CN109913137A - A kind of cleaning paper self-adhesive tape is with destaticing binder and preparation method thereof - Google Patents
A kind of cleaning paper self-adhesive tape is with destaticing binder and preparation method thereof Download PDFInfo
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- CN109913137A CN109913137A CN201910034020.3A CN201910034020A CN109913137A CN 109913137 A CN109913137 A CN 109913137A CN 201910034020 A CN201910034020 A CN 201910034020A CN 109913137 A CN109913137 A CN 109913137A
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Abstract
The present invention provides a kind of cleaning paper self-adhesive tape with binder and preparation method thereof is destaticed, and is related to binder processing technique field.The cleaning paper self-adhesive tape is made of raw material from the following weight with binder is destaticed: 90-100 parts of epoxy resin, 12-18 parts of acrylic resin, 4-6 parts of butyl acrylate, 4-8 parts of salicylide, 3-5 parts of nano-graphene, 4-7 parts of nano zine oxide, 6-10 parts of zinc Isoocatanoate, 2-4 parts of barium sulfate, 3-5 parts of acrylic acid hydroxyl second, 1-2 parts of plasticizer, 1-1.8 parts of dispersing agent, 1-2 parts of antioxidant.Preparation method specifically include that heat melt mixing, high steam processs, concussion homogeneous, stirring heat preservation and etc..The present invention overcomes the deficiencies in the prior art, add various metals ion, make product have effects that eliminate electrostatic, and product caking property is good, ingredient safety and environmental protection, production is suitble to promote.
Description
Technical field
The present invention relates to binder processing technique fields, and in particular to a kind of cleaning paper self-adhesive tape with destatic binder and its
Preparation method.
Background technique
Cleaning paper self-adhesive tape is that one kind is cylindrical, and binder is on the outside of adhesive tape, and rolling tape is using binder viscosity clothing
The dust adherency that the surfaces such as object, textile fabric, knitting wool are covered with the article of fiber removes, and reaches a kind of product of clean effect.
The cleaning most important ingredient of paper self-adhesive tape is binder, and the quality of binder directly determines the cleaning of cleaning paper self-adhesive tape
Degree and have to cleaning products it is not damaged, it is existing cleaning paper self-adhesive tape binder can accomplish effective sticky removing clothing mostly
The dust on the surfaces such as object, and it is small to clothing damaging, but autumn and winter arrives, clothing, textile fabric, knitting wool and other items are easy
Electrostatic Absorption dust is carried, although cleaning paper self-adhesive tape can remove dust, quickly due to electrostatic interaction clothing and other items meeting again
Gathering dust weakens cleaning effect significantly, and impacts to daily life quality, so adhering to cleaning paper adhesive tape
It is the general orientation studied now that electrostatic is eliminated while dust.
Summary of the invention
In view of the shortcomings of the prior art, the present invention provides a kind of cleaning paper self-adhesive tape with destaticing binder and preparation method thereof,
Various metals ion is added, makes product have effects that eliminate electrostatic, and product caking property is good, ingredient safety and environmental protection, is suitble to
Production is promoted.
In order to achieve the above object, technical solution of the present invention is achieved by the following technical programs:
A kind of cleaning paper self-adhesive tape is with destaticing binder, and the cleaning paper self-adhesive tape is with destaticing binder by following parts by weight
Raw material be made: 90-100 parts of epoxy resin, 4-6 parts of butyl acrylate, 4-8 parts of salicylide, is received 12-18 parts of acrylic resin
3-5 parts of graphene of rice, 4-7 parts of nano zine oxide, 6-10 parts of zinc Isoocatanoate, 2-4 parts of barium sulfate, 3-5 parts of acrylic acid hydroxyl second, plasticising
1-2 parts of agent, 1-1.8 parts of dispersing agent, 1-2 parts of antioxidant.
Preferably, the cleaning paper self-adhesive tape is made of raw material from the following weight with binder is destaticed: epoxy resin 95
Part, 15 parts of acrylic resin, 5 parts of butyl acrylate, 6 parts of salicylide, 4 parts of nano-graphene, 6 parts of nano zine oxide, isooctyl acid
8 parts of zinc, 3 parts of barium sulfate, 4 parts of acrylic acid hydroxyl second, 1.5 parts of plasticizer, 1.4 parts of dispersing agent, 1.5 parts of antioxidant.
Preferably, the plasticizer is phthalic acid two (2- ethyl hexyl) ester, adipate ester, phosphate, carboxymethyl fibre
Tie up the mixture that plain sodium mass ratio is 6: 2: 2: 1.
