CN109912294A - A kind of foamed ceramic material pre-oxidation manufacturing method - Google Patents

A kind of foamed ceramic material pre-oxidation manufacturing method Download PDF

Info

Publication number
CN109912294A
CN109912294A CN201811095106.9A CN201811095106A CN109912294A CN 109912294 A CN109912294 A CN 109912294A CN 201811095106 A CN201811095106 A CN 201811095106A CN 109912294 A CN109912294 A CN 109912294A
Authority
CN
China
Prior art keywords
kiln
foamed ceramic
powder
manufacturing
oxidizes
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811095106.9A
Other languages
Chinese (zh)
Inventor
王昌平
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201811095106.9A priority Critical patent/CN109912294A/en
Publication of CN109912294A publication Critical patent/CN109912294A/en
Pending legal-status Critical Current

Links

Classifications

    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P40/00Technologies relating to the processing of minerals
    • Y02P40/60Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes

Abstract

The invention discloses a kind of foamed ceramic materials to pre-oxidize manufacturing method, includes the following steps: (1) feedstock processing;(2) it pre-oxidizes: mixed powder is put into revolution kiln drying calcining, the mixed powder in stirring calcining with the rotation of rotary kiln in rotary kiln, obtain it is fully oxidized, calcination temperature be 500-1000 DEG C, time 20-40 minute obtains aoxidizing thorough calcinated powder material;(3) foaming firing;(4) finished product is processed.

