CN109943258A - A kind of water proof building glue and preparation method thereof - Google Patents
A kind of water proof building glue and preparation method thereof Download PDFInfo
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- CN109943258A CN109943258A CN201910243060.9A CN201910243060A CN109943258A CN 109943258 A CN109943258 A CN 109943258A CN 201910243060 A CN201910243060 A CN 201910243060A CN 109943258 A CN109943258 A CN 109943258A
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Abstract
The present invention relates to a kind of water proof building glue and preparation method thereof, the water proof building glue is raw material by using polyvinyl alcohol, epoxy resin, hydroxylated cellulose, acrylic emulsion, styrene-acrylic emulsion, titanium dioxide, silica flour, carbon fiber particles, surfactant, silane coupling agent and carries out appropriate weight proportion, water proof building glue is prepared through ad hoc approach, good waterproof performance, bonding force is strong, and resistance to compression and tensile strength are high, and film forming and curing time are short, easy to use, construction efficiency is high.Data show that the peel strength of water proof building glue of the present invention reaches 17Mpa or more, and tensile shear strength reaches 20Mpa or more；And after boiling 14 days, cementability is still kept good with the substrate, waterproof performance is good through 97 DEG C.
Description
Technical field
The invention belongs to building adhesive technical fields, and in particular to a kind of water proof building glue and preparation method thereof.
Background technique
Building adhesive is essential material in architectural engineering using very extensive in architectural engineering.Building adhesive application
In each process or even each material of building trade.Building sealant is mainly used for the various seams of building or hole
Sealing prevent structural material to be destroyed in displacement structure to prevent gas, liquid, solids passage, thus play heat preservation,
Sound insulation, waterproof and dustproof, gas-tight, fire prevention, anticorrosion, damping and the function of preventing seam accumulation foreign matter.
Existing building adhesive waterproof performance is insufficient, for a long time by direct sunlight and rain drop erosion, between two blocks of construction materials
Aging easily occurs for glue, and construction material is caused to be easy to be corroded.
Summary of the invention
In order to solve the above problems existing in the present technology, the present invention provides a kind of water proof building glue and its preparation sides
Method.The water proof building glue, good waterproof performance, bonding force is strong, and resistance to compression and tensile strength are high, and film forming and curing time are short, user
Just, construction efficiency is high.
The technical scheme adopted by the invention is as follows:
A kind of water proof building glue, raw material components include:
Polyvinyl alcohol, 20-60 parts by weight；
Epoxy resin, 10-20 parts by weight；
Hydroxylated cellulose, 1-5 parts by weight；
Acrylic emulsion, 10-20 parts by weight；
Styrene-acrylic emulsion, 10-20 parts by weight；
Titanium dioxide, 0.5-2 parts by weight；
Silica flour, 0.5-2 parts by weight；
Carbon fiber particles, 0.8-2 parts by weight；
Surfactant, 1.2-2.4 parts by weight；
Silane coupling agent, 1.2-2.4 parts by weight；
Deionized water, 200-500 parts by weight.
The raw material components of the further preferred water proof building glue include:
Polyvinyl alcohol, 40 parts by weight；
Epoxy resin, 15 parts by weight；
Hydroxylated cellulose, 3 parts by weight；
Acrylic emulsion, 10-20 parts by weight；
Styrene-acrylic emulsion, 10-20 parts by weight；
Titanium dioxide, 0.5-2 parts by weight；
Silica flour, 0.5-2 parts by weight；
Carbon fiber particles, 1.4 parts by weight；
Surfactant, 1.8 parts by weight；
Silane coupling agent, 1.8 parts by weight；
Deionized water, 350 parts by weight.
The hydroxylated cellulose includes one of hydroxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl methyl cellulose
Or several mixture.
The hydroxylated cellulose is hydroxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl methyl cellulose according to molar ratio
The mixture of 1-2:1-2:1-2 composition.
