CN109997910A - A kind of processing method extending myotonin storage period - Google Patents
A kind of processing method extending myotonin storage period Download PDFInfo
- Publication number
- CN109997910A CN109997910A CN201910269286.6A CN201910269286A CN109997910A CN 109997910 A CN109997910 A CN 109997910A CN 201910269286 A CN201910269286 A CN 201910269286A CN 109997910 A CN109997910 A CN 109997910A
- Authority
- CN
- China
- Prior art keywords
- myotonin
- storage period
- processing method
- temperature
- stirring
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000003860 storage Methods 0.000 title claims abstract description 29
- 238000003672 processing method Methods 0.000 title claims abstract description 15
- 230000001954 sterilising effect Effects 0.000 claims abstract description 17
- 238000004659 sterilization and disinfection Methods 0.000 claims abstract description 17
- 238000004140 cleaning Methods 0.000 claims abstract description 15
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 claims abstract description 13
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 13
- 238000004108 freeze drying Methods 0.000 claims abstract description 10
- 150000001875 compounds Chemical class 0.000 claims abstract description 6
- 238000007710 freezing Methods 0.000 claims abstract description 6
- 230000008014 freezing Effects 0.000 claims abstract description 6
- 230000008030 elimination Effects 0.000 claims abstract description 5
- 238000003379 elimination reaction Methods 0.000 claims abstract description 5
- 239000012535 impurity Substances 0.000 claims abstract description 5
- 238000004806 packaging method and process Methods 0.000 claims abstract description 5
- 238000003756 stirring Methods 0.000 claims description 39
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 39
- 238000005868 electrolysis reaction Methods 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 16
- 239000000706 filtrate Substances 0.000 claims description 15
- 238000002791 soaking Methods 0.000 claims description 15
- 238000001914 filtration Methods 0.000 claims description 13
- 230000008569 process Effects 0.000 claims description 13
- 239000002253 acid Substances 0.000 claims description 8
- 239000003381 stabilizer Substances 0.000 claims description 8
- 238000005406 washing Methods 0.000 claims description 8
- CDBYLPFSWZWCQE-UHFFFAOYSA-L sodium carbonate Substances [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 7
- 238000009423 ventilation Methods 0.000 claims description 7
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 6
- 238000013329 compounding Methods 0.000 claims description 5
- 238000004080 punching Methods 0.000 claims description 5
- 239000003518 caustics Substances 0.000 claims description 4
- 238000001816 cooling Methods 0.000 claims description 4
- 230000002045 lasting effect Effects 0.000 claims description 4
- 238000012856 packing Methods 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 4
- 239000000047 product Substances 0.000 claims description 4
- 239000004576 sand Substances 0.000 claims description 4
- 230000007480 spreading Effects 0.000 claims description 4
- 238000003892 spreading Methods 0.000 claims description 4
- 240000007594 Oryza sativa Species 0.000 claims description 3
- 235000007164 Oryza sativa Nutrition 0.000 claims description 3
- 235000009566 rice Nutrition 0.000 claims description 3
- 230000018044 dehydration Effects 0.000 claims description 2
- 238000006297 dehydration reaction Methods 0.000 claims description 2
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims 6
- 229920001353 Dextrin Polymers 0.000 claims 2
- 239000004375 Dextrin Substances 0.000 claims 2
- 235000019425 dextrin Nutrition 0.000 claims 2
- 240000002853 Nelumbo nucifera Species 0.000 claims 1
- 235000006508 Nelumbo nucifera Nutrition 0.000 claims 1
- 235000006510 Nelumbo pentapetala Nutrition 0.000 claims 1
- 230000003647 oxidation Effects 0.000 abstract description 13
- 238000007254 oxidation reaction Methods 0.000 abstract description 13
- WHGYBXFWUBPSRW-UHFFFAOYSA-N Cycloheptaamylose Natural products O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO WHGYBXFWUBPSRW-UHFFFAOYSA-N 0.000 abstract description 11
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract description 11
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical compound OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 abstract description 11
- 239000012476 oxidizable substance Substances 0.000 abstract description 11
- 239000001301 oxygen Substances 0.000 abstract description 11
- 229910052760 oxygen Inorganic materials 0.000 abstract description 11
- 230000009471 action Effects 0.000 abstract description 6
- 230000007774 longterm Effects 0.000 abstract description 6
