CN110044657A - A kind of fluid sample sampler suitable for pipeline spectra collection - Google Patents

A kind of fluid sample sampler suitable for pipeline spectra collection Download PDF

Info

Publication number
CN110044657A
CN110044657A CN201910315673.9A CN201910315673A CN110044657A CN 110044657 A CN110044657 A CN 110044657A CN 201910315673 A CN201910315673 A CN 201910315673A CN 110044657 A CN110044657 A CN 110044657A
Authority
CN
China
Prior art keywords
sampler
sample
liquid
detection
pipeline
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910315673.9A
Other languages
Chinese (zh)
Inventor
程腾
江伟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
West Patel (beijing) Technology Co Ltd
Original Assignee
West Patel (beijing) Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by West Patel (beijing) Technology Co Ltd filed Critical West Patel (beijing) Technology Co Ltd
Priority to CN201910315673.9A priority Critical patent/CN110044657A/en
Publication of CN110044657A publication Critical patent/CN110044657A/en
Pending legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/01Arrangements or apparatus for facilitating the optical investigation
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/359Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light using near infrared light
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/01Arrangements or apparatus for facilitating the optical investigation
    • G01N2021/0106General arrangement of respective parts
    • G01N2021/0112Apparatus in one mechanical, optical or electronic block

Landscapes

  • Physics & Mathematics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Hydrology & Water Resources (AREA)
  • Optical Measuring Cells (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)

Abstract

The invention discloses a kind of fluid sample samplers suitable for pipeline spectra collection, it mainly include flange, detection sleeve, sampler and reflecting plate, the bubble entered in liquid is effectively eliminated, the accuracy of spectral detection is improved, realizes hand-held spectrometer liquid on-line detection.