Preferably, the dispersing agent is triethyl group hexyl phosphoric acid, lauryl sodium sulfate, methyl anyl alcohol, polyacrylamide
At least one of.
Preferably, the antioxidant is 2,6- three-level butyl -4- methylphenol, pentaerythritol ester, three monooctyl ester mass ratioes 1
: 3: 1 mixture.
It is described cleaning paper self-adhesive tape with destatic binder preparation method the following steps are included:
(1) it stirs, obtains mixed in blender high speed after melting epoxy resin, acrylic resin, the butyl acrylate heat of mixing
Resin is spare；
(2) nano-graphene, salicylide is added in blender after mixing evenly in above-mentioned hybrid resin, then placed it in
In high steam pot, 60-80min is handled using high-pressure hot steam, it is spare to obtain mixed resin；
(3) will above-mentioned mixed resin it is dry after be ground up, sieved, obtain mixed-powder, by mixed-powder, nano zine oxide,
Deionized water is added after zinc Isoocatanoate, barium sulfate, the mixing of acrylic acid hydroxyl second, carries out shaking in ultrasonic vibration instrument after stirring
It is spare to obtain homogenizing fluid for matter；
(4) plasticizer, dispersing agent and antioxidant is added in above-mentioned homogenizing fluid, after heating in blender insulated and stirred one
The section time stands cooling cleaning paper self-adhesive tape of the invention with destaticing binder afterwards.
Preferably, the temperature of mixing hot melt is 160-180 DEG C in the step (1), and the revolving speed of high-speed stirred is 1200-
1400r/min, mixing time 15-20min.
Preferably, the revolving speed stirred evenly in the step (2) be 400-600r/min, mixing time 10-15min,
And pressure when high-pressure hot steam processing is 18-20MPa, and temperature is 90-100 DEG C, and the processing time is 20-30min.
Preferably, ground 620 mesh of mixed resin in the step (3), addition deionized water are mixed-powder, nanometer
Zinc oxide, zinc Isoocatanoate, barium sulfate, 3-5 times of acrylic acid hydroxyl second mixed volume, the frequency of ultrasonic vibration are 40KHz, power
For 120W, homogenizing time 5-8min.
Preferably, the temperature heated in the step (4) is 60-80 DEG C, and the revolving speed of blender stirring is 200-400r/
Min, mixing time 40-50min.
The present invention provides a kind of cleaning paper self-adhesive tape with binder and preparation method thereof is destaticed, compared with prior art advantage
It is:
(1) present invention is added with the substances such as nano-graphene, nano zine oxide, zinc Isoocatanoate, barium sulfate in a binder,
It is used after effectively making product binder preparation cleaning paper self-adhesive tape, the electrostatic on the surfaces such as clothing can be removed, promote the use effect of product
Fruit and function.
(2) present invention is adopted after being mixed using epoxy resin, acrylic resin, butyl acrylate, nano-graphene, salicylide
It is handled with high-pressure hot steam, can effectively enhance the stability of product, enhanced the active force of substance between product, prevent later period binder
Remain on the using effect on cleaning products, being promoted product when use.
(3) by the way of the present invention mixes homogeneous after by base-material drying and grinding, effectively each component is uniformly mixed, is promoted
The stability of product, reinforces the using effect of product, and reduces mixing temperature, reduces production cost, promotes economic benefit.
Specific embodiment
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below with reference to the embodiment of the present invention pair
Technical solution in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is a part of the invention
Embodiment, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not making wound
Every other embodiment obtained under the premise of the property made labour, shall fall within the protection scope of the present invention.
Embodiment 1:
A kind of cleaning paper self-adhesive tape is with destaticing binder, and the cleaning paper self-adhesive tape is with destaticing binder by following parts by weight
Raw material be made: 90 parts of epoxy resin, 12 parts of acrylic resin, 4 parts of butyl acrylate, 4 parts of salicylide, 3 parts of nano-graphene,
It is 4 parts of nano zine oxide, 6 parts of zinc Isoocatanoate, 2 parts of barium sulfate, 3 parts of acrylic acid hydroxyl second, 1 part of plasticizer, 1 part of dispersing agent, anti-oxidant
1 part of agent.
The plasticizer is phthalic acid two (2- ethyl hexyl) ester, adipate ester, phosphate, sodium carboxymethylcellulose matter
Amount is than the mixture for 6: 2: 2: 1；The dispersing agent is triethyl group hexyl phosphoric acid, lauryl sodium sulfate, methyl anyl alcohol, poly- third
At least one of acrylamide；The antioxidant is 2,6- three-level butyl -4- methylphenol, pentaerythritol ester, three monooctyl ester matter
Amount compares 1: 3: 1 mixture.
