CN110075445A - A kind of preparation method of intelligent fire fighting patch - Google Patents
A kind of preparation method of intelligent fire fighting patch Download PDFInfo
- Publication number
- CN110075445A CN110075445A CN201910477017.9A CN201910477017A CN110075445A CN 110075445 A CN110075445 A CN 110075445A CN 201910477017 A CN201910477017 A CN 201910477017A CN 110075445 A CN110075445 A CN 110075445A
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- China
- Prior art keywords
- patch
- parts
- microballoon
- preparation
- fire
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Classifications
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- A—HUMAN NECESSITIES
- A62—LIFE-SAVING; FIRE-FIGHTING
- A62C—FIRE-FIGHTING
- A62C2/00—Fire prevention or containment
-
- A—HUMAN NECESSITIES
- A62—LIFE-SAVING; FIRE-FIGHTING
- A62C—FIRE-FIGHTING
- A62C3/00—Fire prevention, containment or extinguishing specially adapted for particular objects or places
-
- A—HUMAN NECESSITIES
- A62—LIFE-SAVING; FIRE-FIGHTING
- A62D—CHEMICAL MEANS FOR EXTINGUISHING FIRES OR FOR COMBATING OR PROTECTING AGAINST HARMFUL CHEMICAL AGENTS; CHEMICAL MATERIALS FOR USE IN BREATHING APPARATUS
- A62D1/00—Fire-extinguishing compositions; Use of chemical substances in extinguishing fires
- A62D1/0007—Solid extinguishing substances
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- Business, Economics & Management (AREA)
- Emergency Management (AREA)
- Health & Medical Sciences (AREA)
- Public Health (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Fire-Extinguishing Compositions (AREA)
- Fireproofing Substances (AREA)
Abstract
The present invention relates to a kind of preparation methods of intelligent fire fighting patch, the intelligent fire fighting patch is made by following steps: (1) by 1-5 parts of drier, 1-6 parts of defoaming agent, 1-25 parts of rheium oxide, 25-40 parts of adhesive mix in the high-speed mixer that revolving speed is 1000-1500r/min；(2) prepare carrier patch, and the mixture obtained in carrier patch upper (1)；(3) it will quickly put out a fire microballoon 30-60 parts and be paved on the carrier patch for being cast with mixture, press lightly on fire extinguishing microballoon, it submerges fire extinguishing about 1/4~2/3 volume of microballoon in mixture, the carrier patch for being paved with fire extinguishing microballoon is dried or dried, intelligent fire fighting patch is obtained.The intelligent fire fighting patch prepared can according to circumstances clip and paste the inner wall in protected object.Patch preparation is simple, and easy for installation, strong operability can be triggered in Initial Stage of Fire, and then discharges a large amount of extinguishing chemicals and effectively put out a fire, and then reduce loss.
Description
Technical field
The invention belongs to fire-fighting fire extinguishing Material Fields, and in particular to a kind of preparation method of intelligent fire fighting patch.
Background technique
With the rapid growth of China's economic society, fire increasingly takes place frequently, and how to effectively prevent and control fire, it has also become
Important research theme.Along with the increase of electricity consumption, the generation of appliance fire is also at abruptly increase situation.Electrical fire, which usually occurs, is
In various small-sized confined spaces, such as: the narrow sky such as power distribution cabinet, motor cabinet, electric socket board, Air conditioner cabinet, gas tank storage cabinet
Between.These places, since prolonged dust is fallen into, electrical overload, plug or the factors such as interface damage and power utilization environment are abnormal,
Cause power outlet, electricity consumption interface on fire, although electric cabinet and socket have fire proofing package, prolonged use makes
Pipeline aging, interface loosen all the reason of being triggering fire, so that the security of the lives and property to people threatens.It develops efficient
Fire extinguishing note is just particularly important.
Summary of the invention
The object of the present invention is to provide a kind of water resistance, salt spray corrosion resistance are excellent, good extinguishing effect is at low cost,
The preparation method of the intelligent fire fighting patch of contamination-free.
