CN109908855A - A kind of explosion-protection equipment and its application method extracted for plant proline with the processing of assay boiling water bath - Google Patents
A kind of explosion-protection equipment and its application method extracted for plant proline with the processing of assay boiling water bath Download PDFInfo
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- CN109908855A CN109908855A CN201910161438.0A CN201910161438A CN109908855A CN 109908855 A CN109908855 A CN 109908855A CN 201910161438 A CN201910161438 A CN 201910161438A CN 109908855 A CN109908855 A CN 109908855A
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- bath pipe
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Abstract
The present invention relates to a kind of explosion-protection equipments and its application method extracted for plant proline with the processing of assay boiling water bath.The explosion-protection equipment, ceramic cap, water-bath pipe, water-bath tube sheet are pressed including dimension, several tube sheet threaded holes are evenly distributed on the water-bath tube sheet, the middle and upper part outer wall of the water-bath pipe is equipped with water-bath pipe outer wall screw thread, water-bath pipe is threadedly connected in tube sheet threaded hole by water-bath pipe outer wall, and dimension pressure ceramic cap is installed in the top nozzle of water-bath pipe.Using explosion-protection equipment and application method of the invention, easy to operate, plant proline extraction operation is safer, reduces error caused by due to water-bath pipe lid pops and reaction solution is lost, assay accuracy improves, and can effectively improve the treatment effeciency of plant proline extraction and assay.
Description
Technical field
The present invention relates to chemical experiment device technical fields, more particularly to one kind to extract for plant proline and contain measurement
Determine the explosion-protection equipment and its application method of boiling water bath processing.
Background technique
Plant proline has extremely important influence for the vital movement of animals and plants.Proline is animal collagen
Important component exists in various plants albumen, and the formation with plant cell wall has highly important relationship.Plant is dry
Drought, high temperature under a variety of adverse circumstances such as low temperature, salt stress, often there is apparent plant Proline Accumulation.Plant proline is clinical, raw
Object material, industry etc. are widely used.The extraction of plant proline and assay are carried out in laboratory, it can be by adding
There is the reaction solution of plant proline to carry out boiling water bath to heat to realize.This process is usually by plant tissue and to be heated anti-
It answers liquid to be added in the water-bath pipe of nozzle connection lid to carry out boiling processing.When boiling water bath heats, due to the High Temperature Gas of reaction solution generation
Body can quickly flick pipe lid, cause reaction solution to be easy contaminated or overflow, to influence experimental result.
Currently, the pipe lid of the extraction of plant proline and assay boiling water bath treatment process easily pops in laboratory, this is lacked
It falls into and effective solution is not yet received, also can improve this problem without specific instrument.
Summary of the invention
The purpose of the present invention is to provide a kind of extracted for plant proline handle with assay boiling water bath it is explosion-proof
Device and its application method, to solve the above technical problems.To achieve the above object, the invention adopts the following technical scheme:
A kind of explosion-protection equipment extracted for plant proline with the processing of assay boiling water bath, including dimension pressure ceramic cap, water-bath
It manages, water-bath tube sheet, is evenly distributed with several tube sheet threaded holes on the water-bath tube sheet, the middle and upper part outer wall of the water-bath pipe is set
There is water-bath pipe outer wall screw thread, water-bath pipe is threadedly connected in tube sheet threaded hole by water-bath pipe outer wall, and dimension pressure ceramic cap is installed on
In the top nozzle of water-bath pipe.
As a further solution of the present invention, water-bath tube sheet uses the hollow tube sheet of glass fiber plastic production, is distributed with thereon
30 tube sheet threaded holes, and the diameter of each tube sheet threaded hole is 2 centimetres.
As a further solution of the present invention, water-bath pipe is glass fiber plastic water-bath pipe, and length 10cm, overall diameter 2cm are interior
Diameter 1.6-1.8cm, pipe thickness 1-2mm, water-bath pipe top are annular groove, are equipped at the one third of its outer wall middle and upper part
Water-bath pipe outer wall screw thread when water-bath pipe is connected in tube sheet threaded hole, fills the bottom of the water-bath pipe equipped with reaction solution with boiling water
The outer wall middle part of tap touching, water-bath pipe has graduation indication line, indicates that this position is at liquor capacity 10ml.
