CN109928368A - The molten sulfur pond composite cover of Recovered sulphur steam - Google Patents
The molten sulfur pond composite cover of Recovered sulphur steam Download PDFInfo
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- CN109928368A CN109928368A CN201910321159.6A CN201910321159A CN109928368A CN 109928368 A CN109928368 A CN 109928368A CN 201910321159 A CN201910321159 A CN 201910321159A CN 109928368 A CN109928368 A CN 109928368A
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- Prior art keywords
- chilling roller
- cooling medium
- molten sulfur
- sulphur
- chilling
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- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 title claims abstract description 118
- 239000005864 Sulphur Substances 0.000 title claims abstract description 57
- 229910052717 sulfur Inorganic materials 0.000 title claims abstract description 52
- 239000011593 sulfur Substances 0.000 title claims abstract description 52
- 239000002131 composite material Substances 0.000 title claims abstract description 21
- 239000002826 coolant Substances 0.000 claims abstract description 40
- 150000001875 compounds Chemical class 0.000 claims abstract description 11
- 238000001816 cooling Methods 0.000 claims description 2
- 238000009833 condensation Methods 0.000 abstract description 17
- 230000005494 condensation Effects 0.000 abstract description 17
- 239000006071 cream Substances 0.000 abstract description 2
- 235000001508 sulfur Nutrition 0.000 description 46
- 238000000034 method Methods 0.000 description 11
- 239000000126 substance Substances 0.000 description 9
- 230000000694 effects Effects 0.000 description 7
- 239000007788 liquid Substances 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 230000006378 damage Effects 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 230000002159 abnormal effect Effects 0.000 description 2
- 230000002411 adverse Effects 0.000 description 2
- 239000004568 cement Substances 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000004939 coking Methods 0.000 description 2
- 238000009792 diffusion process Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 210000002345 respiratory system Anatomy 0.000 description 2
- 239000003643 water by type Substances 0.000 description 2
- PCTMTFRHKVHKIS-BMFZQQSSSA-N (1s,3r,4e,6e,8e,10e,12e,14e,16e,18s,19r,20r,21s,25r,27r,30r,31r,33s,35r,37s,38r)-3-[(2r,3s,4s,5s,6r)-4-amino-3,5-dihydroxy-6-methyloxan-2-yl]oxy-19,25,27,30,31,33,35,37-octahydroxy-18,20,21-trimethyl-23-oxo-22,39-dioxabicyclo[33.3.1]nonatriaconta-4,6,8,10 Chemical compound C1C=C2C[C@@H](OS(O)(=O)=O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2.O[C@H]1[C@@H](N)[C@H](O)[C@@H](C)O[C@H]1O[C@H]1/C=C/C=C/C=C/C=C/C=C/C=C/C=C/[C@H](C)[C@@H](O)[C@@H](C)[C@H](C)OC(=O)C[C@H](O)C[C@H](O)CC[C@@H](O)[C@H](O)C[C@H](O)C[C@](O)(C[C@H](O)[C@H]2C(O)=O)O[C@H]2C1 PCTMTFRHKVHKIS-BMFZQQSSSA-N 0.000 description 1
- FGRBYDKOBBBPOI-UHFFFAOYSA-N 10,10-dioxo-2-[4-(N-phenylanilino)phenyl]thioxanthen-9-one Chemical compound O=C1c2ccccc2S(=O)(=O)c2ccc(cc12)-c1ccc(cc1)N(c1ccccc1)c1ccccc1 FGRBYDKOBBBPOI-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- CUZMQPZYCDIHQL-VCTVXEGHSA-L calcium;(2s)-1-[(2s)-3-[(2r)-2-(cyclohexanecarbonylamino)propanoyl]sulfanyl-2-methylpropanoyl]pyrrolidine-2-carboxylate Chemical compound [Ca+2].N([C@H](C)C(=O)SC[C@@H](C)C(=O)N1[C@@H](CCC1)C([O-])=O)C(=O)C1CCCCC1.N([C@H](C)C(=O)SC[C@@H](C)C(=O)N1[C@@H](CCC1)C([O-])=O)C(=O)C1CCCCC1 CUZMQPZYCDIHQL-VCTVXEGHSA-L 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000009510 drug design Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 1
- 229910010271 silicon carbide Inorganic materials 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Processing Of Solid Wastes (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a kind of molten sulfur pond composite covers for removing sulphur steam, including compound lid (1), chilling roller rotary positioning frame (9) are equipped in the compound lid (1), the chilling roller (2) that one row can rotate is installed on the chilling roller rotary positioning frame (9), the one end of each chilling roller (2) is fixedly connected with a rotation gear, and the rotation gear of all chilling roller (2) ends after chilling roller rotation drive chain (7) connection with chilling roller rotation drive device (6) by connecting.The characteristics of composite cover, is, the chilling roller of interior logical cooling medium is set in lid, the condensation condensation after sulphur steam that molten sulfur pond generates rises to composite cover, and the sulphur condensed in chilling roller is periodically cut knife in chilling roller directional-rotation and cuts, and returns to molten sulfur pond.The molten sulfur pond composite cover provided by the invention for removing sulphur steam can effectively prevent to condense the generation of phenomenon everywhere in workplace due to sulphur steam in sulfur cream, improve the working environment quality of worker.
