CN110039804A - A kind of functional high-polymer thin film preparation process - Google Patents
A kind of functional high-polymer thin film preparation process Download PDFInfo
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- CN110039804A CN110039804A CN201910259820.5A CN201910259820A CN110039804A CN 110039804 A CN110039804 A CN 110039804A CN 201910259820 A CN201910259820 A CN 201910259820A CN 110039804 A CN110039804 A CN 110039804A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29D—PRODUCING PARTICULAR ARTICLES FROM PLASTICS OR FROM SUBSTANCES IN A PLASTIC STATE
- B29D7/00—Producing flat articles, e.g. films or sheets
- B29D7/01—Films or sheets
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/18—Manufacture of films or sheets
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2300/00—Characterised by the use of unspecified polymers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2367/00—Characterised by the use of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Derivatives of such polymers
- C08J2367/02—Polyesters derived from dicarboxylic acids and dihydroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K13/00—Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
- C08K13/02—Organic and inorganic ingredients
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2217—Oxides; Hydroxides of metals of magnesium
- C08K2003/2224—Magnesium hydroxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2227—Oxides; Hydroxides of metals of aluminium
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K3/2279—Oxides; Hydroxides of metals of antimony
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/09—Carboxylic acids; Metal salts thereof; Anhydrides thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K7/00—Use of ingredients characterised by shape
- C08K7/22—Expanded, porous or hollow particles
- C08K7/24—Expanded, porous or hollow particles inorganic
- C08K7/26—Silicon- containing compounds
Abstract
The invention discloses a kind of functional high-polymer thin film preparation processes, including following raw material proportioning: 10~20 parts of aerosil powder, 5~8 parts of film forming agent, 10~12 parts of antimony oxide, 5~10 parts of magnesium hydroxide, 3~5 parts of aluminium hydroxide, 5~8 parts of stearic acid, 20~30 parts of polymer base material, 50~70 parts of water, 10~15 parts of curing agent, 3~5 parts of additive, 8~15 parts of aluminium powder, 5~10 parts of polyester resin, the preparation method of film is relatively simple, reduce the processing cost of film, the film produced has heat-insulated, it is fire-retardant, the effect of insulation, there is excellent barrier property to steam and oxygen simultaneously, can have a wide range of application.
Description
Technical field
The present invention relates to thin film preparation process fields, more particularly, to a kind of functional high-polymer thin film preparation process.
Background technique
In modern society, the application of plastics is extremely wide, miscellaneous in particular with the growth of light industry
Plastics emerge one after another, currently, the plastics being most widely used are vinyon and igelite.Both traditional senses
On plastics gradually permeated in each field in people's life, still, this plastics there is also many defects,
Such as non-refractory low temperature, be not easy hydrolytic degradation, be difficult to be recovered degradation, physical property is poor, and largely use can
Cause " white pollution ".
Summary of the invention
The present invention is to overcome above situation insufficient, it is desirable to provide a kind of technical solution that can solve the above problem.
A kind of functional high-polymer thin film preparation process, including following raw material proportioning: aerosil powder 10~20
Part, 5~8 parts of film forming agent, 10~12 parts of antimony oxide, 5~10 parts of magnesium hydroxide, 3~5 parts of aluminium hydroxide, stearic acid 5~8
Part, 20~30 parts of polymer base material, 50~70 parts of water, 10~15 parts of curing agent, 3~5 parts of additive, 8~15 parts of aluminium powder, terylene
5~10 parts of resin, including following preparation step:
Step 1: aerosil powder, film forming agent, water are added in polyester resin, carry out mixed at high speed, mixing
Temperature is 80 DEG C, and incorporation time is 1~2H, obtains counterdie original agent;
Step 2: polymer base material is subjected to high-temperature digestion, obtains polymer base material solution;
Step 3: water, antimony oxide, magnesium hydroxide, aluminium hydroxide, stearic acid are added in polymer base material solvent,
It is mixed, mixing temperature is 100 DEG C, incorporation time 1H, obtains pellicle original agent;
Step 4: aluminium powder, additive, curing agent being added in pellicle original agent, mixed, and mixing temperature is 100 DEG C,
Incorporation time is 1~1.5H;
Step 5: counterdie original agent being added in membrane material equipment and carries out film material forming, obtains counterdie, while by pellicle original agent
It is added in membrane material equipment and carries out film material forming, obtain pellicle;
Step 6: pellicle is added in overlay film abutted equipment together with counterdie, by the laminating surface to counterdie of pellicle,
Form functional high-polymer film;
Step 7: carrying out the detection of functional high-polymer film, and qualified functional high-polymer film is packaged.
