CN109911877A - A kind of lithium hexafluoro phosphate prepares Multi-purpose cabinet - Google Patents

A kind of lithium hexafluoro phosphate prepares Multi-purpose cabinet Download PDF

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Publication number
CN109911877A
CN109911877A CN201910191573.XA CN201910191573A CN109911877A CN 109911877 A CN109911877 A CN 109911877A CN 201910191573 A CN201910191573 A CN 201910191573A CN 109911877 A CN109911877 A CN 109911877A
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CN
China
Prior art keywords
cabinet
door
air inlet
exhaust pipe
valve
Prior art date
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Pending
Application number
CN201910191573.XA
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Chinese (zh)
Inventor
蔡显威
夏磊
谢斌
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Qinghai Poly Source New Materials Co Ltd
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Qinghai Poly Source New Materials Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Qinghai Poly Source New Materials Co Ltd filed Critical Qinghai Poly Source New Materials Co Ltd
Priority to CN201910191573.XA priority Critical patent/CN109911877A/en
Publication of CN109911877A publication Critical patent/CN109911877A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a kind of lithium hexafluoro phosphates to prepare Multi-purpose cabinet, including left cabinet, left cabinet door, left partition door, left isolation gloves, right isolation gloves, inner valve, middle cabinet, right isolating door, right cabinet, right cabinet door, left cabinet air inlet pipe, left cabinet exhaust pipe, middle cabinet air inlet pipe, materail tube, middle cabinet exhaust pipe, right cabinet air inlet pipe, right cabinet exhaust pipe, left cabinet intake valve, left cabinet exhaust valve, middle cabinet intake valve, Material valve, middle cabinet exhaust valve, right cabinet intake valve, right cabinet exhaust valve, PFA sample bottle, supporting leg, wheel, Multi-purpose cabinet cabinet body sealing is internal filled with inert gas shielding, reasonably it is divided into three spaces, Synthesis liquid in lithium hexafluoro phosphate preparation process can be met, mother liquor, intermediate product, the safety sampling of multiple materials such as finished product, cabinet body front panel it is transparent and with can isolated operation gloves, pacify sampling work Full strong operability avoids personal injury and environmental pollution.

