CN110022697A - A kind of atomization basal liquid and preparation method thereof - Google Patents
A kind of atomization basal liquid and preparation method thereof Download PDFInfo
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- CN110022697A CN110022697A CN201680089516.5A CN201680089516A CN110022697A CN 110022697 A CN110022697 A CN 110022697A CN 201680089516 A CN201680089516 A CN 201680089516A CN 110022697 A CN110022697 A CN 110022697A
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- atomization
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
Abstract
It provides a kind of containing triethylene-glycol, tetraethylene-glycol, polyethylene glycol, the atomization basal liquid of 1,3-BDO solution and preparation method thereof, is atomized the mixed liquor that basal liquid is triethylene-glycol solution or tetraethylene-glycol solution and polyglycol solution.Atomization basal liquid atomization of the invention is good, aerosol production quantity is big, tar and nitroso compound are generated when avoiding heating cracking simultaneously, it is low with feed liquid density, process is not limited by environment temperature, the features such as low energy consumption, utilization rate of equipment and installations is high, can be widely applied to electronic cigarette atomizing liquid, stage and video display special efficacy smoke agent, military smoke agent, medical atomized agent and ultrasonic microgrid Alevaire and manufacture.
Description
Summary of the invention
In order to overcome the problems, such as in the prior art, the present invention provides one kind to contain triethylene-glycol solution or tetraethylene-glycol solution, polyglycol solution, 1, the atomization basis liquid and preparation method thereof of 3- butanediol solution, the tar and nitroso compound formed when can be to avoid heating cracking, basal liquid is atomized without any peculiar smell, it is environmentally friendly, to no damage to human body.
The present invention uses the mixed liquor of multiple compounds, wherein triethylene-glycol: no color or smell has hygroscopic thick liquid, and (20 DEG C) of density are 1.1254g/cm3, fusing point is -4.3 DEG C, and boiling point (normal pressure) is 288 DEG C, and LD50 value is (rat oral) 16.8ml/kg, and toxicity is low, and aerosol production quantity is moderate after heating, and the humectant that can be used as high cigarette uses.
Tetraethylene-glycol: transparency liquid, can be miscible with water, alcohol, do not dissolve in benzene, toluene and aliphatic hydrocarbon.(20 DEG C) of density are 1.123-1.126g/cm3Boiling point (normal pressure) is 327.3 DEG C, LD50 value is (rat oral) 34.65g/kg, LD50 (rabbit is percutaneous) value is 22.5g/kg, it is higher with boiling point, aerosol production quantity is big, the low advantage of toxicity, the atomized liquid and smoke agent more suitable for aerosol amount needed for preparing.
Glycerin, mixed triester with caprylic acid capric acid: colourless, tasteless transparency liquid, (20 DEG C) of density are 0.94-0.96g/cm3, LD50 value is (rat oral) 15g/kg, and viscosity is the half of general vegetable oil.Freezing point is low, and oxidation stability is good.There is good intersolubility with various solvents, grease, some oxidants, vitamin.Its emulsibility, dissolubility, extensibility and lubricity are better than common grease.
Chitosan: transparency liquid; chemical stability is good; about 185 DEG C of decomposition; it is nontoxic; it is dissolved in the chitosan salt colloidal solution that diluted acid generates clear viscous; the H+ in solution generates positively charged polymer substance i.e. in conjunction with the amino in molecule at this time, can be acylated, carboxylated, hydroxylating, alkanisation, esterification (Sulfation), aldimine, Azide, react at salt, hydrolysis, chelating, oxidation, chlorination, steatolysis and crosslinking etc..
Polyethylene glycol: odorless, nonirritant, have a hygroscopic clear, colorless thick liquid, fusing point is -65 DEG C, and boiling point (normal pressure) is 250 DEG C, and (20 DEG C) of density are 1.125g/cm3。
1,3-BDO: colourless, thick liquid, < -54 DEG C of fusing point, boiling point (normal pressure) is 207 DEG C,
(20 DEG C) of density are 1.001g/cm3, LD50 value is (rat oral): 29.6g/kg.
Ethyl cellulose: white to yellowish-brown liquid, (20 DEG C) of density are 1.07-1.18g/cm3, fusing point is 240-255 DEG C, refractive index 1.479.