Description

A kind of fluid sample sampler suitable for pipeline spectra collection
Technical field
The present invention relates to a kind of fluid sample sampler, in particular to a kind of liquid-like suitable for pipeline spectra collection Product sampler.
Background technique
In recent years, with the development of Chemical Measurement, optical fiber and computer technology, hand-held near infrared spectrometer is just with frightened The speed applications of people are in many fields including agriculture and animal husbandry, food, chemical industry, petrochemical industry, pharmacy, tobacco etc..Hand-held near-infrared Its sample of spectrometer can be measured directly without pretreatment, and measurement method has transmission, reflection and diffusing reflection diversified forms, be suitble to measurement The sample of the forms such as liquid, solid and pulpous state, thus it is widely used.
For on-line checking of liquid during pipeline transportation, is mostly sampled, limited hand-held using the mode of flow cell Application of the spectrometer in liquid on-line detection;Another aspect liquid flowing when, especially flowing velocity quickly when can be in liquid A large amount of bubbles are generated in body, influence the accuracy of measurement result.
Summary of the invention
In order to overcome drawbacks described above, the present invention discloses a kind of fluid sample sampler suitable for pipeline spectra collection, It mainly include that flange, detection sleeve, sampler and reflecting plate, sampler are fixed on the inner wall of flange, detection sleeve passes through method Orchid is inserted in sampler, and reflecting plate is fixed in the outer surface of the sampler;It is characterized by:
Detection sleeve is the bolt with hollow sleeve, for accommodating spectral instrument probe, carries out spectral information acquisition;
The sampler face ontology A has fluid collection chamber, test chamber, sample holes, current limiting plate, slit, overflow hole, liquid outlet and detection window Mouthful, the face B has opening;Current limiting plate is covered at sample holes upper opening, and the flow of sample holes is entered for limiting liquid;Slit Connection sample holes and fluid collection chamber, detection window are located in test chamber, with opening coaxial communication;
Liquid is flowed by sample holes in pipeline, is entered fluid collection chamber by slit, is then flowed into test chamber by overflow hole, liquid level reaches Sampler is flowed out at overflow hole, while respectively sampler is discharged in fluid collection chamber and test chamber bottom hydrops by liquid outlet;
When spectra collection, it will test probe first and be against on detection window across detection sleeve, the light for sending of popping one's head in is through detection Sample in window and test chamber enters detection probe by baffle reflection, realizes spectral information acquisition.
Narrow-gap channel wide 5mm, high 0.6mm.
Liquid outlet upper opening is the circular hole of diameter 0.6mm, and lower part uses the shape of inverted funnel;Be conducive to fluid collection chamber and inspection It surveys chamber bottom liquid stream to go out, avoids the formation of dead sample.
Beneficial effect is mainly shown as: by the design of current limiting plate, slit and fluid collection chamber, being effectively eliminated into liquid Bubble, improves the accuracy of spectral detection, while realizing hand-held spectrometer and detecting for liquid on-line.
Detailed description of the invention
Fig. 1 sampler overall schematic and planing surface figure along the direction GG;
Fig. 2 sampler overall schematic;
Planing surface figure of the face sampler B Fig. 3 along the direction EE;
Planing surface figure of Fig. 4 sampler B face left view along the direction FF;
1 flange, 2 detection sleeves, 3 samplers, 4 reflecting plates, 301 current limiting plates, 302 sample holes, 303 slits, 304 fluid collection chambers, 305 Test chamber, 306 overflow holes, 307 overflow holes, 308 liquid outlets, 309 liquid outlets, 310 detection windows, 311 openings.
Specific embodiment
Following embodiment further illustrates situations such as structure of the invention, function and application, is that the present invention compares Good application form, but the scope of the present invention is not limited in following embodiment.
As shown in Figure 1, a kind of fluid sample sampler suitable for pipeline spectra collection, mainly includes flange 1, detection Sleeve 2, sampler 3 and reflecting plate 4, sampler is fixed on the inner wall of flange, and detection sleeve passes through flange and is inserted in sampler, Reflecting plate is fixed in the outer surface of the sampler.
Detection sleeve 2 is the bolt with hollow sleeve, for accommodating spectral instrument probe, carries out spectral information acquisition.
As shown in Figure 2,3, 4,3 face ontology A of sampler has fluid collection chamber 304, test chamber 305, sample holes 302, current limiting plate 301, slit 303, overflow hole 306,307, liquid outlet 308,309 and detection window 310, the face B have opening 311.Current limiting plate 301 It is covered at 302 upper opening of sample holes, the flow of sample holes is entered for limiting liquid.Slit 303 width 5mm, high 0.6mm, Connection sample holes 302 and fluid collection chamber 304, detection window 310 are located in test chamber 305, with 311 coaxial communications that are open;
Liquid is flowed by sample holes 302 in pipeline, is entered fluid collection chamber 304 by slit 303, is then flowed into and examined by overflow hole 306 Chamber 305 is surveyed, liquid level reaches outflow sampler 3 at overflow hole 307, while liquid outlet 308 and 309 is respectively by fluid collection chamber 304 and inspection It surveys 305 bottom hydrops of chamber and sampler is discharged.The upper opening of liquid outlet 308 and 309 is the circular hole of diameter 0.6mm, and lower part uses The shape of funnel is conducive to fluid collection chamber 304 and the outflow of 305 bottom liquid of test chamber, avoids the formation of dead sample.
When spectra collection, it will test probe first and be against on detection window 310 across detection sleeve 2, the light for sending of popping one's head in Detection probe is reflected by reflecting plate 5 through the sample in detection window 310 and test chamber 305, realizes spectral information acquisition.
By the design of current limiting plate, slit and fluid collection chamber, effectively eliminates into the bubble in liquid, improve spectral detection Accuracy, while realizing hand-held set and being detected for liquid on-line.

