CN110055427A - Reactor with the big lid of anti-inlet seal in a kind of titanium sponge production - Google Patents
Reactor with the big lid of anti-inlet seal in a kind of titanium sponge production Download PDFInfo
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- CN110055427A CN110055427A CN201910531482.6A CN201910531482A CN110055427A CN 110055427 A CN110055427 A CN 110055427A CN 201910531482 A CN201910531482 A CN 201910531482A CN 110055427 A CN110055427 A CN 110055427A
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- Prior art keywords
- reactor
- flange
- big lid
- titanium
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Classifications
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1263—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
- C22B34/1268—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams
- C22B34/1272—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams reduction of titanium halides, e.g. Kroll process
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1295—Refining, melting, remelting, working up of titanium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
- C22B9/02—Refining by liquating, filtering, centrifuging, distilling, or supersonic wave action including acoustic waves
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Environmental & Geological Engineering (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Acoustics & Sound (AREA)
- Manufacture And Refinement Of Metals (AREA)
Abstract
Reactor with the big lid of anti-inlet seal in a kind of titanium sponge production, including reactor flange, seal gasket, big Gai Falan, big lid and bolt；Connection is bolted between reactor flange and big lid flange；Corresponding position is respectively opened up there are two annular groove on reactor flange and big lid flange, and two stainless steel waterpipes are equipped in a wherein annular groove, and seal gasket is equipped between two stainless steel waterpipes；It is equipped with adsorbent equipment in another annular groove, is ring-shaped；Adsorbent equipment constitutes a cavity by bottom plate, outer barrel with holes, panel and inner cylinder with holes, interior to be equipped with titanium foam.The present invention sets seal gasket between two stainless steel waterpipes, the section of itself and water pipe forms linear sealing, it is passed through the integrity that cooling water guarantees seal gasket, the probability for then leaking air inlet greatly reduces, adsorbent equipment avoids gas leakage and enters pollution Sponge Titanium in reactor, achievees the purpose that Sponge Titanium quality not by gaseous contamination.
Description
Technical field
The present invention relates to the reactor assembly in a kind of titanium sponge production, in particular in a kind of titanium sponge production band prevent into
The reactor of the big lid of hermetic seal.
Background technique
Industrial production titanium sponge is all made of magnesium-reduced titanium tetrachloride method both at home and abroad at present, in distillation process, it is necessary to
1000 DEG C of high temperature or so, high vacuum reaches to be produced under 5Pa or so operating condition, and type of furnace majority is produced using inverse u shape combination method,
Its main feature is that single furnace output is big, high-grade-goods rate is high, the advantage that low energy consumption.To reduce production cost, each state is all by equipment enlarging
As technological development direction.But with the increase of the type of furnace, big lid reactor is the capital equipment of reduction distillation process, in reality
In the production process of border, the leakproofness of the assembling of big lid and reactor is a big technical problem, due to the limitation of production technology, now
The face sealing that most titanium sponge production producers all use, face airtight quality is poor, and titanium sponge is distilled under high vacuum state will lead to
Product air inlet influences the quality of product.Slow air inlet is can not to discover, and will continue to produce, seriously affects Sponge Titanium quality；
If any apparent leakage, meeting shutdown maintenance increases the labor intensity of worker, manufacturing schedule can be also affected by it.
Summary of the invention
The present invention is to lead to the skill of product air inlet to solve big lid and reactor assembling leakage during production titanium sponge
Art problem.
In order to solve the above technical problems, the invention adopts the following technical scheme:
Reactor 1 with the big lid of anti-inlet seal in a kind of titanium sponge production, including reactor flange 2, seal gasket 4, great Gai
Flange 5, big lid 7 and bolt 8；It is fixedly connected between reactor flange 2 and big lid flange 5 by bolt 8；
Corresponding position is respectively opened up there are two annular groove on reactor flange 2 and big lid flange 5, wherein an annular groove
Two stainless steel waterpipes 3 are inside equipped with, seal gasket 4 is equipped between two stainless steel waterpipes 3；It is equipped in another annular groove
Adsorbent equipment 6 is ring-shaped；
The adsorbent equipment is made of bottom plate 601, outer barrel with holes 602, titanium foam 603, panel 604 and inner cylinder with holes 605；
Titanium foam 603 is equipped in the cavity being made of bottom plate 601, outer barrel with holes 602, panel 604 and inner cylinder with holes 605.
The annular groove is circular groove.