Cleaning paper self-adhesive tape with destatic binder preparation method the following steps are included:
(1) it stirs, obtains mixed in blender high speed after melting epoxy resin, acrylic resin, the butyl acrylate heat of mixing
Resin is spare；
(2) nano-graphene, salicylide is added in blender after mixing evenly in above-mentioned hybrid resin, then placed it in
In high steam pot, 60-80min is handled using high-pressure hot steam, it is spare to obtain mixed resin；
(3) will above-mentioned mixed resin it is dry after be ground up, sieved, obtain mixed-powder, by mixed-powder, nano zine oxide,
Deionized water is added after zinc Isoocatanoate, barium sulfate, the mixing of acrylic acid hydroxyl second, carries out shaking in ultrasonic vibration instrument after stirring
It is spare to obtain homogenizing fluid for matter；
(4) plasticizer, dispersing agent and antioxidant is added in above-mentioned homogenizing fluid, after heating in blender insulated and stirred one
The section time stands cooling cleaning paper self-adhesive tape of the invention with destaticing binder afterwards.
Wherein, the temperature of mixing hot melt is 160-180 DEG C in the step (1), and the revolving speed of high-speed stirred is 1200-
1400r/min, mixing time 15-20min；The revolving speed stirred evenly in the step (2) is 400-600r/min, when stirring
Between be 10-15min, and high-pressure hot steam handle when pressure be 18-20MPa, temperature be 90-100 DEG C, processing the time be
20-30min；Ground 620 mesh of mixed resin in the step (3), addition deionized water are mixed-powder, nano oxidized
The frequency of zinc, zinc Isoocatanoate, barium sulfate, 3-5 times of acrylic acid hydroxyl second mixed volume, ultrasonic vibration is 40KHz, and power is
120W, homogenizing time 5-8min；The temperature heated in the step (4) is 60-80 DEG C, and the revolving speed of blender stirring is 200-
400r/min, mixing time 40-50min.
Embodiment 2:
A kind of cleaning paper self-adhesive tape is with destaticing binder, and the cleaning paper self-adhesive tape is with destaticing binder by following parts by weight
Raw material be made: 100 parts of epoxy resin, 18 parts of acrylic resin, 6 parts of butyl acrylate, 8 parts of salicylide, nano-graphene 5
Part, 7 parts of nano zine oxide, 10 parts of zinc Isoocatanoate, 4 parts of barium sulfate, 5 parts of acrylic acid hydroxyl second, 2 parts of plasticizer, 1.8 parts of dispersing agent,
2 parts of antioxidant.
The plasticizer is phthalic acid two (2- ethyl hexyl) ester, adipate ester, phosphate, sodium carboxymethylcellulose matter
Amount is than the mixture for 6: 2: 2: 1；The dispersing agent is triethyl group hexyl phosphoric acid, lauryl sodium sulfate, methyl anyl alcohol, poly- third
At least one of acrylamide；The antioxidant is 2,6- three-level butyl -4- methylphenol, pentaerythritol ester, three monooctyl ester matter
Amount compares 1: 3: 1 mixture.
Cleaning paper self-adhesive tape with destatic binder preparation method the following steps are included:
(1) it stirs, obtains mixed in blender high speed after melting epoxy resin, acrylic resin, the butyl acrylate heat of mixing
Resin is spare；
(2) nano-graphene, salicylide is added in blender after mixing evenly in above-mentioned hybrid resin, then placed it in
In high steam pot, 60-80min is handled using high-pressure hot steam, it is spare to obtain mixed resin；
(3) will above-mentioned mixed resin it is dry after be ground up, sieved, obtain mixed-powder, by mixed-powder, nano zine oxide,
Deionized water is added after zinc Isoocatanoate, barium sulfate, the mixing of acrylic acid hydroxyl second, carries out shaking in ultrasonic vibration instrument after stirring
It is spare to obtain homogenizing fluid for matter；
(4) plasticizer, dispersing agent and antioxidant is added in above-mentioned homogenizing fluid, after heating in blender insulated and stirred one
The section time stands cooling cleaning paper self-adhesive tape of the invention with destaticing binder afterwards.