The technical solution adopted by the present invention is that: a kind of preparation method of intelligent fire fighting patch, comprising the following steps:
(1) by 1-5 parts of drier, 1-6 parts of defoaming agent, 1-25 parts of rheium oxide, 25-40 parts of adhesive are 1000- in revolving speed
It is mixed in the high-speed mixer of 1500r/min, obtains mixture；
(2) prepare carrier patch, and the mixture obtained in carrier patch upper step (1)；
(3) it will quickly put out a fire microballoon 30-60 parts and be paved on the carrier patch for being cast with mixture, it is micro- to press lightly on fire extinguishing
Ball submerges the volume of fire extinguishing microballoon 1/4~2/3 in mixture, and then the carrier patch for being paved with fire extinguishing microballoon is dried or dried in the air
It is dry, obtain intelligent fire fighting patch.
Further, the drier is dibutyl tin dilaurate.
Further, the defoaming agent is that polyoxyethylene polyoxy propyl alcohol amidogen ether, polypropylene glycerol aether or polyoxypropylene are poly-
The mixing of one or more of ethylene oxide glycerin ether.
Further, described adhesive be phenolic resin glue, polyvinyl acetate resin adhesive, urea-formaldehyde resin adhesive, polyurethane adhesive,
The mixing of one or more of polyacrylic acid ester gum or butadiene-styrene rubber.
Further, the preparation method of the fire extinguishing microballoon includes: the 0.1-5 parts of detergent alkylate sulphurs of addition in reaction kettle
Sour sodium, 5-30 part extinguishing chemical and 20-50 parts of water emulsify 5-30min, and 1-5 parts of wall materials are then added, are warming up to after microballoon is formed
50-110 DEG C is solidified, and washing obtains fire extinguishing microballoon.
Further, the extinguishing chemical is AFFF (aqueous film-forming foam extinguishing agent), FP (fluoroprotein foam extinguishing agent), seven fluorine
The mixing of one or more of propane, pentafluoroethane, fluoroform, hexafluoropropane or three fluoro- iodomethane.
Further, the wall material is styrene, Lauxite prepolymer, methyl methacrylate or phenolic resin pre-polymerization
The mixing of one or more of object.
The beneficial effects of the present invention are:
1, the intelligent fire fighting patch prepared using method of the invention have transport storage it is convenient, cheap, using simply,
The high advantage of safety, fire extinguishing effectiveness.
2, synthetic method of the present invention is simple, and technical maturity, raw material sources are extensive, at low cost, and industrialized production may be implemented.
3, the intelligent fire fighting patch that will be prepared using method of the invention according to circumstances clip and paste protected object (such as: power distribution cabinet,
Motor cabinet, electric socket board, Air conditioner cabinet and gas tank storage cabinet) inner wall, easy for installation, strong operability can be in Initial Stage of Fire
It is triggered, and then discharges a large amount of extinguishing chemicals and effectively put out a fire, and then reduce loss.
4, rhenium is a kind of metallic element, 3180 DEG C of fusing point, one of refractory metal, for manufacturing electric lamp filament, artificial satellite
With shell, the protective plate of atomic pile of rocket etc., the oxide of rhenium and its rhenium equally has very high fusing point, goes out intelligently
Contain rheium oxide in the adhesive of fire patch, substantially increases the fire resistance of the adhesive of intelligent fire fighting note.It is pasted in intelligent fire fighting
When normal work, the fire extinguishing exposed wall material outside adhesive of microballoon can be discharged extinguishing chemical by thermal fracture, reach fixed point release
Effect.
Specific embodiment
Embodiment 1
1, the preparation of intelligent fire fighting patch
(1) 1.5 parts of neopelexes, 20 parts AFFF and 30 part the preparation of fire extinguishing microballoon: are added in reaction kettle
Water emulsifies 5-30min, and 3.5 parts of Lauxite prepolymers are then added, 50 DEG C are warming up to after microballoon is formed and is solidified, to
Water washing collection product after the completion of solidification, as fire extinguishing microballoon；
(2) by 2 parts of dibutyl tin dilaurate, 2.6 parts of amidogen ether of polyoxyethylene polyoxy propyl alcohol, 5 parts of rheium oxide, polyurethane adhesive
32 parts mix in the high-speed mixer that revolving speed is 1000-1500r/min, obtain mixture；
(3) prepare carrier patch, and the mixture obtained in carrier patch upper step (2)；
(4) it will quickly put out a fire 38 parts of microballoon and be paved on the carrier patch for being cast with mixture, press lightly on fire extinguishing microballoon, make
Fire extinguishing about 1/3 volume of microballoon is submerged in mixture, and the carrier patch for being paved with fire extinguishing microballoon is dried or dried, intelligence is obtained and goes out
Fire patch.
