CN109852156A - A kind of high aluminum-carbon refractory material and preparation method thereof can be improved corrosion resistance - Google Patents
A kind of high aluminum-carbon refractory material and preparation method thereof can be improved corrosion resistance Download PDFInfo
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- CN109852156A CN109852156A CN201811361652.2A CN201811361652A CN109852156A CN 109852156 A CN109852156 A CN 109852156A CN 201811361652 A CN201811361652 A CN 201811361652A CN 109852156 A CN109852156 A CN 109852156A
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- corrosion resistance
- refractory material
- carbon refractory
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Abstract
The invention discloses a kind of high aluminum-carbon refractory materials that can be improved corrosion resistance, including following component (by mass percentage): polystyrene resin 15~22%, organic siliconresin 8-12%, C9 Petropols 5.5-7.5%, metallic silicon power 4.8-6.4%, water are surplus;The invention also discloses a kind of preparation methods of high aluminum-carbon refractory material that can be improved corrosion resistance, comprising the following steps: ingredient, mixing prepare modified maleic acid solution, secondary mixing and filtering;Formula of the invention is more reasonable, using polystyrene resin, organic siliconresin and C9 Petropols after different processing, cooperation addition increases metallic silicon power, silicon carbide and a variety of high alumina graphite materials of aluminium oxide, increase the compactness of products molecule space structure, and then increase the corrosion resistance of product, the corrosion resistance of product is improved, the raw material of use is non-toxic material, has environment friendly and pollution-free feature.
Description
Technical field
The present invention relates to technical field of refractory materials, specially a kind of high alumina carbonaceous fire proofed wood that can be improved corrosion resistance
Material and preparation method thereof.
Background technique
Refractory material, which refers to, is painted on body surface, can prevent fire, and fire spreading is prevented to propagate or be isolated fire source,
Extend substrate ignition time or increase heat-insulating property to postpone a kind of coating of structural deterioration time, continuous casting steel machine uses at present
Aluminum-carbon refractory material is to be coated directly on the surface of steel, but existing aluminum-carbon refractory material, also generally existing anti-erosion
The disadvantage of property weak, anti-corrosion and persistence difference, for this purpose, it is proposed that a kind of high aluminum-carbon refractory material that can be improved corrosion resistance
And preparation method thereof.
Summary of the invention
The purpose of the present invention is to provide a kind of high aluminum-carbon refractory material that can be improved corrosion resistance and its preparation sides
Method, to solve the problems, such as that background technique proposes.
To achieve the above object, the invention provides the following technical scheme: a kind of high alumina carbonaceous that can be improved corrosion resistance
Refractory material, including following component (by mass percentage): polystyrene resin 15~22%, organic siliconresin 8-12%,
C9 Petropols 5.5-7.5%, metallic silicon power 4.8-6.4%, silicon carbide 3.2-3.8%, aluminium oxide 3.8-4.2%, You Jirong
Agent 5.65-6.12%, it polyethylene wax 2.45-3.15%, acetic acid butanol 2.24-4.58%, aluminum stearate 1.39-3.25%, helps
Agent 5-10%, water are surplus.
Preferably, including following component (by mass percentage): polystyrene resin 22%, organic siliconresin 8%, C9
Petropols 5.5%, metallic silicon power 4.8%, silicon carbide 3.2%, aluminium oxide 3.8%, organic solvent 5.65%, polyethylene wax
2.45%, acetic acid butanol 2.24%, aluminum stearate 1.39%, auxiliary agent 5%, water are surplus.
Preferably, including following component (by mass percentage): polystyrene resin 20%, organic siliconresin 11%,
C9 Petropols 7%, metallic silicon power 6%, silicon carbide 3.6%, aluminium oxide 4.1%, organic solvent 5.95%, polyethylene wax
2.87%, acetic acid butanol 4.13%, aluminum stearate 2.85%, auxiliary agent 8%, water are surplus.
Preferably, including following component (by mass percentage): polystyrene resin 17%, organic siliconresin 9%, C9
Petropols 6.5%, metallic silicon power 5.5%, silicon carbide 3.4%, aluminium oxide 3.9%, organic solvent 5.72%, polyethylene wax
2.61%, acetic acid butanol 3.64%, aluminum stearate 1.87%, auxiliary agent 6%, water are surplus.
Preferably, including following component (by mass percentage): polystyrene resin 15%, organic siliconresin 12%,
C9 Petropols 7.5%, metallic silicon power 6.4%, silicon carbide 3.8%, aluminium oxide 4.2%, organic solvent 6.12%, polyethylene wax
3.15%, acetic acid butanol 4.58%, aluminum stearate 3.25%, auxiliary agent 10%, water are surplus.