- 239000003963 antioxidant agent Substances 0.000 abstract description 5
- 238000006243 chemical reaction Methods 0.000 abstract description 5
- 239000003205 fragrance Substances 0.000 abstract description 5
- 230000013011 mating Effects 0.000 abstract description 5
- 230000001681 protective effect Effects 0.000 abstract description 5
- 239000000126 substance Substances 0.000 abstract description 5
- 238000002955 isolation Methods 0.000 abstract description 2
- 238000012545 processing Methods 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 20
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 12
- 239000013049 sediment Substances 0.000 description 7
- 239000004310 lactic acid Substances 0.000 description 6
- 235000014655 lactic acid Nutrition 0.000 description 6
- 238000001035 drying Methods 0.000 description 5
- 210000000582 semen Anatomy 0.000 description 5
- 244000077995 Coix lacryma jobi Species 0.000 description 4
- 235000007354 Coix lacryma jobi Nutrition 0.000 description 4
- 230000002378 acidificating effect Effects 0.000 description 3
- 238000005119 centrifugation Methods 0.000 description 3
- 235000011194 food seasoning agent Nutrition 0.000 description 3
- 238000012546 transfer Methods 0.000 description 3
- 241000209504 Poaceae Species 0.000 description 2
- 238000002425 crystallisation Methods 0.000 description 2
- 230000008025 crystallization Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000004519 grease Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 210000000952 spleen Anatomy 0.000 description 2
- 240000008042 Zea mays Species 0.000 description 1
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000008151 electrolyte solution Substances 0.000 description 1
- 238000005363 electrowinning Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 235000009973 maize Nutrition 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B9/00—Preservation of edible seeds, e.g. cereals
- A23B9/08—Drying; Subsequent reconstitution
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B9/00—Preservation of edible seeds, e.g. cereals
- A23B9/14—Coating with a protective layer; Compositions or apparatus therefor
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B9/00—Preservation of edible seeds, e.g. cereals
- A23B9/16—Preserving with chemicals
- A23B9/18—Preserving with chemicals in the form of gases, e.g. fumigation; Compositions or apparatus therefor
- A23B9/20—Preserving with chemicals in the form of gases, e.g. fumigation; Compositions or apparatus therefor in a controlled atmosphere, e.g. partial vacuum, comprising only CO2, N2, O2 or H2O
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B9/00—Preservation of edible seeds, e.g. cereals
- A23B9/16—Preserving with chemicals
- A23B9/24—Preserving with chemicals in the form of liquids or solids
- A23B9/26—Organic compounds; Microorganisms; Enzymes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B9/00—Preservation of edible seeds, e.g. cereals
- A23B9/16—Preserving with chemicals
- A23B9/24—Preserving with chemicals in the form of liquids or solids
- A23B9/30—Inorganic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/20—Removal of unwanted matter, e.g. deodorisation or detoxification
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Polymers & Plastics (AREA)
- Food Science & Technology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Microbiology (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Storage Of Fruits Or Vegetables (AREA)
Abstract
The present invention relates to foodstuff processing technology fields, and in particular to a kind of processing method for extending myotonin storage period.Including selecting the manufacturing procedures such as classification, electrolytic cleaned, acidolysis impurity elimination, allotment cleaning, freeze-drying, ozone sterilization, packaging；In conjunction with the addition of cycloheptaamylose; package action is generated to myotonin; volatile substances is steady in a long-term in holding myotonin; and under the mating reaction of HA compound antioxidant; layer protecting film is formed on myotonin surface, there is good protective effect to myotonin color, fragrance etc., remaining readily oxidizable substance in myotonin is isolated and is contacted with oxygen; and then isolation oxidation, extend the storage period of myotonin；Finally cooperation freezing and Freeze Drying Technique, remove the moisture in myotonin, remain the main component and value of myotonin, effectively improve the storage shelf-life of myotonin.
Description
Technical field
The present invention relates to foodstuff processing technology fields, and in particular to a kind of processing method for extending myotonin storage period.