As a further solution of the present invention, the medial center of dimension pressure ceramic cap is hemispherical projections structure, and hemispherical is convex
Play structure matching corresponding with the nozzle of matched water-bath pipe.When heating operation starts, by gravity, dimension presses ceramic cap
Hemispherical projections structure can be tightly attached to the nozzle of water-bath pipe.After the boiling of water-bath liquid in pipe, steam rising opens top dimension pressure
It is escaped after ceramic cap, drops to water-bath overpressure within the scope of safety value.
As a further solution of the present invention, the inside of dimension pressure ceramic cap is two Spring Cards of lower edge symmetrical configuration
Son, spring clip matching corresponding with the annular groove of water-bath pipe, after the boiling of water-bath liquid in pipe, steam rising opens top
When dimension pressure ceramic cap, by the fixed function of spring clip dimension pressure ceramic cap will not fall off.
As a further solution of the present invention, gap of the spring clip top with 2mm on the inside of dimension pressure ceramic cap, is being heated
Dimension pressure ceramic cap is tightly attached to water-bath nozzle by the effect of gravity when operation starts, and after liquid in pipe boiling, steam rising is opened
Top dimension pressure ceramic cap guarantees that dimension pressure ceramic cap rises certain altitude, has sufficient space to make gas in water-bath pipe by this gap
It discharges.
As a further solution of the present invention, water-bath tube sheet and water it is discontiguous above be distributed with multiple 0.5 cm's of diameter
Tube sheet gas vent floats on the boiling water of water-bath for tube sheet.
As a further solution of the present invention, dimension pressure ceramic cap is made of ceramic material.
A kind of plant proline extracts the application method of the explosion-protection equipment handled with assay boiling water bath, including following step
It is rapid:
1), water-bath pipe is screwed on hollow water-bath tube sheet by water-bath pipe outer wall, by water-bath tube sheet and water-bath pipe two
Fixation is tightened by screw thread in part, causes inner reaction tube liquid to escape to be detached from water-bath tube sheet, the failure of an experiment and device is caused to damage,
Guarantee that the opening direction of water-bath pipe is consistent with the tube sheet gas vent direction of water-bath tube sheet simultaneously；
2), various reagents solution to be reacted proportionally is sequentially added in water-bath pipe, for guarantee experimental result accuracy,
Institute's reagent adding total volume should be no more than the graduation indication line of water-bath pipe, that is, be no more than 10ml；
3), dimension pressure ceramic cap is connected to the upper orifice of water-bath pipe, the spring clip of dimension pressure ceramic cap is made to block water-bath pipe top
The annular groove of nozzle lower edge；
4), entire explosion-protection equipment is placed in water-bath, heating boil, boil reaction reach measurement require after, stop plus
Heat operation, it is cooling to take out explosion-protection equipment.
Compared with prior art, the invention has the following advantages that using explosion-protection equipment and application method of the invention, operation
Simplicity, plant proline extraction operation is safer, reduces error caused by due to water-bath pipe lid pops and reaction solution is lost,
Assay accuracy improves, and can effectively improve the treatment effeciency of plant proline extraction and assay.
Detailed description of the invention
Fig. 1 is explosion-protection equipment structural schematic diagram of the invention；
Fig. 2 is water-bath pipe and dimension pressure ceramic cap structural profile illustration of the invention；
Fig. 3 is that dimension of the invention presses ceramic cap structural profile illustration；
Fig. 4 is water-bath tube plate structure diagram of the invention.
In Fig. 1-4: 1, dimension pressure ceramic cap, 2, hemispherical projections structure, 3, spring clip, 4, annular groove, 5, water-bath pipe
Outer wall thread, 6, graduation indication line, 7, water-bath pipe, 8, water-bath tube sheet, 9, tube sheet gas vent, 10, tube sheet threaded hole, 11, water-bath
Pot.
Specific embodiment
The present invention is further elaborated in the following with reference to the drawings and specific embodiments.
