CN109970295A - A kind of oil sludge processing equipment and technique - Google Patents

A kind of oil sludge processing equipment and technique Download PDF

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Publication number
CN109970295A
CN109970295A CN201910311966.XA CN201910311966A CN109970295A CN 109970295 A CN109970295 A CN 109970295A CN 201910311966 A CN201910311966 A CN 201910311966A CN 109970295 A CN109970295 A CN 109970295A
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oil
water
sludge
pipeline
outlet
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CN109970295B (en
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朱永杰
谢勤峰
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Jiangsu Lian Chang Environmental Protection Equipment Co Ltd
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Jiangsu Lian Chang Environmental Protection Equipment Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F11/00Treatment of sludge; Devices therefor
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F11/00Treatment of sludge; Devices therefor
    • C02F11/12Treatment of sludge; Devices therefor by de-watering, drying or thickening
    • C02F11/121Treatment of sludge; Devices therefor by de-watering, drying or thickening by mechanical de-watering
    • C02F11/127Treatment of sludge; Devices therefor by de-watering, drying or thickening by mechanical de-watering by centrifugation
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F11/00Treatment of sludge; Devices therefor
    • C02F11/12Treatment of sludge; Devices therefor by de-watering, drying or thickening
    • C02F11/14Treatment of sludge; Devices therefor by de-watering, drying or thickening with addition of chemical agents
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Hydrology & Water Resources (AREA)
  • Mechanical Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Physical Water Treatments (AREA)
  • Treatment Of Sludge (AREA)

Abstract

The present invention relates to a kind of oil sludge processing equipment and techniques.The equipment includes oil sludge storage tank, ultrasonic wave affector, supercentrifuge and low speed centrifuge, oil sludge storage tank acts on one import of device assembly with ultrasonic wave by pipeline and connect, the outlet of ultrasonic wave effect device assembly one is connect with supercentrifuge import, there are two outlets for supercentrifuge setting, supercentrifuge second outlet is connect by pipeline with low speed centrifuge, and there are two outlets for setting on low speed centrifuge;Technique using the equipment includes adding water and stirring dilution, the demulsification of ultrasonic wave affector, oil separation, mud-water separation.This kind of oil sludge processing technique is physical treatment, changes existing process for treating oil-containing sludge, can first recycle oil reservoir, then be separated by solid-liquid separation to sludge water, realizes water, oil, mud separation sufficiently, the oily rate of recovery is high;Flocculant is added less, reduces the generation of solid waste;During the separation process, it reduces and repeats a possibility that emulsifying, avoid repetitive operation;Cycling utilization of wastewater is recycled, energy-saving ring Poly is useless.

Description

A kind of oil sludge processing equipment and technique
Technical field
The invention belongs to contained Mud Treatment Technology fields, and in particular to a kind of oil sludge processing equipment and technique.
Background technique
Oil sludge is the major pollutants generated in oil exploitation, transport and storage and transport process, wherein the oil-containing in oil plant Sludge mainly from " three mud ", including generated when sewage from oil refinery processing oil separator bed mud, air-flotation process when the flotation that generates Residual active sludge in pond dross and aerobic treatment.The characteristics of oil plant oily sludge is that water content is big, and component is multiple It is miscellaneous, impurity is more, processing difficulty is big.Usually used by oil-in-water, Water-In-Oil and solid suspension and in process of production The stable emulsion liquid system of various inorganic agent compositions, separating difficulty are very high.
The processing method of domestic and international oil sludge mainly has solidification method, incineration method, hot water washing, solvent extraction, ultrasound Wave method, pyrolysis method, bioanalysis etc..
Wherein hot water washing is the processing method for being mainly used in ground sludge at present, mainly passes through thermokalite water or adds Active dose of hot water repeatedly washs greasy filth.Its advantage is that easy to operate, applicability is wide, and cost is relatively low, the disadvantage is that Secondary pollution is be easy to cause in treatment process, and separation degree is not especially high.
Incineration method is a kind of processing method that technology is more mature, and greasy filth burns in special incinerator, thoroughly sloughs it In oil-containing organic matter.Its advantage is that easy to operate, processing speed is fast, can completely remove harmful substance in greasy filth, and burn Generated thermal energy can recycle.The disadvantage is that the crude resources in greasy filth can be lost, and the energy consumption needed is larger, burning is released Gas be likely to result in secondary pollution.
Solvent extraction is to be extracted the oil in greasy filth using organic solvent, realizes the three phase separation of oil, water, mud, And recycling for extractant is realized by distillation technique.The advantages of solvent extraction is that greasy filth separation is thorough, and de-oiling rate is high, former Oily resource can be utilized effectively, the disadvantage is that required Solvent quantity is larger, higher cost.
Solidification method is to utilize either physically or chemically to mix greasy filth with inert base, thus by the harmful substance in greasy filth Coalescence is in solids.Its advantage is that can block by the poisonous and harmful substance in crude oil, avoid causing damages to environment, handle It is at low cost, the disadvantage is that the crude resources in greasy filth can be lost, and need to add a large amount of substrates.
Pyrolysis method is divided into high-temperature decomposition and low-temperature treatment method, and greasy filth is heated to hydrocarbon cracking in the environment of anaerobic Temperature, and by condensation, recycle hydrocarbons.Pyrolysis method processing speed is fast, and separating effect is obvious, the recyclable benefit of some hydrocarbon With reducing resource waste, the disadvantage is that higher cost, operate more complex.