Background technique
Semen coicis is called Semen Coicis, the seed of jog's tears, maize, is the kernel of gramineae.It is cool in nature, it is sweet in flavor, light, enter spleen,
Lung, kidney channel have effects that Li Shui, invigorating the spleen, eliminating impediment, clearing away heat and eliminating pus.Semen Coicis is born in the small plots of land by the side of houses, roads, ponds, etc. and mountain valley gully of warm moist,
2000 meters of height above sea level or less relatively universal.
Since the nutritive value of Semen Coicis is very high, it is known as " king of world gramineae plant "；In Europe, it is referred to as " raw
Order the standing grain of health "；In Japan, it is listed in anti-cancer food again recently, therefore is had a sudden rise in social status.Semen Coicis, which has, to be easy to be digested absorption
Feature, no matter for nourishing or for medical treatment, effect all mitigates very much.
Therefore, myotonin appears widely on mankind's dining table, is increasingly becoming people's daily necessities, still, myotonin one
A season could be harvested year, and myotonin itself is rich in grease, grease is easy to oxidize during storage, generates rancid, generation Kazakhstan
Loudspeaker taste seriously affects myotonin quality, apt to deteriorate in long term storage to addle.
Summary of the invention
To overcome myotonin rancid status to addle in storage, researcher of the invention is dedicated to discussion for many years and mentions
The method of high myotonin shelf-life, and pass through numerous experiments and method, successfully develop a set of extension myotonin storage period
Processing method.
The present invention is achieved by the following technical solutions:
A kind of processing method extending myotonin storage period, comprising the following steps:
A, it selects classification: taking myotonin to be processed, remove not full and rotten particle, color sorting classification；
B, electrolytic cleaned: above-mentioned spare myotonin is fully immersed in clear water, and control clear water temperature is 45~50 DEG C, and
Constant temperature, it is lasting to stir, it is inserted into yin-yang two-stage inert electrode, is electrolysed 25~35min；It is adlay that oxygen is generated during electrolysis water
The oxidation of readily oxidizable substance provides sufficient oxygen in rice, and is stirring under electrolysis, effectively facilitates readily oxidizable substance
Oxidation；
Be added after electrolysis and account for the river sand of myotonin gross weight 1/3, in 3200~3500r/min stir cleaning 10 under speed~
12min, is detached from the oxide of part myotonin superficial oxidation, filtering, and clear water is eluriated 2~3 times, is placed at shady and cool ventilation and drains the water
Point；
C, acidolysis impurity elimination: the above-mentioned myotonin to drain away the water is placed in the lactic acid solution that pH value is 6.5~6.6 and is soaked completely
1~1.5h is steeped, control lactic acid solution temperature is 40~50 DEG C, and constant temperature, and every 30min uniform stirring is primary in soaking process, most
It is standing and soaking 30min or more after primary stirring afterwards, then the screen to filtrate of via hole diameter 3mm while hot；Under acidic environment, electrolysis is allowed
When the partial oxide that generates slowly crystallize, and cooperate the later period to rush and wash in a pan filter progress, remove the sediment crystallized in acid solution；It takes
Myotonin is placed in rush in clear water and wash in a pan 2~3 times after filtering, rushes wash in a pan 3~5min every time, every to rush the sieve mistake for washing in a pan a via hole diameter 3mm
Filter 1~2 time；
The myotonin that above-mentioned acid soak terminates is transferred to Na2CO3It is completely soaked 1~1.5h in solution, controls solution temperature
Degree is 45~55 DEG C, and constant temperature, and every 30min uniform stirring is primary in soaking process, and last time is standing and soaking 30min after stirring
More than, then the screen to filtrate of via hole diameter 3mm allows the partial oxide generated when electrolysis slowly to tie under alkaline environment while hot
Crystalline substance, and cooperate the later period to rush and wash in a pan filter progress, the sediment crystallized in lye is removed, and mention for the allotment cleaning of the myotonin in later period
For a weakly alkaline environment；Take filtering after myotonin be placed in clear water rush wash in a pan 2~3 times, every time rush wash in a pan 3~5min, it is every punching wash in a pan one
The screen to filtrate of secondary via hole diameter 3mm 1~2 time；
D, the myotonin after above-mentioned caustic dip allotment cleaning: is transferred to the centrifuge of 1200~1500r/min
In, clear water is filled with to 3~5cm of myotonin upper surface is not crossed, cycloheptaamylose, HA compounding antioxidative stabilizer is added, and constant speed is stirred
30~35min of cleaning is mixed, repeated washing 1~2 time, moisture is filtered out after cleaning, constant speed 5~10min of centrifugal dehydration repeats 3
~5 times；The addition of cycloheptaamylose generates package action to myotonin, and volatile substances is steady in a long-term in holding myotonin,
And under the mating reaction of antioxidant, layer protecting film is formed on myotonin surface, is had very to myotonin color, fragrance etc.