As a further solution of the present invention: including following raw material proportioning: 10 parts of aerosil powder, film forming agent 5
Part, is consolidated 10 parts of antimony oxide, 5 parts of magnesium hydroxide, 3 parts of aluminium hydroxide, 5 parts of stearic acid, 20 parts of polymer base material, 50 parts of water
10 parts of agent, 3 parts of additive, 8 parts of aluminium powder, 5 parts of polyester resin.
As a further solution of the present invention: 20 parts of aerosil powder, 8 parts of film forming agent, 12 parts of antimony oxide,
10 parts of magnesium hydroxide, 5 parts of aluminium hydroxide, 8 parts of stearic acid, 30 parts of polymer base material, 70 parts of water, 15 parts of curing agent, additive 5
Part, 15 parts of aluminium powder, 10 parts of polyester resin.
As a further solution of the present invention: the film forming agent is albumen film forming agent or acrylic resin film forming agent.
As a further solution of the present invention: the curing agent is UV curing agent.
Compared with prior art, the beneficial effects of the present invention are: the preparation method of film is relatively simple, film is reduced
Processing cost, the film produced has the effect of heat-insulated, fire-retardant, insulation, while having excellent barrier property to steam and oxygen
Can, can have a wide range of application, while material used in preparation is degradable, has certain environmental-protecting performance.
Additional aspect and advantage of the invention will be set forth in part in the description, and will partially become from the following description
Obviously, or practice through the invention is recognized.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common
Technical staff's every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
In the embodiment of the present invention, a kind of functional high-polymer thin film preparation process, including following raw material proportioning: silica
10~20 parts of airsetting rubber powder, 5~8 parts of film forming agent, 10~12 parts of antimony oxide, 5~10 parts of magnesium hydroxide, aluminium hydroxide 3~5
Part, 5~8 parts of stearic acid, 20~30 parts of polymer base material, 50~70 parts of water, 10~15 parts of curing agent, 3~5 parts of additive, aluminium
8~15 parts of powder, 5~10 parts of polyester resin, including following preparation step:
Step 1: aerosil powder, film forming agent, water are added in polyester resin, carry out mixed at high speed, mixing
Temperature is 80 DEG C, and incorporation time is 1~2H, obtains counterdie original agent;
Step 2: polymer base material is subjected to high-temperature digestion, obtains polymer base material solution;
Step 3: water, antimony oxide, magnesium hydroxide, aluminium hydroxide, stearic acid are added in polymer base material solvent,
It is mixed, mixing temperature is 100 DEG C, incorporation time 1H, obtains pellicle original agent;
Step 4: aluminium powder, additive, curing agent being added in pellicle original agent, mixed, and mixing temperature is 100 DEG C,
Incorporation time is 1~1.5H;
Step 5: counterdie original agent being added in membrane material equipment and carries out film material forming, obtains counterdie, while by pellicle original agent
It is added in membrane material equipment and carries out film material forming, obtain pellicle;
Step 6: pellicle is added in overlay film abutted equipment together with counterdie, by the laminating surface to counterdie of pellicle,
Form functional high-polymer film;
Step 7: carrying out the detection of functional high-polymer film, and qualified functional high-polymer film is packaged.
The film forming agent is albumen film forming agent or acrylic resin film forming agent.
The curing agent is UV curing agent.
Embodiment one:
A kind of functional high-polymer thin film preparation process, including following raw material proportioning: 10 parts of aerosil powder, at
5 parts of film, 10 parts of antimony oxide, 5 parts of magnesium hydroxide, 3 parts of aluminium hydroxide, 5 parts of stearic acid, 20 parts of polymer base material, water 50
Part, 10 parts of curing agent, 3 parts of additive, 8 parts of aluminium powder, 5 parts of polyester resin, including following preparation step:
Step 1: aerosil powder, film forming agent, water are added in polyester resin, carry out mixed at high speed, mixing
Temperature is 80 DEG C, and incorporation time is 1~2H, obtains counterdie original agent;
Step 2: polymer base material is subjected to high-temperature digestion, obtains polymer base material solution;
Step 3: water, antimony oxide, magnesium hydroxide, aluminium hydroxide, stearic acid are added in polymer base material solvent,
It is mixed, mixing temperature is 100 DEG C, incorporation time 1H, obtains pellicle original agent;
Step 4: aluminium powder, additive, curing agent being added in pellicle original agent, mixed, and mixing temperature is 100 DEG C,
Incorporation time is 1~1.5H;
Step 5: counterdie original agent being added in membrane material equipment and carries out film material forming, obtains counterdie, while by pellicle original agent
It is added in membrane material equipment and carries out film material forming, obtain pellicle;
Step 6: pellicle is added in overlay film abutted equipment together with counterdie, by the laminating surface to counterdie of pellicle,
Form functional high-polymer film;
Step 7: carrying out the detection of functional high-polymer film, and qualified functional high-polymer film is packaged.