The effects of supercritical ultrasonics technology is the mechanical oscillation using ultrasonic wave reduces the viscosity of greasy filth Crude Oil, makees its adherency With being remarkably decreased, to make oil, mud and water separation.Useful supercritical ultrasonics technology handles the report of oil sludge both at home and abroad at present, but uses Supercritical ultrasonics technology handle oil plant oily sludge, there is also some difficulties, especially oil plant oily sludge be usually by oil-in-water, The stable emulsion liquid system of Water-In-Oil and solid suspension and the various inorganic agents used in process of production composition, separation are difficult It spends very high.
Chinese patent notification number: CN102757162B discloses a kind of Oil Containing Sludge Treatment and equipment, belongs to ultrasound Wave method, referring to Figure 5, the equipment include disposal of oily sludge system and for being controlled disposal of oily sludge system Automatic control system, and the power supply unit 5-34 to power for disposal of oily sludge system and automatic control system, the oil-containing Sludge treating system includes blender 5-12 for being diluted with water to oily sludge, for being demulsified to oily sludge The ultrasonic emulsion breaking equipment 5-14 of processing, for carrying out the centrifuge 5-16 of solid-liquid separation treatment to oily sludge and for oil-containing Sewage carries out the ultrafiltration system 5-20 of water-oil separating processing, and the greasy filth for storing oily sludge stores pond 5-9, for depositing Put the mud sump 5-17 of mud point, the centrifugation reservoir 5-18 for storing oily wastewater, the concentration basin 5-21 for storing oil and Funnel 5-11 is provided on reservoir 5-22, the blender 5-12 for storing moisture;The greasy filth storage pond 5-9 passes through First oily sludge transfer pipeline and centrifugal pump are connect with oil tank, and the greasy filth storage pond 5-9 is conveyed by the second oily sludge Pipeline and screw pump 5-10 are connect with funnel 5-11, and the blender 5-12 is straight by third oily sludge transfer pipeline and first Column pump 5-13 connect with ultrasonic emulsion breaking equipment 5-14, the ultrasonic emulsion breaking equipment 5-14 pass through the 4th oily sludge transfer pipeline with Second inline pump 5-15 is connect with centrifuge 5-16, and the mud sub-export of the centrifuge 5-16 divides transfer pipeline and mud sump by mud The oily wastewater outlet of 5-17 connection, the centrifuge 5-16 passes through the first oily wastewater transfer pipeline and centrifugation reservoir 5-18 Connection, the centrifugation reservoir 5-18 pass through the second oily wastewater transfer pipeline and the first high-pressure pump 5-19 and ultrafiltration system 5-20 The oil outlet of connection, the ultrafiltration system 5-20 is connect by oil transfer pipeline with concentration basin 5-21, the ultrafiltration system The moisture outlet of 5-20 is connect by the first moisture conveying pipeline with the water inlet of reservoir 5-22, and the of the reservoir 5-22 One water outlet is connect by the second moisture conveying pipeline and the second high-pressure pump with funnel 5-11, and the second of the reservoir 5-22 goes out The mouth of a river is connect by third moisture conveying pipeline and backwashing pump with ultrafiltration system 5-20;The blender 5-12, ultrasonic emulsion breaking are set Standby 5-14, centrifuge 5-16, ultrafiltration system 5-20, centrifugal pump, screw pump 5-10, the first inline pump 5-13, the second inline pump 5- 15, the first high-pressure pump 5-19, the second high-pressure pump and backwashing pump are connect with the automatic control system.
When handling oily sludge using the device, the oily sludge in usual oil tank is stored in greasy filth storage pond through centrifugal pump In, enter in the funnel above blender through screw pump, orally all enters blender, blender is carried out to oily sludge plus water is dilute It releases;Oily sludge after agitation and dilution enters ultrasonic emulsion breaking equipment through the first inline pump, ultrasonic emulsion breaking equipment to oily sludge into Row demulsification processing;Oily sludge after demulsification enters centrifuge through the second inline pump, and centrifuge carries out solid-liquid point to oily sludge From processing, mud point and oily wastewater are obtained, mud point is discharged into mud sump, and oily wastewater enters centrifugation reservoir and waits water-oil separating;From Oily wastewater in heart reservoir enters ultrafiltration system through the first high-pressure pump, and ultrafiltration system carries out at water-oil separating oily wastewater Reason, obtains oil and moisture, and oil is discharged into concentration basin, moisture is discharged into reservoir, the moisture in reservoir one The second high-pressure pump of lease making enters in funnel, enters blender through funnel and is diluted for blender to oily sludge, another portion Lease making backwashing pump enters ultrafiltration system and carries out cleaning operation.
It in the prior art, is tiny dross particles due to there is part in oily sludge solid, granularity is small, density It is small, and add water and stir part dross particles in dilution and suspend in water, when being separated by solid-liquid separation using centrifuge, it is easy to make Ingredient contains a large amount of solids --- dross particles from insufficient in the oily wastewater that solid-liquid separation treatment obtains;For this purpose, When being separated by solid-liquid separation to the oily sludge being demulsified, needs to be added a large amount of inorganic adsorbent in oily sludge and part is wadded a quilt with cotton Additives, the solid additive amounts being generally added such as solidifying agent reach 25% or so of oily sludge weight, to increase granularity and close Degree, so that dross particles be made to reunite and precipitate.This kind of processing method is due to needing to be added a large amount of solid additive, after separation Solid waste quantity increases considerably, and the presence due to there is " oil ", and inorganic adsorbent and flocculant is added, so that be demulsified Oily sludge is emulsified again, and solid-liquid separation effect is bad;Meanwhile part oil can be also adsorbed onto solid waste by inorganic adsorbent, Reduce the rate of recovery of oil.