Good protective effect is isolated remaining readily oxidizable substance in myotonin and continues to aoxidize, extends the storage period of myotonin；
E, be freeze-dried: the myotonin after above-mentioned allotment is cleaned is placed in spreading for cooling at shady and cool ventilation and drips completely to surface moisture
Dry, transferring in air flow dryer and being dried to water content is 25~40%, and taking-up is cooled to room temperature, and is transferred to -45~-40 DEG C
3~5h is freezed in freezing chamber, is finally transferred in freeze drier and is dried to moisture content≤10%；
F, ozone sterilization: by the myotonin that above-mentioned freeze-drying terminates be placed in dry environment return warm to room temperature after, transfer
Into closed environment, it is continually fed into the ozone that concentration is 0.1ppm, stops the addition of ozone after stirring sterilization 15s, continues stirring 5
~10min terminates sterilization；
G, it packs: the myotonin after above-mentioned sterilization being sealed packaging by required packing specification, drying is protected from light storage
It deposits to get finished product myotonin.
Preferably, required size of current is 8~15A when the electrolysis.
Preferably, the Na2CO3Solution concentration is 0.06~0.12%.
Preferably, the additional amount of the cycloheptaamylose is 0.25~0.32% of myotonin gross weight in centrifuge.
Preferably, the additional amount of HA compounding antioxidative stabilizer be myotonin gross weight in centrifuge 0.007~
0.010%.
Preferably, the hot-air seasoning temperature is 85~90 DEG C, hot wind humidity is 15~20%, wind-force is 4 grades and wind.
Preferably, the freeze-drying temperature is -30~-35 DEG C, pressure is 1.5~2.6Pa.
The beneficial effects of the present invention are:
Compared with prior art, the present invention provides sufficient oxygen for myotonin in the electrolytic solution by electrowinning process,
Under electric current and stirring action, the readily oxidizable substance in myotonin is allowed quickly to aoxidize, and is washed in a pan under later period acid solution and alkaline environment
It washes, allows the oxide rapid crystallization of myotonin Surface Creation in electrolytic process, the filters such as combined filtering centrifugation allow crystallization
Sediment and myotonin are detached from, and then remove ingredient oxidizable in myotonin, allow myotonin will not be because in later period storage process
The oxidation of readily oxidizable substance and cause myotonin oxidative rancidity；
In conjunction with the addition of cycloheptaamylose, package action is generated to myotonin, keeps volatile substances in myotonin
Steadily in the long term, and under the mating reaction of HA compound antioxidant, layer protecting film is formed on myotonin surface, it is cream-coloured to adlay
Pool, fragrance etc. have good protective effect, and remaining readily oxidizable substance in myotonin is isolated and contacts with oxygen, and then isolation from oxygen
Change, extends the storage period of myotonin；
Finally, cooperation freezing and Freeze Drying Technique, remove the moisture in myotonin, remain the main component of myotonin
And value, effectively improve the storage shelf-life of myotonin.
Specific embodiment
The present invention is further described in detail With reference to embodiment, but technical solution provided by the invention
It not only include the content showed in embodiment.