Description

A kind of foamed ceramic material pre-oxidation manufacturing method
Technical field
The present invention relates to a kind of foamed ceramic materials to pre-oxidize manufacturing method.
Background technique
Foamed ceramic is a kind of building material product, mainly uses waste ceramic brick, industrial residue, coal powder, dressing plant's tail Mine, mud of cleaning up the pond etc. are raw material, by special foam process, produce the products such as light cellular partition board, external wall insulation, are had light The advantages that matter, high-strength, sound insulation, waterproof is the environmental protection project for reducing solid waste pollution, resource regeneration.Current manufacturer All it is the production technology production for taking comparison traditional, is all to prepare raw material by formula to wear into mud in the ball mill, with by spraying Dry or filters pressing drying beats powder into powder, and then powder is tiled to the enterprising kiln of refractory slab and is burnt into, the powder without calcining is directly flat Paving firing, powder is more, spread thick, internal moisture is high, easy to oxidize into kiln rear surface, and internal moisture volatilization and oxidation are slowly.It is raw The greatest problem of production process is exactly that firing time is long, and energy consumption is high, at high cost.Oxidization time is very long, has elongated firing week significantly Phase increases energy consumption, and production capacity is very low, improves cost, thus affects the product competitiveness of enterprise and the economic benefit of enterprise, It popularizes and promotes in the market for also affecting such product simultaneously.
Summary of the invention
It is an object of the invention in place of overcome the deficiencies in the prior art, provide a kind of foamed ceramic material pre-oxidation system Method is made, solves the problems in above-mentioned background technique.
The technical solution adopted by the present invention to solve the technical problems is: a kind of foamed ceramic material pre-oxidation manufacturer Method includes the following steps:
(1) feedstock processing: taking raw material to mix with foam powder, and in grinding in ball mill, obtaining fineness is 250 mesh, tail over≤ 1.5% mud, mud are put into mud pit after being sieved with vibrating screen, and slurry in mud pit is made by spray drying tower drying Grain, obtains the mixed powder of raw material;The mixed powder moisture content is 5~8%;
(2) pre-oxidize: by mixed powder be put into revolution kiln drying calcining, the mixed powder in rotary kiln with return The rotation of rotary kiln and stir calcined oxide, the rotative speed of the rotary kiln is 3~5 revs/min, calcination temperature 500-1000 DEG C, time 20-40 minute, the calcinated powder material for obtaining surface oxidation is stored to filler bin;
(3) foaming firing: the enterprising kiln of the refractory slab that above-mentioned calcinated powder material is placed in kiln car or roller kilns stick frame is burnt into, Firing temperature is about 1100-1200 DEG C, and firing time is 7~14 hours, and kiln discharge obtains semifinished material;
(4) finished product is processed: above-mentioned semifinished material is carried out to the foamed ceramic plate for being cut into needs.
In a preferred embodiment of the present invention, the raw material and foam powder are mixed with the ratio of mass ratio 30-35:5, wherein Raw material components are made of by quality point 68-72 parts of waste ceramic brick, 9-11 parts of cullet, 14-16 parts of sludge.
In a preferred embodiment of the present invention, the raw material and foam powder are mixed with the ratio of mass ratio 32:5, the original Material component is made of by quality point 70 parts of waste ceramic brick, 10 parts of cullet, 15 parts of sludge.
In a preferred embodiment of the present invention, the calcining tail gas of rotary kiln is transmitted back to spray drying in the step (2) Tower carries out secondary use;
In a preferred embodiment of the present invention, the kiln tail gas of firing is transmitted back to rotary kiln in the step (3) and is carried out Secondary use.
In a preferred embodiment of the present invention, slurry in mud pit is formed by filter press filters pressing in the step (1) Mud cake is shredded through vacuum pugging shredding machine and is dried, obtains the mixed powder of raw material by mud cake;
In a preferred embodiment of the present invention, preoxidation time is about 20~30 minutes in the step (2).
In a preferred embodiment of the present invention, Shao Shi Liang≤2% of calcinated powder material in the step (2).
In a preferred embodiment of the present invention, firing temperature is 1150 DEG C in the step (3).
The technical program compared with the background art, it has the following advantages:
(1) pre-oxidation process is increased newly, required physical-chemical reaction into kiln before being burnt into when by original firing product It completes, since powder is state of dynamically stirring in rotary kiln, moisture evaporation and oxidation rate are fast, the thermal efficiency is high, oxidation is equal It is even thorough.Powder by pre-oxidation can directly heat up into kiln firing, and blowing temperature is mentioned in the short time, burning is greatly shortened At the period, kiln production capacity is improved, reduces energy consumption;
(2) powder by calcining is burnt into kiln, and kiln tail gas moisture is low, and temperature is high, can be sent to calcining kiln and calcining Hot gas merges, and is dried, is calcined to powder, and calcining kiln exhaust gas is used for spray drying tower again and carries out spray drying powder processed (calcining Kiln is equivalent to the hot-blast stove of drying tower), or dried for cachaza, achieve the purpose that waste heat makes full use of, in this way, energy saving Effect is obvious, product cost sharp fall.
Detailed description of the invention
Fig. 1 is 1 process flow chart of embodiment.
Specific embodiment
Embodiment 1
Fig. 1 is please referred to, a kind of foamed ceramic material of the present embodiment pre-oxidizes manufacturing method, includes the following steps:
(1) feedstock processing: taking raw material to mix with foam powder, and in grinding in ball mill, obtaining fineness is 250 mesh, tail over≤ 1.5% mud, mud are put into mud pit after being sieved with vibrating screen, and slurry in mud pit is made by spray drying tower drying Grain, obtains the mixed powder of raw material;The mixed powder moisture content 5~8%.
In the present embodiment, spray drying can also be substituted by following manner: forming mud cake by filter press filters pressing, mud cake is passed through The chopping drying of vacuum pugging shredding machine, obtains the mixed powder of raw material;
Wherein, the raw material and foam powder are mixed with the ratio of mass ratio 32:5, the raw material components by quality respectively by 70 parts of waste ceramic brick, 10 parts of cullet, 15 parts of sludge compositions.
(2) pre-oxidize: by mixed powder be put into revolution kiln drying calcining, the mixed powder in rotary kiln with return The rotation of rotary kiln and stir calcined oxide, the rotative speed of the rotary kiln is 3~5 revs/min, calcination temperature 500-1000 DEG C, the time 30 minutes, the calcinated powder material for obtaining surface oxidation was stored to filler bin.
The rotary kiln includes cylinder, wheel belt, support roller, gear wheel, sealing device and transmission device, mixed powder by kiln hood into Enter cylinder, drives barrel body rotation through driving wheel, powder stirs calcined oxide with the rotation of rotary kiln, sent again by kiln tail later Out, stirring pre-oxidation can make powder directly contact high temperature and oxygen, and powder quick heating, oxidation is fast, oxidation is uniform;
The calcining tail gas of rotary kiln is transmitted back to spray drying tower in the step (2) and carries out secondary use, by pre- oxygen The powder of change is burnt into kiln, and kiln tail gas moisture is low, and temperature is high, can be sent to calcining kiln and calcining hot gas merges, to powder into Row drying, calcining, calcining kiln exhaust gas are used for spray drying tower again and carry out being spray-dried powder processed that (calcining kiln is equivalent to the heat of drying tower Wind furnace), or dried for cachaza, achieve the purpose that waste heat makes full use of;
(3) foaming calcining: the enterprising kiln of the refractory slab that above-mentioned calcinated powder material is placed in kiln car or roller kilns stick frame is burnt into, It is 1150 or so DEG C at temperature is burnt, firing time is 7~14 hours, and kiln discharge obtains semifinished material;
Burning kiln tail gas is transmitted back to rotary kiln in the step (3) and carries out secondary use.
(4) finished product is processed: above-mentioned semifinished material is carried out to the foamed ceramic plate for being cut into needs.
The above is only the preferred embodiment of the present invention, the range implemented of the present invention that therefore, it cannot be limited according to, i.e., according to Equivalent changes and modifications made by the invention patent range and description, should still be within the scope of the present invention.