Summary of the invention
The technical problem to be solved by the present invention is in view of the foregoing drawbacks, the present invention provide a kind of oil sludge processing equipment and Technique changes existing contained Mud Treatment Technology, and sufficiently, the oily rate of recovery is high for water, oil, mud separation;Few, reduction is added in flocculant The generation of solid waste;During the separation process, it reduces and repeats a possibility that emulsifying, avoid repetitive operation;Recycle cycling utilization of wastewater, section It can environmental protection and waste utilization.
It is as follows that the technical scheme adopted by the invention to solve the technical problem:
A kind of oil sludge processing equipment, has oil sludge storage tank, and ultrasonic wave acts on device assembly one, supercentrifuge and low speed Centrifuge, the oil sludge storage tank pass through the first separate pipeline and the feeding engine one being arranged in the first separate pipeline and ultrasound Wave acts on one import of device assembly connection;The outlet of the ultrasonic wave effect device assembly one is connect with supercentrifuge import;It is described Supercentrifuge is provided with supercentrifuge first outlet and supercentrifuge second outlet;Supercentrifuge second outlet passes through Second separate pipeline and the feeding engine two being arranged in the second separate pipeline are connect with low speed centrifuge;On the low speed centrifuge It is provided with low speed centrifuge first outlet and low speed centrifuge second outlet.
It further, further include oil sludge pretreatment unit and primary centrifuge machine;The oil sludge pretreatment unit packet It includes ultrasonic wave effect device assembly two, first and pre-processes pipeline and the second pretreatment pipeline;The oil sludge outlet passes through the The import of one pretreatment pipeline connection ultrasonic wave effect device assembly two, and ultrasonic wave affector is connected by the second pretreatment pipeline The outlet of component two is connect with oil sludge reservoir inlet, is formed oil sludge and is pre-processed circulator;And
Oil sludge storage tank connects the one of third separate pipeline by the threeway that the feeding engine one in the first separate pipeline exports End, the other end of third separate pipeline are connect with the import of primary centrifuge machine;The primary centrifuge machine is provided with primary centrifuge machine First outlet and primary centrifuge machine second outlet;The import of the primary centrifuge machine second outlet and ultrasonic wave effect device assembly one Connection;
Sludge water tank and sludge water tank are provided between the supercentrifuge second outlet and low speed centrifuge import It is arranged between supercentrifuge second outlet and feeding engine two;
Flocculant case and the first pipe are additionally provided between the supercentrifuge second outlet and low speed centrifuge import Road static mixer;The first pipe static mixer is arranged between feeding engine two and low speed centrifuge import, the first pipe The outlet end of road static mixer is connect with low speed centrifuge import, the main input end and feeding engine of first pipe static mixer Two outlet end connection;The flocculant case is connected to first pipe static mixer by pipeline and flocculant delivery pump Secondary input end;The feeding engine two of the connection sludge water tank is also connect by doing over again pipeline with oil sludge storage tank.
Further, the supercentrifuge first outlet is connect by pipeline with drain oil recovery equipment;Low speed centrifuge Second outlet is connected with vibrating screen and waste water tank in turn by pipeline;Waste water row is provided in the outlet conduit of the waste water tank Water outlet pump, waste water discharge water pump are connected with two outlets by three, and first outlet is directly connected to sewage conduct, and second outlet passes through Water return pipeline is connect with boiler;The vapor pipeline collet heating that the boiler passes through setting;And
The hot water tank outlet by cleaning pipeline respectively with oil sludge storage tank, primary centrifuge machine, supercentrifuge It is connected with low speed centrifuge;
The water return pipeline can directly be connect with boiler;It can also be total with a part of water return pipeline and pipeline of doing over again With.
Further, it is also wrapped on the first pretreatment pipeline that the feeding engine one is connect with ultrasonic wave effect device assembly two Include second pipe static mixer;It further include third pipe in the third separate pipeline that the feeding engine one is connect with primary centrifuge machine Road static mixer;The 4th pipeline is additionally provided on the pipeline that the ultrasonic wave effect device assembly one is connect with supercentrifuge Static mixer.
Further, the sump oil storage tank is at least 1;Ultrasonic wave effect device assembly one is acted on by 1 to 6 ultrasonic wave Device unit is composed in series;The ultrasonic wave effect device assembly two of the oil sludge pretreatment unit is by 1 to 6 ultrasonic wave affector It is composed in series.
A kind of sump oil sludge treatment technology, comprising the following steps:
Step a, add water and stir dilution: oil sludge is stored in oil sludge storage tank, and water, sump oil are added into oil sludge storage tank The stirring paddle stirring being arranged in mud storage tank, water are uniformly mixed with oil sludge;
Step b, the demulsification of ultrasonic wave affector: uniformly mixed oil sludge liquid is pumped into ultrasonic wave effect by feeding engine one In device assembly one, the sump oil cement of emulsification is demulsified in the case where ultrasonic wave effect device assembly one acts on, oil, sludge water layering;
Step c, oil separation: oil and sludge water after demulsification are connected to supercentrifuge, supercentrifuge fortune by pipeline Under turning, oil reservoir and sludge water layer are layered, and oil reservoir is separated from supercentrifuge first outlet;
Step d, mud-water separation: remove oil reservoir sludge water layer be pumped into from supercentrifuge second outlet through feeding engine two it is low In fast centrifuge, low speed centrifuge operating, mud layer and water layer separation, mud layer are separated from low speed centrifuge first outlet, water Layer is separated from low speed centrifuge second outlet.