The present invention adopts the following technical scheme:
A kind of atomization basal liquid, the atomization basal liquid include tetraethylene-glycol solution and polyglycol solution.
Further, the percent by volume of the tetraethylene-glycol solution and polyglycol solution is 1-99%:99-1%.
It further, also include 1,3-BDO solution in the atomization basal liquid.
Further, tetraethylene-glycol, polyglycol solution are mixed in the atomization basal liquid with arbitrary proportion, and the percent by volume of tetraethylene-glycol, polyethylene glycol mixed liquor and 1,3-BDO solution is 90-95%:5-10%.
Further, the atomization basal liquid includes triethylene-glycol solution, polyglycol solution, Glycerin, mixed triester with caprylic acid capric acid solution and chitosan solution.
Further, the percentage by volume of triethylene-glycol solution is 70-87% in the atomization basal liquid, the percentage by volume of polyglycol solution is 1-10%, and the percentage by volume of Glycerin, mixed triester with caprylic acid capric acid solution is 1-10%, and the percentage by volume of chitosan solution is 1-10%.
Further, the percentage by volume of triethylene-glycol solution is 85% in the atomization basal liquid, and the percentage by volume of polyglycol solution is 5%, and the percentage by volume of Glycerin, mixed triester with caprylic acid capric acid solution is 5%, and the percentage by volume of chitosan solution is 5%.
Further, the atomization basal liquid includes tetraethylene-glycol solution, 1,3-BDO solution and ethyl cellulose solution.
Further, tetraethylene-glycol solution and 1,3-BDO solution are mixed in the atomization basal liquid with arbitrary proportion, and the percent by volume of the mixed liquor and ethyl cellulose solution is 99.55-99.8%:0.45-0.2%.
Further, the atomization basal liquid includes tetraethylene-glycol solution, 1,3-BDO solution and cactus slag body leaching liquor.
Further, the percent by volume of the tetraethylene-glycol solution, 1,3-BDO solution and cactus slag body leaching liquor is 80-90%:5-10%:5-10%.
A kind of preparation method being atomized basal liquid, comprising the following steps:
Tetraethylene-glycol solution and polyglycol solution are measured by volume, are carried out uniform, slow, adequately stirring, are obtained as clear as crystal, the clear atomization basal liquid of quality.
Further, comprising the following steps:
Step 1: measuring tetraethylene-glycol solution and polyglycol solution by volume, carries out uniform, slow, adequately stirring, obtains mixed liquor；
Step 2: measuring the mixed liquor and 1,3-BDO solution by volume, uniformly, slowly, adequately stir, obtains as clear as crystal, the clear atomization basal liquid of quality.
Further, comprising the following steps:
Triethylene-glycol solution, polyglycol solution, Glycerin, mixed triester with caprylic acid capric acid solution and chitosan solution are measured by volume, are carried out uniform, slow, adequately stirring, are obtained as clear as crystal, the clear atomization basal liquid of quality.
Further, comprising the following steps:
Step 1: measuring tetraethylene-glycol solution and 1,3-BDO solution by volume, is heated to 45-50 DEG C, carries out uniform, slow, adequately stirring, obtains mixed liquor；
Step 2: measuring the mixed liquor and ethyl cellulose solution by volume, uniformly, slowly, adequately stir, obtains as clear as crystal, the clear atomization basal liquid of quality.
Further, comprising the following steps:
Step 1: cactus washing and sterilizing is extracted into slag body portion to be separated by solid-liquid separation pulper slurrying；
Step 2: tetraethylene-glycol solution and the mixing of 1,3-BDO solution are measured by volume, is set
In 50-65 DEG C of water-bath；
Step 3: example weighs the slag body by volume, is added into the mixed solution of tetraethylene-glycol solution and 1,3-BDO solution, and stirring extracts completely；
Step 4: filtrate is placed in natural subsidence at room temperature by filtering and removing slag, and obtaining supernatant is the atomization basal liquid.
A kind of purposes being atomized basal liquid, the atomization basal liquid are used to prepare the atomized liquid of electronic cigarette.