The molecular weight ranges of the epoxy resin are 8000-200000, epoxide number 0.48-0.54.
The partial size of the carbon fiber particles is 5-100nm.
The surfactant is sodium alkyl sulfonate, sodium alklyarylsulfonate, sodium alkyl sulfate according to molar ratio 1-2:1-
The mixture of 2:1-2 composition.
The silane coupling agent is aminopropyl Ethoxysilane, mercaptopropyl trimethoxysilane, three ethoxy of ethylenediamine propyl
The mixture that base silane is formed according to molar ratio 1-2:1-2:1-2.
The preparation method of the water proof building glue, includes the following steps:
(1) polyvinyl alcohol, epoxy resin, hydroxylated cellulose are taken respectively, are carried out being sufficiently mixed uniformly under heating condition, be obtained
Mixture A；
(2) acrylic emulsion, styrene-acrylic emulsion, titanium dioxide, silica flour, carbon fiber particles are taken respectively, are carried out under heating condition
It is sufficiently mixed uniformly, obtains mixture B；
(3) it takes surfactant and silane coupling agent to be uniformly mixed respectively, 40-50 DEG C is warming up to, by mixture A and mixing
Object B is added, and 20-30min is mixed to get the water proof building glue.
In step (1), it is heated to 45-55 DEG C；
In step (2), it is heated to 45-55 DEG C.
The invention has the benefit that
Water proof building glue of the present invention, by using polyvinyl alcohol, epoxy resin, hydroxylated cellulose, propylene yogurt
Liquid, styrene-acrylic emulsion, titanium dioxide, silica flour, carbon fiber particles, surfactant, silane coupling agent are raw material and carry out suitably heavy
Amount proportion, is prepared water proof building glue through ad hoc approach, and good waterproof performance, bonding force is strong, and resistance to compression and tensile strength are high, film forming and
Curing time is short, easy to use, and construction efficiency is high.Data show that the peel strength of water proof building glue of the present invention reaches 17Mpa
More than, tensile shear strength reaches 20Mpa or more；And after boiling 14 days, cementability, waterproof are still kept good with the substrate through 97 DEG C
Performance is good.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, technical solution of the present invention will be carried out below
Detailed description.Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Base
Embodiment in the present invention, those of ordinary skill in the art are obtained all without making creative work
Other embodiment belongs to the range that the present invention is protected.
1g is represented in following example with 1 parts by weight.
Material polyethylene alcohol used in following example is 1799 type of technical grade, and the molecular weight ranges of epoxy resin are
8000-200000, epoxide number 0.48-0.54.
Embodiment 1
The present embodiment provides a kind of water proof building glue, raw material components include:
Polyvinyl alcohol, 20 parts by weight；
Epoxy resin, 20 parts by weight；
Hydroxymethyl cellulose, 1 parts by weight；
Acrylic emulsion, 20 parts by weight；
Styrene-acrylic emulsion, 10 parts by weight；
Partial size is the titanium dioxide of 5-10nm, 2 parts by weight；
Partial size is the silica flour of 5-10nm, 0.5 parts by weight；
Partial size is the carbon fiber particles of 5-10nm, 0.8 parts by weight；
Surfactant is dodecyl sodium sulfate, neopelex, lauryl sodium sulfate according to molar ratio
The mixture of 1:2:1 composition, 2.4 parts by weight；
Silane coupling agent is propyl Ethoxysilane, mercaptopropyl trimethoxysilane, ethylenediaminepropyltriethoxysilane
According to the mixture that molar ratio 1:2:1 is formed, 1.2 parts by weight；
Deionized water, 500 parts by weight.