Further, the step a also has following steps after adding water and stirring dilution:
Step a1, oil sludge pretreatment: uniformly mixed oil sludge system enters ultrasonic wave effect device assembly two and is demulsified, just The sump oil muddy water of grade demulsification is recycled in oil sludge storage tank from pretreatment pipe-line system;
The separation of solid-liquid primary: step a2 is pumped into just by the pretreated sump oil muddy water of oil sludge system by feeding engine one In grade centrifuge, bulky grain sludge settles in centrifugal process, is separated by solid-liquid separation, and bulky grain sludge is from primary centrifuge machine first outlet Discharge, the oil sludge are pumped into ultrasonic wave effect device assembly one by feeding engine and are handled.
Further, if also remaining the oil reservoir more than setting value in water after the step c oil separating step, also having It has the following steps:
Step c1, sludge water are done over again: after the supercentrifuge separation oil-yielding stratum, sludge water enters sludge water tank, if Oil content in sludge water is more than setting value, then sludge water is pumped into oil sludge storage tank from sludge water tank by doing over again pipeline.
Dross flocculating setting: after the separation of step c oil, flocculant is added in the sludge water isolated, dross is being wadded a quilt with cotton in step c2 The solidifying lower sedimentation of reuniting of agent effect.
Further, after the step d mud-water separation, water layer from low speed centrifuge second outlet separate after can be with It is recycled, specific steps are as follows:
Step e: cycling utilization of wastewater, water layer enter waste water tank after the separation of low speed centrifuge second outlet, and waste water tank is logical It crosses water return pipeline system to be connected in boiler, the boiler is heated by vapor, and the hot water after heating is by clear Pipe-line system is washed to respectively enter in oil sludge storage tank, primary centrifuge machine, supercentrifuge and low speed centrifuge.
Further, temperature is set as 60 DEG C to 90 DEG C in the oil sludge storage tank.
The beneficial effects of the present invention are:
1, the sump oil sludge treatment technology that the present invention uses, change is first separated by solid-liquid separation in the prior art, then carries out grease Isolated processing mode, due to the gap of granularity and density, passes through centrifugation after the application is demulsified under the effect of ultrasonic wave affector Effect first separates oil from solid water (mixture of solid and water), then carries out solid water separation, and by water, from mud, (solid is useless Object) in separate.
2, by increasing oil sludge pretreatment system, oil sludge is first subjected to demulsification circular treatment, is conducive to oil sludge Abundant demulsification, be also beneficial to the subsequent continuous separating treatment to oil sludge.
3, increase primary centrifuge machine, convenient for the bulky grain solid object in oil sludge is first removed, be conducive to mitigate high speed from Damage of the bulky grain solid to supercentrifuge when scheming first separates oil from oil water mixture is also beneficial to avoid big Blocking of the granular solids to pipeline.
4, it deposits in oil sludge storage tank by pretreated oil sludge, convey in the duct, and in primary centrifuge machine In while isolate bulky grain solid object, emulsified again there are also a small amount of solid small particles object.For this purpose, in supercentrifuge Ultrasonic wave is set before import and acts on device assembly one, is pumped into height again after secondary demulsification being carried out from the oil sludge that primary centrifuge machine is discharged Fast centrifuge is conducive to supercentrifuge and separates oil from oil sludge, and this separation is more adequately oily recycling Rate is high.
5, it is provided with vibrating screen between low speed centrifuge and waste water tank, remains in when can filter low speed centrifuge separation A small amount of dross in water layer, and can rupture when flocculant is mixed with muddy water layer and a large amount of froth bubbles occur, avoid bubble from depositing There is situations such as overflow, improving the quality of recycling waste water, is reducing particle content in water.
6, by oil after separating in oil sludge, a small amount of flocculant is added in solid water mixture, it is easy to will be tiny Dross particles reunite, increase granularity, so that readily solid water mixture be separated by low speed centrifuge;And due to The road " oil " Yi Qian is separated, even if a small amount of flocculant is added in solid water mixture, solid water will not be caused to mix The emulsification again of object.
7, second pipe static state is increased separately in ultrasonic wave effect device assembly two, primary centrifuge machine, supercentrifuge front end Mixer, the 4th pipeline static mixer, third pipeline static mixer, so that oil sludge is transported according to itself during transportation The power sent mixes more evenly in pipeline static mixer, be conducive to demulsification, separation more sufficiently, improve oil removing, desilt Processing quality and treatment effeciency.
8, the waste water circulatory system is increased, i.e., increases water return pipeline in waste water tank, and export in boiler and increase cleaning Pipeline, the water in system can recycle, and are conducive to protect environment, reduce cost;The vibrating screen being arranged before waste water tank simultaneously, Remaining dross content in waste water is further decreased, corrosion of the waste water to pipeline is reduced, extends making for the oil sludge processing equipment Use the service life.
9, by the way that at least one oil sludge storage tank is arranged, one oil sludge storage tank of every increase is equivalent to and increases a set of sump oil Mud processing equipment, it is cover while using more, improve the treatment effeciency of oil sludge.
Detailed description of the invention
Through the following detailed description taken in conjunction with the accompanying drawings, present invention objects, features and advantages above-mentioned and other will become Obviously.