A kind of purposes being atomized basal liquid, the atomization basal liquid are used to prepare stage smoke agent.
A kind of purposes being atomized basal liquid, the atomization basal liquid are used to prepare video display special efficacy smoke agent.
A kind of purposes being atomized basal liquid, the atomization basal liquid are used to prepare military affairs smoke agent.
A kind of purposes being atomized basal liquid, the atomization basal liquid are used to prepare medical atomized agent.
A kind of purposes being atomized basal liquid, the atomization basal liquid are used to prepare ultrasonic microgrid Alevaire.
By adopting the above technical scheme, the invention has the following beneficial effects:
First: atomization basal liquid produced by the present invention is without any peculiar smell, it is excellent with various flavors and fragrancess used in electronic cigarette and auxiliary material compatibility, because being free of glycerol and propylene glycol, atomization is good, while avoiding the tar and nitroso compound formed when heating cracking, and there is feed liquid density to reduce, process is not limited by environment temperature, it is solution-stabilized, to no damage to human body, environmentally friendly advantage.
Second: preparation process low energy consumption, utilization rate of equipment and installations is high, and production process is simple to operation, pollution-free.
Third: the present invention is widely used in electronic cigarette atomizing liquid, stage and video display special efficacy smoke agent, military smoke agent, medical atomized agent and ultrasonic microgrid Alevaire and manufactures.Finished product storage temperature is resistant to -30 DEG C of low temperature, does not crystallize and muddiness does not occur, and solves the problems, such as the transport of the extremely frigid zones such as China northeast and Northern Europe and uses.
In order to make the objectives, technical solutions, and advantages of the present invention clearer, below with reference to implementation
Example, the present invention will be described in further detail.It should be appreciated that described herein, specific examples are only used to explain the present invention, is not intended to limit the present invention.
Embodiment 1:
A kind of atomization basal liquid, the atomization basal liquid are made of tetraethylene-glycol solution and polyglycol solution, and wherein the volume ratio of tetraethylene-glycol solution and polyglycol solution is 40%:60%.The atomization basal liquid is prepared, using following preparation method:
It measures tetraethylene-glycol solution and polyglycol solution respectively in proportion, carries out uniform, slow, adequately stirring, obtain as clear as crystal, the clear atomization basal liquid of quality.
The applicable field of atomization basal liquid of the present embodiment includes but is not limited to atomized liquid, stage and video display special efficacy smoke agent, military smoke agent, medical atomized agent, the ultrasonic microgrid Alevaire of electronic cigarette.
Embodiment 2:
A kind of atomization basal liquid, the atomization basal liquid are made of tetraethylene-glycol solution and polyglycol solution, and wherein the volume ratio of tetraethylene-glycol solution and polyglycol solution is 90%:10%.The atomization basal liquid is prepared, using following preparation method:
It measures tetraethylene-glycol solution and polyglycol solution respectively in proportion, carries out uniform, slow, adequately stirring, obtain as clear as crystal, the clear atomization basal liquid of quality.
The applicable field of atomization basal liquid of the present embodiment includes but is not limited to atomized liquid, stage and video display special efficacy smoke agent, military smoke agent, medical atomized agent, the ultrasonic microgrid Alevaire of electronic cigarette.
Embodiment 3:
A kind of atomization basal liquid, the atomization basal liquid is by tetraethylene-glycol solution, polyglycol solution and 1,3-BDO solution composition.Wherein the volume ratio of tetraethylene-glycol solution and polyglycol solution is 80%:20%.This two kinds of solution are mixed, obtain mixed liquor, the volume ratio of mixed liquor and 1,3-BDO solution is 95%:5%.The atomization basal liquid is prepared, using following preparation method:
Step 1: measuring tetraethylene-glycol solution and polyglycol solution in proportion, carries out uniform, slow, adequately stirring, obtains as clear as crystal, the clear tetraethylene-glycol solution of quality and poly- second
The mixed liquor of glycol solution；
Step 2: measuring the mixed liquor and 1,3-BDO solution of tetraethylene-glycol solution, polyglycol solution in proportion, carries out uniform, slow, adequately stirring, obtains as clear as crystal, the clear atomization basal liquid of quality.