Preferably, the auxiliary agent includes high-temperature-resistant adhesive, bleeding agent, defoaming agent and diluent, and high-temperature-resistant adhesive,
The ratio of bleeding agent, defoaming agent and diluent is 2:2:1:1, and the bleeding agent is Disodium sulfosuccinate solvent, the defoaming
Agent is organosiloxane, and the diluent is Vinylidene Chloride.
A kind of preparation method for the high aluminum-carbon refractory material can be improved corrosion resistance as described above, including following step
It is rapid:
Step 1: ingredient ingredient: is carried out according to the set component of high aluminum-carbon refractory material;
Step 2: mixing: polystyrene resin and organic siliconresin are added in magnetic stirring apparatus, and the mixing of 50% water, temperature is added
Degree control at 45~65 DEG C, then use magnetic stirring apparatus with 140~170 revs/min stirring 10-20 minutes, obtain hybrid resin
Solution;
Step 3: it prepares modified maleic acid solution: acetic acid butanol and polyethylene wax being mixed and heated to 150~170 DEG C, instead
It is spare that modified acetic acid butanol is obtained after answering completely, is then heated to aluminum stearate, C9 Petropols and remaining 50% water mixing
65~80 DEG C of formation mixed solutions, then modified acetic acid butanol, maleic acid and mixed solution are mixed, pass through magnetic stirring apparatus
It is stirred 20~30 minutes with 200~300 revs/min, obtains modified maleic acid solution;
Step 4: secondary mixing: modified maleic acid solution obtained in step 3 is added in mixed resin solution, then
Metallic silicon power, silicon carbide, silicon carbide and organic solvent are sequentially added, starts to stir, mixing time 240-360r/min, stirring
When temperature setting be 35-55 DEG C, stirring 3-7 minute after auxiliary agent is added, continue stir 10-20 minutes, obtain mixed material;
Step 5: filtering: mixed material obtained in step 4 is added in filter and is filtered, fineness is obtained after filtering
For 20~40 μm of material, filtered material is high aluminum-carbon refractory material.
Compared with prior art, the beneficial effects of the present invention are: formula of the invention is more reasonable, using polystyrene
After different processing, cooperation addition increases metallic silicon power, silicon carbide and oxygen for resin, organic siliconresin and C9 Petropols
Change a variety of high alumina graphite materials of aluminium, increase the compactness of products molecule space structure, and then increase the corrosion resistance of product,
Present invention employs modified maleic acid, modified maleic acid and butyl acetate react to each other cooperation, form oiliness and prevent
Rotten agent improves the corrosion resistance of product, and the raw material of use is non-toxic material, has environment friendly and pollution-free feature;And
Preparation method of the invention is more scientific and reasonable, and equipment requirement is low, has good promotion effect.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment one:
A kind of high aluminum-carbon refractory material can be improved corrosion resistance, including following component (by mass percentage): polyphenyl
Vinyl 22%, organic siliconresin 8%, C9 Petropols 5.5%, metallic silicon power 4.8%, silicon carbide 3.2%, aluminium oxide
3.8%, organic solvent 5.65%, polyethylene wax 2.45%, acetic acid butanol 2.24%, aluminum stearate 1.39%, auxiliary agent 5%, water
For surplus.
Further, auxiliary agent includes high-temperature-resistant adhesive, bleeding agent, defoaming agent and diluent, and high-temperature-resistant adhesive, infiltration
The ratio of saturating agent, defoaming agent and diluent is 2:2:1:1, and bleeding agent is Disodium sulfosuccinate solvent, and defoaming agent is organosilicon
Oxygen alkane, diluent are Vinylidene Chloride.
