue to reduce, at the same above-mentioned high mucilage materials with it is organic
Silica gel directly contacts, and due to the low-surface-energy characteristic of organic silica gel, the adhesion of above-mentioned high mucilage materials and organic silica gel is complete
It is insufficiently resistant to the extraneous mechanical force given, leads to that above-mentioned high mucilage materials and organic silica gel disengaging and residue glue occurs, fall glue
Etc. bad.
Summary of the invention
The purpose of the present invention is being directed to disadvantages mentioned above in the prior art, provide it is a kind of have high refractive index it is ultra-thin in indirectly
The AB glue of layer.It is coated with one layer of ultra-thin intermediate following layer among silica gel and high viscose glue, bonds two class glue systems by following layer,
The PET in traditional AB glue material is eliminated, with thickness is low, adhesiveness is good, flexibility is good, light transmittance is high, refractive index is high, mist
It spends low and is influenced small advantage by coating process, and high temperature and humidity (60 DEG C/90%RH) aging in 30 days can be subjected to without quality comparison.
The purpose of the present invention is achieved through the following technical solutions:
A kind of AB glue with the ultra-thin intermediate following layer of high refractive index, including the ultra-thin intermediate following layer of high refractive index, the centre
The upper surface of following layer is pasted with one layer of low viscous silica gel layer, and intermediate following layer lower surface is pasted with one layer of high adhesive-layer, described
The lower surface of high adhesive-layer is pasted with one layer of silicone release film, and the upper surface of the layer of silica gel is pasted with one layer of pretreatment PET
Film;
The ultra-thin intermediate following layer of high refractive index is to introduce inorganic nanoparticles with a high refractive index to have high refractive index
Organic coating in, the organic coating is coated on the high adhesive-layer, is had in hardness and high-transmittance simultaneously
Between following layer.
Further, the peeling force for pre-processing PET film is 2~10 times of peeling force of the silicone release film.
Further, the processing mode for pre-processing PET film, which is selected from, to be modified, by the coating of fluorine element mould release without the release coating of silicon
Modified, polyester primary coat processing is modified, polyurethane primary coat processing is modified, sided corona treatment is modified.
Further, the sticky range of the high adhesive-layer is 0.1~15000gf/inch, with a thickness of 20 μm~500 μ
m.Wherein, the high adhesive-layer is acrylic material, polyurethane material, rubber type of material, silicone material, polyesters material
Material, polyamide polymer, epoxy-like materials, vinyl alkyl ethers material, fluorine class material.
In above-mentioned high mucilage materials, acrylic material and rubber type of material can be properly used.Wherein, from heat-resisting
Property, having excellent weather resistance etc. considers, preferred acrylic material.Acrylic material with acrylic acid series polymeric compounds be mainly at
Point or base polymer.In addition, as basic polymer (basis of high viscose glue), it is preferable to use with the carbon atom number of alkyl
(methyl) alkyl acrylate (alkyl acrylate, alkyl methacrylate) for 4~12 is the poly- of monomer main component
Close object.Being somebody's turn to do (methyl) acrylic acid C4-12 Arrcostab based polymer can be used alone, can also two kinds of combination of the above uses.
(methyl) alkyl acrylate ((methyl) acrylic acid C4-12 that carbon atom number as the alkyl is 4~12
Arrcostab), as long as (methyl) alkyl acrylate that the carbon atom number of alkyl is 4~12, is not particularly limited, if enumerated
It is workable to include but is not limited to: (methyl) butyl acrylate, (methyl) isobutyl acrylate, (methyl) acrylic acid, (methyl)
Tert-butyl acrylate, (methyl) amyl acrylate, (methyl) isoamyl acrylate, (methyl) acrylic acid peopentyl ester, (methyl) third
The own ester of olefin(e) acid, (methyl) heptylacrylate, (methyl) 2-EHA, (methyl) 2-ethyl hexyl acrylate, (methyl) propylene
The different monooctyl ester of acid, (methyl) nonyl acrylate, the different nonyl ester of (methyl) acrylic acid, (methyl) decyl acrylate, (methyl) acrylic acid are different
Last of the ten Heavenly stems ester, (methyl) acrylic acid hendecane base ester, (methyl) dodecylacrylate etc..(methyl) acrylic acid C4-12 Arrcostab
It can be used alone, it can also two kinds of combination of the above uses.