The applicable field of atomization basal liquid of the present embodiment includes but is not limited to atomized liquid, stage and video display special efficacy smoke agent, military smoke agent, medical atomized agent, the ultrasonic microgrid Alevaire of electronic cigarette.
Embodiment 4:
A kind of atomization basal liquid, the atomization basal liquid is by tetraethylene-glycol solution, polyglycol solution and 1,3-BDO solution composition.Wherein the volume ratio of tetraethylene-glycol solution and polyglycol solution is 60%:40%.This two kinds of solution are mixed, obtain mixed liquor, the volume ratio of mixed liquor and 1,3-BDO solution is 90%:10%.Preparation atomization basal liquid, using following preparation method:
Step 1: measuring tetraethylene-glycol solution and polyglycol solution in proportion, carries out uniform, slow, adequately stirring, obtains the mixed liquor of as clear as crystal quality clear tetraethylene-glycol solution and polyglycol solution；
Step 2: measuring the mixed liquor and 1,3-BDO solution of tetraethylene-glycol solution, polyglycol solution in proportion, carries out uniform, slow, adequately stirring, obtains as clear as crystal, the clear atomization basal liquid of quality.
The applicable field of atomization basal liquid of the present embodiment includes but is not limited to atomized liquid, stage and video display special efficacy smoke agent, military smoke agent, medical atomized agent, the ultrasonic microgrid Alevaire of electronic cigarette.
Embodiment 5:
A kind of atomization basal liquid, the atomization basal liquid is by triethylene-glycol solution, polyglycol solution, Glycerin, mixed triester with caprylic acid capric acid solution and chitosan solution composition, wherein the volume ratio of triethylene-glycol solution is 85%, the volume ratio of polyglycol solution is 5%, and the volume ratio of Glycerin, mixed triester with caprylic acid capric acid solution is 5%, and the volume ratio of chitosan solution is 5%.The atomization basal liquid is prepared, following method can be used:
It is molten to measure triethylene-glycol solution, polyglycol solution, Glycerin, mixed triester with caprylic acid capric acid respectively in proportion
Liquid and chitosan solution uniformly, slowly, adequately stir, obtain as clear as crystal, the clear atomization basal liquid of quality.
The applicable field of atomization basal liquid of the present embodiment includes but is not limited to atomized liquid, stage and video display special efficacy smoke agent, military smoke agent, medical atomized agent, the ultrasonic microgrid Alevaire of electronic cigarette.
Embodiment 6:
A kind of atomization basal liquid, the atomization basal liquid is by triethylene-glycol solution, polyglycol solution, Glycerin, mixed triester with caprylic acid capric acid solution and chitosan solution composition, wherein the volume ratio of triethylene-glycol solution is 70%, the volume ratio of polyglycol solution is 10%, and the volume ratio of Glycerin, mixed triester with caprylic acid capric acid solution is 10%, and the volume ratio of chitosan solution is 10%.The atomization basal liquid is prepared, following method can be used:
It measures triethylene-glycol solution, polyglycol solution, Glycerin, mixed triester with caprylic acid capric acid solution and chitosan solution respectively in proportion, carries out uniform, slow, adequately stirring, obtain as clear as crystal, the clear atomization basal liquid of quality.
The applicable field of atomization basal liquid of the present embodiment includes but is not limited to atomized liquid, stage and video display special efficacy smoke agent, military smoke agent, medical atomized agent, the ultrasonic microgrid Alevaire of electronic cigarette.
Embodiment 7:
A kind of atomization basal liquid, the atomization basal liquid are made of tetraethylene-glycol solution, 1,3-BDO solution and ethyl cellulose solution.Wherein the volume ratio of tetraethylene-glycol solution, 1,3 butylene glycol solution and ethyl cellulose solution is 90%:9.8%:0.2%.The atomization basal liquid is prepared, the preparation method is as follows:
Step 1: measuring tetraethylene-glycol solution and 1,3-BDO solution by volume, is heated to 45 DEG C, carries out uniform, slow, adequately stirring, obtains mixed liquor；
Step 2: measuring the mixed liquor and ethyl cellulose solution by volume, uniformly, slowly, adequately stir, obtains as clear as crystal, the clear atomization basal liquid of quality.
