CN106400598A - Preparation method of alternanthera philoxeroides reinforced type air filter paper - Google Patents

Preparation method of alternanthera philoxeroides reinforced type air filter paper Download PDF

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Publication number
CN106400598A
CN106400598A CN201610778337.4A CN201610778337A CN106400598A CN 106400598 A CN106400598 A CN 106400598A CN 201610778337 A CN201610778337 A CN 201610778337A CN 106400598 A CN106400598 A CN 106400598A
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CN
China
Prior art keywords
filter paper
air filter
glass fiber
enhancement mode
short glass
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610778337.4A
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Chinese (zh)
Inventor
张申元
林凯
赵海飞
潘建峰
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SUZHOU HUATAI AIR FILTER CO Ltd
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SUZHOU HUATAI AIR FILTER CO Ltd
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Priority to CN201610778337.4A priority Critical patent/CN106400598A/en
Publication of CN106400598A publication Critical patent/CN106400598A/en
Pending legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H27/00Special paper not otherwise provided for, e.g. made by multi-step processes
    • D21H27/08Filter paper
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B17/00Layered products essentially comprising sheet glass, or glass, slag, or like fibres
    • B32B17/02Layered products essentially comprising sheet glass, or glass, slag, or like fibres in the form of fibres or filaments
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B37/00Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
    • B32B37/12Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by using adhesives
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C5/00Other processes for obtaining cellulose, e.g. cooking cotton linters ; Processes characterised by the choice of cellulose-containing starting materials
    • D21C5/005Treatment of cellulose-containing material with microorganisms or enzymes
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21FPAPER-MAKING MACHINES; METHODS OF PRODUCING PAPER THEREON
    • D21F13/00Making discontinuous sheets of paper, pulpboard or cardboard, or of wet web, for fibreboard production
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H13/00Pulp or paper, comprising synthetic cellulose or non-cellulose fibres or web-forming material
    • D21H13/36Inorganic fibres or flakes
    • D21H13/38Inorganic fibres or flakes siliceous
    • D21H13/40Inorganic fibres or flakes siliceous vitreous, e.g. mineral wool, glass fibres
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/02Material of vegetable origin
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/20Macromolecular organic compounds
    • D21H17/33Synthetic macromolecular compounds
    • D21H17/46Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D21H17/52Epoxy resins
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/20Macromolecular organic compounds
    • D21H17/33Synthetic macromolecular compounds
    • D21H17/46Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D21H17/54Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen
    • D21H17/55Polyamides; Polyaminoamides; Polyester-amides
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/20Macromolecular organic compounds
    • D21H17/33Synthetic macromolecular compounds
    • D21H17/46Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D21H17/54Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen
    • D21H17/56Polyamines; Polyimines; Polyester-imides
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/14Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2250/00Layers arrangement
    • B32B2250/20All layers being fibrous or filamentary
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2255/00Coating on the layer surface
    • B32B2255/02Coating on the layer surface on fibrous or filamentary layer
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2262/00Composition or structural features of fibres which form a fibrous or filamentary layer or are present as additives
    • B32B2262/10Inorganic fibres
    • B32B2262/101Glass fibres

Abstract

The invention discloses a preparation method of alternanthera philoxeroides reinforced type air filter paper; the novel air filter paper is prepared by using chopped glass fibers with different fiber diameters and glass wool fibers, and at the same time, alternanthera philoxeroides is added for further improving the filtering effect. The process is simple and reasonable, the finished product rate is high, the production cost is low, the chopped glass fibers with different fiber diameters and the glass wool fibers are used for preparing the double-layer composite type air filter paper, the filtering efficiency is improved, moreover, the wind dragging is reduced, the dust holding capacity is improved, the alternanthera philoxeroides additive is increased, the filtering effect of formaldehyde and other harmful gases can be further improved on one hand, and the dust holding capacity is further increased.