Description

A kind of lithium hexafluoro phosphate prepares Multi-purpose cabinet
Technical field
The present invention relates to lithium hexafluoro phosphate preparation technical fields, and in particular to a kind of lithium hexafluoro phosphate samples more when preparing Purposes cabinet.
Background technique
In lithium hexafluoro phosphate preparation process, lithium hexafluoro phosphate Synthesis liquid, mother liquor, intermediate product, finished product etc. are taken Sample test verification, in the prior art, the sampling for Synthesis liquid, mother liquor usually do an easy device, and sampling bottle is opened Lid is placed on the inside sampling, usually does easy sampling bag for intermediate product, finished product sampling and is sampled, not only causes sampling tired Difficulty, protects not in place, also easily causes sample contaminated, influences testing result, while preparing during lithium hexafluoro phosphate and have HF etc. Toxic gas, if sampler blow-by, sampling process are lack of standardization, it is easy to safety accident occur, cause personal injury, cause The pollution of ambient enviroment.
Summary of the invention
To solve problems of the prior art, the present invention provides a kind of lithium hexafluoro phosphate and prepares Multi-purpose cabinet, should, it should The sealing of Multi-purpose cabinet cabinet body is internal filled with inert gas shielding, is reasonably divided into three spaces, can meet lithium hexafluoro phosphate system The safety sampling of multiple materials such as Synthesis liquid, mother liquor, intermediate product, finished product during standby, cabinet body front panel are transparent and with can be every Gloves from operation, two sides are equipped with side door, keep sampling work safe operability strong, solve and prepared in lithium hexafluoro phosphate Sampling is difficult when being sampled in journey using the prior art, and protection is not in place, it is contaminated to easily cause sample, and toxic gas easily leaks, The problem of being easy to happen safety accident, causing personal injury and the pollution of ambient enviroment.
To achieve the purpose of the present invention, the invention adopts the following technical scheme:
A kind of lithium hexafluoro phosphate prepares Multi-purpose cabinet, including left cabinet, left cabinet door, left partition door, left isolation gloves, right isolation gloves, Inner valve, middle cabinet, right isolating door, right cabinet, right cabinet door, the left cabinet, middle cabinet, right cabinet are cuboid case structure, institute The left cabinet stated is located on the left of middle cabinet, and the right cabinet is located on the right side of middle cabinet, and the left cabinet and right cabinet body product are identical, described Middle cabinet it is higher than left cabinet 1 and right cabinet, sealable left cabinet door is installed, on the right side of the left cabinet on the left of the left cabinet Between sealable left partition door is installed between cabinet, opening left partition door can be connected to left cabinet with middle cabinet, peace on the right side of the right cabinet Equipped with sealable right cabinet door, sealable right partition door is installed between middle cabinet on the left of the right cabinet, opens right partition door Right cabinet can be connected to middle cabinet, materail tube is connected at the top of middle cabinet, materail tube protrudes into middle cabinet, the PFA sample bottle 25 are located at middle cabinet materials inside pipe, and material can be directly entered PFA sample bottle 25, form the confined space of a sampling, institute The materail tube stated protrudes into and is equipped with inner valve on the pipeline of middle cabinet, and the inner valve can make operator inside centre 7 Control sampling, left cabinet, can be right by the conveying with the left partition door of middle cabinet progress sample as intermediate product, the storage cabinet of finished product Cabinet can pass through the conveying with the right partition door of middle cabinet progress sample as Synthesis liquid, the storage cabinet of mother liquor;
Further, panel composition is made using macromolecule anticorrosive material in the middle cabinet, and the middle cabinet front panel is adopted It is made of transparent polymer anticorrosive material, the left isolation gloves 4 and right isolation gloves 5 are mounted on middle cabinet front panel simultaneously It protrudes into middle cabinet 7, operator can be allowed freely to carry out the operations in cabinet;
Further, the left cabinet door, left partition door, right isolating door, be equipped with that its door body can be made to close fastening is close in right cabinet door The locking buckle of envelope, the left cabinet door, right isolating door, are provided with transparent window in right cabinet door at left partition door, and transparent window is using saturating Bright macromolecule anticorrosive material is made;
Further, the left cabinet top portion is equipped with left cabinet air inlet pipe and left cabinet exhaust pipe, is equipped with centre at the top of middle cabinet Cabinet air inlet pipe and middle cabinet exhaust pipe, the right cabinet top portion are equipped with right cabinet air inlet pipe and right cabinet exhaust pipe, the left cabinet Air inlet pipe, middle cabinet air inlet pipe, right cabinet air inlet pipe are connected to inertial gas tank, and inert gas can pass through left cabinet air inlet respectively Pipe, middle cabinet air inlet pipe, right cabinet air inlet pipe enter left cabinet, middle cabinet, right cabinet in;Left cabinet, middle cabinet, right cabinet have independence Exhaust system, the left cabinet exhaust pipe, middle cabinet exhaust pipe, right cabinet exhaust pipe are connected to the general pipeline of exhaust, guarantee multi-purpose Pressure balance inside the cabinet of way;
Further, left cabinet intake valve is installed, the left cabinet exhaust pipe is equipped with left cabinet row in the left cabinet air inlet pipe Air valve is equipped with middle cabinet intake valve in the middle cabinet air inlet pipe, is equipped with middle cabinet on the middle cabinet exhaust pipe Exhaust valve is equipped with Material valve on the materail tube.
Further, the Multi-purpose cabinet bottom four corners install a supporting leg, are equipped with a vehicle on each supporting leg Wheel, two, left side wheel are directional wheel, and two, right side wheel is universal wheel.
Compared with the prior art, the present invention has the following beneficial effects:
1, Multi-purpose cabinet can meet multiple materials such as Synthesis liquid in lithium hexafluoro phosphate preparation process, mother liquor, intermediate product, finished product Safety sampling, realizes a kind of equipment multiple use, saves resource, improves use value.