Description
Technical field
The invention belongs to sulfur recovery technology and environment protection field, it is related to vapour oxid-reclamatiom technique sour in coking, petrochemical industry
The device of the molten sulfur pond sulfur vapor recycling used, the molten sulfur pond composite cover of specially a kind of Recovered sulphur steam.
Background technique
China's coking, petrochemical industry will contain sour vapour using oxid-reclamatiom technique generally using claus oven or sulphur furnace processed
Sulfuric acid vapour is converted into sulphur simple substance and is recycled.The liquid sulphur simple substance of generation is drained in molten sulfur pond and keeps in, and molten sulfur pond temperature is general
It is 135 ~ 155 DEG C, at a temperature of this, Molten sulphur in molten sulfur pond is added due to sulphur, Sublimated Sulphur and the heat preservation steam in steam
The sulphur steam evaporated when hot, diffuses in working environment, since temperature reduction causes sulphur to crystallize rapidly, is easy in molten sulfur pond
More than liquid level, on chamber wall, in Chi Gai, especially working environment, sulphur condensation phenomenon is serious, causes to deposit everywhere in workplace
In sulphur solid, there is stronger corrosiveness to equipment and pipeline, former pond lid exhausting pipeline etc. is also frequently occluded.Sulphur in air
Sulphur is more more serious to the respiratory tract harm of worker, and a large amount of sulphur steam release can also cause ambient enviroment centainly to pollute.
So existing acid vapour is using in oxid-reclamatiom technique, molten sulfur Chi Chikou is covered usually using muti-piece cement cover board
Lid, since sulphur simple substance easily distils under liquid condition and expand calculations, cement cover board can only play blocking and spread and insulation effect, due to
Sealing effect is poor, and a large amount of sulfur vapor diffusions, have an adverse effect: 1. pairs of surrounding metal reactors and pipeline cause to corrode;2.
It causes damages to operator's respiratory system;3. blow-down pipe results in blockage;4. sulphur simple substance yield causes damages.In summary it asks
Topic, removes the sulphur in the working environment, becomes the environmental issue for needing to solve.
Summary of the invention
The present invention is intended to provide a kind of molten sulfur pond composite cover for removing sulphur steam, can effectively solve sulphur by condensing recovery
Steam is from molten sulfur pond top diffusion problem, to effectively solve the adverse effect generated in the prior art.
The present invention is achieved by the following technical scheme:
A kind of molten sulfur pond composite cover of Recovered sulphur steam, including compound lid, the composite cover body are interior fixed equipped with chilling roller rotation
Position frame, installs the chilling roller that a row can rotate on the chilling roller rotary positioning frame, the one end of each chilling roller is fixedly connected with one
Gear is rotated, the rotation gear of all chilling roller ends is rotated by chilling roller to be connected after drive chain connects with chilling roller rotation drive device
It connects;It is located at each chilling roller side on the chilling roller rotary positioning frame and is equipped with bite;Each chilling roller one end enters equipped with cooling medium
Mouth hose, the other end are equipped with cooling medium outlet hose, between the cooling medium inlet hose and cooling medium outlet hose
By being located at the heat-exchanging spiral-coil contacted in chilling roller and with chilling roller inner wall connection;The cooling medium inlet hose of each chilling roller converges
After collection and cooling medium upper hose A and low pressure steam pipe C are met, after the cooling medium outlet hose of each chilling roller collects and connects cooling
Medium outlet pipe B and steam condensate (SC) pipe D.