Fig. 1 is 1 structural schematic diagram of the invention patent embodiment;
Fig. 2 is 2 structural schematic diagram of the invention patent embodiment;
Fig. 3 is 3 structural schematic diagram of the invention patent embodiment;
Fig. 4 is 4 structural schematic diagram of the invention patent embodiment;
Fig. 5 is the structural schematic diagram in the application background technique;
Wherein: 1 is oil sludge storage tank, and 11 be outlet, and 12 be storage tank import, and 13 be the first separate pipeline, and 14 be to send Material pump one, 15 be the first pretreatment pipeline, and 16 be the second pretreatment pipeline, and 17 be third separate pipeline, and 18 be triple valve, and 2 are Ultrasonic wave acts on device assembly one, and 3 be supercentrifuge, and 30 be recycling fuel tank, and 31 be supercentrifuge first outlet, and 32 be high speed Centrifuge second outlet, 33 be supercentrifuge import, and 34 be the second separate pipeline, and 35 be feeding engine two, and 36 be sludge water tank, 37 be flocculant case, and 38 be first pipe static mixer, and 381 be outlet end, and 382 be main input end, and 383 be secondary input end, 39 be pipeline of doing over again, and 4 be low speed centrifuge, and 41 be low speed centrifuge import, and 42 be low speed centrifuge first outlet, and 43 be low speed Centrifuge second outlet, 44 are waste water tank, and 45 be vibrating screen, and 46 be sludge box two, and 47 be water return pipeline, and 48 are discharged water for waste water Pump, 481 be first outlet, and 482 be second outlet, and 5 act on device assembly two for ultrasonic wave, and 6 be primary centrifuge machine, 61 for it is primary from Scheming first outlet, 62 be primary centrifuge machine second outlet, and 63 be sludge box one, and 7 be oil sludge storage tank two, and 8 be boiler, 81 It is cleaning pipeline for vapor pipeline, 82,91 be second pipe static mixer, and 92 be third pipeline static mixer, and 93 are 4th pipeline static mixer, A are oil sludge, and B is water, and C is water vapour.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, below in conjunction with attached drawing and example, to this Invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, not For limiting the present invention.
Embodiment 1:
Shown in referring to Fig.1, a kind of oil sludge processing equipment has oil sludge storage tank 1, and ultrasonic wave acts on device assembly 1, height Fast centrifuge 3 and low speed centrifuge 4, the oil sludge storage tank 1 is by the first separate pipeline 13 and is arranged in the first separating pipe Feeding engine 1 on road 13 is connect with ultrasonic wave effect one 2 import of device assembly;The outlet of the ultrasonic wave effect device assembly 1 It is connect with supercentrifuge import 33;The supercentrifuge 3 is provided with supercentrifuge first outlet 31 and supercentrifuge Second outlet 32;The supercentrifuge first outlet 31 is connect by pipeline with drain oil recovery equipment 30;Supercentrifuge Two outlets 32 pass through the second separate pipeline 34 and the feeding engine 2 35 being arranged in the second separate pipeline and low speed centrifuge import 41 connections;Low speed centrifuge first outlet 42 and low speed centrifuge second outlet 43 are provided on the low speed centrifuge 4;Low speed Centrifuge second outlet 43 is connected with vibrating screen 45 and waste water tank 44 in turn by pipeline.
Technique using oil sludge equipment processing oil sludge is as follows:
Step a adds water and stirs dilution: the oil sludge enters oil sludge by pipeline from oil sludge storage tank import 12 In storage tank 1, into oil sludge storage tank, 1 is pumped into the stirring paddle stirring being arranged after water by oil sludge storage tank 1, and is heated to 85 DEG C, oil sludge is uniformly mixed;
Step b, the demulsification of ultrasonic wave affector: uniformly mixed oil sludge liquid is from outlet 11, by setting the Feeding engine 1 in one separate pipeline 13 is pumped into ultrasonic wave effect device assembly 1, and the sump oil cement of emulsification is made in ultrasonic wave Lower demulsification, oil, sludge water layering are acted on device assembly 1;
Step c, oil separation: oil and sludge water after demulsification are connected to supercentrifuge 3, supercentrifuge fortune by pipeline Under turning, oil reservoir and sludge water layer are layered, and oil reservoir is separated from supercentrifuge first outlet 31;
Step d, mud-water separation: the sludge water layer for removing oil reservoir is pumped from supercentrifuge second outlet 32 through feeding engine 2 35 Enter in low speed centrifuge 4, low speed centrifuge 4 operates, and mud layer and water layer separation, mud layer are separated from low speed centrifuge first outlet 42 Out, water layer is separated from low speed centrifuge second outlet 43.
Embodiment 2:
Referring to shown in Fig. 2, a kind of oil sludge processing equipment has oil sludge storage tank 1, and ultrasonic wave acts on device assembly 1, height Fast centrifuge 3 and low speed centrifuge 4, the ultrasonic wave effect device assembly 1 are composed in series by three ultrasonic wave affector units; It further include oil sludge pretreatment unit and primary centrifuge machine 6;The oil sludge pretreatment unit includes ultrasonic wave affector group Part 25, first pre-processes pipeline 15 and the second pretreatment pipeline 16;The ultrasonic wave affector of the oil sludge pretreatment unit Component 25 is composed in series by three ultrasonic wave affector;The oil sludge outlet 11 is connected by the first pretreatment pipeline 15 The import of ultrasonic wave effect device assembly 25 is connect, and ultrasonic wave is connected by the second pretreatment pipeline 16 and acts on going out for device assembly 25 Mouth is connect with oil sludge reservoir inlet 12, is formed oil sludge and is pre-processed circulator;And oil sludge storage tank 1 passes through first point From on pipeline 13 feeding engine 1 export threeway connection third separate pipeline 17 one end, third separate pipeline 17 it is another End is connect with the import of primary centrifuge machine 6;The primary centrifuge machine 6 is provided with primary centrifuge machine first outlet 61 and primary centrifuge Machine second outlet 62;The primary centrifuge machine second outlet 62 is connect with the import of ultrasonic wave effect device assembly 1;The height It is provided with sludge water tank 36 between fast centrifuge second outlet 32 and low speed centrifuge import 41 and sludge water tank 36 is arranged in height Between fast centrifuge second outlet 32 and feeding engine 2 35;The supercentrifuge second outlet 32 and low speed centrifuge import Flocculant case 37 and first pipe static mixer 38 are additionally provided between 41;The setting of first pipe static mixer 38 exists Between feeding engine 2 35 and low speed centrifuge import 41, the outlet end 381 of first pipe static mixer 38 and low speed centrifuge Import 41 connects, and the main input end 382 of first pipe static mixer 38 is connect with the outlet end of feeding engine 2 35;The wadding Solidifying agent case 37 is connected to the secondary input end 383 of first pipe static mixer 38 by pipeline and flocculant delivery pump;Described The feeding engine 2 35 of connection sludge water tank 36 is also connect by doing over again pipeline 39 with oil sludge storage tank 1;The waste water tank 44 Waste water discharge water pump 48 is provided in outlet conduit, waste water discharge water pump 48 is connected with two outlets by three, and first outlet 481 is straight It is connected to sewage conduct in succession, second outlet 482 is connect by water return pipeline 47 with boiler 8.