The applicable field of atomization basal liquid of the present embodiment include but is not limited to electronic cigarette atomized liquid,
Stage and video display special efficacy smoke agent, military smoke agent, medical atomized agent, ultrasonic microgrid Alevaire.
Embodiment 8:
A kind of atomization basal liquid, the atomization basal liquid are made of tetraethylene-glycol solution, 1,3-BDO solution and ethyl cellulose solution.Wherein the volume ratio of tetraethylene-glycol solution, 1,3 butylene glycol solution and ethyl cellulose solution is 99%:0.55%:0.45%.The atomization basal liquid is prepared, the preparation method is as follows:
Step 1: measuring tetraethylene-glycol solution and 1,3-BDO solution by volume, is heated to 50 DEG C, carries out uniform, slow, adequately stirring, obtains mixed liquor；
Step 2: measuring the mixed liquor and ethyl cellulose solution by volume, uniformly, slowly, adequately stir, obtains as clear as crystal, the clear atomization basal liquid of quality.
The applicable field of atomization basal liquid of the present embodiment includes but is not limited to atomized liquid, stage and video display special efficacy smoke agent, military smoke agent, medical atomized agent, the ultrasonic microgrid Alevaire of electronic cigarette.
Embodiment 9:
A kind of atomization basal liquid, the atomization basal liquid by tetraethylene-glycol solution, 1,3-BDO solution and cactus slag body leaching liquor group at.Being atomized the volume ratio of tetraethylene-glycol solution and 1,3-BDO solution and cactus slag body leaching liquor in basal liquid is 80%:10%:10%, prepares the atomization basal liquid, with the following method:
Step 1: it is spare to be extracted into slag body portion to be separated by solid-liquid separation pulper slurrying for cactus washing and sterilizing；
Step 2: tetraethylene-glycol solution and 1,3-BDO solution are measured in proportion, is placed in 50 DEG C of water-baths；
Step 3: the cactus slag body leaching liquor that volume ratio is 10% is weighed, is added into the mixed liquor of tetraethylene-glycol solution and 1,3-BDO solution, is extracted completely；
Step 4: with three layers of negative pressure filtration of fast qualitative filter paper, filtrate is placed in natural subsidence at room temperature is abundant, and obtaining supernatant is the atomization basal liquid.
The applicable field of atomization basal liquid of the present embodiment includes but is not limited to atomized liquid, stage and video display special efficacy smoke agent, military smoke agent, medical atomized agent, the ultrasonic microgrid Alevaire of electronic cigarette.
Embodiment 10:
A kind of atomization basal liquid, the atomization basal liquid by tetraethylene-glycol solution, 1,3-BDO solution and cactus slag body leaching liquor group at.Being atomized the volume ratio of tetraethylene-glycol solution and 1,3-BDO solution and cactus slag body leaching liquor in basal liquid is 85%:10%:5%, prepares the atomization basal liquid, with the following method:
Step 1: it is spare to be extracted into slag body portion to be separated by solid-liquid separation pulper slurrying for cactus washing and sterilizing；
Step 2: tetraethylene-glycol solution and 1,3-BDO solution are measured in proportion, is placed in 60 DEG C of water-baths；
Step 3: the cactus slag body leaching liquor that volume ratio is 5% is weighed, the mixed liquor of tetraethylene-glycol solution and 1,3-BDO solution is added into, is extracted completely；
Step 4: with three layers of negative pressure filtration of fast qualitative filter paper, filtrate is placed in natural subsidence at room temperature is abundant, and obtaining supernatant is the atomization basal liquid.
The applicable field of atomization basal liquid of the present embodiment includes but is not limited to atomized liquid, stage and video display special efficacy smoke agent, military smoke agent, medical atomized agent, the ultrasonic microgrid Alevaire of electronic cigarette.The physicochemical property and wholesomeness index in the various embodiments described above are detected, table one is made.
Table one
Continued one
Embodiments of the present invention above described embodiment only expresses, the description thereof is more specific and detailed, and but it cannot be understood as limitations on the scope of the patent of the present invention.It should be pointed out that for those of ordinary skill in the art, without departing from the inventive concept of the premise, various modifications and improvements can be made, and these are all within the scope of protection of the present invention.Therefore, the scope of protection of the patent of the invention shall be subject to the appended claims.