The principle that molten sulfur pond composite cover removes sulphur steam is the sulfur vapor from molten sulfur pond, and it is multiple to rise to molten sulfur pond
When closing lid, sulfur vapor in temperature lower than the chilling roller surface condensation condensation for leading to cooling medium in sulphur fusing point, through after a period of time
Condensation, chilling roller surface can condense one layer of crystalline solid sulphur.When chilling roller is by the timing driving rotation of chilling roller rotation drive device, condensation
The simple substance sulphur on chilling roller surface is set in the case where being cut under bite acts on, falls back to molten sulfur surface under gravity.
The sulphur concentration for diffusing to molten sulfur pool surface is effectively reduced in this kind of equipment, and by sulphur recovery therein, and effectively improves sulphur
Output capacity.
Have that chilling roller is multiple in composite cover body, each chilling roller is respectively equipped with cooling medium and steam inlet and outlet.Under normal circumstances
It is passed through cooling medium in chilling roller, when occurring condensing under the abnormal conditions that sulphur can not be cut in chilling roller, changes logical low-pressure steam and carries out
Melt the sulphur for being condensed in chilling roller surface.
The present invention solves the problems, such as that the sulphur partial vapour pressure in existing Claus method molten sulfur pond is excessively high, and it is stifled to solve elemental sulfur
The problem for filling in pipeline etc., solves molten sulfur pond workplace sulphur condensation problem, solves as caused by sulphur devaporation
Sulphur loses problem, solves the problem of environmental pollution as caused by sulphur steam.
The present invention has rational design, has good practical application and promotional value.
Detailed description of the invention
Fig. 1 shows molten sulfur pond composite cover side views.
Fig. 2 indicates that chilling roller arranges top view in the composite cover of molten sulfur pond.
Fig. 3 indicates molten sulfur pond and composite cover assembling schematic diagram.
In figure: the compound lid of 1-, 2- chilling roller, 3- bite, 4- cooling medium inlet hose, the outlet of 5- cooling medium are soft
Pipe, 6- chilling roller rotation drive device, 7- chilling roller rotate drive chain, 8- molten sulfur pond, 9- chilling roller rotary positioning frame;A- cooling medium
Upper hose, B- cooling medium downcomer, C- low pressure steam pipe, D- steam condensate (SC) pipe.
Specific embodiment
Specific embodiments of the present invention are described in detail with reference to the accompanying drawing.
A kind of molten sulfur pond composite cover removing sulphur steam, including it is lid, chilling roller, bite, chilling roller rotary positioning frame, cold
Roller rotation drive device, chilling roller rotation driving toothed chain.Specific structure is as shown in Figure 1, 2, including compound lid 1, in compound lid 1
Equipped with chilling roller rotary positioning frame 9, the chilling roller 2 that a row (multiple) can rotate, each chilling roller 2 are installed on chilling roller rotary positioning frame 9
One end be fixedly connected with a rotation gear and the gear is fixed on the end of chilling roller, the rotation gear of all 2 ends of chilling roller
It is rotated by chilling roller and is connect after drive chain 7 connects with chilling roller rotation drive device 6, chilling roller rotation is driven by chain conveyer;It is cold
It is located at each 2 side of chilling roller on roller rotary positioning frame 9 and is equipped with bite 3, bite and chilling roller side is clearance fit;It is each cold
2 one end of roller is equipped with cooling medium inlet hose 4, the other end is equipped with cooling medium outlet hose 5, can pass through branch in lid two sides
The fixed cooling medium inlet hose of frame and cooling medium outlet hose, hose is without rotation, the cooling medium at each chilling roller both ends
Connected between inlet hose 4 and cooling medium outlet hose 5 by being located at the heat-exchanging spiral-coil contacted in chilling roller and with chilling roller inner wall
It connects, which only provides heat exchange function, can be fixed by the bracket on chilling roller rotary positioning frame;Each chilling roller 2
After cooling medium inlet hose 4 collects and cooling medium upper hose A and low pressure steam pipe C are met, the cooling medium of each chilling roller 2 goes out
Mouth hose 5, which collects afterwards and connects, is mounted on valve on cooling medium outlet pipe B and steam condensate (SC) pipe D, pipe ABCD.Normal condition
Under, the valve on pipe AB is opened, the valve closure on pipe CD, is passed through cooling medium in the heat exchanger tube in chilling roller;When there is chilling roller
Under the abnormal conditions that upper condensation sulphur can not be cut, the valve on pipe AB is closed, and the valve on pipe CD is opened, the heat exchange in chilling roller
Change logical low-pressure steam in pipe to carry out melting the sulphur for being condensed in chilling roller surface.