The water return pipeline 47 can directly be connect with boiler 8;It can also be with a part of water return pipeline 47 and pipe of doing over again Road 39 shares.
81 collet of the vapor pipeline heating that the boiler 8 passes through setting;And 8 water outlet of boiler is logical Over cleaning pipeline 82 is connect with oil sludge storage tank 1, primary centrifuge machine 6, supercentrifuge 3 and low speed centrifuge 4 respectively.
Technique using oil sludge equipment processing oil sludge is as follows:
Step a adds water and stirs dilution: the oil sludge enters oil sludge by pipeline from oil sludge storage tank import 12 In storage tank 1, into oil sludge storage tank, 1 is added the stirring paddle stirring being arranged after water by oil sludge storage tank 1, and is heated to 75 DEG C, water is uniformly mixed with oil sludge;
Step a1, oil sludge pretreatment: uniformly mixed oil sludge system enters ultrasonic wave effect device assembly 25 and is demulsified, The sump oil muddy water of primary demulsification is recycled in oil sludge storage tank 1 from the second pretreatment pipeline 16;
The separation of solid-liquid primary: step a2 is pumped by the pretreated sump oil muddy water of oil sludge system by feeding engine 1 In primary centrifuge machine 6, bulky grain sludge settles in centrifugal process, is separated by solid-liquid separation, and bulky grain sludge is from primary centrifuge machine first Outlet 61 is discharged into sludge box 1, and the oil sludge is pumped into ultrasonic wave by feeding engine and acts in device assembly 1 Reason.
Step b, ultrasonic wave affector demulsification: uniformly mixed oil sludge liquid by feeding engine be pumped into three it is concatenated surpass In sound wave effect device assembly 1, the sump oil cement of emulsification is demulsified in the case where ultrasonic wave effect device assembly 1 acts on, water oil layer;
Step c, oil separation: oil and sludge water after demulsification are connected to supercentrifuge 3, supercentrifuge 3 by pipeline Under operating, oil reservoir and sludge water layer are layered, and oil reservoir are separated from supercentrifuge first outlet 31 into recycling fuel tank 30;
Step c1, sludge water are done over again: after the supercentrifuge 3 separates oil-yielding stratum, sludge water enters sludge water tank 36, If the oil content in sludge water is more than setting value, it is pumped into oil sludge storage tank 1 by doing over again pipeline 39 from sludge water tank 36, Recycle above-mentioned steps a1, step a2, step b, step c;If setting value is not higher than without oil reservoir or oil content in sludge water, under One step;
Step c2, dross flocculating setting: removing and flocculant be added in the sludge water of oil reservoir, and flocculant and sludge water are by the One pipeline static mixer 38 is uniformly mixed, and is pumped into low speed centrifuge 4, and dross is reunited under flocculant effect to be settled;
Step d, mud-water separation: the sludge water and flocculant mixed from first pipe static mixer 38 is in low-speed centrifugal In the effect of machine 4, low speed centrifuge 4 is operated, and mud layer and water layer separation, dry mud come out from low speed centrifuge first outlet separation 42, Water layer is separated from low speed centrifuge second outlet 43.
Step e, cycling utilization of wastewater: after the mud-water separation, water layer is after the separation of low speed centrifuge second outlet 43 Into vibrating screen 45, waste water tank 44 is entered after vibrating screen filtering, waste water tank 44 is connected in boiler 8 by water return pipeline 47, The boiler 8 is heated by water vapour, hot water after heating by cleaning pipeline 82 respectively enter oil sludge storage tank 1, In primary centrifuge machine 6, supercentrifuge 3 and low speed centrifuge 4.
Embodiment 3:
Referring to shown in Fig. 3, on the basis of embodiment 2, the present embodiment increases oil sludge storage tank 27, oil sludge and sump oil Mud storage tank and two connecting pipe of oil sludge storage tank are provided with triple valve 18, the outlet 11 of the oil sludge storage tank 1 and dirt The outlet of greasy filth storage tank 27 passes through pretreatment pipeline respectively and is connected to the ultrasonic wave of pretreatment system effect device assembly two, And connect by the first separate pipeline with primary centrifuge machine, the primary centrifuge machine 6, ultrasonic wave described in remaining act on device assembly one 2, supercentrifuge 3, sludge water tank, flocculant case, low speed centrifuge 4, waste water tank, the connection between boiler 8 are constant, then this It does not repeat them here.