By adopting the above technical scheme the utility model has the advantages that
1, the present invention is put into seal gasket between two stainless steel waterpipes, and the section of seal gasket and stainless steel waterpipe forms
Linear sealing, and it is passed through cooling water, guarantee the integrity of seal gasket, since titanium sponge terminates to enter high vacuum distillation rank in reduction
Section, the section using water pipe are linear sealing, and the sealing performance of linear sealing is sealed better than face, then the probability for leaking air inlet subtracts significantly
It is few, overcome big lid and the bad problem of reactor face sealing effect.
2, the present invention more reduces seal gasket Leakage probability because using linear sealing.
3, the present invention avoids gas leakage and enters pollution Sponge Titanium in reactor, reach because using adsorbent equipment
Sponge Titanium quality is not by the purpose of gaseous contamination.
Detailed description of the invention:
Fig. 1 is cross-sectional view of the invention；
In figure: 1- reactor, 2- reactor flange, 3- stainless steel waterpipe, 4- seal gasket, 5- big Gai Falan, 6- inhale
The big lid of adsorption device, 7-, 8- bolt；
Fig. 2 is the schematic view of the mounting position of stainless steel waterpipe and adsorbent equipment of the invention；
In figure: 3- stainless steel waterpipe, 6- adsorbent equipment；
Fig. 3 is adsorbent equipment schematic diagram of the invention；
In figure: 601- bottom plate, 602- outer barrel with holes, 603- titanium foam, 604- panel, 605- inner cylinder with holes.
Specific embodiment
The present invention is described in further detail below in conjunction with the accompanying drawings.
As shown in Figure 1, the reactor 1 with the big lid of anti-inlet seal in a kind of titanium sponge production, including reactor flange 2,
Seal gasket 4, big lid flange 5, big lid 7 and bolt 8；It is fixedly connected between reactor flange 2 and big lid flange 5 by bolt 8；
Corresponding position is respectively opened up there are two annular groove on reactor flange 2 and big lid flange 5；It is opened on reactor flange 2
If annular groove in soldering stainless steel water pipe 3, soldering stainless steel water pipe 3 in the annular groove opened up on big lid flange 5, at two
Seal gasket 4 is equipped between stainless steel waterpipe 3；Mainly play a part of to be passed through cooling water coolant seal rubber mat 4 and linear sealing；Another
It is equipped with adsorbent equipment 6 in one annular groove, is ring-shaped；Mainly play a part of to adsorb gas leakage；
As shown in figure 3, adsorbent equipment is by bottom plate 601, outer barrel with holes 602, titanium foam 603, panel 604 and inner cylinder with holes
605 compositions；Foam is equipped in the cavity being made of bottom plate 601, outer barrel with holes 602, panel 604 and inner cylinder with holes 605
Titanium 603, the distillation of titanium foam 603 under high temperature to oxygen, water and the strong feature of other compositions adsorption capacity in air, to product
Production has good effect.
The annular groove is circular groove.
In titanium sponge distillation, due to the requirement of titanium sponge production process conditions, it is necessary at 1000 DEG C of high temperature or so, high vacuum
It is produced under up to 5Pa or so operating condition, especially high to the sealing effect requirement of big lid 7 and reactor 1, the present invention is former face sealing
It is changed to linear sealing, and water pipe cooling is directlyed adopt to seal gasket 4, guarantees to also assure while seal gasket 4 is not burned
The reliability of linear sealing.Once there is gas leakage phenomenon, the gas of entrance can also be adsorbed the titanium foam in device 6 at once
603 absorption avoid gas leakage and enter pollution Sponge Titanium in reactor 1, reach Sponge Titanium not by gaseous contamination
Purpose, product quality is largely increased.
The present invention effectively overcome face be sealed in high temperature, seal under high pressures performance it is bad and leakage air inlet problem, solve
Big lid and reactor in process of production gas leakage the problems such as, while reducing production cost and reducing the labour of operator
Intensity.
Claims (2)
1. the reactor (1) with the big lid of anti-inlet seal in a kind of titanium sponge production, including reactor flange (2), seal gasket
(4), big Gai Falan (5), big lid (7) and bolt (8)；It is fixed by bolt (8) between reactor flange (2) and big Gai Falan (5)
Connection；It is characterized by:
Corresponding position is respectively opened up there are two annular groove on reactor flange (2) and big Gai Falan (5), wherein a ring
It is equipped with two stainless steel waterpipes (3) in shape slot, is equipped with seal gasket (4) between two stainless steel waterpipes (3)；In another ring
Adsorbent equipment (6) are equipped in shape slot, are ring-shaped；
The adsorbent equipment is by bottom plate (601), outer barrel with holes (602), titanium foam (603), panel (604) and inner cylinder with holes
(605) it forms；In the cavity being made of bottom plate (601), outer barrel with holes (602), panel (604) and inner cylinder with holes (605)
It is interior to be equipped with titanium foam (603).
