CN110041715A - A kind of Masterbatch and preparation method thereof - Google Patents
A kind of Masterbatch and preparation method thereof Download PDFInfo
- Publication number
- CN110041715A CN110041715A CN201910284874.7A CN201910284874A CN110041715A CN 110041715 A CN110041715 A CN 110041715A CN 201910284874 A CN201910284874 A CN 201910284874A CN 110041715 A CN110041715 A CN 110041715A
- Authority
- CN
- China
- Prior art keywords
- masterbatch
- toner
- calcium powder
- stearic acid
- added
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/20—Compounding polymers with additives, e.g. colouring
- C08J3/22—Compounding polymers with additives, e.g. colouring using masterbatch techniques
- C08J3/223—Packed additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2423/00—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers
- C08J2423/02—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers not modified by chemical after treatment
- C08J2423/04—Homopolymers or copolymers of ethene
- C08J2423/06—Polyethene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2491/00—Characterised by the use of oils, fats or waxes; Derivatives thereof
- C08J2491/06—Waxes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/09—Carboxylic acids; Metal salts thereof; Anhydrides thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Developing Agents For Electrophotography (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
Abstract
The present invention relates to technical field of polymer materials, disclose a kind of Masterbatch, the Masterbatch is by stearic acid, the mixture of calcium powder and toner composition, wherein stearic acid, mixing forms in any proportion between calcium powder and toner three, a kind of preparation method of Masterbatch, stearic acid is added in agitator first and is warmed to 52 DEG C of -130 DEG C of thawings, it is successively separately added into toner and calcium powder again, side is stirred while toner and calcium powder is added, continue heating and forms color masterbatch mixture, the present invention is mixed using above-mentioned ingredient, the color masterbatch produced can be used in EVA, rubber, make in the production high molecular material such as PVC, use scope is wide, color difference is small.
Description
Technical field
The present invention relates to technical field of polymer materials, and in particular to a kind of Masterbatch.
Background technique
Masterbatch is by a high proportion of pigment or additive and carrier (EVA, PVC, rubber), through colouring made of fine dispersion
Agent, selected by carrier to colorant have good wet and peptizaiton, and with by coloured material have good phase
Capacitive, therefore, Masterbatch have extensive purposes.But the carrier of existing Masterbatch is used to produce EVA composite wood using EVA
Material, when such as producing rubber composite material, the carrier of Masterbatch can only select rubber as carrier, and use scope is restricted, and
And use rear poor dispersion, color difference, be affected to masterbatch performance.
Summary of the invention
The purpose of the present invention is to solve above-mentioned technical problems, provide a kind of color masterbatch that use scope is not limited by major ingredient
Grain, the Masterbatch have dispersibility well, and color difference is small, and use scope is wide.
To achieve the above object, The technical solution adopted by the invention is as follows: a kind of Masterbatch, it is characterised in that: the color masterbatch
The mixture that grain is made of stearic acid, calcium powder and toner, is wherein mixed between stearic acid, calcium powder and toner three in any proportion
It is combined into.
The invention also includes paraffin and polyethylene wax.
Preferably, the proportion of stearic acid of the present invention, calcium powder and toner is 3:3:2.
Stearic acid is added in agitator first and is warmed to 52 DEG C -130 DEG C and melts by a kind of preparation method of above-mentioned Masterbatch
Change, then be successively separately added into toner and calcium powder, side is stirred while toner and calcium powder is added, and is continued heating and is formed color masterbatch mixing
Object.
Compared with prior art, the invention has the following advantages:
1, the present invention is mixed using above-mentioned ingredient, and the color masterbatch produced, which can be used, makes height in EVA, rubber, PVC etc.
It is used in molecular material, use scope is wide, color difference is small.
2, invention increases toners can be with good toughness, and glossiness is high, and stability is good, while improving toner utilization rate,
To reduce production cost.
Specific embodiment
Below with reference to embodiment, the invention will be further described, and mode of the invention includes but are not limited to following implementation
Example.
Embodiment 1
A kind of Masterbatch, the mixture which is made of stearic acid, calcium powder and toner, the stearic acid, calcium powder and color
The proportion of powder is 6:2:1.
The stearic acid of said ratio, is added in agitator is warmed to 58 first by a kind of preparation method of above-mentioned Masterbatch
DEG C melt, then is successively separately added into toner and calcium powder, side is stirred while toner and calcium powder is added, and is continued heating and is formed color masterbatch
Mixture, the color masterbatch mixture produced can be used to be used in the production polymer composite such as EVA, rubber, PVC,
Use scope is wide, color difference is small.