2, cabinet body front panel it is transparent and with can isolated operation gloves, two sides are equipped with side door, become sampling work Safe and environment-friendly, strong operability.
3, cabinet body sealing is internal filled with inert gas shielding, is reasonably divided into three spaces, effectively avoids sample quilt The problems such as pollution, toxic gas leakage, environmental pollution.
Detailed description of the invention
Fig. 1 is the structural schematic diagram that a kind of lithium hexafluoro phosphate of the present invention prepares Multi-purpose cabinet;
In figure: left cabinet -1, left cabinet door -2, left partition door -3, left isolation gloves -4, right isolation gloves -5, inner valve -6, middle cabinet - 7, right isolating door -8, right cabinet -9, right cabinet door -10, left cabinet air inlet pipe -11, left cabinet exhaust pipe -12, middle cabinet air inlet pipe -13, object Expects pipe -14, middle cabinet exhaust pipe -15, right cabinet air inlet pipe -16, right cabinet exhaust pipe -17, left cabinet intake valve -18, left cabinet exhaust valve - 19, middle cabinet intake valve -20, Material valve -21, middle cabinet exhaust valve -22, right cabinet intake valve -23, right cabinet exhaust valve -24, PFA Sample bottle -25, supporting leg -26, wheel -27.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention;Technical solution in the embodiment of the present invention carries out clear, complete Site preparation description;
As shown in Figure 1, in one embodiment of the invention, a kind of lithium hexafluoro phosphate prepares Multi-purpose cabinet, including left cabinet 1, left Cabinet door 2, left partition door 3, left isolation gloves 4, right isolation gloves 5, inner valve 6, middle cabinet 7, right isolating door 8, right cabinet 9, right cabinet door 10, left cabinet air inlet pipe 11, left cabinet exhaust pipe 12, middle cabinet air inlet pipe 13, materail tube 14, middle cabinet exhaust pipe 15, right cabinet air inlet Pipe 16, right cabinet exhaust pipe 17, left cabinet intake valve 18, left cabinet exhaust valve 19, middle cabinet intake valve 20, Material valve 21, middle cabinet row Air valve 22, right cabinet intake valve 23, right cabinet exhaust valve 24, PFA sample bottle 25, supporting leg 26, wheel 27, the left cabinet 1, centre Cabinet 7, right cabinet 9 are cuboid case structure, and the left cabinet 1 is located at 7 left side of middle cabinet, and it is right that the right cabinet 9 is located at middle cabinet 7 Side, the left cabinet 1 is identical with right 9 volume of cabinet, and the middle cabinet 7 is higher than left cabinet 1 and right cabinet 9, pacifies on the left of the left cabinet 1 Equipped with sealable left cabinet door 2, sealable left partition door 3 is installed between 1 right side of left cabinet and middle cabinet 7, is opened left Left cabinet 1 can be connected to by partition door 3 with middle cabinet 7, and sealable right cabinet door 10, the right cabinet 9 are equipped on the right side of the right cabinet 9 Sealable right partition door 8 is installed, opening right partition door 8 can be connected to right cabinet 9 with middle cabinet 7, intermediate between left side and middle cabinet 7 Cabinet 7 as Synthesis liquid, mother liquor, intermediate product, finished product sampling cabinet, materail tube 14 is connected at the top of middle cabinet 7, during materail tube 14 protrudes into Between in cabinet 7 so that middle cabinet 7 is attached with sample point, material can be directly entered the PFA sample bottle for having been subjected to special processing 25, the confined space of a sampling is formed, the materail tube 14 protrudes on the pipeline of middle cabinet 7 and is equipped with inner valve 6, described Inner valve 6 operator can be made to sample in 7 internal control of middle cabinet, left cabinet 1 can lead to as intermediate product, the storage cabinet of finished product Cross the conveying that sample is carried out with the left partition door 3 of middle cabinet 7, right cabinet 9 as Synthesis liquid, the storage cabinet of mother liquor, can by with centre The right partition door of cabinet 7 carries out the conveying of sample, and 7 panel of middle cabinet is made of macromolecule anticorrosive material, in fluorination hydrogen Body environment is not corroded, and 7 front panel of middle cabinet is made of transparent polymer anticorrosive material, it can be seen that entire sampling Process, the left isolation gloves 4 and right isolation gloves 5 are mounted on 7 front panel of middle cabinet and protrude into middle cabinet 7, described Left isolation gloves 4 and right isolation gloves 5 be special anti-AHF special gloves, operator can be allowed freely to carry out in cabinet Operations;The left cabinet door 2, right isolating door 8, is equipped with locking buckle in right cabinet door 10 at left partition door 3, can make its door Body closes fit sealing, and the left cabinet door 2, right isolating door 8, is provided with transparent window, transparency window in right cabinet door 10 at left partition door 3 Mouth is made of transparent polymer anticorrosive material, convenient for observing when operator's operation;
Left cabinet air inlet pipe 11 and left cabinet exhaust pipe 12 are installed at the top of the left cabinet 1, be equipped at the top of middle cabinet 7 middle cabinet into Tracheae 13 and middle cabinet exhaust pipe 15 are equipped with right cabinet air inlet pipe 16 and right cabinet exhaust pipe 17 at the top of the right cabinet 9, described Left cabinet air inlet pipe 11, middle cabinet air inlet pipe 13, right cabinet air inlet pipe 16 are connected to inertial gas tank, and inert gas can pass through respectively Left cabinet air inlet pipe 11, middle cabinet air inlet pipe 13, right cabinet air inlet pipe 16 enter left cabinet 1, middle cabinet 7, right cabinet into 9;Left cabinet 1, Middle cabinet 7, right cabinet 9 have independent exhaust system, the left cabinet exhaust pipe 12, middle cabinet exhaust pipe 15, right cabinet exhaust pipe 17 are connected to the general pipeline of exhaust, guarantee the pressure balance inside Multi-purpose cabinet;
Left cabinet intake valve 18 is installed, the left cabinet exhaust pipe 12 is equipped with left cabinet exhaust valve in the left cabinet air inlet pipe 11 19, middle cabinet intake valve 20 is installed in the middle cabinet air inlet pipe 13, is equipped on the middle cabinet exhaust pipe 15 Between cabinet exhaust valve 22, Material valve 21 is installed on the materail tube 14, the sealing of Multi-purpose cabinet can be increased by closing each valve Property, it can be realized by control Material valve 21 and be externally controlled sample rate.
The Multi-purpose cabinet bottom four corners install 4 supporting legs 26, are equipped with a wheel 27 on each supporting leg 26, Two, left side wheel 27 is directional wheel, and two, right side wheel 27 is universal wheel, and the multiple equipment that can satisfy on different location takes Sample demand.

