CN110044657A - A kind of fluid sample sampler suitable for pipeline spectra collection - Google Patents
A kind of fluid sample sampler suitable for pipeline spectra collection Download PDFInfo
- Publication number
- CN110044657A CN110044657A CN201910315673.9A CN201910315673A CN110044657A CN 110044657 A CN110044657 A CN 110044657A CN 201910315673 A CN201910315673 A CN 201910315673A CN 110044657 A CN110044657 A CN 110044657A
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- sampler
- sample
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- detection
- pipeline
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- 239000012530 fluid Substances 0.000 title claims abstract description 27
- 238000001228 spectrum Methods 0.000 title claims abstract description 13
- 238000001514 detection method Methods 0.000 claims abstract description 34
- 239000007788 liquid Substances 0.000 claims abstract description 34
- 230000003595 spectral effect Effects 0.000 claims abstract description 11
- 239000000523 sample Substances 0.000 claims description 41
- 238000012360 testing method Methods 0.000 claims description 19
- 241000521257 Hydrops Species 0.000 claims description 3
- 206010030113 Oedema Diseases 0.000 claims description 3
- 230000015572 biosynthetic process Effects 0.000 claims description 3
- 238000005259 measurement Methods 0.000 description 3
- 238000004891 communication Methods 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 238000007689 inspection Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 1
- 241000208125 Nicotiana Species 0.000 description 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 1
- 241000233855 Orchidaceae Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000000691 measurement method Methods 0.000 description 1
- 239000013307 optical fiber Substances 0.000 description 1
- 238000002203 pretreatment Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/10—Devices for withdrawing samples in the liquid or fluent state
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/01—Arrangements or apparatus for facilitating the optical investigation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
- G01N21/359—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light using near infrared light
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/01—Arrangements or apparatus for facilitating the optical investigation
- G01N2021/0106—General arrangement of respective parts
- G01N2021/0112—Apparatus in one mechanical, optical or electronic block
Landscapes
- Physics & Mathematics (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Hydrology & Water Resources (AREA)
- Optical Measuring Cells (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
Abstract
The invention discloses a kind of fluid sample samplers suitable for pipeline spectra collection, it mainly include flange, detection sleeve, sampler and reflecting plate, the bubble entered in liquid is effectively eliminated, the accuracy of spectral detection is improved, realizes hand-held spectrometer liquid on-line detection.
Description
Technical field
The present invention relates to a kind of fluid sample sampler, in particular to a kind of liquid-like suitable for pipeline spectra collection
Product sampler.
Background technique
In recent years, with the development of Chemical Measurement, optical fiber and computer technology, hand-held near infrared spectrometer is just with frightened
The speed applications of people are in many fields including agriculture and animal husbandry, food, chemical industry, petrochemical industry, pharmacy, tobacco etc..Hand-held near-infrared
Its sample of spectrometer can be measured directly without pretreatment, and measurement method has transmission, reflection and diffusing reflection diversified forms, be suitble to measurement
The sample of the forms such as liquid, solid and pulpous state, thus it is widely used.
For on-line checking of liquid during pipeline transportation, is mostly sampled, limited hand-held using the mode of flow cell
Application of the spectrometer in liquid on-line detection;Another aspect liquid flowing when, especially flowing velocity quickly when can be in liquid
A large amount of bubbles are generated in body, influence the accuracy of measurement result.
Summary of the invention
In order to overcome drawbacks described above, the present invention discloses a kind of fluid sample sampler suitable for pipeline spectra collection,
It mainly include that flange, detection sleeve, sampler and reflecting plate, sampler are fixed on the inner wall of flange, detection sleeve passes through method
Orchid is inserted in sampler, and reflecting plate is fixed in the outer surface of the sampler;It is characterized by:
Detection sleeve is the bolt with hollow sleeve, for accommodating spectral instrument probe, carries out spectral information acquisition;
The sampler face ontology A has fluid collection chamber, test chamber, sample holes, current limiting plate, slit, overflow hole, liquid outlet and detection window
Mouthful, the face B has opening;Current limiting plate is covered at sample holes upper opening, and the flow of sample holes is entered for limiting liquid;Slit
Connection sample holes and fluid collection chamber, detection window are located in test chamber, with opening coaxial communication;
Liquid is flowed by sample holes in pipeline, is entered fluid collection chamber by slit, is then flowed into test chamber by overflow hole, liquid level reaches
Sampler is flowed out at overflow hole, while respectively sampler is discharged in fluid collection chamber and test chamber bottom hydrops by liquid outlet;
When spectra collection, it will test probe first and be against on detection window across detection sleeve, the light for sending of popping one's head in is through detection
Sample in window and test chamber enters detection probe by baffle reflection, realizes spectral information acquisition.
Narrow-gap channel wide 5mm, high 0.6mm.
Liquid outlet upper opening is the circular hole of diameter 0.6mm, and lower part uses the shape of inverted funnel;Be conducive to fluid collection chamber and inspection
It surveys chamber bottom liquid stream to go out, avoids the formation of dead sample.
Beneficial effect is mainly shown as: by the design of current limiting plate, slit and fluid collection chamber, being effectively eliminated into liquid
Bubble, improves the accuracy of spectral detection, while realizing hand-held spectrometer and detecting for liquid on-line.