Embodiment 2
1, the preparation of intelligent fire fighting patch
(1) 4 parts of neopelexes, 30 parts of FP and 50 part of water, cream the preparation of fire extinguishing microballoon: are added in reaction kettle
Change 5-30min, 5 parts of methyl methacrylates are then added, 65 DEG C are warming up to after microballoon is formed and is solidified, completion to be solidified
Water washing collection product afterwards, as fire extinguishing microballoon；
(2) by 2.5 parts of dibutyl tin dilaurate, 2.6 parts of amidogen ether of polyoxyethylene polyoxy propyl alcohol, 5 parts of rheium oxide, polyurethane
25 parts of glue mix in the high-speed mixer that revolving speed is 1000-1500r/min, obtain mixture；
(3) prepare carrier patch, and the mixture obtained in carrier patch upper step (2)；
(4) it will quickly put out a fire 32 parts of microballoon and be paved on the carrier patch for being cast with mixture, press lightly on fire extinguishing microballoon, make
Fire extinguishing about 1/3 volume of microballoon is submerged in mixture, and the carrier patch for being paved with fire extinguishing microballoon is dried or dried, intelligence is obtained and goes out
Fire patch.
Embodiment 3
1, the preparation of intelligent fire fighting patch
(1) put out a fire microballoon preparation: in reaction kettle be added 2 parts of neopelexes, 10 part of three fluoro- iodomethane and
25 parts of water emulsify 5-30min, and 3.5 parts of phenolic resin prepolymers are then added, 65 DEG C are warming up to after microballoon is formed and is consolidated
Change, water washing collection product after the completion to be solidified, as fire extinguishing microballoon；
(2) by 2.5 parts of dibutyl tin dilaurate, 3.5 parts of polypropylene glycerol aether, 8 parts of rheium oxide, 28 parts of butadiene-styrene rubber exists
It is mixed in the high-speed mixer that revolving speed is 1000-1500r/min, obtains mixture；
(3) prepare carrier patch, and the mixture obtained in carrier patch upper step (2)；
(4) it will quickly put out a fire 45 parts of microballoon and be paved on the carrier patch of pour mixture, press lightly on fire extinguishing microballoon, make to go out
About 1/3 volume of fiery microballoon is submerged in mixture, and the carrier patch for being paved with fire extinguishing microballoon is dried or dried, intelligent fire fighting is obtained
Patch.
Embodiment 4
1, the preparation of intelligent fire fighting patch
(1) 1.5 parts of neopelexes, 20 parts AFFF and 40 part the preparation of fire extinguishing microballoon: are added in reaction kettle
Water emulsifies 5-30min, and 3.5 parts of methyl methacrylates are then added, 60 DEG C are warming up to after microballoon is formed and is solidified, to
Water washing collection product after the completion of solidification；
(2) by 2 parts of dibutyl tin dilaurate, 3 parts of polypropylene glycerol aether, 15 parts of rheium oxide, 30 parts of butadiene-styrene rubber are turning
It is mixed in the high-speed mixer that speed is 1000-1500r/min, obtains mixture；
(3) prepare carrier patch, and the mixture obtained in carrier patch upper step (2)；
(4) it will quickly put out a fire 50 parts of microballoon and be paved on the carrier patch of pour mixture, press lightly on fire extinguishing microballoon, make to go out
About 1/3 volume of fiery microballoon is submerged in mixture, and the carrier patch for being paved with fire extinguishing microballoon is dried or dried, intelligent fire fighting is obtained
Patch.