Description

A kind of preparation method of water peanut enhancement mode air filter paper
Technical field
The present invention relates to field of air filtration, more particularly, to a kind of preparation method of water peanut enhancement mode air filter paper.
Background technology
Air filter paper, as the critical piece of high efficiency particulate air filter, decides the filter efficiency of high efficiency particulate air filter.Air mistake The fibre diameter of filter paper is less, and the particle diameter removing in the air microgranule is less, and filter efficiency is also higher, but relative windage Bigger, the rate of filtration is slower, and dust containing capacity reduces.Traditional single filter paper cannot meet the air to high-quality for the people Require that of environment, therefore a kind of filter efficiency of demand are high, the air filter of the big composite highly effective of dust containing capacity.
Water peanut, as a kind of common water plant, does not only never utilize, simultaneously because excessive multiplication, once The balance of harm aquatic environment.
Content of the invention
Goal of the invention:The present invention is to solve the above problems, there is provided a kind of preparation of water peanut enhancement mode air filter paper Method.
Technical scheme:A kind of preparation method of water peanut enhancement mode air filter paper, comprises the following steps:
Step 1, water intaking Semen arachidis hypogaeae grinds making beating, is subsequently adding protease and saccharifying enzyme, and keeping temperature is 28-35 DEG C, standing 60-72 hour, is then centrifuged, and rotating speed is 3500r/min, takes lower sediment thing to dry, is ground to more than 200 mesh, Add water and make the solution that concentration is 2%, add dispersant, stir, make water peanut additive;
Step 2, take average diameter 6-10 μm short glass fiber add pH value pull an oar in the saline solution of 6-8, plus Enter dispersant, then discongested on fluffer, discongest revolution and turn for 10000-15000;
Step 3, adds polyamide polyamine epichlorhydrin resin solution, so in the short glass fiber solution to after discongest Molding on wet moulding machine afterwards, makes short glass fiber handsheet, puts into drying and moulding in drying machine, and baking temperature is 70-90 DEG C, make short glass fiber filter paper;
Step 4, in a face coated with adhesive of short glass fiber filter paper, then uniformly coats water peanut on binding agent Additive, is dried 30-60min at 30-35 DEG C;
Step 5, goes glass cotton below 2 μm for the average diameter to add pH value to pull an oar in the acid solution of 5-6, adds dispersion Agent, is then discongested on fluffer, discongests revolution and turns for 15000-25000;
Step 6, the glass cotton after discongesting is put into molding on wet moulding machine, and the staple glass after step 4 is processed Fiber filter paper is placed on forming net, makes glass cotton coat to become in the one side of water peanut additive in short glass fiber filter paper Type, then 80-100 DEG C of drying, makes water peanut enhancement mode air filter paper.
As a preferred embodiment of the present invention, polyamide polyamine epichlorhydrin resin solution described in step 3 dense Spend for 0.5-1%.
As a preferred embodiment of the present invention, the short glass fiber layer of described water peanut enhancement mode air filter paper Thickness is 1 with the ratio of the thickness of glass cotton layer:2-1∶1.
As a preferred embodiment of the present invention, described water peanut enhancement mode air filter paper thickness is 0.5-0.6mm.
Beneficial effect:The present invention compared with prior art, has an advantage in that, present invention process advantages of simple, high yield rate, Low production cost, makes the air filtration of double-layer composite using the different short glass fiber of fibre diameter and microglass fiber Paper, improves filter efficiency, reduces windage simultaneously, improves dust containing capacity, increases water peanut additive simultaneously, on the one hand permissible Improve the filter effect of the harmful gass such as PARA FORMALDEHYDE PRILLS(91,95) further, and further increase the dust containing capacity of the present invention.
Specific embodiment
With reference to specific embodiment, it is further elucidated with the present invention.
Embodiment
A kind of preparation method of water peanut enhancement mode air filter paper, comprises the following steps:
Step 1, water intaking Semen arachidis hypogaeae grinds making beating, is subsequently adding protease and saccharifying enzyme, and keeping temperature is 28-35 DEG C, standing 60-72 hour, is then centrifuged, and rotating speed is 3500r/min, takes lower sediment thing to dry, is ground to more than 200 mesh, Add water and make the solution that concentration is 2%, add dispersant, stir, make water peanut additive;
Step 2, take average diameter 6-10 μm short glass fiber add pH value pull an oar in the saline solution of 6-8, plus Enter dispersant, then discongested on fluffer, discongest revolution and turn for 10000-15000;
Step 3, adds polyamide polyamine epichlorhydrin resin solution, so in the short glass fiber solution to after discongest Molding on wet moulding machine afterwards, makes short glass fiber handsheet, puts into drying and moulding in drying machine, and baking temperature is 70-90 DEG C, make short glass fiber filter paper;Polyamide polyamine epichlorhydrin resin is added to be prevented from two-layer compound tense short Cut glass fiber filter paper surface fracture, during polyamide polyamine epichlorhydrin resin solution is mixed with fibrous raw material, Because polyamide polyamine epichlorhydrin resin is in cationic, and fibrous raw material is in often anionic property in the solution, quiet In the presence of electro-adsorption, PPE resin can be adsorbed to the surface of fiber during mixing with comparalive ease.Thereafter, exist In dry run after fiberizing, it is adsorbed between the polyamide polyamine epichlorhydrin molecular resin of fiber surface and gathers Amide polymeric amine epichlorohydrin molecular resin and the chemical group of fiber surface, such as hydroxyl, carboxyl etc. crosslinks reaction, is formed The covalent bond of the water resistants such as methylene ether link, makes the combination between fiber have a water resisting property.When again running into water after filter material is dried, Filter material can have certain intensity, without frotation and breakage.Described polyamide polyamine epichlorhydrin resin is molten The concentration of liquid is preferably 0.5-1%.
Step 4, in a face coated with adhesive of short glass fiber filter paper, then uniformly coats water peanut on binding agent Additive, is dried 30-60min at 30-35 DEG C;
Step 5, goes glass cotton below 2 μm for the average diameter to add pH value to pull an oar in the acid solution of 5-6, adds dispersion Agent, is then discongested on fluffer, discongests revolution and turns for 15000-25000;
Step 6, the glass cotton after discongesting is put into molding on wet moulding machine, and the staple glass after step 4 is processed Fiber filter paper is placed on forming net, makes glass cotton coat to become in the one side of water peanut additive in short glass fiber filter paper Type, then 80-100 DEG C of drying, makes water peanut enhancement mode air filter paper.
The thickness of short glass fiber layer of described water peanut enhancement mode air filter paper and the ratio of the thickness of glass cotton layer For 1:2-1:1, so can obtain more preferable dust containing capacity and filter efficiency.
Described water peanut enhancement mode air filter paper thickness is preferably 0.5-0.6mm.
Present invention process advantages of simple, high yield rate, low production cost, using the different short glass fiber of fibre diameter Make the air filter paper of double-layer composite with microglass fiber, improve filter efficiency, reduce windage simultaneously, improve appearance Dust quantity, increases water peanut additive simultaneously, on the one hand can improve the filter effect of the harmful gass such as PARA FORMALDEHYDE PRILLS(91,95) further, and Further increase the dust containing capacity of the present invention.,
Multiple modifications to embodiment will be apparent from for those skilled in the art, is determined herein The General Principle of justice can be realized without departing from the spirit or scope of the present invention in other embodiments.Therefore, originally Invention is not intended to be limited to the embodiments shown herein, and is to fit to and principles disclosed herein and features of novelty Consistent scope the widest.