Detailed description of the invention
Fig. 1 sampler overall schematic and planing surface figure along the direction GG;
Fig. 2 sampler overall schematic;
Planing surface figure of the face sampler B Fig. 3 along the direction EE;
Planing surface figure of Fig. 4 sampler B face left view along the direction FF;
1 flange, 2 detection sleeves, 3 samplers, 4 reflecting plates, 301 current limiting plates, 302 sample holes, 303 slits, 304 fluid collection chambers, 305
Test chamber, 306 overflow holes, 307 overflow holes, 308 liquid outlets, 309 liquid outlets, 310 detection windows, 311 openings.
Specific embodiment
Following embodiment further illustrates situations such as structure of the invention, function and application, is that the present invention compares
Good application form, but the scope of the present invention is not limited in following embodiment.
As shown in Figure 1, a kind of fluid sample sampler suitable for pipeline spectra collection, mainly includes flange 1, detection
Sleeve 2, sampler 3 and reflecting plate 4, sampler is fixed on the inner wall of flange, and detection sleeve passes through flange and is inserted in sampler,
Reflecting plate is fixed in the outer surface of the sampler.
Detection sleeve 2 is the bolt with hollow sleeve, for accommodating spectral instrument probe, carries out spectral information acquisition.
As shown in Figure 2,3, 4,3 face ontology A of sampler has fluid collection chamber 304, test chamber 305, sample holes 302, current limiting plate
301, slit 303, overflow hole 306,307, liquid outlet 308,309 and detection window 310, the face B have opening 311.Current limiting plate 301
It is covered at 302 upper opening of sample holes, the flow of sample holes is entered for limiting liquid.Slit 303 width 5mm, high 0.6mm,
Connection sample holes 302 and fluid collection chamber 304, detection window 310 are located in test chamber 305, with 311 coaxial communications that are open;
Liquid is flowed by sample holes 302 in pipeline, is entered fluid collection chamber 304 by slit 303, is then flowed into and examined by overflow hole 306
Chamber 305 is surveyed, liquid level reaches outflow sampler 3 at overflow hole 307, while liquid outlet 308 and 309 is respectively by fluid collection chamber 304 and inspection
It surveys 305 bottom hydrops of chamber and sampler is discharged.The upper opening of liquid outlet 308 and 309 is the circular hole of diameter 0.6mm, and lower part uses
The shape of funnel is conducive to fluid collection chamber 304 and the outflow of 305 bottom liquid of test chamber, avoids the formation of dead sample.
When spectra collection, it will test probe first and be against on detection window 310 across detection sleeve 2, the light for sending of popping one's head in
Detection probe is reflected by reflecting plate 5 through the sample in detection window 310 and test chamber 305, realizes spectral information acquisition.
By the design of current limiting plate, slit and fluid collection chamber, effectively eliminates into the bubble in liquid, improve spectral detection
Accuracy, while realizing hand-held set and being detected for liquid on-line.
Claims (3)
1. a kind of fluid sample sampler suitable for pipeline spectra collection mainly includes flange (1), detection sleeve (2), takes
Sample device (3) and reflecting plate (4), sampler is fixed on the inner wall of flange, and detection sleeve passes through flange and is inserted in sampler, is reflected
Plate is fixed in the outer surface of the sampler;It is characterized by:
Detecting sleeve (2) is the bolt with hollow sleeve, for accommodating spectral instrument probe, carries out spectral information acquisition;
Sampler (3) face ontology A has fluid collection chamber (304), test chamber (305), sample holes (302), current limiting plate (301), slit
(303), overflow hole (306), (307), liquid outlet (308), (309) and detection window (310), the face B have opening (311);Limit
Flowing plate (301) is covered at sample holes (302) upper opening, and the flow of sample holes is entered for limiting liquid;Slit (303) is even
Logical sample holes (302) and fluid collection chamber (304), detection window (310) are located in test chamber (305), and opening (311) is coaxial connects
It is logical;
Liquid is flowed by sample holes (302) in pipeline, enters fluid collection chamber (304) by slit (303), then by overflow hole
(306) test chamber (305) are flowed into, liquid level reaches at overflow hole (307) outflow sampler (3), while liquid outlet (308) and
(309) sampler is discharged in fluid collection chamber (304) and test chamber (305) bottom hydrops respectively;
When spectra collection, it will test probe first and be against on detection window (310) across detection sleeve (2), the light for sending of popping one's head in
Detection probe is reflected by reflecting plate (5) through the sample in detection window (310) and test chamber (305), realizes spectrum letter
Breath acquisition.
2. a kind of fluid sample sampler suitable for pipeline spectra collection according to claim 1, the slit (303)
Wide 5mm, high 0.6mm.
3. a kind of fluid sample sampler suitable for pipeline spectra collection according to claim 1, the liquid outlet
(308), (309) upper opening is the circular hole of diameter 0.6mm, and lower part uses the shape of inverted funnel;Be conducive to fluid collection chamber (330) and
The outflow of test chamber (350) bottom liquid, avoids the formation of dead sample.
Priority Applications (1)
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CN201910315673.9A CN110044657A (en) | 2019-04-19 | 2019-04-19 | A kind of fluid sample sampler suitable for pipeline spectra collection |
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CN201910315673.9A CN110044657A (en) | 2019-04-19 | 2019-04-19 | A kind of fluid sample sampler suitable for pipeline spectra collection |
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CN110044657A true CN110044657A (en) | 2019-07-23 |
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