Further, it is organic pressure-sensitive gel or organic silicon rubber, viscosity that the low viscous silica gel layer, which is the layer of silica gel,
Range is 0.1~100gf/inch, with a thickness of 20 μm~200 μm.The organic pressure-sensitive gel is hydroxyl condensation type organosilicon pressure
Quick glue, peroxide cure condensed type organic silicon pressure sensitive adhesive, addition curable organic pressure-sensitive gel, room temperature vulcanized organosilicon pressure
One or more of mixture in quick glue and organotin catalyzed type silicon pressure sensitive adhesive.
Preferably, the organic silicon rubber is liquid silastic, hydroxyl condensation type organic silicon rubber, peroxide cure contracting
Mould assembly organic silicon rubber, addition curable organic silicon rubber, room temperature vulcanized organic silicon rubber and organotin catalyzed type silicon rubber
The mixture of middle one or more.
Preferably, the organic pressure-sensitive gel is to wrap solvent-laden organic pressure-sensitive gel, and the solvent is toluene, dimethylbenzene
Or 100~No. 120 solvent naphthas.
The ultra-thin intermediate following layer of high refractive index the preparation method is as follows:
(1) Sol A containing inorganic nanoparticles is prepared, the inorganic nanoparticles are TiO2、ZnO、SiO2Or ZrO;
(2) organic monomer with a high refractive index and Sol A are compounded, they are organic monomer according to mass ratio: 35 ~ 50 parts, colloidal sol
A:15 ~ 30 part, under high velocity agitation instill Sol A in the mixture of organic monomer and solvent, temperature by 100 ~ 200 parts of solvent
It is 25 ~ 50 DEG C, mixing time is 1 ~ 3 hour, and 1 ~ 5 part of curing agent is added, and 1 ~ 10 part of levelling agent is adjusted by evaporating the amount of solvent
The viscosity of mixture is saved, the viscosity of obtained organic coating is 15 ~ 35cps.
(3) intermediate following layer is coated on high adhesive-layer, the organic coating made from step (2), selecting line number is 120
The anilox roll of~180LPI, diameter 30mm adjust 5~10m/min of coating machine linear speed, anilox roll 40~50r/min of revolving speed, coating
On high adhesive-layer, through oven drying, temperature is set in 80~150 DEG C, and solvent is made to volatilize, and organic coating solidification obtains high folding
Penetrate the ultra-thin intermediate following layer of rate.
Preferably, the organic monomer is polyvinyl alcohol, in polymethyl methacrylate, polyamide, polyethylene, polypropylene
One kind;The organic solvent is one of isopropanol, ethyl alcohol, ethyl acetate, butanone.
Further, the intermediate following layer with a thickness of 0.01~8 μm.
Further, the refractive index of the intermediate following layer is 1.4 ~ 1.6.
Further, the silicone release film thickness is at 20 μm~200 μm, and the pretreatment PET film thickness is at 38 μm
~250 μm.
The invention has the benefit that
(1) existing display screen protection AB glue needs coating silica gel and other viscose glue materials on a thickness of 20~100 μm of substrates
Material, the AB glue with the ultra-thin intermediate following layer of high refractive index of the invention are free of intermediate base material, AB glue thickness can be greatly reduced, mention
Light transmittance, the refractive index for rising AB glue, increase the flexibility and deformability of AB glue.Light transmittance is up to 95% or more, and mist degree is lower than
0.2%, refractive index > 1.4, the screen colour gamut that will not influence the display screens such as mobile phone show, and does not have watermark, no Newton's ring, residue glue,
It is bad to fall glue, xanthochromia etc., it is simple using fitting.