When it is implemented, materials'use stainless steel, ceramics, silicon carbide for contacting in compound lid with sulfur vapor etc. are corrosion-resistant
Material.Lead to 20 ~ 55 DEG C of cooling medium in cooling medium pipe, cooling medium can be process recycled water, sulphur washing tail gas circulation
Liquid etc..
When specifically used, as shown in figure 3, compound lid 1 is hingedly installed on molten sulfur pond 8, reserved on compound lid
Cooling medium upper hose A and cooling medium outlet pipe B connect cooling medium source, low pressure steam pipe C and steam condensate (SC) pipe D connect low
Press vapour source.
The method that molten sulfur pond composite cover removes sulphur steam, (1) sulphur condensation condensation: from 135 ~ 155 DEG C of molten sulfurs of pond temperature
The sulfur vapor in pond, when rising to molten sulfur pond composite cover, sulfur vapor is in temperature lower than 20 ~ 55 DEG C of cooling mediums logical in sulphur fusing point
The condensation of chilling roller surface condensation, through condensation after a period of time, chilling roller surface can condense one layer of crystalline solid sulphur;(2) sulphur is cut back
It receives: being set in the simple substance sulphur on chilling roller surface, in chilling roller timing rotation, under being cut under bite effect,
Molten sulfur surface is fallen back under the action of gravity.In addition, chilling roller rotation drive device can also drive chilling roller to reversely rotate.Next
It after a condensation condensation period, reversely rotates, condensation sulphur, which is also cut, in chilling roller drops back into molten sulfur surface.
Illustrate the beneficial effect that the present invention obtains below by specific implementation process.
Example 1: industrial molten sulfur pool volume is 20m3, molten sulfur height 2m, 150 DEG C of molten sulfur temperature, at the 5m of molten sulfur pond in air
Elemental sulfur powder concn 0.3g/m3.Start after being passed through 30 DEG C of process recycled waters in molten sulfur composite cover, operating parameter is setting time
9 minutes, rotary cutting 3 minutes, concentration of elemental substance sulfur in air was lower than 1mg/m at the 5m of molten sulfur pond3。
Example 2: industrial molten sulfur pool volume is 20m3, molten sulfur height 1.5m, 140 DEG C of molten sulfur temperature, air at the 5m of molten sulfur pond
Middle simple substance sulphur concentration 0.5g/m3.Molten sulfur lid starts after being passed through 20 DEG C of process recycled waters, and operating parameter is setting time 7 minutes, rotation
Turn cutting 2 minutes, concentration of elemental substance sulfur in air is lower than 1mg/m at the 5m of molten sulfur pond3。
In short, the molten sulfur pond composite cover provided by the invention for removing sulphur steam and the method for removing sulphur steam can have
Effect prevents to condense the generation of phenomenon everywhere in workplace due to sulphur steam in sulfur cream, improves the working environment of worker
Quality.
Embodiments above only does illustrative explanation to the present invention, and the case study on implementation detail is merely to explanation
The present invention does not represent whole technical solutions under present inventive concept, any that essentially identical technology is solved based on the present invention
Problem, or realize essentially identical technical effect, made ground simple change, equivalent replacement or modification etc. belong to this hair
In bright protection scope.
Claims (1)
1. a kind of molten sulfur pond composite cover for removing sulphur steam, it is characterised in that: including compound lid (1), the compound lid
(1) chilling roller rotary positioning frame (9) are equipped in, the chilling roller (2) that a row can rotate is installed on the chilling roller rotary positioning frame (9),
The one end of each chilling roller (2) is fixedly connected with a rotation gear, and the rotation gear of all chilling roller (2) ends is rotated by chilling roller
It is connect after drive chain (7) connection with chilling roller rotation drive device (6);It is located on the chilling roller rotary positioning frame (9) each cold
Roller (2) side is equipped with bite (3);Each chilling roller (2) one end is equipped with cooling medium inlet hose (4), the other end is equipped with cooling
Media outlet hose (5), by being located at chilling roller between the cooling medium inlet hose (4) and cooling medium outlet hose (5)
Heat-exchanging spiral-coil connection that is interior and being contacted with chilling roller inner wall;The cooling medium inlet hose (4) of each chilling roller (2) collect after simultaneously
Cooling medium upper hose A and low pressure steam pipe C are met, after the cooling medium outlet hose (5) of each chilling roller (2) collects and connects cooling
Medium outlet pipe B and steam condensate (SC) pipe D.