Claims (9)

1. a kind of foamed ceramic material pre-oxidizes manufacturing method, which comprises the steps of:
(1) feedstock processing: taking raw material to mix with foam powder, and in grinding in ball mill, obtaining fineness is 250 meshes, tail over≤ 1.5% mud, mud are put into mud pit after being sieved with vibrating screen, and slurry in mud pit is made by spray drying tower drying Grain, obtains the mixed powder of raw material;The mixed powder moisture content is 5~8%;
(2) pre-oxidize: by mixed powder be put into revolution kiln drying calcining, the mixed powder in rotary kiln with rotary kiln Rotation and stir calcined oxide, the slewing rate of the rotary kiln is 3~5 revs/min, and calcination temperature is 500-1000 DEG C, It time 20-40 minute, obtains aoxidizing thorough calcinated powder material and stores to filler bin;
(3) foaming firing: the enterprising kiln of the refractory slab that above-mentioned calcinated powder material is placed in kiln car or roller kilns stick frame is burnt into, firing Temperature is 1100-1200 DEG C, and firing time is 7~14 hours, and kiln discharge obtains semifinished material;
(4) finished product is processed: above-mentioned semifinished material is carried out to the foamed ceramic plate for being cut into needs.
2. a kind of foamed ceramic material according to claim 1 pre-oxidizes manufacturing method, it is characterised in that: the raw material with Foam powder is mixed with the ratio of mass ratio 30-35:5, and wherein raw material components are by quality point by 68-72 parts of waste ceramic brick, cullet 9-11 parts, 14-16 parts of sludge compositions.
3. a kind of foamed ceramic material according to claim 1 pre-oxidizes manufacturing method, it is characterised in that: the raw material with Foam powder is mixed with the ratio of mass ratio 32:5, and the raw material components are by quality point by 70 parts of waste ceramic brick, 10 parts of cullet, dirt 15 parts of mud compositions.
4. a kind of foamed ceramic material according to claim 1 pre-oxidizes manufacturing method, it is characterised in that: the step (2) the calcining tail gas of rotary kiln is transmitted back to spray drying tower in and carries out secondary use.
5. a kind of foamed ceramic material according to claim 1 pre-oxidizes manufacturing method, it is characterised in that: the step (3) firing product kiln tail gas is transmitted back to rotary kiln in and carries out secondary use.
6. a kind of foamed ceramic material according to claim 1 pre-oxidizes manufacturing method, it is characterised in that: the step (1) slurry in mud pit is formed into mud cake by filter press filters pressing in, mud cake is shredded through vacuum pugging shredding machine and is dried, is obtained The mixed powder of raw material.
7. a kind of foamed ceramic material according to claim 1 pre-oxidizes manufacturing method, it is characterised in that: the step (2) preoxidation time is 20~30 minutes in.
8. a kind of foamed ceramic material according to claim 1 pre-oxidizes manufacturing method, it is characterised in that: the step (2) Liang≤2%. Shao Shi of calcinated powder material in
9. a kind of foamed ceramic material according to claim 1 pre-oxidizes manufacturing method, it is characterised in that: the step (3) firing temperature is 1150 DEG C in.
CN201811095106.9A 2018-09-19 2018-09-19 A kind of foamed ceramic material pre-oxidation manufacturing method Pending CN109912294A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811095106.9A CN109912294A (en) 2018-09-19 2018-09-19 A kind of foamed ceramic material pre-oxidation manufacturing method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811095106.9A CN109912294A (en) 2018-09-19 2018-09-19 A kind of foamed ceramic material pre-oxidation manufacturing method