Embodiment 1
A kind of processing method for extending myotonin storage period is present embodiments provided, detailed process is as follows:
A, it selects classification: taking myotonin to be processed, remove not full and rotten particle, color sorting classification；
B, electrolytic cleaned: above-mentioned spare myotonin is fully immersed in clear water, and control clear water temperature is 50 DEG C, and permanent
Temperature, it is lasting to stir, it is inserted into yin-yang two-stage inert electrode, is electrolysed 25min, size of current 15A；Oxygen is generated during electrolysis water
Gas provides sufficient oxygen for the oxidation of readily oxidizable substance in myotonin, and is stirring under electrolysis, effectively facilitates easily
The oxidation of oxidation material；
The river sand for accounting for myotonin gross weight 1/3 is added after electrolysis, cleans 12min in stirring under speed for 3200r/min, is detached from
The oxide of part myotonin superficial oxidation, filtering, clear water are eluriated 2 times, are placed at shady and cool ventilation and drain away the water；
C, acidolysis impurity elimination: the above-mentioned myotonin to drain away the water being placed in the lactic acid solution that pH value is 6.6 and is completely soaked 1h,
Controlling lactic acid solution temperature is 50 DEG C, and constant temperature, and every 30min uniform stirring is primary in soaking process, and last time is quiet after stirring
It sets and impregnates 30min or more, then the screen to filtrate of via hole diameter 3mm while hot；Under acidic environment, allow electrolysis when the part oxygen that generates
Compound slowly crystallizes, and cooperates the later period to rush and wash in a pan filter progress, removes the sediment crystallized in acid solution；Myotonin after filtering is taken to set
It is 2 times naughty to rush in clear water, rushes wash in a pan 5min every time, every the screen to filtrate 1 time for rushing a naughty via hole diameter 3mm；
The myotonin that above-mentioned acid soak terminates is transferred to Na2CO3It is completely soaked 1.5h in solution, controls solution temperature
It is 45 DEG C, and constant temperature, every 30min uniform stirring is primary in soaking process, and last time is standing and soaking 30min or more after stirring,
Then the screen to filtrate of via hole diameter 3mm allows the partial oxide generated when electrolysis slowly to crystallize under alkaline environment while hot, and
Cooperate the later period to rush and wash in a pan filter progress, removes the sediment crystallized in lye, and provide one for the allotment cleaning of the myotonin in later period
A weakly alkaline environment；Take filtering after myotonin be placed in clear water rush wash in a pan 3 times, every time rush wash in a pan 3min, it is every rush wash in a pan a via hole diameter 3mm
The screen to filtrate 2 times；
D, allotment cleaning: the myotonin after above-mentioned caustic dip is transferred in the centrifuge of 1200r/min, is filled with
To myotonin upper surface 5cm is not crossed cycloheptaamylose is added, HA compounds antioxidative stabilizer, the addition of cycloheptaamylose in clear water
Amount is that the additional amount of 0.25%, the HA compounding antioxidative stabilizer of myotonin gross weight in centrifuge is myotonin gross weight in centrifuge
0.010%；Constant speed stirring and washing 30min after addition repeated washing 2 times, filters out moisture, constant speed centrifugation after cleaning
It is dehydrated 5min, is repeated 5 times；The addition of cycloheptaamylose generates package action to myotonin, keeps volatile substances in myotonin
It is steady in a long-term, and under the mating reaction of antioxidant, form layer protecting film on myotonin surface, to myotonin color,
Fragrance etc. has good protective effect, and remaining readily oxidizable substance in myotonin is isolated and continues to aoxidize, extends the storage of myotonin
Deposit the phase；
E, be freeze-dried: the myotonin after above-mentioned allotment is cleaned is placed in spreading for cooling at shady and cool ventilation and drips completely to surface moisture
Dry, transferring in air flow dryer and being dried to water content is 25%, and hot-air seasoning temperature is 90 DEG C, hot wind humidity is 15%, wind
Power is 4 grades and wind；Heat is taken out after drying and is cooled to room temperature, and is transferred in -40 DEG C of freezing chamber and freezes 5h, is finally transferred to cold
Being dried in lyophilizer to moisture content is 10%, and freeze-drying temperature is -30 DEG C, pressure 2.6Pa；
F, ozone sterilization: by the myotonin that above-mentioned freeze-drying terminates be placed in dry environment return warm to room temperature after, transfer
Into closed environment, it is continually fed into the ozone that concentration is 0.1ppm, stops the addition of ozone after stirring sterilization 15s, continues to stir
10min terminates sterilization；
G, it packs: the myotonin after above-mentioned sterilization being sealed packaging by required packing specification, drying is protected from light storage
It deposits to get finished product myotonin.