Claims (5)

1. a kind of lithium hexafluoro phosphate prepares Multi-purpose cabinet, including left cabinet, left cabinet door, left partition door, left isolation gloves, right isolation hand Set, inner valve, middle cabinet, right isolating door, right cabinet, right cabinet door, it is characterised in that: the left cabinet, middle cabinet, right cabinet are rectangular Body case structure, the left cabinet are located on the left of middle cabinet, and the right cabinet is located on the right side of middle cabinet, the left cabinet and right cabinet Volume is identical, and the middle cabinet is higher than left cabinet and right cabinet, is equipped with sealable left cabinet door on the left of the left cabinet, described Sealable left partition door is installed between middle cabinet on the right side of left cabinet, sealable right cabinet door is installed on the right side of the right cabinet, Sealable right partition door is installed between middle cabinet on the left of the right cabinet, connects materail tube at the top of middle cabinet, materail tube is stretched Enter in middle cabinet, the PFA sample bottle is located at middle cabinet materials inside pipe, and the materail tube protrudes into the pipeline of middle cabinet On inner valve is installed, can be by carrying out the conveying of sample with the right partition door of middle cabinet, the middle cabinet is resistance to using macromolecule Panel composition is made in rotten material, and the middle cabinet front panel is made of transparent polymer anticorrosive material, the left isolation Gloves and right isolation gloves are mounted on middle cabinet front panel and protrude into middle cabinet.
2. a kind of lithium hexafluoro phosphate according to claim 1 prepares Multi-purpose cabinet, it is characterised in that: the left cabinet door, Left partition door, right isolating door are equipped with the locking buckle that its door body can be made to close fit sealing in right cabinet door, the left cabinet door, Left partition door, right isolating door are provided with transparent window in right cabinet door, and transparent window is made of transparent polymer anticorrosive material.
3. a kind of lithium hexafluoro phosphate according to claim 1 prepares Multi-purpose cabinet, it is characterised in that: the left cabinet top portion Left cabinet air inlet pipe and left cabinet exhaust pipe are installed, middle cabinet air inlet pipe and middle cabinet exhaust pipe are installed at the top of middle cabinet, it is described Right cabinet top portion right cabinet air inlet pipe and right cabinet exhaust pipe, the left cabinet air inlet pipe, middle cabinet air inlet pipe, right cabinet air inlet are installed Pipe is connected to inertial gas tank, and the left cabinet exhaust pipe, middle cabinet exhaust pipe, right cabinet exhaust pipe are connected to the total of exhaust Pipe.
4. a kind of lithium hexafluoro phosphate according to claim 3 prepares Multi-purpose cabinet, it is characterised in that: the left cabinet air inlet Left cabinet intake valve is installed, the left cabinet exhaust pipe is equipped with left cabinet exhaust valve, pacifies in the middle cabinet air inlet pipe on pipe Equipped with middle cabinet intake valve, middle cabinet exhaust valve is installed on the middle cabinet exhaust pipe, is equipped on the materail tube Material valve.
5. a kind of lithium hexafluoro phosphate according to claim 4 prepares Multi-purpose cabinet, it is characterised in that: the Multi-purpose cabinet Bottom four corners are respectively equipped with 1 supporting leg, a wheel are equipped on each supporting leg, two, left side wheel is directional wheel, right The wheel of side two is universal wheel.
CN201910191573.XA 2019-03-14 2019-03-14 A kind of lithium hexafluoro phosphate prepares Multi-purpose cabinet Pending CN109911877A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910191573.XA CN109911877A (en) 2019-03-14 2019-03-14 A kind of lithium hexafluoro phosphate prepares Multi-purpose cabinet

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910191573.XA CN109911877A (en) 2019-03-14 2019-03-14 A kind of lithium hexafluoro phosphate prepares Multi-purpose cabinet

Publications (1)

Publication Number Publication Date
CN109911877A true CN109911877A (en) 2019-06-21

Family

ID=66964754

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910191573.XA Pending CN109911877A (en) 2019-03-14 2019-03-14 A kind of lithium hexafluoro phosphate prepares Multi-purpose cabinet

Country Status (1)

Country Link
CN (1) CN109911877A (en)

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