Further, the present embodiment provides a kind of preparation method of water proof building glue, include the following steps:
(1) polyvinyl alcohol, epoxy resin and hydroxylated cellulose are taken respectively, are heated to 45-55 DEG C and be sufficiently mixed
It is even, obtain mixture A；
(2) acrylic emulsion, styrene-acrylic emulsion, titanium dioxide, silica flour, carbon fiber particles are taken respectively, are heated to 45-55 DEG C simultaneously
Be sufficiently mixed uniformly, obtains mixture B；
(3) it takes surfactant and silane coupling agent to be uniformly mixed respectively, 40-50 DEG C is warming up to, by mixture A and mixing
Object B is added, and 20-30min is mixed to get the water proof building glue.
Embodiment 2
The present embodiment provides a kind of water proof building glue, raw material components include:
Polyvinyl alcohol, 60 parts by weight；
Epoxy resin, 10 parts by weight；
Hydroxymethyl cellulose, 5 parts by weight；
Acrylic emulsion, 10 parts by weight；
Styrene-acrylic emulsion, 20 parts by weight；
Partial size is the titanium dioxide of 10-20nm, 0.5 parts by weight；
Partial size is the silica flour of 10-20nm, 2 parts by weight；
Partial size is the carbon fiber particles of 10-20nm, 2 parts by weight；
Surfactant is dodecyl sodium sulfate, neopelex, lauryl sodium sulfate according to molar ratio
The mixture of 2:1:2 composition, 1.2 parts by weight；
Silane coupling agent is propyl Ethoxysilane, mercaptopropyl trimethoxysilane, ethylenediaminepropyltriethoxysilane
According to the mixture that molar ratio 2:1:2 is formed, 2.4 parts by weight；
Deionized water, 200 parts by weight.
Further, the present embodiment provides a kind of preparation method of water proof building glue, include the following steps:
(1) polyvinyl alcohol, epoxy resin and hydroxylated cellulose are taken respectively, are heated to 45-55 DEG C and be sufficiently mixed
It is even, obtain mixture A；
(2) acrylic emulsion, styrene-acrylic emulsion, titanium dioxide, silica flour, carbon fiber particles are taken respectively, are heated to 45-55 DEG C simultaneously
Be sufficiently mixed uniformly, obtains mixture B；
(3) it takes surfactant and silane coupling agent to be uniformly mixed respectively, 40-50 DEG C is warming up to, by mixture A and mixing
Object B is added, and 20-30min is mixed to get the water proof building glue.
Embodiment 3
The present embodiment provides a kind of water proof building glue, raw material components include:
Polyvinyl alcohol, 40 parts by weight；
Epoxy resin, 15 parts by weight；
The mixing that hydroxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl methyl cellulose are formed according to molar ratio 1:1:1
Object, 3 parts by weight；
Acrylic emulsion, 15 parts by weight；
Styrene-acrylic emulsion, 15 parts by weight；
Partial size is the titanium dioxide of 20-40nm, 1.25 parts by weight；
Partial size is the silica flour of 20-40nm, 1.25 parts by weight；
Partial size is the carbon fiber particles of 20-40nm, 1.4 parts by weight；
Surfactant is dodecyl sodium sulfate, neopelex, lauryl sodium sulfate according to molar ratio
The mixture of 1:1:1 composition, 1.8 parts by weight；
Silane coupling agent is propyl Ethoxysilane, mercaptopropyl trimethoxysilane, ethylenediaminepropyltriethoxysilane
According to the mixture that molar ratio 1:1:1 is formed, 1.8 parts by weight；
Deionized water, 350 parts by weight.
Further, the present embodiment provides a kind of preparation method of water proof building glue, include the following steps:
(1) polyvinyl alcohol, epoxy resin and hydroxylated cellulose are taken respectively, are heated to 45-55 DEG C and be sufficiently mixed
It is even, obtain mixture A；
(2) acrylic emulsion, styrene-acrylic emulsion, titanium dioxide, silica flour, carbon fiber particles are taken respectively, are heated to 45-55 DEG C simultaneously
Be sufficiently mixed uniformly, obtains mixture B；
(3) it takes surfactant and silane coupling agent to be uniformly mixed respectively, 40-50 DEG C is warming up to, by mixture A and mixing
Object B is added, and 20-30min is mixed to get the water proof building glue.