(2) the ultra-thin intermediate following layer of high refractive index of the invention is to introduce inorganic nanoparticles with a high refractive index to have
Have in the organic coating of high refractive index, while so that ultra-thin intermediate following layer is met high refractive index, and there is certain hardness, make
AB glue is unlikely to deform, and facilitates operation.
(3) AB glue of the present invention by the Sol A containing inorganic nanoparticles and organic monomer with a high refractive index compounding and
At, have excellent anti-aging property, proved by long-term ageing, can reach long-term stable transparent effect.
Detailed description of the invention
The present invention will be further described with reference to the accompanying drawings, but the embodiment in attached drawing is not constituted to any limit of the invention
System, for those of ordinary skill in the art, without creative efforts, can also obtain according to the following drawings
Other attached drawings.
Fig. 1 is the structural schematic diagram of a preferred embodiment of the invention.
Wherein 1 is silicone release film, and 2 be high adhesive-layer, and 3 be the ultra-thin following layer of high refractive index, and 4 be low viscous silica gel
Layer, 5 be pretreatment PET film.
Specific embodiment
It is described further below with reference to technical effect of the attached drawing to design of the invention, specific structure and generation, with
It is fully understood from the purpose of the present invention, feature and effect.
As shown in Figure 1, a kind of AB glue with the ultra-thin intermediate following layer of high refractive index of the present embodiment, including high refractive index
Ultra-thin intermediate following layer, the upper surface of the intermediate following layer are pasted with one layer of low viscous silica gel layer, intermediate following layer lower surface
Be pasted with one layer of high adhesive-layer, the lower surface of the high adhesive-layer is pasted with one layer of silicone release film, the layer of silica gel it is upper
Surface is pasted with one layer of pretreatment PET film;The ultra-thin intermediate following layer of high refractive index inorganic is received with a high refractive index
Rice grain is introduced into organic coating with a high refractive index, and the organic coating is coated on the high adhesive-layer, is obtained same
When there is following layer among hardness and high-transmittance.The ultra-thin intermediate following layer of high refractive index the preparation method is as follows:
(1) preparation contains TiO2The Sol A of nano particle, (2) compound acrylic monomers with a high refractive index and Sol A,
It is acrylic monomers according to mass ratio: 35 parts, Sol A: 15 parts, 100 parts of solvent isopropanol, under high velocity agitation drips Sol A
In the mixture for entering acrylic monomers and isopropanol, temperature is 25 ~ 30 DEG C, and mixing time is 2 hours, and 1 ~ 5 part of curing agent is added,
1 ~ 10 part of levelling agent, adjusts the viscosity of mixture by evaporating the amount of solvent, and the viscosity of obtained organic coating is 15 ~
20cps.(3) intermediate following layer, the organic coating made from step (2) are coated on high adhesive-layer, selection line number is 120LPI
Anilox roll, diameter 30mm adjusts coating machine linear speed 5m/min, and anilox roll revolving speed 40r/min is coated on high adhesive-layer, passes through
Oven drying, temperature are set in 80~100 DEG C, solvent are made to volatilize, and organic coating solidification obtains the ultra-thin centre of high refractive index then
Layer.
The curing agent is preferably vinyl triamine, diaminodiphenyl-methane, dimethylamine propylamine.
The levelling agent is preferably dimethyl silicone polymer, acrylate.