A kind of preparation method of the high aluminum-carbon refractory material that can be improved corrosion resistance as above, comprising the following steps:
Step 1: ingredient ingredient: is carried out according to the set component of high aluminum-carbon refractory material;
Step 2: mixing: polystyrene resin and organic siliconresin are added in magnetic stirring apparatus, and the mixing of 50% water, temperature is added
Then degree control is used magnetic stirring apparatus to be stirred 10 minutes with 140 revs/min, obtains mixed resin solution at 45 DEG C;
Step 3: it prepares modified maleic acid solution: acetic acid butanol and polyethylene wax being mixed and heated to 150 DEG C, reacted
It is spare that modified acetic acid butanol is obtained after complete, and aluminum stearate, C9 Petropols and remaining 50% water mixing are then heated to 65 DEG C
Form mixed solution, then modified acetic acid butanol, maleic acid and mixed solution mixed, by magnetic stirring apparatus with 200 turns/
Divide stirring 20 minutes, obtains modified maleic acid solution;
Step 4: secondary mixing: modified maleic acid solution obtained in step 3 is added in mixed resin solution, then
Metallic silicon power, silicon carbide, silicon carbide and organic solvent are sequentially added, starts to stir, mixing time 240r/min, temperature when stirring
Degree is set as 35 DEG C, and auxiliary agent is added after 3 minutes in stirring, continues stirring 10 minutes, obtains mixed material;
Step 5: filtering: mixed material obtained in step 4 is added in filter and is filtered, fineness is obtained after filtering
For 20 μm of material, filtered material is high aluminum-carbon refractory material.
Embodiment two:
A kind of high aluminum-carbon refractory material can be improved corrosion resistance, including following component (by mass percentage): polyphenyl
Vinyl 20%, organic siliconresin 11%, C9 Petropols 7%, metallic silicon power 6%, silicon carbide 3.6%, aluminium oxide
4.1%, organic solvent 5.95%, polyethylene wax 2.87%, acetic acid butanol 4.13%, aluminum stearate 2.85%, auxiliary agent 8%, water
For surplus.
Further, auxiliary agent includes high-temperature-resistant adhesive, bleeding agent, defoaming agent and diluent, and high-temperature-resistant adhesive, infiltration
The ratio of saturating agent, defoaming agent and diluent is 2:2:1:1, and bleeding agent is Disodium sulfosuccinate solvent, and defoaming agent is organosilicon
Oxygen alkane, diluent are Vinylidene Chloride.
A kind of preparation method of the high aluminum-carbon refractory material that can be improved corrosion resistance as above, comprising the following steps:
Step 1: ingredient ingredient: is carried out according to the set component of high aluminum-carbon refractory material;
Step 2: mixing: polystyrene resin and organic siliconresin are added in magnetic stirring apparatus, and the mixing of 50% water, temperature is added
Then degree control is used magnetic stirring apparatus to be stirred 13 minutes with 150 revs/min, obtains mixed resin solution at 55 DEG C;
Step 3: it prepares modified maleic acid solution: acetic acid butanol and polyethylene wax being mixed and heated to 155 DEG C, reacted
It is spare that modified acetic acid butanol is obtained after complete, and aluminum stearate, C9 Petropols and remaining 50% water mixing are then heated to 70 DEG C
Form mixed solution, then modified acetic acid butanol, maleic acid and mixed solution mixed, by magnetic stirring apparatus with 220 turns/
Divide stirring 25 minutes, obtains modified maleic acid solution;
Step 4: secondary mixing: modified maleic acid solution obtained in step 3 is added in mixed resin solution, then
Metallic silicon power, silicon carbide, silicon carbide and organic solvent are sequentially added, starts to stir, mixing time 280r/min, temperature when stirring
Degree is set as 40 DEG C, and auxiliary agent is added in stirring after five minutes, continues stirring 14 minutes, obtains mixed material;
Step 5: filtering: mixed material obtained in step 4 is added in filter and is filtered, fineness is obtained after filtering
For 25 μm of material, filtered material is high aluminum-carbon refractory material.
Embodiment three:
A kind of high aluminum-carbon refractory material can be improved corrosion resistance, including following component (by mass percentage): polyphenyl
Vinyl 17%, organic siliconresin 9%, C9 Petropols 6.5%, metallic silicon power 5.5%, silicon carbide 3.4%, aluminium oxide
3.9%, organic solvent 5.72%, polyethylene wax 2.61%, acetic acid butanol 3.64%, aluminum stearate 1.87%, auxiliary agent 6%, water
For surplus.
Further, auxiliary agent includes high-temperature-resistant adhesive, bleeding agent, defoaming agent and diluent, and high-temperature-resistant adhesive, infiltration
The ratio of saturating agent, defoaming agent and diluent is 2:2:1:1, and bleeding agent is Disodium sulfosuccinate solvent, and defoaming agent is organosilicon
Oxygen alkane, diluent are Vinylidene Chloride.