Embodiment 4
The present embodiment provides a kind of water proof building glue, raw material components include:
Polyvinyl alcohol, 30 parts by weight；
Epoxy resin, 12 parts by weight；
The mixing that hydroxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl methyl cellulose are formed according to molar ratio 1:2:1
Object, 2 parts by weight；
Acrylic emulsion, 12 parts by weight；
Styrene-acrylic emulsion, 18 parts by weight；
Partial size is the titanium dioxide of 40-60nm, 1 parts by weight；
Partial size is the silica flour of 40-60nm, 1 parts by weight；
Partial size is the carbon fiber particles of 40-60nm, 1 parts by weight；
Surfactant is dodecyl sodium sulfate, 1.5 parts by weight；
Silane coupling agent is propyl Ethoxysilane, 1.5 parts by weight；
Deionized water, 300 parts by weight.
Further, the present embodiment provides a kind of preparation method of water proof building glue, include the following steps:
(1) polyvinyl alcohol, epoxy resin and hydroxylated cellulose are taken respectively, are heated to 45-55 DEG C and be sufficiently mixed
It is even, obtain mixture A；
(2) acrylic emulsion, styrene-acrylic emulsion, titanium dioxide, silica flour, carbon fiber particles are taken respectively, are heated to 45-55 DEG C simultaneously
Be sufficiently mixed uniformly, obtains mixture B；
(3) it takes surfactant and silane coupling agent to be uniformly mixed respectively, 40-50 DEG C is warming up to, by mixture A and mixing
Object B is added, and 20-30min is mixed to get the water proof building glue.
Embodiment 5
The present embodiment provides a kind of water proof building glue, raw material components include:
Polyvinyl alcohol, 40 parts by weight；
Epoxy resin, 15 parts by weight；
The mixing that hydroxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl methyl cellulose are formed according to molar ratio 2:1:2
Object, 3 parts by weight；
Acrylic emulsion, 18 parts by weight；
Styrene-acrylic emulsion, 12 parts by weight；
Partial size is the titanium dioxide of 20-40nm, 1.5 parts by weight；
Partial size is the silica flour of 20-40nm, 1.5 parts by weight；
Partial size is the carbon fiber particles of 20-40nm, 1.4 parts by weight；
Surfactant is neopelex, 1.8 parts by weight；
Silane coupling agent is mercaptopropyl trimethoxysilane, 1.8 parts by weight；
Deionized water, 350 parts by weight.
Further, the present embodiment provides a kind of preparation method of water proof building glue, include the following steps:
(1) polyvinyl alcohol, epoxy resin and hydroxylated cellulose are taken respectively, are heated to 45-55 DEG C and be sufficiently mixed
It is even, obtain mixture A；
(2) acrylic emulsion, styrene-acrylic emulsion, titanium dioxide, silica flour, carbon fiber particles are taken respectively, are heated to 45-55 DEG C simultaneously
Be sufficiently mixed uniformly, obtains mixture B；
(3) it takes surfactant and silane coupling agent to be uniformly mixed respectively, 40-50 DEG C is warming up to, by mixture A and mixing
Object B is added, and 20-30min is mixed to get the water proof building glue.
Embodiment 6
The present embodiment provides a kind of water proof building glue, raw material components include:
Polyvinyl alcohol, 40 parts by weight；
Epoxy resin, 15 parts by weight；
The mixing that hydroxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl methyl cellulose are formed according to molar ratio 1:1:1
Object, 3 parts by weight；
Acrylic emulsion, 15 parts by weight；
Styrene-acrylic emulsion, 15 parts by weight；
Partial size is the titanium dioxide of 40-80nm, 1.25 parts by weight；
Partial size is the silica flour of 40-80nm, 1.25 parts by weight；
Partial size is the carbon fiber particles of 40-80nm, 1.4 parts by weight；
Surfactant is dodecyl sodium sulfate, neopelex, lauryl sodium sulfate according to molar ratio
The mixture of 1:1:1 composition, 1.8 parts by weight；
Silane coupling agent is propyl Ethoxysilane, mercaptopropyl trimethoxysilane, ethylenediaminepropyltriethoxysilane
According to the mixture that molar ratio 1:1:1 is formed, 1.8 parts by weight；
Deionized water, 350 parts by weight.