Wherein, the temperature of mixing hot melt is 160-180 DEG C in the step (1), and the revolving speed of high-speed stirred is 1200-
1400r/min, mixing time 15-20min；The revolving speed stirred evenly in the step (2) is 400-600r/min, when stirring
Between be 10-15min, and high-pressure hot steam handle when pressure be 18-20MPa, temperature be 90-100 DEG C, processing the time be
20-30min；Ground 620 mesh of mixed resin in the step (3), addition deionized water are mixed-powder, nano oxidized
The frequency of zinc, zinc Isoocatanoate, barium sulfate, 3-5 times of acrylic acid hydroxyl second mixed volume, ultrasonic vibration is 40KHz, and power is
120W, homogenizing time 5-8min；The temperature heated in the step (4) is 60-80 DEG C, and the revolving speed of blender stirring is 200-
400r/min, mixing time 40-50min.
Embodiment 3:
A kind of cleaning paper self-adhesive tape is with destaticing binder, and the cleaning paper self-adhesive tape is with destaticing binder by following parts by weight
Raw material be made: 95 parts of epoxy resin, 15 parts of acrylic resin, 5 parts of butyl acrylate, 6 parts of salicylide, 4 parts of nano-graphene,
6 parts of nano zine oxide, 3 parts of barium sulfate, 4 parts of acrylic acid hydroxyl second, 1.5 parts of plasticizer, 1.4 parts of dispersing agent, resists 8 parts of zinc Isoocatanoate
1.5 parts of oxidant.
The plasticizer is phthalic acid two (2- ethyl hexyl) ester, adipate ester, phosphate, sodium carboxymethylcellulose matter
Amount is than the mixture for 6: 2: 2: 1；The dispersing agent is triethyl group hexyl phosphoric acid, lauryl sodium sulfate, methyl anyl alcohol, poly- third
At least one of acrylamide；The antioxidant is 2,6- three-level butyl -4- methylphenol, pentaerythritol ester, three monooctyl ester matter
Amount compares 1: 3: 1 mixture.
Cleaning paper self-adhesive tape with destatic binder preparation method the following steps are included:
(1) it stirs, obtains mixed in blender high speed after melting epoxy resin, acrylic resin, the butyl acrylate heat of mixing
Resin is spare；
(2) nano-graphene, salicylide is added in blender after mixing evenly in above-mentioned hybrid resin, then placed it in
In high steam pot, 60-80min is handled using high-pressure hot steam, it is spare to obtain mixed resin；
(3) will above-mentioned mixed resin it is dry after be ground up, sieved, obtain mixed-powder, by mixed-powder, nano zine oxide,
Deionized water is added after zinc Isoocatanoate, barium sulfate, the mixing of acrylic acid hydroxyl second, carries out shaking in ultrasonic vibration instrument after stirring
It is spare to obtain homogenizing fluid for matter；
(4) plasticizer, dispersing agent and antioxidant is added in above-mentioned homogenizing fluid, after heating in blender insulated and stirred one
The section time stands cooling cleaning paper self-adhesive tape of the invention with destaticing binder afterwards.
Wherein, the temperature of mixing hot melt is 160-180 DEG C in the step (1), and the revolving speed of high-speed stirred is 1200-
1400r/min, mixing time 15-20min；The revolving speed stirred evenly in the step (2) is 400-600r/min, when stirring
Between be 10-15min, and high-pressure hot steam handle when pressure be 18-20MPa, temperature be 90-100 DEG C, processing the time be
20-30min；Ground 620 mesh of mixed resin in the step (3), addition deionized water are mixed-powder, nano oxidized
The frequency of zinc, zinc Isoocatanoate, barium sulfate, 3-5 times of acrylic acid hydroxyl second mixed volume, ultrasonic vibration is 40KHz, and power is
120W, homogenizing time 5-8min；The temperature heated in the step (4) is 60-80 DEG C, and the revolving speed of blender stirring is 200-
400r/min, mixing time 40-50min.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.In the absence of more restrictions, the element limited by sentence "including a ...", it is not excluded that
There is also other identical elements in process, method, article or equipment including the element.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although with reference to the foregoing embodiments
Invention is explained in detail, those skilled in the art should understand that: it still can be to aforementioned each implementation
Technical solution documented by example is modified or equivalent replacement of some of the technical features；And these modification or
Replacement, the spirit and scope for technical solution of various embodiments of the present invention that it does not separate the essence of the corresponding technical solution.
Claims (10)
1. a kind of cleaning paper self-adhesive tape is with destaticing binder, which is characterized in that the cleaning paper self-adhesive tape with destatic binder by
The raw material of following parts by weight is made: 90-100 parts of epoxy resin, 12-18 parts of acrylic resin, 4-6 parts of butyl acrylate, bigcatkin willow
4-8 parts of aldehyde, 3-5 parts of nano-graphene, 4-7 parts of nano zine oxide, 6-10 parts of zinc Isoocatanoate, 2-4 parts of barium sulfate, acrylic acid hydroxyl second
3-5 parts, 1-2 parts of plasticizer, 1-1.8 parts of dispersing agent, 1-2 parts of antioxidant.