Claims (3)

1. a kind of fluid sample sampler suitable for pipeline spectra collection mainly includes flange (1), detection sleeve (2), takes Sample device (3) and reflecting plate (4), sampler is fixed on the inner wall of flange, and detection sleeve passes through flange and is inserted in sampler, is reflected Plate is fixed in the outer surface of the sampler;It is characterized by:
Detecting sleeve (2) is the bolt with hollow sleeve, for accommodating spectral instrument probe, carries out spectral information acquisition;
Sampler (3) face ontology A has fluid collection chamber (304), test chamber (305), sample holes (302), current limiting plate (301), slit (303), overflow hole (306), (307), liquid outlet (308), (309) and detection window (310), the face B have opening (311);Limit Flowing plate (301) is covered at sample holes (302) upper opening, and the flow of sample holes is entered for limiting liquid;Slit (303) is even Logical sample holes (302) and fluid collection chamber (304), detection window (310) are located in test chamber (305), and opening (311) is coaxial connects It is logical;
Liquid is flowed by sample holes (302) in pipeline, enters fluid collection chamber (304) by slit (303), then by overflow hole (306) test chamber (305) are flowed into, liquid level reaches at overflow hole (307) outflow sampler (3), while liquid outlet (308) and (309) sampler is discharged in fluid collection chamber (304) and test chamber (305) bottom hydrops respectively;
When spectra collection, it will test probe first and be against on detection window (310) across detection sleeve (2), the light for sending of popping one's head in Detection probe is reflected by reflecting plate (5) through the sample in detection window (310) and test chamber (305), realizes spectrum letter Breath acquisition.
2. a kind of fluid sample sampler suitable for pipeline spectra collection according to claim 1, the slit (303) Wide 5mm, high 0.6mm.
3. a kind of fluid sample sampler suitable for pipeline spectra collection according to claim 1, the liquid outlet (308), (309) upper opening is the circular hole of diameter 0.6mm, and lower part uses the shape of inverted funnel;Be conducive to fluid collection chamber (330) and The outflow of test chamber (350) bottom liquid, avoids the formation of dead sample.
CN201910315673.9A 2019-04-19 2019-04-19 A kind of fluid sample sampler suitable for pipeline spectra collection Pending CN110044657A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910315673.9A CN110044657A (en) 2019-04-19 2019-04-19 A kind of fluid sample sampler suitable for pipeline spectra collection

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910315673.9A CN110044657A (en) 2019-04-19 2019-04-19 A kind of fluid sample sampler suitable for pipeline spectra collection

Publications (1)

Publication Number Publication Date
CN110044657A true CN110044657A (en) 2019-07-23

Family

ID=67277905

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910315673.9A Pending CN110044657A (en) 2019-04-19 2019-04-19 A kind of fluid sample sampler suitable for pipeline spectra collection

Country Status (1)

Country Link
CN (1) CN110044657A (en)