Further, the present embodiment provides a kind of preparation method of water proof building glue, include the following steps:
(1) polyvinyl alcohol, epoxy resin and hydroxylated cellulose are taken respectively, are heated to 45-55 DEG C and be sufficiently mixed
It is even, obtain mixture A；
(2) acrylic emulsion, styrene-acrylic emulsion, titanium dioxide, silica flour, carbon fiber particles are taken respectively, are heated to 45-55 DEG C simultaneously
Be sufficiently mixed uniformly, obtains mixture B；
(3) it takes surfactant and silane coupling agent to be uniformly mixed respectively, 40-50 DEG C is warming up to, by mixture A and mixing
Object B is added, and 20-30min is mixed to get the water proof building glue.
Embodiment 7
The present embodiment provides a kind of water proof building glue, raw material components include:
Polyvinyl alcohol, 40 parts by weight；
Epoxy resin, 15 parts by weight；
The mixing that hydroxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl methyl cellulose are formed according to molar ratio 1:1:1
Object, 3 parts by weight；
Acrylic emulsion, 15 parts by weight；
Styrene-acrylic emulsion, 15 parts by weight；
Partial size is the titanium dioxide of 80-100nm, 1.25 parts by weight；
Partial size is the silica flour of 80-100nm, 1.25 parts by weight；
Partial size is the carbon fiber particles of 80-100nm, 1.4 parts by weight；
Surfactant is dodecyl sodium sulfate, neopelex, lauryl sodium sulfate according to molar ratio
The mixture of 1:1:1 composition, 1.8 parts by weight；
Silane coupling agent is propyl Ethoxysilane, mercaptopropyl trimethoxysilane, ethylenediaminepropyltriethoxysilane
According to the mixture that molar ratio 1:1:1 is formed, 1.8 parts by weight；
Deionized water, 350 parts by weight.
Further, the present embodiment provides a kind of preparation method of water proof building glue, include the following steps:
(1) polyvinyl alcohol, epoxy resin and hydroxylated cellulose are taken respectively, are heated to 45-55 DEG C and be sufficiently mixed
It is even, obtain mixture A；
(2) acrylic emulsion, styrene-acrylic emulsion, titanium dioxide, silica flour, carbon fiber particles are taken respectively, are heated to 45-55 DEG C simultaneously
Be sufficiently mixed uniformly, obtains mixture B；
(3) it takes surfactant and silane coupling agent to be uniformly mixed respectively, 40-50 DEG C is warming up to, by mixture A and mixing
Object B is added, and 20-30min is mixed to get the water proof building glue.
Comparative example 1
This comparative example provides a kind of building adhesive, and raw material components and the difference of embodiment 3 are only that: raw material does not add carbon fiber
Particle, other raw material components and preparation method are same as Example 3.
Comparative example 2
This comparative example provides a kind of building adhesive, and raw material components and the difference of embodiment 3 are only that: raw material does not add hydroxyl fibre
Dimension element, other raw material components and preparation method are same as Example 3.
Experimental example
It makes a service test to building adhesive made from above-described embodiment and comparative example, test data is as shown in table 1.
The performance test data of table 1- difference building adhesive sample
As it can be seen from table 1 the present invention provides building adhesive, film forming and curing time are short, and peel strength reaches 17Mpa or more,
Tensile shear strength reaches 20Mpa or more, has good adhesive property, and through 97 DEG C after boiling 14 days, still keeps good with substrate
Good cementability, waterproof performance are good.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Those familiar with the art in the technical scope disclosed by the present invention, can easily think of the change or the replacement, and should all contain
Lid is within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.
