CN109895294A - A kind of preparation method of Novel rubber tire isolation release agent - Google Patents
A kind of preparation method of Novel rubber tire isolation release agent Download PDFInfo
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- CN109895294A CN109895294A CN201711313551.3A CN201711313551A CN109895294A CN 109895294 A CN109895294 A CN 109895294A CN 201711313551 A CN201711313551 A CN 201711313551A CN 109895294 A CN109895294 A CN 109895294A
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- release agent
- rubber tire
- novel rubber
- preparation
- tire isolation
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Abstract
The present invention provides a kind of preparation method of Novel rubber tire isolation release agent, comprising the following steps: matches according to deal and claims polytetrafluoroethylene (PTFE), methyl-silicone oil, polyacrylamide, fatty alcohol, polyglycol ether, toluene, is put into blender after above-mentioned raw materials are mixed；Fat ether sulfate, phthalandione N-butyl, sodium xylene sulfonate, isomeric alcohol polyethenoxy ether are weighed according to deal proportion, is put into the blender in 1, stirs after above-mentioned raw materials are mixed；Deionized water, crosslinking agent and catalyst is added, continues to stir 15-30min, a kind of Novel rubber tire isolation release agent can be obtained.The preparation method of Novel rubber tire isolation release agent of the present invention, stable chemical performance have the advantages that be easily dispersed, adding proportion is low etc., and when preparing uniform film and complex-shaped molding with it, accurate size, the high formed products of qualification rate can be obtained.
Description
Technical field
The present invention relates to rubber chemicals field, in particular to a kind of rubber tyre.
Background technique
Novel rubber tire isolation release agent can improve outside product as the important auxiliary agent of one of rubber tyre production process
Sight and performance improve product quality.Common release agent kind has wax class, silicone oil, soaps etc., has their own characteristics each；And it commonly uses
Interleaving agent be mainly inorganic particle such as talcum powder etc., white critical defect is emitted in use process there are dust pollution and product,
Developing one kind overcomes disadvantages described above at present, and the separating releasing agent for having both the two advantage is necessary.
Nanometer calcium carbonate refers to calcium carbonate of the partial size between 1-100nm, can be used as plastics, rubber, macromolecule resin etc.
Reinforcing agent, improve properties of product, improve product quality.It is typically due to calcium carbonate surface and contains the presentations table such as calcium ion, hydroxyl
The hydrophilic and oleophobic feature in face, is easy to reunite in high molecular material system, cannot disperse very well, and it is modified to change to need to carry out surface
It is apt to the compatibility of itself and organic material and high molecular material.
Due to inorganic nano grade particle have the advantages that possess than common micro grade particle it is many incomparable, extensively
For the modifying process of industrial products, to enhance product performance.So, using suitable emulsification system, nano-sized carbon is prepared in situ
Sour calcium lotion, then again with film forming matter lotion mixing and emulsifying, it is expected to obtain a kind of nothing of calcium carbonate particle containing organic/inorganic nano
Machine-organic composite rubber separating releasing agent.Have no that pertinent literature is reported at present.
Summary of the invention
To solve the above-mentioned problems, the present invention provides a kind of preparation methods of Novel rubber tire isolation release agent.
A kind of preparation method of Novel rubber tire isolation release agent, preparation method the following steps are included:
(1), it is matched according to deal and claims polytetrafluoroethylene (PTFE), methyl-silicone oil, polyacrylamide, fatty alcohol, polyglycol ether, toluene,
Be put into blender after above-mentioned raw materials are mixed, 50-90 DEG C at a temperature of, persistently stir 40-70min；
(1), fat ether sulfate, phthalandione N-butyl, sodium xylene sulfonate, isomery alcohol polyoxyethylene are weighed according to deal proportion
Ether is put into the blender in (1) after mixing above-mentioned raw materials, 60-90 DEG C at a temperature of, persistently stir 40-60min；
(3), deionized water is added in the blender in (2), after 20-30min is sufficiently stirred, adds crosslinking agent and catalyst, after
Continuous stirring 15-30min, can be obtained a kind of Novel rubber tire isolation release agent.
The preparation method of Novel rubber tire isolation release agent of the invention, the polytetrafluoroethylene (PTFE), methyl-silicone oil, polypropylene
Amide, fatty alcohol weight ratio be 150-180:35-55:22-38:15-28.
The preparation method of Novel rubber tire isolation release agent of the invention, the polyglycol ether, fat ether sulfate, phthalandione
N-butyl, the weight ratio of sodium xylene sulfonate are 20-36:90-130:19-33:21-26.
The preparation method of Novel rubber tire isolation release agent of the invention, the mica powder, toluene, isomery alcohol polyoxyethylene
Ether, deionized water weight ratio be 25-40:13-24:7-12:180-270.
The beneficial effects of the present invention are:
The preparation method of Novel rubber tire isolation release agent of the present invention, stable chemical performance have and are easily dispersed, add
Accurate size can be obtained when preparing uniform film and complex-shaped molding with it in the advantages such as ratio is low, and qualification rate is high
Formed products.