Embodiment 2
A kind of Masterbatch, the mixture which is made of polyethylene wax, calcium powder and toner, the polyethylene wax, calcium powder
Proportion with toner is 6:2:2.
The polyethylene wax of said ratio, is added in agitator is warmed to first by a kind of preparation method of above-mentioned Masterbatch
113 DEG C of thawings, then it is successively separately added into toner and calcium powder, side is stirred while toner and calcium powder is added, and is continued heating and is formed
Color masterbatch mixture, the color masterbatch mixture produced can be used to be made in the production polymer composite such as EVA, rubber, PVC
With use scope is wide, color difference is small.
Embodiment 3
A kind of Masterbatch, the mixture which is made of stearic acid, paraffin, calcium powder and toner, the stearic acid, stone
The proportion of wax, calcium powder and toner is 3:3:2:3.
The stearic acid of said ratio and paraffin are added in agitator add first by a kind of preparation method of above-mentioned Masterbatch
Temperature is melted to 120 DEG C, then is successively separately added into toner and calcium powder, and side is stirred while toner and calcium powder is added, and continues to heat
Color masterbatch mixture is formed, the color masterbatch mixture produced, which can be used, makes polymer composite in EVA, rubber, PVC etc.
Middle use, use scope is wide, color difference is small.
Embodiment 4
A kind of Masterbatch, the mixture which is made of paraffin, calcium powder and toner, the paraffin, calcium powder and toner
Proportion is 6:1:1.
The paraffin of said ratio, is added in agitator is warmed to 55 DEG C first by a kind of preparation method of above-mentioned Masterbatch
Melt, then be successively separately added into toner and calcium powder, side is stirred while toner and calcium powder is added, and continuing heating, to form color masterbatch mixed
Object is closed, the color masterbatch mixture produced can be used to be used in the production polymer composite such as EVA, rubber, PVC, is made
With range is wide, color difference is small.
Embodiment 5
A kind of Masterbatch, the mixture which is made of stearic acid, polyethylene wax, calcium powder and toner, the stearic acid,
The proportion of polyethylene wax, calcium powder and toner is 4:2:1:3.
A kind of preparation method of above-mentioned Masterbatch, is added to agitator for the stearic acid of said ratio and polyethylene wax first
52 DEG C of thawings are inside warmed to, then are successively separately added into toner and calcium powder, side is stirred while toner and calcium powder is added, and continues to add
Temperature forms color masterbatch mixture, and the color masterbatch mixture produced, which can be used, makes macromolecule composite wood in EVA, rubber, PVC etc.
It is used in material, use scope is wide, color difference is small.
Embodiment 6
A kind of Masterbatch, the mixture which is made of stearic acid, paraffin, polyethylene wax, calcium powder and toner are described hard
Ester acid, paraffin, polyethylene wax, calcium powder and toner proportion be 4:1:1:2:2.
The stearic acid of said ratio, paraffin, polyethylene wax, are added to stir first by a kind of preparation method of above-mentioned Masterbatch
It mixes and is warmed to 122 DEG C of thawings in bucket, then be successively separately added into toner and calcium powder, side is stirred while toner and calcium powder is added,
Continue heating and form color masterbatch mixture, the color masterbatch mixture produced, which can be used, makes macromolecule in EVA, rubber, PVC etc.
It is used in composite material, use scope is wide, color difference is small.
Above-described embodiment is only the preferred embodiment of the present invention, should not be taken to limit protection scope of the present invention, but
It is all in body design thought of the invention and mentally make have no the change of essential meaning or polishing, the technology solved
Problem is still consistent with the present invention, should all be included within protection scope of the present invention.
Claims (4)
1. a kind of Masterbatch, it is characterised in that: the mixture that the Masterbatch is made of stearic acid, calcium powder and toner, wherein firmly
Mixing forms in any proportion between ester acid, calcium powder and toner three.
2. a kind of Masterbatch according to claim 1, it is characterised in that: it further include paraffin and polyethylene wax.
3. a kind of Masterbatch according to claim 1, it is characterised in that: the proportion of the stearic acid, calcium powder and toner
For 6:3:2.