Embodiment two:
A kind of functional high-polymer thin film preparation process, including following raw material proportioning: 20 parts of aerosil powder, at
8 parts of film, 12 parts of antimony oxide, 10 parts of magnesium hydroxide, 5 parts of aluminium hydroxide, 8 parts of stearic acid, 30 parts of polymer base material, water 70
Part, 15 parts of curing agent, 5 parts of additive, 15 parts of aluminium powder, 10 parts of polyester resin, including following preparation step:
Step 1: aerosil powder, film forming agent, water are added in polyester resin, carry out mixed at high speed, mixing
Temperature is 80 DEG C, and incorporation time is 1~2H, obtains counterdie original agent;
Step 2: polymer base material is subjected to high-temperature digestion, obtains polymer base material solution;
Step 3: water, antimony oxide, magnesium hydroxide, aluminium hydroxide, stearic acid are added in polymer base material solvent,
It is mixed, mixing temperature is 100 DEG C, incorporation time 1H, obtains pellicle original agent;
Step 4: aluminium powder, additive, curing agent being added in pellicle original agent, mixed, and mixing temperature is 100 DEG C,
Incorporation time is 1~1.5H;
Step 5: counterdie original agent being added in membrane material equipment and carries out film material forming, obtains counterdie, while by pellicle original agent
It is added in membrane material equipment and carries out film material forming, obtain pellicle;
Step 6: pellicle is added in overlay film abutted equipment together with counterdie, by the laminating surface to counterdie of pellicle,
Form functional high-polymer film;
Step 7: carrying out the detection of functional high-polymer film, and qualified functional high-polymer film is packaged.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
Claims (5)
1. a kind of functional high-polymer thin film preparation process, which is characterized in that including following raw material proportioning: aerosil
It is 10~20 parts of powder, 5~8 parts of film forming agent, 10~12 parts of antimony oxide, 5~10 parts of magnesium hydroxide, 3~5 parts of aluminium hydroxide, hard
5~8 parts of resin acid, 20~30 parts of polymer base material, 50~70 parts of water, 10~15 parts of curing agent, 3~5 parts of additive, aluminium powder 8~
15 parts, 5~10 parts of polyester resin, including following preparation step:
Step 1: aerosil powder, film forming agent, water are added in polyester resin, carry out mixed at high speed, mixing temperature
It is 80 DEG C, incorporation time is 1~2H, obtains counterdie original agent;
Step 2: polymer base material is subjected to high-temperature digestion, obtains polymer base material solution;
Step 3: water, antimony oxide, magnesium hydroxide, aluminium hydroxide, stearic acid are added in polymer base material solvent, carried out
It is mixed, mixing temperature is 100 DEG C, incorporation time 1H, obtains pellicle original agent;
Step 4: aluminium powder, additive, curing agent being added in pellicle original agent, mixed, and mixing temperature is 100 DEG C, mixing
Time is 1~1.5H;
Step 5: counterdie original agent being added in membrane material equipment and carries out film material forming, obtains counterdie, while pellicle original agent being added
Film material forming is carried out into membrane material equipment, obtains pellicle;
Step 6: pellicle is added in overlay film abutted equipment together with counterdie, by the laminating surface to counterdie of pellicle, is formed
Functional high-polymer film;
Step 7: carrying out the detection of functional high-polymer film, and qualified functional high-polymer film is packaged.
2. a kind of functional high-polymer thin film preparation process according to claim 1, which is characterized in that including following raw material
Proportion: 10 parts of aerosil powder, 5 parts of film forming agent, 10 parts of antimony oxide, 5 parts of magnesium hydroxide, 3 parts of aluminium hydroxide, hard
5 parts of resin acid, 20 parts of polymer base material, 50 parts of water, 10 parts of curing agent, 3 parts of additive, 8 parts of aluminium powder, 5 parts of polyester resin.