A kind of explosion-protection equipment extracted for plant proline with the processing of assay boiling water bath, including dimension pressure ceramic cap 1,
Water-bath pipe 7, water-bath tube sheet 8, the hollow tube sheet that water-bath tube sheet 8 is made of glass fiber plastic (such as PEEK plastic material) are described
Several tube sheet threaded holes 10 are evenly distributed on water-bath tube sheet 8, preferred distribution there are 30 tube sheet threaded holes 10 thereon, and each
10 diameter of tube sheet threaded hole is 2 centimetres.And water-bath tube sheet 8 and water is discontiguous that the tube sheet of multiple 0.5 cm of diameter is distributed with above
Gas vent 9 floats on the boiling water of water-bath 11 for tube sheet；
Water-bath pipe 7 be glass fiber plastic water-bath pipe, length 10cm, overall diameter 2cm, internal diameter 1.6-1.8cm, pipe thickness 1-2mm,
7 top of water-bath pipe is annular groove 4, and water-bath pipe outer wall screw thread 5, water-bath pipe 7 are equipped at the one third of wherein external wall of upper portion
When being connected in tube sheet threaded hole 10, come into full contact with the bottom of the water-bath pipe 7 equipped with reaction solution and boiling water without influencing boiling water
The outer wall middle part of the effect of bath, water-bath pipe 7 has graduation indication line 6, indicates that this position is water-bath pipe 7 at liquor capacity 10ml
It is connected in tube sheet threaded hole 10 by water-bath pipe outer wall screw thread 5；Dimension pressure ceramic cap is made of ceramic material, dimension pressure ceramic cap 1
It is installed in the top nozzle of water-bath pipe 7；
The medial center of dimension pressure ceramic cap 1 is hemispherical projections structure 2, the pipe of hemispherical projections structure 2 and matched water-bath pipe 7
The corresponding matching of mouth can be tightly attached to when heating operation starts by the hemispherical projections structure 2 of gravity, dimension pressure ceramic cap 1
The nozzle of water-bath pipe 7, after liquid boiling in water-bath pipe 7, steam rising opens top dimension pressure ceramic cap 1 and escapes, and makes water-bath pipe 7
Interior pressure drops within the scope of safety value.
The inside for tieing up pressure ceramic cap 1 is that there are two symmetrical spring clip 3, spring clip 3 and water-bath pipes 7 for lower edge tool
The corresponding matching of annular groove 4 when steam rising opens top dimension pressure ceramic cap 1, passes through bullet after the boiling of water-bath liquid in pipe
The fixed function of spring clamp 3 will not fall off dimension pressure ceramic cap 1.Dimension pressure 1 inside spring clip of ceramic cap, 3 top has 2mm
Gap, when heating operation starts, dimension pressure ceramic cap 1 by the effect of gravity is tightly attached to water-bath nozzle, when liquid in pipe boils
Afterwards, steam rising opens top dimension pressure ceramic cap 1, by this gap, guarantees that dimension pressure ceramic cap 1 rises certain altitude, has enough
Space discharges gas in water-bath pipe.
Dimension pressure ceramic cap 1 uses ceramic reason are as follows: ceramic quality is close, density is big, high temperature resistant, is unlikely to deform, it
Quality is larger, can't be displaced under the impact of a degree of gas.
The plant proline extracts the application method with the explosion-protection equipment of assay boiling water bath processing, including following step
It is rapid:
1), water-bath pipe is screwed on hollow water-bath tube sheet by water-bath pipe outer wall, by water-bath tube sheet and water-bath pipe two
Fixation is tightened by screw thread in part, to avoid water-bath pipe disengaging water-bath tube sheet causes inner reaction tube when heating operation in water-bath
Liquid evolution causes the failure of an experiment and device to damage, while guaranteeing the opening direction of water-bath pipe and the tube sheet gas vent of water-bath tube sheet
Direction is consistent；
2), various reagents solution to be reacted proportionally is sequentially added in water-bath pipe, for guarantee experimental result accuracy,
Institute's reagent adding total volume should be no more than the graduation indication line of water-bath pipe, that is, be no more than 10ml；
3), dimension pressure ceramic cap is connected to the upper orifice of water-bath pipe, the spring clip of dimension pressure ceramic cap is made to block water-bath pipe top
The annular groove of nozzle lower edge；
4), entire explosion-protection equipment is placed in water-bath, heating boil, boil reaction reach measurement require after, stop plus
It is cooling to take out explosion-protection equipment for heat.Water-bath tube sheet and dimension pressure ceramic cap answer direction upward, this explosion-protection equipment does not turn-over absolutely use.