Publications (1)

Publication Number Publication Date
CN109912294A true CN109912294A (en) 2019-06-21

Family

ID=66959510

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201811095106.9A Pending CN109912294A (en) 2018-09-19 2018-09-19 A kind of foamed ceramic material pre-oxidation manufacturing method

Country Status (1)

Country Link
CN (1) CN109912294A (en)

Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH11199342A (en) * 1998-01-07 1999-07-27 Shinko Yogyo Kk Production of expanded ceramics
CN1887756A (en) * 2006-07-13 2007-01-03 马克文 Foamed glass and ceramic product and its making process
CN101830728A (en) * 2010-05-26 2010-09-15 浙江大学 Method for producing foamed ceramics by using ceramic waste
CN102219545A (en) * 2011-03-18 2011-10-19 赵坚强 Light functional material product with internal wall decorating and environment improving functions and manufacturing method of light functional material product
CN103011876A (en) * 2012-11-23 2013-04-03 佛山欧神诺陶瓷股份有限公司 Heat-insulation foamed ceramic plate and preparation method thereof
CN103172399A (en) * 2011-12-22 2013-06-26 沈阳临德陶瓷研发有限公司 Method for producing low-temperature foamed porcelain corrosion-resistant brick by using waste porcelain
CN104557103A (en) * 2013-10-11 2015-04-29 华楙生技股份有限公司 Lightweight ceramic plate and composition for preparing lightweight ceramic plate
CN106431486A (en) * 2016-09-29 2017-02-22 湖北壁玉新材料科技有限公司 Inorganic heat-insulating decorative material
CN106747603A (en) * 2016-12-14 2017-05-31 广东格莱斯陶瓷有限公司 A kind of production method of environment friendly light architectural pottery
CN107285738A (en) * 2017-08-02 2017-10-24 四川省蓝扬科技有限公司 A kind of combined light sound insulation wall brick
CN107382278A (en) * 2017-08-23 2017-11-24 文鹏涛 A kind of foamed ceramic partition plate and preparation method thereof
CN108238811A (en) * 2016-12-27 2018-07-03 中磊企业集团装饰有限公司 A kind of preparation method of foamed ceramic plates