Embodiment 5
1, the preparation of intelligent fire fighting patch
(1) 2 parts of neopelexes, 20 parts of FP and 30 part of water, cream the preparation of fire extinguishing microballoon: are added in reaction kettle
Change 5-30min, 4 parts of styrene are then added, is formed to microballoon, then heats to 60 DEG C and solidified, water after the completion to be solidified
Collection product is washed, as fire extinguishing microballoon；
(2) by 4 parts of dibutyl tin dilaurate, 4 parts of polypropylene glycerol aether, 15 parts of rheium oxide, polyacrylic acid ester gum 35
Part mixes in the high-speed mixer that revolving speed is 1000-1500r/min, obtains mixture；
(3) prepare carrier patch, and the mixture obtained in carrier patch upper step (2)；
(4) it will quickly put out a fire 50 parts of microballoon and be paved on the carrier patch of pour mixture, press lightly on fire extinguishing microballoon, make to go out
Fiery 1/3 volume of microballoon is submerged in mixture, and the carrier patch for being paved with fire extinguishing microballoon is dried or dried, intelligent fire fighting is obtained
Patch.
Embodiment 6
1, the preparation of intelligent fire fighting patch
(1) preparation of fire extinguishing microballoon: being added 4.5 parts of neopelexes, 30 parts of FP and 40 part of water in reaction kettle,
5-30min is emulsified, 5 parts of phenolic resin prepolymers are then added, 70 DEG C are warming up to after microballoon is formed and is solidified, it is to be solidified complete
At rear water washing collection product, as fire extinguishing microballoon；
(2) by 5 parts of dibutyl tin dilaurate, 5 parts of polypropylene glycerol aether, 18 parts of rheium oxide, polyacrylic acid ester gum 38
Part mixes in the high-speed mixer that revolving speed is 1000-1500r/min, obtains mixture；
(3) prepare carrier patch, and the mixture obtained in carrier patch upper step (2)；
(4) it will quickly put out a fire 58 parts of microballoon and be paved on the carrier patch of pour mixture, press lightly on fire extinguishing microballoon, make to go out
About 1/3 volume of fiery microballoon is submerged in mixture, and the carrier patch for being paved with fire extinguishing microballoon is dried or dried, intelligent fire fighting is obtained
Patch.
Performance detection
Intelligent fire fighting note in embodiment 1-6 is tested for the property according to GB/T14907-2002, concrete outcome is shown in Table 1
It is shown:
Table 1
It is noted that above embodiments are only to illustrate the present invention and not limit technical side described in the invention
Case, therefore, although this specification is referring to the above embodiments, the present invention has been described in detail, this field
It is to be appreciated by one skilled in the art that still can modify to the present invention or equivalent replacement；And all do not depart from spirit
With the scheme and its improvement of technical scope, it is intended to be within the scope of the claims of the invention.
Claims (7)
1. a kind of preparation method of intelligent fire fighting patch, which comprises the following steps:
(1) by 1-5 parts of drier, 1-6 parts of defoaming agent, 1-25 parts of rheium oxide, 25-40 parts of adhesive are 1000- in revolving speed
It is mixed in the high-speed mixer of 1500r/min, obtains mixture；
(2) prepare carrier patch, and the mixture obtained in carrier patch upper step (1)；
(3) it will quickly put out a fire microballoon 30-60 parts and be paved on the carrier patch for being cast with mixture, press lightly on fire extinguishing microballoon, make
The volume of fire extinguishing microballoon 1/4~2/3 is submerged in mixture, and then the carrier patch for being paved with fire extinguishing microballoon is dried or dried, is made
Obtain intelligent fire fighting patch.
2. a kind of preparation method of intelligent fire fighting patch as described in claim 1, it is characterised in that: the drier is two laurels
Sour dibutyl tin.
3. a kind of preparation method of intelligent fire fighting patch as described in claim 1, it is characterised in that: the defoaming agent is polyoxy second
One or more of alkene polyoxy propyl alcohol amidogen ether, polypropylene glycerol aether or polyoxyethylene polyoxypropylene glycerin ether mix
It closes.
4. a kind of preparation method of intelligent fire fighting patch as described in claim 1, it is characterised in that: described adhesive is phenolic aldehyde tree
One or both of rouge glue, polyvinyl acetate resin adhesive, urea-formaldehyde resin adhesive, polyurethane adhesive, polyacrylic acid ester gum or butadiene-styrene rubber
Above mixing.