3. a kind of functional high-polymer thin film preparation process according to claim 1, which is characterized in that silica airsetting
It is 20 parts of rubber powder, 8 parts of film forming agent, 12 parts of antimony oxide, 10 parts of magnesium hydroxide, 5 parts of aluminium hydroxide, 8 parts of stearic acid, polymer-based
30 parts of material, 70 parts of water, 15 parts of curing agent, 5 parts of additive, 15 parts of aluminium powder, 10 parts of polyester resin.
4. a kind of functional high-polymer thin film preparation process according to claim 1, which is characterized in that the film forming agent is
Albumen film forming agent or acrylic resin film forming agent.
5. a kind of functional high-polymer thin film preparation process according to claim 1, which is characterized in that the curing agent is
UV curing agent.
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CN201910259820.5A CN110039804A (en) | 2019-04-02 | 2019-04-02 | A kind of functional high-polymer thin film preparation process |
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CN201910259820.5A CN110039804A (en) | 2019-04-02 | 2019-04-02 | A kind of functional high-polymer thin film preparation process |
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CN201910259820.5A Withdrawn CN110039804A (en) | 2019-04-02 | 2019-04-02 | A kind of functional high-polymer thin film preparation process |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111590937A (en) * | 2020-05-07 | 2020-08-28 | 合肥佛斯德新材料科技有限公司 | Preparation method of PET/Al/PE composite film for flexible package |
CN113336983A (en) * | 2021-05-06 | 2021-09-03 | 江苏华美特金属科技有限公司 | High-temperature-resistant insulating polymer film and preparation method thereof |
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CN102751460A (en) * | 2012-05-23 | 2012-10-24 | 杭州福膜新材料科技有限公司 | High-temperature-resisting composite isolation film and preparation method thereof |
CN103770418A (en) * | 2013-12-30 | 2014-05-07 | 佛山佛塑科技集团股份有限公司 | Composite material for building and preparation method thereof |
CN104804391A (en) * | 2015-04-19 | 2015-07-29 | 青岛承天伟业机械制造有限公司 | Agricultural plastic film |
CN106147140A (en) * | 2016-06-28 | 2016-11-23 | 周开雄 | A kind of inflaming retarding membrane and preparation method thereof |
CN106280306A (en) * | 2016-08-11 | 2017-01-04 | 苏州柯创电子材料有限公司 | Heat sealable high-isolating packaging film |
CN107840976A (en) * | 2017-05-05 | 2018-03-27 | 东莞市正程新材料有限公司 | A kind of TPU film and preparation method thereof |
CN109727732A (en) * | 2017-10-30 | 2019-05-07 | 伊利诺斯工具制品有限公司 | A kind of insulated compound film and electric component |
-
2019
- 2019-04-02 CN CN201910259820.5A patent/CN110039804A/en not_active Withdrawn
Patent Citations (7)
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CN102751460A (en) * | 2012-05-23 | 2012-10-24 | 杭州福膜新材料科技有限公司 | High-temperature-resisting composite isolation film and preparation method thereof |
CN103770418A (en) * | 2013-12-30 | 2014-05-07 | 佛山佛塑科技集团股份有限公司 | Composite material for building and preparation method thereof |
CN104804391A (en) * | 2015-04-19 | 2015-07-29 | 青岛承天伟业机械制造有限公司 | Agricultural plastic film |
CN106147140A (en) * | 2016-06-28 | 2016-11-23 | 周开雄 | A kind of inflaming retarding membrane and preparation method thereof |
CN106280306A (en) * | 2016-08-11 | 2017-01-04 | 苏州柯创电子材料有限公司 | Heat sealable high-isolating packaging film |
CN107840976A (en) * | 2017-05-05 | 2018-03-27 | 东莞市正程新材料有限公司 | A kind of TPU film and preparation method thereof |
CN109727732A (en) * | 2017-10-30 | 2019-05-07 | 伊利诺斯工具制品有限公司 | A kind of insulated compound film and electric component |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111590937A (en) * | 2020-05-07 | 2020-08-28 | 合肥佛斯德新材料科技有限公司 | Preparation method of PET/Al/PE composite film for flexible package |
CN113336983A (en) * | 2021-05-06 | 2021-09-03 | 江苏华美特金属科技有限公司 | High-temperature-resistant insulating polymer film and preparation method thereof |
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Application publication date: 20190723 |