AB glue of the present invention with the ultra-thin intermediate following layer of high refractive index, in use, first tearing silicone release film 1
It opens, high adhesive-layer 2 is fitted in into tempered glass entirely, using the strong bonding force of high adhesive-layer 2 and the high flexibility of AB glue, make height
Adhesive-layer 2 is fitted closely with glass;Then pretreatment PET film 5 is torn, layer of silica gel 4 is fitted in into the mobile terminals such as mobile phone and is produced
On product display screen, layer of silica gel 4 has self-bleeding function because of its low viscosity, low-surface-energy, and fitting effect is good, passes through AB glue
Tempered glass is posted on the mobile terminal screens such as mobile phone, the screen of mobile terminal product is protected not scratched, improves movement
The surface impact energy of end product.The present invention have thickness is low, translucency is high, mist degree is low, refractive index is high, flexibility is high,
It is good to non-planar display screen adaptability, use simple, good weatherability, easily the advantages of doing over again.
The preparation process of AB glue of the present invention with the ultra-thin intermediate following layer of high refractive index is as follows:
A. high viscose glue is coated on silicone release film 1, after carrying out drying and glue curing processing, in 1 table of silicone release film
Face forms one layer high adhesive-layer 2;
B. it is coated with the ultra-thin intermediate following layer of high refractive index on high 2 surface of adhesive-layer, after carrying out drying and curing process, made high viscous
2 surface of glue-line forms the ultra-thin following layer 3 of one layer of high refractive index;
C. in the ultra-thin centre of high refractive index, then layer surface is coated with layer of silica gel 4, after carrying out drying and processing, keeps high refractive index ultra-thin
Intermediate then layer surface forms one layer of layer of silica gel 4;
D. cover pretreatment PET film 5 on low 4 surface of viscous silica gel layer, obtain it is of the invention have high refractive index it is ultra-thin in indirectly
The AB glue of layer.
The removing of the embodiment of the present invention pretreatment PET film 5 should be 2~10 times of 1 peeling force of silicone release film.
Preferably, the peeling force of silicone release film 1 is 2~10g.Under the peeling force, facilitate silicone release film 1
It is torn from the surface of high adhesive-layer 2, and it is impaired in die cutting procedure to can effectively avoid material;
Preferably, the peeling force for pre-processing PET film 5 is 20~60g, under the peeling force, can effectively avoid high adhesive-layer 2 and is bonded
When tempered glass, because glue film is taken up caused by tearing silicone release film 1, it can not normally be bonded phenomenon;And in the peeling force
Under, glue film will not be destroyed because of mechanical external force, to be conducive to the tight of the mobile terminals product surface such as layer of silica gel 4 and mobile phone
Closely connected conjunction.
The silicone release film 1 of the present embodiment is the film of PET material trace hydrocarbons organosilicon.
AB glue of the present invention with the ultra-thin intermediate following layer of high refractive index, refractive index 1.55, shore hardness 55HA,
After 150 DEG C, 10 hours thermal aging tests, light transmittance maintains 95% or more.After ultraviolet ageing test in 150 hours, thoroughly
Light rate maintains 92% or more.
It is preferable implementation of the invention to be specifically described, but the present invention is not limited to the embodiments, are familiar with this above
The technical staff in field can make various replacements under the premise of without prejudice to spirit and and deform, these equivalent deformations
And replacement is all contained in that this application claims within restriction.
Claims (8)
1. a kind of AB glue with the ultra-thin intermediate following layer of high refractive index, it is characterised in that: including
The ultra-thin intermediate following layer of high refractive index, the upper surface of the intermediate following layer are pasted with one layer of low viscous silica gel layer, intermediate
Following layer lower surface is pasted with one layer of high adhesive-layer, and the lower surface of the high adhesive-layer is pasted with one layer of silicone release film, institute
The upper surface for stating layer of silica gel is pasted with one layer of pretreatment PET film;
The ultra-thin intermediate following layer of high refractive index is to introduce inorganic nanoparticles with a high refractive index to have high refractive index
Organic coating in, the organic coating is coated on the high adhesive-layer, is had in hardness and high-transmittance simultaneously
Between following layer.