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CN201910321159.6A CN109928368B (en) | 2019-04-22 | 2019-04-22 | Liquid sulfur pool composite cover for recovering sulfur vapor |
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CN201910321159.6A CN109928368B (en) | 2019-04-22 | 2019-04-22 | Liquid sulfur pool composite cover for recovering sulfur vapor |
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CN109928368A true CN109928368A (en) | 2019-06-25 |
CN109928368B CN109928368B (en) | 2023-12-01 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111908430A (en) * | 2020-06-19 | 2020-11-10 | 宁波市化工研究设计院有限公司 | Method for treating solid waste sulfur |
Citations (9)
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FR1220337A (en) * | 1958-02-18 | 1960-05-24 | Blaw Knox Co | Improvements in sulfur treatment |
US5204082A (en) * | 1991-07-18 | 1993-04-20 | C.F. Braun Inc. | Sulfur dioxide generation by submerged combustion and reduced thermal cycling by use of a hot recycle of sulfur |
KR19990051974A (en) * | 1997-12-20 | 1999-07-05 | 이구택 | Improvement of Sulfur Capture Efficiency from Oxidation Furnace for Liquid Sulfur Generation |
CN102344121A (en) * | 2011-06-27 | 2012-02-08 | 张宪诚 | Purification method of industrial waste sulfur |
CN204078535U (en) * | 2014-08-15 | 2015-01-07 | 中国石油天然气股份有限公司长庆石化分公司 | Heating module formula molten sulfur pond heating coil |
CN107511048A (en) * | 2017-09-08 | 2017-12-26 | 中冶焦耐(大连)工程技术有限公司 | A kind of Claus tail gases condensation process technique |
CN207404840U (en) * | 2017-11-13 | 2018-05-25 | 江苏沙钢集团有限公司 | Full-automatic cooling and packaging sulphur unit |
CN109569290A (en) * | 2018-12-29 | 2019-04-05 | 山东齐创石化工程有限公司 | Tail gas of sulphur discharge process technique and device |
CN209740707U (en) * | 2019-04-22 | 2019-12-06 | 山西焦煤集团有限责任公司 | Liquid sulfur pool device for effectively recovering sulfur |
-
2019
- 2019-04-22 CN CN201910321159.6A patent/CN109928368B/en active Active
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR1220337A (en) * | 1958-02-18 | 1960-05-24 | Blaw Knox Co | Improvements in sulfur treatment |
US5204082A (en) * | 1991-07-18 | 1993-04-20 | C.F. Braun Inc. | Sulfur dioxide generation by submerged combustion and reduced thermal cycling by use of a hot recycle of sulfur |
KR19990051974A (en) * | 1997-12-20 | 1999-07-05 | 이구택 | Improvement of Sulfur Capture Efficiency from Oxidation Furnace for Liquid Sulfur Generation |
CN102344121A (en) * | 2011-06-27 | 2012-02-08 | 张宪诚 | Purification method of industrial waste sulfur |
CN204078535U (en) * | 2014-08-15 | 2015-01-07 | 中国石油天然气股份有限公司长庆石化分公司 | Heating module formula molten sulfur pond heating coil |
CN107511048A (en) * | 2017-09-08 | 2017-12-26 | 中冶焦耐(大连)工程技术有限公司 | A kind of Claus tail gases condensation process technique |
CN207404840U (en) * | 2017-11-13 | 2018-05-25 | 江苏沙钢集团有限公司 | Full-automatic cooling and packaging sulphur unit |
CN109569290A (en) * | 2018-12-29 | 2019-04-05 | 山东齐创石化工程有限公司 | Tail gas of sulphur discharge process technique and device |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN111908430A (en) * | 2020-06-19 | 2020-11-10 | 宁波市化工研究设计院有限公司 | Method for treating solid waste sulfur |
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