When handling oil sludge using the oil sludge processing equipment, treatment process is as follows:
Step a: dilution is added water and stirred, selectively enters oil sludge storage tank in the triple valve that the oil sludge passes through pipeline 1 or oil sludge storage tank two in, if oil sludge enters in oil sludge storage tank 1, the hot water of boiler 8 enters in oil sludge storage tank 1, and By the stirring paddle stirring of 1 setting in oil sludge storage tank, and 75 DEG C are heated to, water is uniformly mixed with oil sludge, sump oil laitance Change, the water source in boiler is passed through in oil sludge storage tank 27, completes cleaning operation;On the contrary, if oil sludge enters oil sludge storage tank In 27, the hot water of boiler, which enters in oil sludge storage tank 27, dilutes oil sludge.Increase an oil sludge storage tank, is equivalent to two Set equipment uses simultaneously, improves the treatment effeciency of oil sludge;
Subsequent treatment process step is constant, then this is not repeated them here.
Embodiment 4:
As shown in figure 4, the present embodiment connects in feeding engine 1 and ultrasonic wave effect device assembly 25 on the basis of embodiment 2 The import front end of i.e. ultrasonic wave effect device assembly 25 is additionally provided with second pipe static mixing on the first pretreatment pipeline 15 connect Device 91;The import front end of i.e. primary centrifuge machine 6 is also set in the third separate pipeline 17 that feeding engine 1 is connect with primary centrifuge machine 6 It is equipped with third pipeline static mixer 92;On the pipeline that the ultrasonic wave effect device assembly 1 is connect with supercentrifuge 3 i.e. The import front end of supercentrifuge 3 is additionally provided with the 4th pipeline static mixer 93.Oil sludge is during transportation according to itself The power of transport is uniformly mixed in pipeline static mixer, it will be apparent that, what this mode was more advantageous to and improves oil removing, desilts Handle quality and treatment effeciency.Remaining is connected with 2 structure of embodiment, treatment process is identical, is not being repeated.
In embodiment 1-4, valve is designed in the pipeline of each fluid such as the oil sludge A, water B, water vapour C and muddy water Door, the flow direction and flow of each fluid are controlled by the angle of opening and closing and the unlatching of valve.
Using any of the above-described embodiment to disposal of oily sludge, oil separates, can reach following index after mud-water separation: dirty Oily impurity content≤5%, oil content of wastewater≤500mg/L, sludge solid holdup >=25%, realize the recycle and reuse of sump oil.
Taking the above-mentioned ideal embodiment according to the present invention as inspiration, through the above description, relevant staff is complete Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention Property range is not limited to the contents of the specification, it is necessary to which the technical scope thereof is determined according to the scope of the claim.

Claims (10)

1. a kind of oil sludge processing equipment has oil sludge storage tank (1), ultrasonic wave acts on device assembly one (2), supercentrifuge (3) and low speed centrifuge (4), it is characterised in that: the oil sludge storage tank (1) is by the first separate pipeline (13) and is arranged and exists Feeding engine one (14) in first separate pipeline (13) is connect with ultrasonic wave effect device assembly one (2) import;The ultrasonic wave is made It is connect with the outlet of device assembly one (2) with supercentrifuge import (33);The supercentrifuge (3) is provided with supercentrifuge First outlet (31) and supercentrifuge second outlet (32);Supercentrifuge second outlet (32) passes through the second separate pipeline (34) it is connect with the feeding engine two (35) that is arranged in the second separate pipeline with low speed centrifuge (4);The low speed centrifuge (4) On be provided with low speed centrifuge first outlet (42) and low speed centrifuge second outlet (43).
2. a kind of oil sludge processing equipment as described in claim 1, it is characterised in that: further include oil sludge pretreatment unit and Primary centrifuge machine (6);The oil sludge pretreatment unit includes ultrasonic wave effect device assembly two (5), the first pretreatment pipeline (15) and second pre-processes pipeline (16);The oil sludge outlet (11) passes through the first pretreatment pipeline (15) connection ultrasound Wave acts on the import of device assembly two (5), and connects going out for ultrasonic wave effect device assembly two (5) by the second pretreatment pipeline (16) Mouth is connect with oil sludge reservoir inlet (12), is formed oil sludge and is pre-processed circulator;And
Oil sludge storage tank (1) connects third separating pipe by the threeway of feeding engine one (14) outlet on the first separate pipeline (13) The other end of the one end in road (17), third separate pipeline (17) is connect with the import of primary centrifuge machine (6);The primary centrifuge machine (6) primary centrifuge machine first outlet (61) and primary centrifuge machine second outlet (62) are provided with;The primary centrifuge machine second goes out Mouth (62) is connect with the import of ultrasonic wave effect device assembly one (2);
Be provided between the supercentrifuge second outlet (32) and low speed centrifuge import (41) sludge water tank (36) and Sludge water tank (36) is arranged between supercentrifuge second outlet (32) and feeding engine two (35);
Flocculant case (37) are additionally provided between the supercentrifuge second outlet (32) and low speed centrifuge import (41) With first pipe static mixer (38);The first pipe static mixer (38) setting feeding engine two (35) and low speed from Between scheming import (41), the outlet end (381) of first pipe static mixer (38) is connect with low speed centrifuge import (41), The main input end (382) of first pipe static mixer (38) is connect with the outlet end of feeding engine two (35);The flocculant Case (37) is connected to the secondary input end (383) of first pipe static mixer (38) by pipeline and flocculant delivery pump;It is described The feeding engine two (35) of connection sludge water tank (36) also connect by pipeline of doing over again (39) with oil sludge storage tank (1).