Claims (4)

1. a kind of preparation method of water peanut enhancement mode air filter paper is it is characterised in that comprise the following steps:
Step 1, water intaking Semen arachidis hypogaeae grinds making beating, is subsequently adding protease and saccharifying enzyme, and keeping temperature is 28-35 DEG C, stands 60-72 Hour, then it is centrifuged, rotating speed is 3500r/min, take lower sediment thing to dry, be ground to more than 200 mesh, the system of adding water Become the solution that concentration is 2%, add dispersant, stir, make water peanut additive;
Step 2, take average diameter 6-10 μm short glass fiber add pH value pull an oar in the saline solution of 6-8, add divide Powder, is then discongested on fluffer, discongests revolution and turns for 10000-15000;
Step 3, adds polyamide polyamine epichlorhydrin resin solution, Ran Hou in the short glass fiber solution to after discongest Molding on wet moulding machine, makes short glass fiber handsheet, puts into drying and moulding in drying machine, and baking temperature is 70-90 DEG C, make short glass fiber filter paper;
Step 4, in a face coated with adhesive of short glass fiber filter paper, then on binding agent, uniformly coating water peanut adds Agent, is dried 30-60min at 30-35 DEG C;
Step 5, goes glass cotton below 2 μm for the average diameter to add pH value to pull an oar in the acid solution of 5-6, adds dispersant, Then discongested on fluffer, discongest revolution and turn for 15000-25000;
Step 6, the glass cotton after discongesting is put into molding on wet moulding machine, and the short glass fiber after step 4 is processed Filter paper is placed on forming net, makes glass cotton coat molding in the one side of water peanut additive in short glass fiber filter paper, so 80-100 DEG C of drying, makes water peanut enhancement mode air filter paper afterwards.
2. the preparation method of water peanut enhancement mode air filter paper according to claim 1 is it is characterised in that in step 3 The concentration of described polyamide polyamine epichlorhydrin resin solution is 0.5-1%.
3. the preparation method of water peanut enhancement mode air filter paper according to claim 1 is it is characterised in that described spray The thickness of short glass fiber layer of raw enhancement mode air filter paper is 1 with the ratio of the thickness of glass cotton layer:2-1:1.
4. the preparation method of water peanut enhancement mode air filter paper according to claim 1 is it is characterised in that described spray Raw enhancement mode air filter paper thickness is 0.5-0.6mm.
CN201610778337.4A 2016-08-31 2016-08-31 Preparation method of alternanthera philoxeroides reinforced type air filter paper Pending CN106400598A (en)