Claims (22)
- A kind of atomization basal liquid, which is characterized in that the atomization basal liquid includes tetraethylene-glycol solution and polyglycol solution.
- Atomization basal liquid according to claim 1, which is characterized in that the percent by volume of the tetraethylene-glycol solution and polyglycol solution is 1-99%:99-1%.
- A kind of atomization basal liquid according to claim 1, which is characterized in that also include 1,3-BDO solution in the atomization basal liquid.
- Atomization basal liquid according to claim 3, it is characterized in that, tetraethylene-glycol, polyglycol solution are mixed in the atomization basal liquid with arbitrary proportion, and the percent by volume of tetraethylene-glycol, polyethylene glycol mixed liquor and 1,3-BDO solution is 90-95%:5-10%.
- A kind of atomization basal liquid according to claim 1, which is characterized in that the atomization basal liquid includes triethylene-glycol solution, polyglycol solution, Glycerin, mixed triester with caprylic acid capric acid solution and chitosan solution.
- Atomization basal liquid according to claim 5, it is characterized in that, the percentage by volume of triethylene-glycol solution is 70-87% in the atomization basal liquid, the percentage by volume of polyglycol solution is 1-10%, the percentage by volume of Glycerin, mixed triester with caprylic acid capric acid solution is 1-10%, and the percentage by volume of chitosan solution is 1-10%.
- Atomization basal liquid according to claim 6, it is characterized in that, the percentage by volume of triethylene-glycol solution is 85% in the atomization basal liquid, the percentage by volume of polyglycol solution is 5%, the percentage by volume of Glycerin, mixed triester with caprylic acid capric acid solution is 5%, and the percentage by volume of chitosan solution is 5%.
- A kind of atomization basal liquid according to claim 1, which is characterized in that the atomization basal liquid includes tetraethylene-glycol solution, 1,3-BDO solution and ethyl cellulose solution.
- Atomization basal liquid according to claim 8, it is characterized in that, tetraethylene-glycol solution and 1,3-BDO solution are mixed in the atomization basal liquid with arbitrary proportion, and the percent by volume of the mixed liquor and ethyl cellulose solution is 99.55-99.8%:0.45-0.2%.
- A kind of atomization basal liquid according to claim 1, which is characterized in that the atomization basal liquid includes tetraethylene-glycol solution, 1,3-BDO solution and cactus slag body leaching liquor.
- Atomization basal liquid according to claim 10, which is characterized in that the percent by volume of the tetraethylene-glycol solution, 1,3-BDO solution and cactus slag body leaching liquor is 80-90%:5-10%:5-10%.
- The preparation method of atomization basal liquid according to claim 1, which comprises the following steps:Tetraethylene-glycol solution and polyglycol solution are measured by volume, are carried out uniform, slow, adequately stirring, are obtained as clear as crystal, the clear atomization basal liquid of quality.
- The preparation method of atomization basal liquid according to claim 3, which comprises the following steps:Step 1: measuring tetraethylene-glycol solution and polyglycol solution by volume, carries out uniform, slow, adequately stirring, obtains mixed liquor；Step 2: measuring the mixed liquor and 1,3-BDO solution by volume, uniformly, slowly, adequately stir, obtains as clear as crystal, the clear atomization basal liquid of quality.
- The basic liquid and preparation method thereof of atomization according to claim 5, which comprises the following steps:Triethylene-glycol solution, polyglycol solution, Glycerin, mixed triester with caprylic acid capric acid solution and chitosan solution are measured by volume, are carried out uniform, slow, adequately stirring, are obtained as clear as crystal, the clear atomization basal liquid of quality.
- The basic liquid and preparation method thereof of atomization according to claim 8, which comprises the following steps:Step 1: measuring tetraethylene-glycol solution and 1,3-BDO solution by volume, is heated to 45-50 DEG C, carries out uniform, slow, adequately stirring, obtains mixed liquor；Step 2: measuring the mixed liquor and ethyl cellulose solution by volume, uniformly, slowly, adequately stir, obtains as clear as crystal, the clear atomization basal liquid of quality.