Claims (10)
1. a kind of water proof building glue, which is characterized in that raw material components include:
Polyvinyl alcohol, 20-60 parts by weight；
Epoxy resin, 10-20 parts by weight；
Hydroxylated cellulose, 1-5 parts by weight；
Acrylic emulsion, 10-20 parts by weight；
Styrene-acrylic emulsion, 10-20 parts by weight；
Titanium dioxide, 0.5-2 parts by weight；
Silica flour, 0.5-2 parts by weight；
Carbon fiber particles, 0.8-2 parts by weight；
Surfactant, 1.2-2.4 parts by weight；
Silane coupling agent, 1.2-2.4 parts by weight；
Deionized water, 200-500 parts by weight.
2. water proof building glue according to claim 1, which is characterized in that raw material components include:
Polyvinyl alcohol, 40 parts by weight；
Epoxy resin, 15 parts by weight；
Hydroxylated cellulose, 3 parts by weight；
Acrylic emulsion, 15 parts by weight；
Styrene-acrylic emulsion, 15 parts by weight；
Titanium dioxide, 1.25 parts by weight；
Silica flour, 1.25 parts by weight；
Carbon fiber particles, 1.4 parts by weight；
Surfactant, 1.8 parts by weight；
Silane coupling agent, 1.8 parts by weight；
Deionized water, 350 parts by weight.
3. water proof building glue according to claim 1, which is characterized in that the hydroxylated cellulose includes hydroxylmethyl cellulose
The mixture of one or more of element, hydroxyethyl cellulose, hydroxypropyl methyl cellulose.
4. water proof building glue according to claim 3, which is characterized in that the hydroxylated cellulose be hydroxymethyl cellulose,
The mixture that hydroxyethyl cellulose, hydroxypropyl methyl cellulose are formed according to molar ratio 1-2:1-2:1-2.
5. water proof building glue according to claim 1, which is characterized in that the molecular weight ranges of the epoxy resin are
8000-200000, epoxide number 0.48-0.54.
6. water proof building glue described in claim 1, which is characterized in that the partial size of the carbon fiber particles is 5-100nm.
7. water proof building glue described in claim 1, which is characterized in that the surfactant is sodium alkyl sulfonate, alkyl virtue
The mixture that base sodium sulfonate, sodium alkyl sulfate are formed according to molar ratio 1-2:1-2:1-2.
8. water proof building glue described in claim 1, which is characterized in that the silane coupling agent be aminopropyl Ethoxysilane,
The mixture that mercaptopropyl trimethoxysilane, ethylenediaminepropyltriethoxysilane are formed according to molar ratio 1-2:1-2:1-2.
9. a kind of preparation method of any one of claim 1-8 water proof building glue, which comprises the steps of:
(1) polyvinyl alcohol, epoxy resin and hydroxylated cellulose are taken respectively, are carried out being sufficiently mixed uniformly under heating condition, be mixed
Close object A；
(2) acrylic emulsion, styrene-acrylic emulsion, titanium dioxide, silica flour, carbon fiber particles are taken respectively, are carried out under heating condition abundant
It is uniformly mixed, obtains mixture B；
(3) it takes surfactant and silane coupling agent to be uniformly mixed respectively, 40-50 DEG C is warming up to, by mixture A and mixture B
It is added, 20-30min is mixed to get the water proof building glue.
10. preparation method according to claim 9, which is characterized in that in step (1), be heated to 45-55 DEG C；
In step (2), it is heated to 45-55 DEG C.
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| CN113174223A (en) * | 2021-05-07 | 2021-07-27 | 中威建鑫科技发展有限公司 | Water-based high-bonding-strength tile back glue and preparation method thereof |
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