Embodiment 2
A kind of processing method for extending myotonin storage period is present embodiments provided, detailed process is as follows:
A, it selects classification: taking myotonin to be processed, remove not full and rotten particle, color sorting classification；
B, electrolytic cleaned: above-mentioned spare myotonin is fully immersed in clear water, and control clear water temperature is 45 DEG C, and permanent
Temperature, it is lasting to stir, it is inserted into yin-yang two-stage inert electrode, is electrolysed 35min, size of current 8A；Oxygen is generated during electrolysis water
Gas provides sufficient oxygen for the oxidation of readily oxidizable substance in myotonin, and is stirring under electrolysis, effectively facilitates easily
The oxidation of oxidation material；
The river sand for accounting for myotonin gross weight 1/3 is added after electrolysis, cleans 10min in stirring under speed for 3500r/min, is detached from
The oxide of part myotonin superficial oxidation, filtering, clear water are eluriated 3 times, are placed at shady and cool ventilation and drain away the water；
C, acidolysis impurity elimination: the above-mentioned myotonin to drain away the water is placed in the lactic acid solution that pH value is 6.5 and is completely soaked
1.5h, control lactic acid solution temperature is 40 DEG C, and constant temperature, and every 30min uniform stirring is primary in soaking process, and last time stirs
After be standing and soaking 30min or more, the then the screen to filtrate of via hole diameter 3mm while hot；Under acidic environment, allow electrolysis when the portion that generates
Sub-oxide slowly crystallizes, and cooperates the later period to rush and wash in a pan filter progress, removes the sediment crystallized in acid solution；Take adlay after filtering
Rice is placed in punching in clear water and washes in a pan 3 times, rushes wash in a pan 3min every time, and the screen to filtrate 2 times of a via hole diameter 3mm are washed in a pan in every punching；
The myotonin that above-mentioned acid soak terminates is transferred to Na2CO31h is completely soaked in solution, control solution temperature is
55 DEG C, and constant temperature, every 30min uniform stirring is primary in soaking process, and last time is standing and soaking 30min or more after stirring, so
The screen to filtrate of via hole diameter 3mm allows the partial oxide generated when electrolysis slowly to crystallize, and match under alkaline environment while hot afterwards
It closes the later period and rushes naughty filter progress, remove the sediment crystallized in lye, and provide one for the allotment cleaning of the myotonin in later period
Weakly alkaline environment；It takes after filtering myotonin to be placed in rush in clear water and wash in a pan 2 times, rushes wash in a pan 5min every time, every punching washes in a pan via hole diameter 3mm's
The screen to filtrate 1 time；
D, allotment cleaning: the myotonin after above-mentioned caustic dip is transferred in the centrifuge of 1500r/min, is filled with
To myotonin upper surface 3cm is not crossed cycloheptaamylose is added, HA compounds antioxidative stabilizer, the addition of cycloheptaamylose in clear water
Amount is that the additional amount of 0.32%, the HA compounding antioxidative stabilizer of myotonin gross weight in centrifuge is myotonin gross weight in centrifuge
0.007%；Constant speed stirring and washing 35min after addition repeated washing 1 time, filters out moisture, constant speed centrifugation after cleaning
It is dehydrated 10min, is repeated 3 times；The addition of cycloheptaamylose generates package action to myotonin, keeps volatile matter in myotonin
Matter it is steady in a long-term, and under the mating reaction of antioxidant, form layer protecting film on myotonin surface, it is cream-coloured to adlay
Pool, fragrance etc. have good protective effect, and remaining readily oxidizable substance in myotonin is isolated and continues to aoxidize, extends myotonin
Storage period；
E, be freeze-dried: the myotonin after above-mentioned allotment is cleaned is placed in spreading for cooling at shady and cool ventilation and drips completely to surface moisture
Dry, transferring in air flow dryer and being dried to water content is 40%, and hot-air seasoning temperature is 85 DEG C, hot wind humidity is 20%, wind
Power is 4 grades and wind；Heat is taken out after drying and is cooled to room temperature, and is transferred in -45 DEG C of freezing chamber and freezes 3h, is finally transferred to cold
Being dried in lyophilizer to moisture content is 8%, and freeze-drying temperature is -35 DEG C, pressure 1.5Pa；
F, ozone sterilization: by the myotonin that above-mentioned freeze-drying terminates be placed in dry environment return warm to room temperature after, transfer
Into closed environment, it is continually fed into the ozone that concentration is 0.1ppm, stops the addition of ozone after stirring sterilization 15s, continues to stir
5min terminates sterilization；
G, it packs: the myotonin after above-mentioned sterilization being sealed packaging by required packing specification, drying is protected from light storage
It deposits to get finished product myotonin.