2. a kind of AB glue with the ultra-thin intermediate following layer of high refractive index according to claim 1, which is characterized in that described
The peeling force of pretreatment PET film is 2~10 times of the peeling force of the silicone release film.
3. a kind of AB glue with the ultra-thin intermediate following layer of high refractive index according to claim 1, which is characterized in that pre- place
The processing mode of reason PET film is selected from, without silicon release coating modified, polyester primary coat processing modified by the coating of fluorine element mould release and changes
Property, polyurethane primary coat processing is modified, sided corona treatment is modified.
4. a kind of AB glue with the ultra-thin intermediate following layer of high refractive index according to claim 1, which is characterized in that described
The sticky range of high adhesive-layer is 0.1~15000gf/inch, with a thickness of 20 μm~500 μm;The low viscous silica gel layer viscosity
Range is 0.1~100gf/inch, with a thickness of 20 μm~200 μm.
5. a kind of AB glue with the ultra-thin intermediate following layer of high refractive index according to claim 1, which is characterized in that described
The ultra-thin intermediate following layer of high refractive index the preparation method is as follows:
(1) Sol A containing inorganic nanoparticles is prepared, the inorganic nanoparticles are TiO2、ZnO、SiO2Or ZrO;
(2) organic monomer with a high refractive index and Sol A are compounded, they are organic monomer according to mass ratio: 35 ~ 50 parts, colloidal sol
A:15 ~ 30 part, under high velocity agitation instill Sol A in the mixture of organic monomer and solvent, temperature by 100 ~ 200 parts of solvent
It is 25 ~ 50 DEG C, mixing time is 1 ~ 3 hour, and 1 ~ 5 part of curing agent is added, and 1 ~ 10 part of levelling agent is adjusted by evaporating the amount of solvent
The viscosity of mixture is saved, the viscosity of obtained organic coating is 15 ~ 35cps;
(3) be coated with intermediate following layer on high adhesive-layer, the organic coating made from step (2), select line number be 120~
The anilox roll of 180LPI, diameter 30mm adjust 5~10m/min of coating machine linear speed, and anilox roll 40~50r/min of revolving speed is coated on
On high adhesive-layer, through oven drying, temperature is set in 80~150 DEG C, and solvent is made to volatilize, and organic coating solidification obtains high refraction
The ultra-thin intermediate following layer of rate.
6. a kind of AB glue with the ultra-thin intermediate following layer of high refractive index according to claim 5, which is characterized in that described
Organic monomer is one of polyvinyl alcohol, polymethyl methacrylate, polyamide, polyethylene, polypropylene;The organic solvent
For one of isopropanol, ethyl alcohol, ethyl acetate, butanone.
7. a kind of AB glue with the ultra-thin intermediate following layer of high refractive index according to claim 5, which is characterized in that described
Intermediate following layer with a thickness of 0.01~8 μm.
8. a kind of AB glue with the ultra-thin intermediate following layer of high refractive index according to claim 5, which is characterized in that described
The refractive index of intermediate following layer is 1.4 ~ 1.6.
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CN201910476760.2A CN110079238A (en) | 2019-06-03 | 2019-06-03 | A kind of AB glue with the ultra-thin intermediate following layer of high refractive index |
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Cited By (2)
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CN115991961A (en) * | 2022-12-15 | 2023-04-21 | 太湖金张科技股份有限公司 | Organic silicon optical adhesive with different double-sided adhesive properties |
CN116023866A (en) * | 2023-01-13 | 2023-04-28 | 苏州佳值电子工业有限公司 | High weather-proof ultrathin adhesive tape convenient to attach |
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CN107216821A (en) * | 2016-03-22 | 2017-09-29 | 琳得科株式会社 | The manufacture method of double-faced pressure-sensitive adhesive sheet, display body and display body |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN115991961A (en) * | 2022-12-15 | 2023-04-21 | 太湖金张科技股份有限公司 | Organic silicon optical adhesive with different double-sided adhesive properties |
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