Specific embodiment
A kind of preparation method of Novel rubber tire isolation release agent, preparation method the following steps are included:
(1), it is matched according to deal and claims polytetrafluoroethylene (PTFE), methyl-silicone oil, polyacrylamide, fatty alcohol, polyglycol ether, toluene,
Be put into blender after above-mentioned raw materials are mixed, 50-90 DEG C at a temperature of, persistently stir 40-70min；
(1), fat ether sulfate, phthalandione N-butyl, sodium xylene sulfonate, isomery alcohol polyoxyethylene are weighed according to deal proportion
Ether is put into the blender in (1) after mixing above-mentioned raw materials, 60-90 DEG C at a temperature of, persistently stir 40-60min；
(3), deionized water is added in the blender in (2), after 20-30min is sufficiently stirred, adds crosslinking agent and catalyst, after
Continuous stirring 15-30min, can be obtained a kind of Novel rubber tire isolation release agent.
The preparation method of Novel rubber tire isolation release agent of the invention, the polytetrafluoroethylene (PTFE), methyl-silicone oil, polypropylene
Amide, fatty alcohol weight ratio be 150-180:35-55:22-38:15-28.
The preparation method of Novel rubber tire isolation release agent of the invention, the polyglycol ether, fat ether sulfate, phthalandione
N-butyl, the weight ratio of sodium xylene sulfonate are 20-36:90-130:19-33:21-26.
The preparation method of Novel rubber tire isolation release agent of the invention, the mica powder, toluene, isomery alcohol polyoxyethylene
Ether, deionized water weight ratio be 25-40:13-24:7-12:180-270.
In addition to this patent disclosure, protection scope of the present invention is also belonged to according to the innovation and creation on this patent basis.
Claims (4)
1. a kind of preparation method of Novel rubber tire isolation release agent, which comprises the following steps:
(1), it is matched according to deal and claims polytetrafluoroethylene (PTFE), methyl-silicone oil, polyacrylamide, fatty alcohol, polyglycol ether, toluene,
Be put into blender after above-mentioned raw materials are mixed, 50-90 DEG C at a temperature of, persistently stir 40-70min；
(1), fat ether sulfate, phthalandione N-butyl, sodium xylene sulfonate, isomery alcohol polyoxyethylene are weighed according to deal proportion
Ether is put into the blender in (1) after mixing above-mentioned raw materials, 60-90 DEG C at a temperature of, persistently stir 40-60min；
(3), deionized water is added in the blender in (2), after 20-30min is sufficiently stirred, adds crosslinking agent and catalyst, after
Continuous stirring 15-30min, can be obtained a kind of Novel rubber tire isolation release agent.
2. the preparation method of Novel rubber tire isolation release agent according to claim 1, which is characterized in that the polytetrafluoroethyl-ne
Alkene, methyl-silicone oil, polyacrylamide, fatty alcohol weight ratio be 150-180:35-55:22-38:15-28.
3. the preparation method of Novel rubber tire isolation release agent according to claim 1, which is characterized in that the polyethylene glycol
Ether, fat ether sulfate, phthalandione N-butyl, the weight ratio of sodium xylene sulfonate are 20-36:90-130:19-33:21-26.
4. the preparation method of Novel rubber tire isolation release agent according to claim 1, which is characterized in that the mica powder,
Toluene, isomeric alcohol polyethenoxy ether, the weight ratio of deionized water are 25-40:13-24:7-12:180-270.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711313551.3A CN109895294A (en) | 2017-12-09 | 2017-12-09 | A kind of preparation method of Novel rubber tire isolation release agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711313551.3A CN109895294A (en) | 2017-12-09 | 2017-12-09 | A kind of preparation method of Novel rubber tire isolation release agent |
Publications (1)
| Publication Number | Publication Date |
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| CN109895294A true CN109895294A (en) | 2019-06-18 |
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| CN201711313551.3A Pending CN109895294A (en) | 2017-12-09 | 2017-12-09 | A kind of preparation method of Novel rubber tire isolation release agent |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111633885A (en) * | 2020-06-12 | 2020-09-08 | 欧士曼(台州)高分子科技有限公司 | High-temperature-resistant rubber mold release agent and preparation method thereof |
| CN116554717A (en) * | 2023-04-27 | 2023-08-08 | 天津福尔欣汽车线缆有限公司 | Isolating agent for silicon rubber insulated automobile cable and coating process method |
-
2017
- 2017-12-09 CN CN201711313551.3A patent/CN109895294A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111633885A (en) * | 2020-06-12 | 2020-09-08 | 欧士曼(台州)高分子科技有限公司 | High-temperature-resistant rubber mold release agent and preparation method thereof |
| CN116554717A (en) * | 2023-04-27 | 2023-08-08 | 天津福尔欣汽车线缆有限公司 | Isolating agent for silicon rubber insulated automobile cable and coating process method |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20190618 |
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| WD01 | Invention patent application deemed withdrawn after publication |