3. a kind of oil sludge processing equipment as claimed in claim 1 or 2, it is characterised in that: the supercentrifuge first goes out Mouth (31) is connect by pipeline with drain oil recovery equipment (30);Low speed centrifuge second outlet (43) is connected in turn by pipeline Vibrating screen (45) and waste water tank (44);It is provided with waste water discharge water pump (48) in the outlet conduit of the waste water tank (44), gives up Water discharge water pump (48) is connected with two outlets by three, and first outlet (481) is directly connected to sewage conduct, second outlet (48- 2) it is connect by water return pipeline (47) with boiler (8);Vapor pipeline (81) collet that the boiler (8) passes through setting Heating;And
Boiler (8) water outlet by cleaning pipeline (82) respectively with oil sludge storage tank (1), primary centrifuge machine (6), high Fast centrifuge (3) and low speed centrifuge (4) connection;
The water return pipeline (47) can directly be connect with boiler (8);Can also with a part of water return pipeline (47) with return Work pipeline (39) shares.
4. a kind of oil sludge processing equipment as claimed in claim 2, it is characterised in that: the feeding engine one (14) and ultrasound It further includes second pipe static mixer (91) that wave, which acts in the first pretreatment pipeline (15) that device assembly two (5) connect,;It is described It further include third pipeline static mixer in the third separate pipeline (17) that feeding engine one (14) is connect with primary centrifuge machine (6) (92);It is quiet that the 4th pipeline is additionally provided on the pipeline that ultrasonic wave effect device assembly one (2) is connect with supercentrifuge (3) State mixer (93).
5. a kind of oil sludge processing equipment as claimed in claim 2, it is characterised in that: the sump oil storage tank (1) is at least 1 It is a;
Ultrasonic wave effect device assembly one (2) is composed in series by 1 to 6 ultrasonic wave affector unit;
Ultrasonic wave effect device assembly two (5) of the oil sludge pretreatment unit is by 1 to 6 ultrasonic wave affector series connection group At.
6. a kind of sump oil sludge treatment technology, which comprises the following steps:
Step a, add water and stir dilution: oil sludge is stored in oil sludge storage tank, to addition water, sump oil in oil sludge storage tank (1) The stirring paddle stirring being arranged in mud storage tank (1), water are uniformly mixed with oil sludge;
Step b, the demulsification of ultrasonic wave affector: uniformly mixed oil sludge liquid is pumped into ultrasonic wave effect by feeding engine one (14) In device assembly one (2), the sump oil cement of emulsification is demulsified under ultrasonic wave effect device assembly one (2) effect, oil, sludge water layering;
Step c, oil separation: oil and sludge water after demulsification are connected to supercentrifuge (3) by pipeline, supercentrifuge (3) Under operating, oil reservoir and sludge water layer are layered, and oil reservoir is separated from supercentrifuge first outlet (31);
Step d, mud-water separation: the sludge water layer for removing oil reservoir is pumped from supercentrifuge second outlet (32) through feeding engine two (35) Enter in low speed centrifuge (4), low speed centrifuge (4) operating, mud layer and water layer separation, mud layer is from low speed centrifuge first outlet (42) it separates, water layer is separated from low speed centrifuge second outlet (43).
7. a kind of sump oil sludge treatment technology as claimed in claim 6, which is characterized in that the step a adds water and stirs dilution Also there are following steps afterwards:
Step a1, oil sludge pretreatment: uniformly mixed oil sludge system enters ultrasonic wave effect device assembly two (5) demulsification, just The sump oil muddy water of grade demulsification is recycled in oil sludge storage tank (1) from the second pretreatment pipe-line system (16);
The separation of solid-liquid primary: step a2 is pumped into just by the pretreated sump oil muddy water of oil sludge system by feeding engine one (14) In grade centrifuge (6), bulky grain sludge settles in centrifugal process, is separated by solid-liquid separation, and bulky grain sludge is from primary centrifuge machine first (61) discharge is exported, the oil sludge is pumped into processing in ultrasonic wave effect device assembly one (2) by feeding engine one (14).
8. a kind of sump oil sludge treatment technology as claimed in claim 6, which is characterized in that after the step c oil separating step Also there are following steps:
Step c1, sludge water are done over again: after supercentrifuge (3) the separation oil-yielding stratum, sludge water enters sludge water tank (36), If the oil content in sludge water is more than setting value, sludge water is pumped into oil sludge storage from sludge water tank (36) by doing over again pipeline Tank (1).
Dross flocculating setting: after the separation of step c oil, flocculant is added in the sludge water isolated, dross is in flocculant in step c2 The lower sedimentation of reuniting of effect.
9. a kind of sump oil sludge treatment technology as claimed in claim 6, which is characterized in that after the step d mud-water separation, water Layer can be recycled after separating from low speed centrifuge second outlet (43), specific steps are as follows:
Step e: cycling utilization of wastewater, water layer enter waste water tank (44) after separating from low speed centrifuge second outlet (43), waste water Case (44) is connected in boiler (8) by water return pipeline (47) system, and the boiler (8) is heated by vapor, Hot water after heating respectively enters oil sludge storage tank (1), primary centrifuge machine (6), high speed centrifugation by cleaning pipeline (82) system In machine (3) and low speed centrifuge (4).
10. a kind of sump oil sludge treatment technology as claimed in claim 6, which is characterized in that temperature in the oil sludge storage tank It is set as 60 DEG C to 90 DEG C.
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CN115196845A (en) * 2022-08-01 2022-10-18 湖南宏旺新材料科技有限公司 Oil-sludge separation system and control method
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