2. reactor (1) as described in claim 1, it is characterised in that: the annular groove is circular groove.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910531482.6A CN110055427A (en) | 2019-06-19 | 2019-06-19 | Reactor with the big lid of anti-inlet seal in a kind of titanium sponge production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910531482.6A CN110055427A (en) | 2019-06-19 | 2019-06-19 | Reactor with the big lid of anti-inlet seal in a kind of titanium sponge production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110055427A true CN110055427A (en) | 2019-07-26 |
Family
ID=67325781
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910531482.6A Pending CN110055427A (en) | 2019-06-19 | 2019-06-19 | Reactor with the big lid of anti-inlet seal in a kind of titanium sponge production |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110055427A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112458316A (en) * | 2020-11-13 | 2021-03-09 | 云南国钛金属股份有限公司 | Device and method for preventing gas channel of reactor cover from being blocked |
| CN113337736A (en) * | 2021-07-02 | 2021-09-03 | 遵义钛业股份有限公司 | Deformation-preventing large cover for titanium sponge reduction distillation production |
| CN115074553A (en) * | 2022-06-22 | 2022-09-20 | 洛阳双瑞万基钛业有限公司 | Sealing device of reactor |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001073042A (en) * | 1999-08-31 | 2001-03-21 | Toho Titanium Co Ltd | Reducing vessel for producing sponge titanium |
| CN104357685A (en) * | 2014-12-09 | 2015-02-18 | 遵义钛业股份有限公司 | Reaction device for production of titanium sponge |
| CN206843563U (en) * | 2017-06-20 | 2018-01-05 | 东方弗瑞德（北京）科技有限公司 | A kind of titanium sponge production reactor |
| CN108220628A (en) * | 2018-04-04 | 2018-06-29 | 遵义钛业股份有限公司 | A kind of reduction apparatus produced during titanium sponge |
| CN208829744U (en) * | 2018-08-29 | 2019-05-07 | 遵义钛业股份有限公司 | Reactor with radiator in a kind of titanium sponge production |
| CN210193962U (en) * | 2019-06-19 | 2020-03-27 | 遵义钛业股份有限公司 | Reactor with air-intake-preventing sealing large cover in titanium sponge production |
-
2019
- 2019-06-19 CN CN201910531482.6A patent/CN110055427A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001073042A (en) * | 1999-08-31 | 2001-03-21 | Toho Titanium Co Ltd | Reducing vessel for producing sponge titanium |
| CN104357685A (en) * | 2014-12-09 | 2015-02-18 | 遵义钛业股份有限公司 | Reaction device for production of titanium sponge |
| CN206843563U (en) * | 2017-06-20 | 2018-01-05 | 东方弗瑞德（北京）科技有限公司 | A kind of titanium sponge production reactor |
| CN108220628A (en) * | 2018-04-04 | 2018-06-29 | 遵义钛业股份有限公司 | A kind of reduction apparatus produced during titanium sponge |
| CN208829744U (en) * | 2018-08-29 | 2019-05-07 | 遵义钛业股份有限公司 | Reactor with radiator in a kind of titanium sponge production |
| CN210193962U (en) * | 2019-06-19 | 2020-03-27 | 遵义钛业股份有限公司 | Reactor with air-intake-preventing sealing large cover in titanium sponge production |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112458316A (en) * | 2020-11-13 | 2021-03-09 | 云南国钛金属股份有限公司 | Device and method for preventing gas channel of reactor cover from being blocked |
| CN113337736A (en) * | 2021-07-02 | 2021-09-03 | 遵义钛业股份有限公司 | Deformation-preventing large cover for titanium sponge reduction distillation production |
| CN115074553A (en) * | 2022-06-22 | 2022-09-20 | 洛阳双瑞万基钛业有限公司 | Sealing device of reactor |
| CN115074553B (en) * | 2022-06-22 | 2024-03-01 | 洛阳双瑞万基钛业有限公司 | Sealing device of reactor |
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