- The basic liquid and preparation method thereof of atomization according to claim 10, which comprises the following steps:Step 1: cactus washing and sterilizing is extracted into slag body portion to be separated by solid-liquid separation pulper slurrying；Step 2: tetraethylene-glycol solution and the mixing of 1,3-BDO solution are measured by volume, is placed in 50-65 DEG C of water-bath；Step 3: example weighs the slag body by volume, is added into the mixed solution of tetraethylene-glycol solution and 1,3-BDO solution, and stirring extracts completely；Step 4: filtrate is placed in natural subsidence at room temperature by filtering and removing slag, and obtaining supernatant is the atomization basal liquid.
- A kind of atomization basal liquid described in any one of according to claim 1 or 3 or 5 or 8 or 10, which is characterized in that the atomization basal liquid is used to prepare the atomized liquid of electronic cigarette.
- A kind of atomization basal liquid described in any one of according to claim 1 or 3 or 5 or 8 or 10, which is characterized in that the atomization basal liquid is used to prepare stage smoke agent.
- A kind of atomization basal liquid described in any one of according to claim 1 or 3 or 5 or 8 or 10, which is characterized in that the atomization basal liquid is used to prepare video display special efficacy smoke agent.
- A kind of atomization basal liquid described in any one of according to claim 1 or 3 or 5 or 8 or 10, which is characterized in that the atomization basal liquid is used to prepare military affairs smoke agent.
- A kind of atomization basal liquid described in any one of according to claim 1 or 3 or 5 or 8 or 10, which is characterized in that the atomization basal liquid is used to prepare medical atomized agent.
- A kind of atomization basal liquid described in any one of according to claim 1 or 3 or 5 or 8 or 10, which is characterized in that the atomization basal liquid is used to prepare ultrasonic microgrid Alevaire.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/CN2016/111715 WO2018112885A1 (en) | 2016-12-23 | 2016-12-23 | Basic solution for atomization and preparation method therefor |
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| CN110022697A true CN110022697A (en) | 2019-07-16 |
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| CN201680089516.5A Withdrawn CN110022697A (en) | 2016-12-23 | 2016-12-23 | A kind of atomization basal liquid and preparation method thereof |
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| WO (1) | WO2018112885A1 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114158762A (en) * | 2020-09-10 | 2022-03-11 | 湖南中烟工业有限责任公司 | Smoking agent, smoking material and preparation method thereof |
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| CN111038909B (en) * | 2019-12-06 | 2021-02-02 | 红云红河烟草(集团)有限责任公司 | Raw material preparation process based on heating non-combustion cigarette |
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2016
- 2016-12-23 WO PCT/CN2016/111715 patent/WO2018112885A1/en active Application Filing
- 2016-12-23 CN CN201680089516.5A patent/CN110022697A/en not_active Withdrawn
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101704900A (en) * | 2009-11-10 | 2010-05-12 | 中国烟草总公司郑州烟草研究院 | Extraction method of cactus polysaccharide and application thereof in cigarettes |
| CN102127394A (en) * | 2010-12-16 | 2011-07-20 | 李新建 | Preparation and application of composite aerosol |
| FR3029789A1 (en) * | 2014-12-10 | 2016-06-17 | Greenpharma Sas | USE OF A PAPAVER EXTRACT AND COMPOSITION PERMITTING SAID USE |
| CN105767808A (en) * | 2016-03-31 | 2016-07-20 | 郏县程翔饮品有限公司 | Flower-scented cactus-Chinese waxgourd compound beverage and preparation method thereof |
| CN105747264A (en) * | 2016-04-20 | 2016-07-13 | 贵州中烟工业有限责任公司 | Method for preparing heat-not-burn tobacco bases containing active carbon |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114158762A (en) * | 2020-09-10 | 2022-03-11 | 湖南中烟工业有限责任公司 | Smoking agent, smoking material and preparation method thereof |
| CN114158762B (en) * | 2020-09-10 | 2023-03-03 | 湖南中烟工业有限责任公司 | Smoking agent, smoking material and preparation method thereof |
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| WO2018112885A1 (en) | 2018-06-28 |
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