The above is present pre-ferred embodiments, for the ordinary skill in the art, according to the present invention
Introduction, in the case where not departing from the principle of the present invention and spirit, changes, modifications, replacement and change that embodiment is carried out
Type is still fallen within protection scope of the present invention.
Claims (9)
1. a kind of explosion-protection equipment extracted for plant proline with the processing of assay boiling water bath, which is characterized in that including dimension
Ceramic cap (1), water-bath pipe (7), water-bath tube sheet (8) are pressed, is evenly distributed with several tube sheet threaded holes on the water-bath tube sheet (8)
(10), the middle and upper part outer wall of the water-bath pipe (7) is equipped with water-bath pipe outer wall screw thread (5), and water-bath pipe (7) passes through water-bath pipe outer wall spiral shell
Line (5) is connected in tube sheet threaded hole (10), and dimension pressure ceramic cap (1) is installed in the top nozzle of water-bath pipe (7).
2. a kind of explosion-proof dress extracted for plant proline with the processing of assay boiling water bath according to claim 1
It sets, which is characterized in that water-bath tube sheet (8) uses the hollow tube sheet of glass fiber plastic production, and 30 tube sheet threaded holes are distributed with thereon
(10), and each tube sheet threaded hole (10) diameter is 2 centimetres.
3. a kind of explosion-proof dress extracted for plant proline with the processing of assay boiling water bath according to claim 1
It sets, which is characterized in that water-bath pipe (7) is glass fiber plastic water-bath pipe, length 10cm, overall diameter 2cm, internal diameter 1.6-1.8cm, pipe
Wall thickness 1-2mm, water-bath pipe (7) top are annular groove (4), are equipped with outside water-bath pipe at the one third of its outer wall middle and upper part
Wall screw thread (5), water-bath pipe (7) be connected to tube sheet threaded hole (10) it is interior when, make equipped with reaction solution water-bath pipe (7) bottom and boiling
Water comes into full contact with, and has graduation indication line (6) in the middle part of the outer wall of water-bath pipe (7), indicates that this position is at liquor capacity 10ml.
4. a kind of explosion-proof dress extracted for plant proline with the processing of assay boiling water bath according to claim 3
Set, which is characterized in that dimension pressure ceramic cap (1) medial center be hemispherical projections structure (2), hemispherical projections structure (2) with
The corresponding matching of nozzle of matched water-bath pipe (7), at the beginning of heating, by gravity, the hemispherical of dimension pressure ceramic cap (1)
Bulge-structure (2) can be tightly attached to the nozzle of water-bath pipe (7), and after water-bath pipe (7) interior liquid boiling, steam rising opens top dimension
Ceramic cap (1) evolution is pressed, drops to water-bath pipe (7) interior pressure within the scope of safety value.
5. a kind of plant proline according to claim 4 extracts the explosion-protection equipment with the processing of assay boiling water bath,
It is characterized in that, the inside of dimension pressure ceramic cap (1) is that lower edge has symmetrical two spring clipes (3), spring clip (3) and water
Annular groove (4) corresponding matching of bath pipe (7), after the boiling of water-bath liquid in pipe, steam rising opens top dimension pressure ceramics
When covering (1), by the fixed function of spring clip (3) dimension pressure ceramic cap (1) will not fall off.
6. a kind of plant proline according to claim 5 extracts the explosion-protection equipment with the processing of assay boiling water bath,
It is characterized in that, spring clip (3) top has the gap of 2mm on the inside of dimension pressure ceramic cap (1), at the beginning of heating dimension pressure ceramic cap
(1) it is tightly attached to water-bath nozzle by the effect of gravity, after liquid in pipe boiling, steam rising opens top dimension pressure ceramic cap (1),
By this gap, guarantees that dimension pressure ceramic cap (1) rises certain altitude, there is sufficient space to discharge gas in water-bath pipe.
7. a kind of plant proline according to claim 2 extracts the explosion-protection equipment with the processing of assay boiling water bath,
It is characterized in that, water-bath tube sheet (8) is with the discontiguous tube sheet gas vent (9) that multiple 0.5 cm of diameter are distributed with above of water for managing
Plate floats on the boiling water of water-bath (11).