2. a kind of cleaning paper self-adhesive tape according to claim 1 is with destaticing binder, which is characterized in that the cleaning paper glue
Band is made of raw material from the following weight with binder is destaticed: 95 parts of epoxy resin, 15 parts of acrylic resin, butyl acrylate
5 parts, 6 parts of salicylide, 4 parts of nano-graphene, 6 parts of nano zine oxide, 8 parts of zinc Isoocatanoate, 3 parts of barium sulfate, acrylic acid hydroxyl second 4
Part, 1.5 parts of plasticizer, 1.4 parts of dispersing agent, 1.5 parts of antioxidant.
3. a kind of cleaning paper self-adhesive tape according to claim 1 is with destaticing binder, it is characterised in that: the plasticizer is
Phthalic acid two (2- ethyl hexyl) ester, adipate ester, phosphate, the mixing that sodium carboxymethylcellulose mass ratio is 6: 2: 2: 1
Object.
4. a kind of cleaning paper self-adhesive tape according to claim 1 is with destaticing binder, it is characterised in that: the dispersing agent is
At least one of triethyl group hexyl phosphoric acid, lauryl sodium sulfate, methyl anyl alcohol, polyacrylamide.
5. a kind of cleaning paper self-adhesive tape according to claim 1 is with destaticing binder, it is characterised in that: the antioxidant
For 2,6- three-level butyl -4- methylphenol, pentaerythritol ester, three monooctyl ester mass ratioes 1: 3: 1 mixture.
6. a kind of cleaning paper self-adhesive tape preparation method for destaticing binder, which is characterized in that the cleaning paper self-adhesive tape is quiet with removing
The preparation method of electric binder the following steps are included:
(1) it is stirred after melting epoxy resin, acrylic resin, the butyl acrylate heat of mixing in blender high speed, obtains compound tree
Rouge is spare；
(2) nano-graphene, salicylide is added in blender after mixing evenly in above-mentioned hybrid resin, then places it in high pressure
In steam copper, 60-80min is handled using high-pressure hot steam, it is spare to obtain mixed resin；
(3) will above-mentioned mixed resin it is dry after be ground up, sieved, mixed-powder is obtained, by mixed-powder, nano zine oxide, different pungent
Deionized water is added after sour zinc, barium sulfate, the mixing of acrylic acid hydroxyl second, carries out concussion homogeneous after stirring in ultrasonic vibration instrument, obtains
Homogenizing fluid is spare；
(4) plasticizer, dispersing agent and antioxidant is added in above-mentioned homogenizing fluid, after heating in blender at one section of insulated and stirred
Between, cooling cleaning paper self-adhesive tape of the invention is stood afterwards with destaticing binder.
7. a kind of cleaning paper self-adhesive tape preparation method for destaticing binder according to claim 6, it is characterised in that: institute
The temperature for stating mixing hot melt in step (1) is 160-180 DEG C, and the revolving speed of high-speed stirred is 1200-1400r/min, mixing time
For 15-20min.
8. a kind of cleaning paper self-adhesive tape preparation method for destaticing binder according to claim 6, it is characterised in that: institute
Stating the revolving speed stirred evenly in step (2) is 400-600r/min, mixing time 10-15min, and high-pressure hot steam is handled
When pressure be 18-20MPa, temperature be 90-100 DEG C, the processing time be 20-30min.
9. a kind of cleaning paper self-adhesive tape preparation method for destaticing binder according to claim 6, it is characterised in that: institute
State ground 620 mesh of mixed resin in step (3), addition deionized water be mixed-powder, nano zine oxide, zinc Isoocatanoate,
3-5 times of barium sulfate, acrylic acid hydroxyl second mixed volume, the frequency of ultrasonic vibration are 40KHz, power 120W, homogenizing time
For 5-8min.
10. a kind of cleaning paper self-adhesive tape preparation method for destaticing binder according to claim 6, it is characterised in that:
The temperature heated in the step (4) is 60-80 DEG C, and the revolving speed of blender stirring is 200-400r/min, mixing time 40-
50min。
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| CN201910034020.3A CN109913137A (en) | 2019-01-15 | 2019-01-15 | A kind of cleaning paper self-adhesive tape is with destaticing binder and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910034020.3A CN109913137A (en) | 2019-01-15 | 2019-01-15 | A kind of cleaning paper self-adhesive tape is with destaticing binder and preparation method thereof |
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ID=66960296
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Application publication date: 20190621 |