5. a kind of preparation method of intelligent fire fighting patch as described in claim 1, it is characterised in that: the preparation of the fire extinguishing microballoon
Method includes: that 0.1-5 parts of neopelexes, 5-30 parts of extinguishing chemicals and 20-50 parts of water are added in reaction kettle, emulsifies 5-
Then 30min is added 1-5 parts of wall materials, is warming up to 50-110 DEG C after microballoon is formed and is solidified, wash, obtain fire extinguishing microballoon.
6. a kind of intelligent fire fighting as claimed in claim 5 pastes to obtain preparation method, it is characterised in that: the extinguishing chemical is MJPZ
Fire foam (AFFF), fluoroprotein foam extinguishing agent (FP), heptafluoro-propane, pentafluoroethane, fluoroform, hexafluoropropane or three
The mixing of one or more of fluoro- iodomethane.
7. a kind of preparation method of intelligent fire fighting patch as claimed in claim 5, it is characterised in that: the wall material be styrene,
The mixing of one or more of Lauxite prepolymer, methyl methacrylate or phenolic resin prepolymer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910477017.9A CN110075445A (en) | 2019-06-03 | 2019-06-03 | A kind of preparation method of intelligent fire fighting patch |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910477017.9A CN110075445A (en) | 2019-06-03 | 2019-06-03 | A kind of preparation method of intelligent fire fighting patch |
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| Publication Number | Publication Date |
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| CN110075445A true CN110075445A (en) | 2019-08-02 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201910477017.9A Pending CN110075445A (en) | 2019-06-03 | 2019-06-03 | A kind of preparation method of intelligent fire fighting patch |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114980980A (en) * | 2020-01-24 | 2022-08-30 | 凸版印刷株式会社 | Fire extinguishing body |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1423674A (en) * | 2000-03-23 | 2003-06-11 | 亨克尔洛克泰特公司 | Flame retardant epoxy molding compositions |
| CN105062286A (en) * | 2015-09-23 | 2015-11-18 | 长沙民德消防工程涂料有限公司 | Veneer-type tunnel fire-resistant paint and preparation method thereof |
| CN105218714A (en) * | 2015-10-30 | 2016-01-06 | 浙江中天氟硅材料有限公司 | A kind of flame retardant microcapsule and its preparation method and application |
| EP3173390A1 (en) * | 2015-11-26 | 2017-05-31 | VITRULAN Textile Glass GmbH | Flat textile substrate with at least partial fire protection coating, method for its production and uses thereof |
| CN107537127A (en) * | 2017-10-11 | 2018-01-05 | 公牛集团有限公司 | A kind of composite fire extinguishing paster and preparation method thereof |
| CN108992831A (en) * | 2018-08-20 | 2018-12-14 | 常州扬鹏科技有限公司 | It is pasted from the preparation method of temperature sensitive type fire extinguishing patch and its putting out a fire from temperature sensitive type for preparation |
-
2019
- 2019-06-03 CN CN201910477017.9A patent/CN110075445A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1423674A (en) * | 2000-03-23 | 2003-06-11 | 亨克尔洛克泰特公司 | Flame retardant epoxy molding compositions |
| CN105062286A (en) * | 2015-09-23 | 2015-11-18 | 长沙民德消防工程涂料有限公司 | Veneer-type tunnel fire-resistant paint and preparation method thereof |
| CN105218714A (en) * | 2015-10-30 | 2016-01-06 | 浙江中天氟硅材料有限公司 | A kind of flame retardant microcapsule and its preparation method and application |
| EP3173390A1 (en) * | 2015-11-26 | 2017-05-31 | VITRULAN Textile Glass GmbH | Flat textile substrate with at least partial fire protection coating, method for its production and uses thereof |
| CN107537127A (en) * | 2017-10-11 | 2018-01-05 | 公牛集团有限公司 | A kind of composite fire extinguishing paster and preparation method thereof |
| CN108992831A (en) * | 2018-08-20 | 2018-12-14 | 常州扬鹏科技有限公司 | It is pasted from the preparation method of temperature sensitive type fire extinguishing patch and its putting out a fire from temperature sensitive type for preparation |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114980980A (en) * | 2020-01-24 | 2022-08-30 | 凸版印刷株式会社 | Fire extinguishing body |
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Application publication date: 20190802 |
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