8. a kind of plant proline according to claim 1 extracts the explosion-protection equipment with the processing of assay boiling water bath,
It is characterized in that, dimension pressure ceramic cap is made of ceramic material.
9. a kind of plant proline a method as claimed in any one of claims 1-8 extracts the explosion-protection equipment with the processing of assay boiling water bath
Application method, which comprises the following steps:
1), water-bath pipe is screwed on hollow water-bath tube sheet by water-bath pipe outer wall, by water-bath tube sheet and water-bath pipe two
Fixation is tightened by screw thread in part, and when to avoid carrying out heating operation in water-bath, water-bath pipe, which is detached from water-bath tube sheet, causes pipe
Interior reaction solution evolution, causes the failure of an experiment and device to damage, while guaranteeing the opening direction of water-bath pipe and the tube sheet of water-bath tube sheet
Gas vent direction is consistent；
2), various reagents solution to be reacted proportionally is sequentially added in water-bath pipe, for guarantee experimental result accuracy,
Institute's reagent adding total volume should be no more than the graduation indication line of water-bath pipe, that is, be no more than 10ml；
3), dimension pressure ceramic cap is connected to the upper orifice of water-bath pipe, the spring clip of dimension pressure ceramic cap is made to block water-bath pipe top
The annular groove of nozzle lower edge；
4), entire explosion-protection equipment is placed in water-bath, heating boil, boil reaction reach measurement require after, stop plus
Heat operation, it is cooling to take out explosion-protection equipment.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910161438.0A CN109908855B (en) | 2019-03-04 | 2019-03-04 | Explosion-proof device for plant proline extraction and content determination boiling water bath treatment and use method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910161438.0A CN109908855B (en) | 2019-03-04 | 2019-03-04 | Explosion-proof device for plant proline extraction and content determination boiling water bath treatment and use method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109908855A true CN109908855A (en) | 2019-06-21 |
| CN109908855B CN109908855B (en) | 2021-04-23 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201910161438.0A Expired - Fee Related CN109908855B (en) | 2019-03-04 | 2019-03-04 | Explosion-proof device for plant proline extraction and content determination boiling water bath treatment and use method thereof |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0416759A1 (en) * | 1989-09-08 | 1991-03-13 | CEM Corporation | Ventable rupture diaphragm-protected container for heating contained materials by microwave radiation |
| CN203191235U (en) * | 2013-01-25 | 2013-09-11 | 陈兴旺 | Diffusion vessel for medical examination |
| CN203761794U (en) * | 2014-04-22 | 2014-08-13 | 青岛农业大学 | Reverse-floating preventing device for seed boiling water bath |
| CN203965222U (en) * | 2014-03-03 | 2014-11-26 | 广东省保化检测中心有限公司 | Multi-functional digestion tube |
| CN204469730U (en) * | 2015-02-16 | 2015-07-15 | 许磊 | A kind of anti-spilled centrifuge tube |
| CN204523010U (en) * | 2015-03-31 | 2015-08-05 | 中国矿业大学 | A kind of microwave chemical reaction intensified condenser tube |
-
2019
- 2019-03-04 CN CN201910161438.0A patent/CN109908855B/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0416759A1 (en) * | 1989-09-08 | 1991-03-13 | CEM Corporation | Ventable rupture diaphragm-protected container for heating contained materials by microwave radiation |
| CN203191235U (en) * | 2013-01-25 | 2013-09-11 | 陈兴旺 | Diffusion vessel for medical examination |
| CN203965222U (en) * | 2014-03-03 | 2014-11-26 | 广东省保化检测中心有限公司 | Multi-functional digestion tube |
| CN203761794U (en) * | 2014-04-22 | 2014-08-13 | 青岛农业大学 | Reverse-floating preventing device for seed boiling water bath |
| CN204469730U (en) * | 2015-02-16 | 2015-07-15 | 许磊 | A kind of anti-spilled centrifuge tube |
| CN204523010U (en) * | 2015-03-31 | 2015-08-05 | 中国矿业大学 | A kind of microwave chemical reaction intensified condenser tube |
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| CN109908855B (en) | 2021-04-23 |
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Granted publication date: 20210423 |