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH11199342A (en) * 1998-01-07 1999-07-27 Shinko Yogyo Kk Production of expanded ceramics
CN1887756A (en) * 2006-07-13 2007-01-03 马克文 Foamed glass and ceramic product and its making process
CN101830728A (en) * 2010-05-26 2010-09-15 浙江大学 Method for producing foamed ceramics by using ceramic waste
CN102219545A (en) * 2011-03-18 2011-10-19 赵坚强 Light functional material product with internal wall decorating and environment improving functions and manufacturing method of light functional material product
CN103172399A (en) * 2011-12-22 2013-06-26 沈阳临德陶瓷研发有限公司 Method for producing low-temperature foamed porcelain corrosion-resistant brick by using waste porcelain
CN103011876A (en) * 2012-11-23 2013-04-03 佛山欧神诺陶瓷股份有限公司 Heat-insulation foamed ceramic plate and preparation method thereof
CN104557103A (en) * 2013-10-11 2015-04-29 华楙生技股份有限公司 Lightweight ceramic plate and composition for preparing lightweight ceramic plate
CN106431486A (en) * 2016-09-29 2017-02-22 湖北壁玉新材料科技有限公司 Inorganic heat-insulating decorative material
CN106747603A (en) * 2016-12-14 2017-05-31 广东格莱斯陶瓷有限公司 A kind of production method of environment friendly light architectural pottery
CN108238811A (en) * 2016-12-27 2018-07-03 中磊企业集团装饰有限公司 A kind of preparation method of foamed ceramic plates
CN107285738A (en) * 2017-08-02 2017-10-24 四川省蓝扬科技有限公司 A kind of combined light sound insulation wall brick
CN107382278A (en) * 2017-08-23 2017-11-24 文鹏涛 A kind of foamed ceramic partition plate and preparation method thereof

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
林宗寿: "《无机非金属材料工学》", 31 August 2014, 武汉理工大学出版社 *
陈木青等: "《材料物理实验教程》", 28 February 2018, 华中科技大学出版社 *

Similar Documents

Publication Publication Date Title
CN103693942A (en) Low-temperature fast-fired ceramic tile and production process thereof
CN107459364B (en) High-strength ceramsite prepared by using yellow river sludge and sludge as binder and preparation method thereof
CN104003755B (en) A kind of technique of utilizing polishing slag preparation to breathe brick
CN103992099A (en) Method for preparing environment-friendly honeycomb ceramic heat accumulator by use of waste slag
CN108863432A (en) A kind of hollow haydite of solid waste and preparation method thereof
CN104355575A (en) Fly ash and dyeing sludge geopolymer material and preparing method thereof
CN110818385B (en) Antique blue brick taking lake silt as main raw material and firing method thereof
CN105693210A (en) Ceramic material prepared from red mud, and preparation method of ceramic material
CN101648723A (en) Method for producing precipitated calcium carbonate
CN101353248A (en) Method for producing porous brick with construction sanitary ceramic cold-working waste slag
CN106336200A (en) Inorganic fiber reinforced refractory material and preparation technology thereof
CN106747603A (en) A kind of production method of environment friendly light architectural pottery
CN102180690B (en) Method for producing Al2O3-MgO brick by using Al2O3-MgO-CaO synthetic fireproof raw material
CN108409169A (en) A kind of fast energy-saving preparation method of quick lime
EP1847515B1 (en) Cement clinker and process for producing the same
KR20030070204A (en) Composition for light weight artificial aggregate made from waste material and method for manufacturing the same
CN104211377B (en) A kind of technique utilizing waste ceramic body refuse to prepare ceramics
CN110862272B (en) Device and method for preparing composite exciting agent clinker by using semi-dry desulfurization ash and application of clinker
CN108373274A (en) A kind of fast energy-saving preparation method of lime
CN113307640A (en) Method for preparing alumina-silicon carbide-carbon series refractory raw material by using secondary aluminum ash as raw material
CN112805260B (en) Method for producing synthetic light ceramic sand and application thereof
CN109912294A (en) A kind of foamed ceramic material pre-oxidation manufacturing method
CN104609833B (en) The preparation method of Imitation Rock Porcelain Tiles
CN109734314A (en) A kind of acid and alkali-resistance ceramic glaze and preparation method thereof
KR20000072111A (en) Composition for lightweight aggregate and method for manufacturing the same

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20190621

WD01 Invention patent application deemed withdrawn after publication