Citations (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1477199A (en) * 1974-09-02 1977-06-22 Technicon Instr Sample supply apparatus for automatic analysis systems
US4076420A (en) * 1974-02-22 1978-02-28 Max-Planck-Gesellschaft Zur Forderung Der Wissenschaften E.V. Apparatus for investigating fast chemical reactions by optical detection
US5460055A (en) * 1991-11-22 1995-10-24 Coulter Corporation Sampling metering and transfer valve assembly and analyzing system employing same
CN2499825Y (en) * 2001-11-02 2002-07-10 中国石油天然气股份有限公司 Analytical pool for on-line measuring petroleum product absorption spectrum
CN2612940Y (en) * 2003-01-24 2004-04-21 大庆油田有限责任公司 Low degradation quick-speed high pressure sampler
CN1501060A (en) * 2002-11-18 2004-06-02 ϣɭ������ʽ���� Sample analyzer and its components
CN1900716A (en) * 2002-11-18 2007-01-24 希森美康株式会社 Sample analyzer and its components
TW200712473A (en) * 2005-08-26 2007-04-01 Fiamo Corp Flow analysis system
CN101031786A (en) * 2005-08-26 2007-09-05 先进科技股份有限公司 Flow analysis system
CN201637607U (en) * 2010-03-09 2010-11-17 张卓理 Deaerating device for on-line water-quality analysis sampling water
US20110252898A1 (en) * 2008-12-03 2011-10-20 Mettler-Toledo Ag Sampling device
CN202305265U (en) * 2011-09-21 2012-07-04 上海科星生物技术有限公司 Positioning and sampling device for liquid container
CN102749226A (en) * 2012-07-19 2012-10-24 江苏凯力克钴业股份有限公司 Solution sampling device
CN103063474A (en) * 2012-08-23 2013-04-24 浙江省海洋开发研究院 Shallow water quality sampler
CN203551324U (en) * 2013-08-16 2014-04-16 甘肃瓮福化工有限责任公司 Continuous sampling device for liquid-phase materials
FR3003033A1 (en) * 2013-03-07 2014-09-12 Commissariat Energie Atomique DEVICE FOR COLLECTING A CAPILLARITY LIQUID SAMPLE AND METHOD OF ANALYZING THE SAME
CN204177616U (en) * 2014-11-20 2015-02-25 上海未来企业有限公司 Micro-bubble filtrator
CN104807676A (en) * 2015-05-06 2015-07-29 无锡维邦工业设备成套技术有限公司 NIR (Near Infrared Spectrum) online sampling system
CN105223041A (en) * 2015-11-03 2016-01-06 山东省农业科学院农业质量标准与检测技术研究所 A kind of fluid sample sampler for examining sample detection soon and method
CN206378326U (en) * 2016-12-14 2017-08-04 中国矿业大学 A kind of fluent solution sampling apparatus
CN107850514A (en) * 2015-06-26 2018-03-27 基础科学公司 System for gathering fluid sample
CN109238786A (en) * 2018-10-10 2019-01-18 黄志郎 The sample detection equipment that the movement potential energy stationary flow generated with water supply and drainage is collected
CN210243250U (en) * 2019-04-19 2020-04-03 西派特(北京)科技有限公司 Liquid sample sampling device suitable for pipeline spectrum collection

Patent Citations (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4076420A (en) * 1974-02-22 1978-02-28 Max-Planck-Gesellschaft Zur Forderung Der Wissenschaften E.V. Apparatus for investigating fast chemical reactions by optical detection
GB1477199A (en) * 1974-09-02 1977-06-22 Technicon Instr Sample supply apparatus for automatic analysis systems
US5460055A (en) * 1991-11-22 1995-10-24 Coulter Corporation Sampling metering and transfer valve assembly and analyzing system employing same
CN2499825Y (en) * 2001-11-02 2002-07-10 中国石油天然气股份有限公司 Analytical pool for on-line measuring petroleum product absorption spectrum
CN1501060A (en) * 2002-11-18 2004-06-02 ϣɭ������ʽ���� Sample analyzer and its components
CN1900716A (en) * 2002-11-18 2007-01-24 希森美康株式会社 Sample analyzer and its components
CN2612940Y (en) * 2003-01-24 2004-04-21 大庆油田有限责任公司 Low degradation quick-speed high pressure sampler
TW200712473A (en) * 2005-08-26 2007-04-01 Fiamo Corp Flow analysis system
CN101031786A (en) * 2005-08-26 2007-09-05 先进科技股份有限公司 Flow analysis system
US20110252898A1 (en) * 2008-12-03 2011-10-20 Mettler-Toledo Ag Sampling device
CN102239399A (en) * 2008-12-03 2011-11-09 梅特勒-托利多公开股份有限公司 Sampling device
CN201637607U (en) * 2010-03-09 2010-11-17 张卓理 Deaerating device for on-line water-quality analysis sampling water
CN202305265U (en) * 2011-09-21 2012-07-04 上海科星生物技术有限公司 Positioning and sampling device for liquid container
CN102749226A (en) * 2012-07-19 2012-10-24 江苏凯力克钴业股份有限公司 Solution sampling device
CN103063474A (en) * 2012-08-23 2013-04-24 浙江省海洋开发研究院 Shallow water quality sampler
FR3003033A1 (en) * 2013-03-07 2014-09-12 Commissariat Energie Atomique DEVICE FOR COLLECTING A CAPILLARITY LIQUID SAMPLE AND METHOD OF ANALYZING THE SAME
CN203551324U (en) * 2013-08-16 2014-04-16 甘肃瓮福化工有限责任公司 Continuous sampling device for liquid-phase materials
CN204177616U (en) * 2014-11-20 2015-02-25 上海未来企业有限公司 Micro-bubble filtrator
CN104807676A (en) * 2015-05-06 2015-07-29 无锡维邦工业设备成套技术有限公司 NIR (Near Infrared Spectrum) online sampling system
CN107850514A (en) * 2015-06-26 2018-03-27 基础科学公司 System for gathering fluid sample
CN105223041A (en) * 2015-11-03 2016-01-06 山东省农业科学院农业质量标准与检测技术研究所 A kind of fluid sample sampler for examining sample detection soon and method
CN206378326U (en) * 2016-12-14 2017-08-04 中国矿业大学 A kind of fluent solution sampling apparatus
CN109238786A (en) * 2018-10-10 2019-01-18 黄志郎 The sample detection equipment that the movement potential energy stationary flow generated with water supply and drainage is collected
CN210243250U (en) * 2019-04-19 2020-04-03 西派特(北京)科技有限公司 Liquid sample sampling device suitable for pipeline spectrum collection

