CN104357685A - Reaction device for production of titanium sponge - Google Patents
Reaction device for production of titanium sponge Download PDFInfo
- Publication number
- CN104357685A CN104357685A CN201410744242.1A CN201410744242A CN104357685A CN 104357685 A CN104357685 A CN 104357685A CN 201410744242 A CN201410744242 A CN 201410744242A CN 104357685 A CN104357685 A CN 104357685A
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- reactor
- flange
- titanium
- circular groove
- ring groove
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Abstract
The invention discloses a reaction device for production of titanium sponge. The reaction device mainly consists of a reactor and a big cover of the reactor, wherein a basket is arranged on the upper part of the reactor and mainly consists of a flange, a supporting bar and a circular groove; the flange is connected with the supporting bar which is connected with the circular groove, a lug is welded on the circular groove, waste titanium particles are held in the circular groove, and the flange is hung on the flange of the reactor. By fully utilizing effective space inside the reactor as well as the waste titanium particles in the circular groove of the basket, oxygen and nitrogen entering the reactor due to microleakage caused by equipment reason in a distilling process can be effectively absorbed, so that the content of oxygen and nitrogen in a titanium sponge product is reduced and the product quality is improved.
Description
Technical field
The invention belongs to technical field of production of sponge titanium, the reaction unit particularly in a kind of magnesium method titanium sponge production.
Background technology
All adopt magnesium processes (Kroll method) suitability for industrialized production titanium sponge both at home and abroad at present; magnesium reduction process produces titanium sponge; under argon shield; liquid titanium tetrachloride is added and the disposable molten metal magnesium added reacts in steel reactor; generate titanium sponge and magnesium chloride, titanium sponge obtains the process of finished product titanium sponge after vacuum distilling is purified.In distillation process, reaction unit works for a long time under high vacuum, the condition of high temperature, reactor covers greatly the phenomenon that micro-leakage easily occurs at the places such as each attachment weld, seal gasket and magnesium chloride pipe rubber cushion, once leak, oxygen in air, nitrogen react with Sponge Titanium under the high temperature conditions, easily cause Sponge Titanium oxygen, nitrogen content to increase, product hierarchy reduces.
Summary of the invention
Have problems for solving in prior art, the invention provides a kind of reaction unit for titanium sponge production, make full use of the useful space of inside reactor, can effectively absorb in still-process because of Equipment there is micro-leakage after enter oxygen nitrogen in reactor, thus the oxygen and nitrogen content in reduction Sponge Titanium, improve the quality of products.
Technical scheme of the present invention is as described below:
For a reaction unit for titanium sponge production, primarily of reactor, the large lid composition of reactor, the top in reactor is provided with a hanging basket, and hanging basket is built with useless titanium particle.
Particularly, described hanging basket is primarily of flange, support bar, ring groove composition, and flange is connected with support bar, and support bar is connected with ring groove, and ring groove welds hanger, and in ring groove, splendid attire gives up titanium particle, and flange is hung on reactor flange.
In the present invention, useless titanium particle is filled in the ring groove hanging indigo plant, first will hang in blue loading reactor before the large lid of reactor is installed, making to hang blue flange is hung on reactor flange, and then cover the large lid of reactor, until reduction, distill whole production process and terminate, take out hanging basket after tearing stove open and continue to use, the useless titanium in ring groove can Reusability repeatedly.
Advantage of the present invention and beneficial effect:
The present invention makes full use of the useful space of inside reactor, utilize the useless titanium particle hung in blue ring groove, can effectively absorb in still-process because of Equipment there is micro-leakage after enter oxygen nitrogen in reactor, thus reduce the oxygen and nitrogen content in Sponge Titanium, improve the quality of products.
Accompanying drawing explanation
Fig. 1 is the hanging basket schematic diagram of a kind of reaction unit for titanium sponge production of the present invention;
In figure: 1-flange, 2-support bar, 3-ring groove, 4-hanger, 5-give up titanium particle.
Embodiment
Below in conjunction with accompanying drawing, the present invention is described in further detail, but should not be interpreted as that the scope of theme of the present invention is only limitted to following embodiment at this point, without departing from the idea case in the present invention described above, all make according to ordinary skill knowledge and customary means various amendments, replacement and change, include within the scope of the invention.
embodiment one
For a reaction unit for titanium sponge production, primarily of reactor, the large lid composition of reactor, the top in reactor is provided with a hanging basket, and hanging basket is built with useless titanium particle 5.
As shown in Figure 1, described hanging basket forms primarily of flange 1, support bar 2, ring groove 3, and flange 1 is connected with support bar 2, and support bar 2 is connected with ring groove 3, ring groove 3 welds hanger 4, and in ring groove 3, splendid attire gives up titanium particle 5, and flange 1 is hung on reactor flange.
Claims (2)
1., for a reaction unit for titanium sponge production, primarily of reactor, the large lid composition of reactor, it is characterized in that the top in reactor is provided with a hanging basket, hanging basket is built with useless titanium particle (5).
2. a kind of reaction unit for titanium sponge production according to claim 1, it is characterized in that described hanging basket is primarily of flange (1), support bar (2), ring groove (3) composition, flange (1) is connected with support bar (2), support bar (2) is connected with ring groove (3), ring groove (3) welds hanger (4), ring groove (3) interior splendid attire gives up titanium particle (5), and flange (1) is hung on reactor flange.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410744242.1A CN104357685A (en) | 2014-12-09 | 2014-12-09 | Reaction device for production of titanium sponge |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410744242.1A CN104357685A (en) | 2014-12-09 | 2014-12-09 | Reaction device for production of titanium sponge |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104357685A true CN104357685A (en) | 2015-02-18 |
Family
ID=52524991
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410744242.1A Pending CN104357685A (en) | 2014-12-09 | 2014-12-09 | Reaction device for production of titanium sponge |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104357685A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110055427A (en) * | 2019-06-19 | 2019-07-26 | 遵义钛业股份有限公司 | Reactor with the big lid of anti-inlet seal in a kind of titanium sponge production |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003193151A (en) * | 2001-12-28 | 2003-07-09 | Nikko Materials Co Ltd | Method for recovering titanium from titanium-containing scrap |
| CN201195741Y (en) * | 2008-05-23 | 2009-02-18 | 宝钛华神钛业有限公司 | Production apparatus for hypoxia low-nitrogen titanium sponge |
| CN201857417U (en) * | 2010-11-10 | 2011-06-08 | 攀枝花钢城集团有限公司 | Upper cover of sponge titanium reduction reactor |
| CN204356389U (en) * | 2014-12-09 | 2015-05-27 | 遵义钛业股份有限公司 | A kind of titanium sponge production device |
-
2014
- 2014-12-09 CN CN201410744242.1A patent/CN104357685A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003193151A (en) * | 2001-12-28 | 2003-07-09 | Nikko Materials Co Ltd | Method for recovering titanium from titanium-containing scrap |
| CN201195741Y (en) * | 2008-05-23 | 2009-02-18 | 宝钛华神钛业有限公司 | Production apparatus for hypoxia low-nitrogen titanium sponge |
| CN201857417U (en) * | 2010-11-10 | 2011-06-08 | 攀枝花钢城集团有限公司 | Upper cover of sponge titanium reduction reactor |
| CN204356389U (en) * | 2014-12-09 | 2015-05-27 | 遵义钛业股份有限公司 | A kind of titanium sponge production device |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110055427A (en) * | 2019-06-19 | 2019-07-26 | 遵义钛业股份有限公司 | Reactor with the big lid of anti-inlet seal in a kind of titanium sponge production |
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Legal Events
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20150218 |