The above described is only a preferred embodiment of the present invention, being not intended to limit the present invention in any form, appoint
What without departing from technical solution of the present invention content, according to the technical essence of the invention any modification to the above embodiments, etc.
With variation and modification, all of which are still within the scope of the technical scheme of the invention.
Claims (7)
1. a kind of processing method for extending myotonin storage period, which comprises the following steps:
A, it selects classification: taking myotonin to be processed, remove not full and rotten particle, color sorting classification；
B, electrolytic cleaned: above-mentioned spare myotonin is fully immersed in clear water, and control clear water temperature is 45~50 DEG C, and permanent
Temperature, it is lasting to stir, it is inserted into yin-yang two-stage inert electrode, is electrolysed 25~35min；It is added after electrolysis and accounts for myotonin gross weight 1/3
River sand, stir under speed 10~12min of cleaning in 3200~3500r/min, filtering, clear water is eluriated 2~3 times, is placed in shady and cool logical
It drains away the water at wind；
C, acidolysis impurity elimination: the above-mentioned myotonin to drain away the water is placed in the citric acid solution that pH value is 6.5~6.6 and is completely soaked
1~1.5h, control citric acid solution temperature is 40~50 DEG C, and constant temperature, and every 30min uniform stirring is primary in soaking process, most
It is standing and soaking 30min or more after primary stirring afterwards, then the screen to filtrate of via hole diameter 3mm while hot；Myotonin after filtering is taken to be placed in
It is 2~3 times naughty to rush in clear water, rushes wash in a pan 3~5min every time, every the screen to filtrate 1~2 time for rushing a naughty via hole diameter 3mm；
The myotonin that above-mentioned acid soak terminates is transferred to Na2CO31~1.5h is completely soaked in solution, control solution temperature is
45~55 DEG C, and constant temperature, every 30min uniform stirring is primary in soaking process, last time be standing and soaking after stirring 30min with
On, the then the screen to filtrate of via hole diameter 3mm while hot；Take filtering after myotonin be placed in clear water rush wash in a pan 2~3 times, every time punching wash in a pan 3~
5min, every the screen to filtrate 1~2 time for rushing a naughty via hole diameter 3mm；D, allotment cleaning: by the heart of a lotus seed after above-mentioned caustic dip
Benevolence rice is transferred in the centrifuge of 1200~1500r/min, is filled with clear water to 3~5cm of myotonin upper surface is not crossed, β-ring is added
Shape dextrin, HA compound antioxidative stabilizer, and constant speed 30~35min of stirring and washing repeated washing 1~2 time, is filtered out after cleaning
Moisture, constant speed 5~10min of centrifugal dehydration are repeated 3~5 times；
E, be freeze-dried: the myotonin after above-mentioned allotment is cleaned is placed in spreading for cooling at shady and cool ventilation and drains completely to surface moisture,
Transferring in air flow dryer and being dried to water content is 25~40%, and taking-up is cooled to room temperature, and is transferred to -45~-40 DEG C cold
Freeze and freeze 3~5h in room, is finally transferred in freeze drier and dries to moisture content≤10%；
F, ozone sterilization: by the myotonin that above-mentioned freeze-drying terminates be placed in dry environment return warm to room temperature after, be transferred to close
In closed loop border, be continually fed into concentration be 0.1ppm ozone, stirring sterilization 15s after stop ozone addition, continue stirring 5~
10min terminates sterilization；
G, it packs: the myotonin after above-mentioned sterilization being sealed packaging by required packing specification, dries stored protected from light, i.e.,
Obtain finished product myotonin.