4. a kind of preparation method of Masterbatch described in any one to 2 according to claim 1, it is characterised in that: first
Stearic acid is added in agitator and is warmed to 52 DEG C of -130 DEG C of thawings, then is successively separately added into toner and calcium powder, color is being added
Side is stirred while powder and calcium powder, is continued heating and is formed color masterbatch mixture.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910284874.7A CN110041715A (en) | 2019-04-10 | 2019-04-10 | A kind of Masterbatch and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910284874.7A CN110041715A (en) | 2019-04-10 | 2019-04-10 | A kind of Masterbatch and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110041715A true CN110041715A (en) | 2019-07-23 |
Family
ID=67276724
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910284874.7A Pending CN110041715A (en) | 2019-04-10 | 2019-04-10 | A kind of Masterbatch and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110041715A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110894364A (en) * | 2019-11-15 | 2020-03-20 | 广东天雄新材料科技股份有限公司 | Super-dispersed carrier-free color master batch and preparation method and application thereof |
| CN113004574A (en) * | 2021-02-26 | 2021-06-22 | 广东千千省化工有限公司 | PVC material foaming color mixing auxiliary agent |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102888022A (en) * | 2012-10-18 | 2013-01-23 | 温州大洲无纺布有限公司 | Master batch and manufacturing method thereof |
| CN104672602A (en) * | 2015-03-18 | 2015-06-03 | 绵阳曙光新材料科技有限公司 | Modified high-filling color masterbatch and preparation method thereof |
-
2019
- 2019-04-10 CN CN201910284874.7A patent/CN110041715A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102888022A (en) * | 2012-10-18 | 2013-01-23 | 温州大洲无纺布有限公司 | Master batch and manufacturing method thereof |
| CN104672602A (en) * | 2015-03-18 | 2015-06-03 | 绵阳曙光新材料科技有限公司 | Modified high-filling color masterbatch and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 张治国主编: "《塑料挤出成型技术问答》", 31 March 2012, 印刷工业出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110894364A (en) * | 2019-11-15 | 2020-03-20 | 广东天雄新材料科技股份有限公司 | Super-dispersed carrier-free color master batch and preparation method and application thereof |
| CN113004574A (en) * | 2021-02-26 | 2021-06-22 | 广东千千省化工有限公司 | PVC material foaming color mixing auxiliary agent |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101392077B (en) | Polypropylene color master-batch with pearlescent interference effect and preparation method thereof | |
| CN101392078A (en) | Universal white master batch and preparation method thereof | |
| CN110041715A (en) | A kind of Masterbatch and preparation method thereof | |
| CN101319068A (en) | White master batch applied for polyolefin film and preparation method thereof | |
| CN103649140A (en) | ASA-based graft copolymer composition | |
| US5604279A (en) | Colorant preparation for producing masterbatches | |
| CN104371203A (en) | Heat-sealing high-temperature storage battery shell resin alloy and preparation method thereof | |
| CN106317994B (en) | Oil painting stick core and preparation method thereof | |
| CN106928565A (en) | High glaze polystyrene resin and preparation method thereof | |
| CN103030335B (en) | Colored rock paint and preparation method thereof | |
| CN104817916B (en) | A kind of water-in-water multicolor coating and preparation method thereof | |
| CN110003563A (en) | A kind of weather-resistance flame-retardant Masterbatch | |
| CN104356588B (en) | A kind of high-concentration colorful emulsified asphalt and preparation method thereof | |
| CN107523141A (en) | A kind of preparation method of high-elastic environmentally friendly wax crayon | |
| US8088841B2 (en) | Pigmentable asphalt binder composition | |
| CN101511953B (en) | Crayon and method for producing the same | |
| CN104559700A (en) | Unsaturated polyester gloss black lacquer and method for preparing same | |
| CN107915851A (en) | Improve the colorant and method of injection manikin uniform in color and stability | |
| CN108977123A (en) | A kind of low temperature resistant books and periodicals glue and preparation method thereof | |
| CN102127354A (en) | Water-based paint highly simulating granite and marble and preparation method thereof | |
| KR20120025704A (en) | Colorant composition for silicone synthetic leather and coating liquid having the same | |
| CN105948504A (en) | Blue-green tempered glass printing ink | |
| CN102181223B (en) | Super leveling mirror surface powder coating | |
| CN109535904A (en) | A kind of coating and preparation method thereof | |
| CN104861561A (en) | PET spinning color master batch and preparation method therefor |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190723 |