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
杨学兵等: "一种精度较高的液体比重自动连续测量装置", 工业仪表与自动化装置, pages 43 - 44 *
田地等: "近红外光谱仪器", 分析仪器, pages 39 - 42 *

Similar Documents

Publication Publication Date Title
JP3255597B2 (en) Methods and devices for determining the presence of hemolysis, jaundice or lipemia, methods for determining serum index, methods and devices for transferring samples, and methods and devices for performing pre-tests
DE19535046C2 (en) Handheld device for pipetting and photometric measurement of samples
CN100458405C (en) Spectroscopic fluid analyzer
AU597168B2 (en) Sensor and method for detecting the presence of air bubbles in liquid
US8767194B2 (en) Automated soil measurement device
US3236602A (en) Colorimeter flow cell and holder therefor
CN103558179B (en) The device and method of the cross section phase content of biphase gas and liquid flow in a kind of measuring channel
US20020071123A1 (en) Photometric detection system having multiple path length flow cell
WO1998002727A1 (en) Method and apparatus for performing automated analysis
CN204389386U (en) A kind of multispectral transmission, scattered light urbidmetry and chemiluminescence reflectometry detection detection head and detection turbidimeter
CN105424604B (en) A kind of sensor based on nested waveguide
JP4044163B2 (en) Liquid detection method and apparatus
CN207528618U (en) A kind of dual wavelength sea water COD on-line measurement device
CN205426890U (en) Supporting device of gas analysis appearance examination
CN101203746B (en) Development of disposable/sealable tips for spectroscopic probes
CN106198471A (en) A kind of bio-chemical fluorescent analyser based on light-conducting capillaries and detection method thereof
CN104662406B (en) Determine the instrument and method of Blood Sedimentation rate and associated other parameters
CN208091910U (en) A kind of device for analyzing on-line checking Nitrate In Sea Water content based on optofluidic
CN110044657A (en) A kind of fluid sample sampler suitable for pipeline spectra collection
CN210243250U (en) Liquid sample sampling device suitable for pipeline spectrum collection
CN202092944U (en) Device for detecting ultramicro sample
CN211877756U (en) Flow cell with adjustable optical path and fluid detection device
CN209182229U (en) Water-insoluble palm fibre carbon extinction characteristic on-line measuring device in atmosphere
CN110044867A (en) A kind of fruit surface pesticide residue in-situ acquisition detection device and method
CN110085506A (en) Sample introduction assembly, open type ion source system and mass spectrometer

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20190723

WD01 Invention patent application deemed withdrawn after publication