2. a kind of processing method for extending myotonin storage period according to claim 1, which is characterized in that when the electrolysis
Required size of current is 8~15A.
3. a kind of processing method for extending myotonin storage period according to claim 1, which is characterized in that the Na2CO3
Solution concentration is 0.06~0.12%.
4. a kind of processing method for extending myotonin storage period according to claim 1, which is characterized in that the β-ring-type
The additional amount of dextrin is 0.25~0.32% of myotonin gross weight in centrifuge.
5. a kind of processing method for extending myotonin storage period according to claim 1, which is characterized in that the HA compounding
The additional amount of antioxidative stabilizer is 0.007~0.010% of myotonin gross weight in centrifuge.
6. a kind of processing method for extending myotonin storage period according to claim 1, which is characterized in that the hot wind dries
Dry temperature is 85~90 DEG C, hot wind humidity is 15~20%, wind-force is 4 grades and wind.
7. a kind of processing method for extending myotonin storage period according to claim 1, which is characterized in that the freezing is dry
Dry temperature is -30~-35 DEG C, pressure is 1.5~2.6Pa.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910269286.6A CN109997910A (en) | 2019-04-04 | 2019-04-04 | A kind of processing method extending myotonin storage period |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910269286.6A CN109997910A (en) | 2019-04-04 | 2019-04-04 | A kind of processing method extending myotonin storage period |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109997910A true CN109997910A (en) | 2019-07-12 |
Family
ID=67169907
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910269286.6A Withdrawn CN109997910A (en) | 2019-04-04 | 2019-04-04 | A kind of processing method extending myotonin storage period |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109997910A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110447808A (en) * | 2019-09-04 | 2019-11-15 | 贵州省普安县普白珍稀资源开发有限公司 | A kind of refrigerated storage method of Rhizoma Gastrodiae |
-
2019
- 2019-04-04 CN CN201910269286.6A patent/CN109997910A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110447808A (en) * | 2019-09-04 | 2019-11-15 | 贵州省普安县普白珍稀资源开发有限公司 | A kind of refrigerated storage method of Rhizoma Gastrodiae |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101623024B (en) | Processing method for drying, dehydrating and conditioning radish leaves by hot air | |
| CN105166099A (en) | Processing method for green tea | |
| CN107811237A (en) | A kind of Rosa roxburghii VC microcapsules and preparation method thereof | |
| CN105124011A (en) | Summer and autumn tea bitter and astringent taste lowering green tea processing technology | |
| CN107668587A (en) | A kind of sea-tangle filament processing process | |
| CN105211780A (en) | The processing method of dried carrot | |
| CN114259020A (en) | Fresh dried bean curd stick and processing method thereof | |
| CN107183148A (en) | A kind of preparation method of dried persimmon | |
| CN108323591A (en) | A kind of processing technology of green tea | |
| CN109997910A (en) | A kind of processing method extending myotonin storage period | |
| CN105558210A (en) | Sweet-scented osmanthus black tea making technology | |
| CN103549035A (en) | Processing technology for zanthoxylum oil | |
| CN107906942A (en) | A kind of method of solar energy assisted cryogenic absorption type dehydration and drying preserved apricot | |
| KR101375427B1 (en) | Enzymatic method for preparing gold salt | |
| CN105685287A (en) | Making process for black tea with jasmine flower fragrance | |
| CN105166100A (en) | Processing method for Longjing tea | |
| CN108967568A (en) | A kind of processing technology of white tea | |
| CN107484978A (en) | A kind of production method of the secondary pickling salted duck eggs with health-care efficacy | |
| KR101212718B1 (en) | Preparing method for soybean sauce using Salicornia herbacea powder by high pressure water extracting | |
| KR101986226B1 (en) | Manufacturing method for functional seasoned laver and functional seasoned laver manufactured by the same | |
| CN107232352A (en) | A kind of preparation method of rose tea | |
| CN104770465A (en) | High-efficiency drying method for shepherd's purse | |
| JPH10136946A (en) | Production of oyster meat essence | |
| CN104974547A (en) | Method for extraction of cocoa bean pigment | |
| CN107821648A (en) | A kind of preparation method of selenium-rich Zanthoxylum essential oil |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20190712 |