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Application Number Priority Date Filing Date Title
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107119487A (en) * 2017-04-27 2017-09-01 舒尔环保科技(合肥)有限公司 A kind of preparation method of the air filter paper containing plant cellulose
CN107178006A (en) * 2017-06-30 2017-09-19 常州亚环环保科技有限公司 A kind of preparation method of resistant to dissolution type oil-water separation filter paper
CN108315373A (en) * 2018-04-28 2018-07-24 济宁学院 Alternanthera philoxeroides hydrolysis and saccharification technique

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2000070646A (en) * 1998-08-31 2000-03-07 Mitsubishi Paper Mills Ltd Air purifying filter member
CN102059025A (en) * 2010-12-01 2011-05-18 重庆再升科技发展有限公司 Double-layer filter material, preparation method thereof and multilayer product
CN104364441A (en) * 2012-05-25 2015-02-18 金伯利-克拉克环球有限公司 High strength macroalgae pulps
CN104532683A (en) * 2014-12-26 2015-04-22 重庆再升科技股份有限公司 Antibacterial mildewproof glass fiber composite air filter paper and preparation method of antibacterial mildewproof glass fiber composite air filter paper
CN105233571A (en) * 2015-10-22 2016-01-13 南京航空航天大学 Antibacterial glass-fiber composite filter paper and preparation method thereof
CN105495040A (en) * 2015-12-15 2016-04-20 苏州市阳澄农业科技有限公司 Aquatic plant fish granulated feed and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2000070646A (en) * 1998-08-31 2000-03-07 Mitsubishi Paper Mills Ltd Air purifying filter member
CN102059025A (en) * 2010-12-01 2011-05-18 重庆再升科技发展有限公司 Double-layer filter material, preparation method thereof and multilayer product
CN104364441A (en) * 2012-05-25 2015-02-18 金伯利-克拉克环球有限公司 High strength macroalgae pulps
CN104532683A (en) * 2014-12-26 2015-04-22 重庆再升科技股份有限公司 Antibacterial mildewproof glass fiber composite air filter paper and preparation method of antibacterial mildewproof glass fiber composite air filter paper
CN105233571A (en) * 2015-10-22 2016-01-13 南京航空航天大学 Antibacterial glass-fiber composite filter paper and preparation method thereof
CN105495040A (en) * 2015-12-15 2016-04-20 苏州市阳澄农业科技有限公司 Aquatic plant fish granulated feed and preparation method thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107119487A (en) * 2017-04-27 2017-09-01 舒尔环保科技(合肥)有限公司 A kind of preparation method of the air filter paper containing plant cellulose
CN107178006A (en) * 2017-06-30 2017-09-19 常州亚环环保科技有限公司 A kind of preparation method of resistant to dissolution type oil-water separation filter paper
CN107178006B (en) * 2017-06-30 2018-11-02 上海名冠净化材料股份有限公司 A kind of preparation method of resistant to dissolution type oil-water separation filter paper
CN108315373A (en) * 2018-04-28 2018-07-24 济宁学院 Alternanthera philoxeroides hydrolysis and saccharification technique

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Application publication date: 20170215