A kind of preparation method of the high aluminum-carbon refractory material that can be improved corrosion resistance as above, comprising the following steps:
Step 1: ingredient ingredient: is carried out according to the set component of high aluminum-carbon refractory material;
Step 2: mixing: polystyrene resin and organic siliconresin are added in magnetic stirring apparatus, and the mixing of 50% water, temperature is added
Then degree control is used magnetic stirring apparatus to be stirred 18 minutes with 160 revs/min, obtains mixed resin solution at 60 DEG C;
Step 3: it prepares modified maleic acid solution: acetic acid butanol and polyethylene wax being mixed and heated to 165 DEG C, reacted
It is spare that modified acetic acid butanol is obtained after complete, and aluminum stearate, C9 Petropols and remaining 50% water mixing are then heated to 75 DEG C
Form mixed solution, then modified acetic acid butanol, maleic acid and mixed solution mixed, by magnetic stirring apparatus with 280 turns/
Divide stirring 28 minutes, obtains modified maleic acid solution;
Step 4: secondary mixing: modified maleic acid solution obtained in step 3 is added in mixed resin solution, then
Metallic silicon power, silicon carbide, silicon carbide and organic solvent are sequentially added, starts to stir, mixing time 320r/min, temperature when stirring
Degree is set as 50 DEG C, and auxiliary agent is added after 6 minutes in stirring, continues stirring 17 minutes, obtains mixed material;
Step 5: filtering: mixed material obtained in step 4 is added in filter and is filtered, fineness is obtained after filtering
For 35 μm of material, filtered material is high aluminum-carbon refractory material.
Example IV:
A kind of high aluminum-carbon refractory material can be improved corrosion resistance, including following component (by mass percentage): polyphenyl
Vinyl 15%, organic siliconresin 12%, C9 Petropols 7.5%, metallic silicon power 6.4%, silicon carbide 3.8%, aluminium oxide
4.2%, organic solvent 6.12%, polyethylene wax 3.15%, acetic acid butanol 4.58%, aluminum stearate 3.25%, auxiliary agent 10%, water
For surplus.
Further, auxiliary agent includes high-temperature-resistant adhesive, bleeding agent, defoaming agent and diluent, and high-temperature-resistant adhesive, infiltration
The ratio of saturating agent, defoaming agent and diluent is 2:2:1:1, and bleeding agent is Disodium sulfosuccinate solvent, and defoaming agent is organosilicon
Oxygen alkane, diluent are Vinylidene Chloride.
A kind of preparation method of the high aluminum-carbon refractory material that can be improved corrosion resistance as above, comprising the following steps:
Step 1: ingredient ingredient: is carried out according to the set component of high aluminum-carbon refractory material;
Step 2: mixing: polystyrene resin and organic siliconresin are added in magnetic stirring apparatus, and the mixing of 50% water, temperature is added
Then degree control is used magnetic stirring apparatus to be stirred 20 minutes with 170 revs/min, obtains mixed resin solution at 65 DEG C;
Step 3: it prepares modified maleic acid solution: acetic acid butanol and polyethylene wax being mixed and heated to 170 DEG C, reacted
It is spare that modified acetic acid butanol is obtained after complete, and aluminum stearate, C9 Petropols and remaining 50% water mixing are then heated to 80 DEG C
Form mixed solution, then modified acetic acid butanol, maleic acid and mixed solution mixed, by magnetic stirring apparatus with 300 turns/
Divide stirring 30 minutes, obtains modified maleic acid solution;
Step 4: secondary mixing: modified maleic acid solution obtained in step 3 is added in mixed resin solution, then
Metallic silicon power, silicon carbide, silicon carbide and organic solvent are sequentially added, starts to stir, mixing time 360r/min, temperature when stirring
Degree is set as 55 DEG C, and auxiliary agent is added after 7 minutes in stirring, continues stirring 20 minutes, obtains mixed material;
Step 5: filtering: mixed material obtained in step 4 is added in filter and is filtered, fineness is obtained after filtering
For 40 μm of material, filtered material is high aluminum-carbon refractory material.
High aluminum-carbon refractory material can be made in above four groups of embodiments, and formula of the invention is more reasonable, adopts
With polystyrene resin, organic siliconresin and C9 Petropols after different processing, cooperation addition increase metallic silicon power,
Silicon carbide and a variety of high alumina graphite materials of aluminium oxide, increase the compactness of products molecule space structure, and then increase product
Corrosion resistance, present invention employs modified maleic acid, modified maleic acid and butyl acetate react to each other cooperation, shape
At oiliness preservative, the corrosion resistance of product is improved, the raw material of use is non-toxic material, is had environment friendly and pollution-free
Feature;And preparation method of the invention is more scientific and reasonable, and equipment requirement is low, has good promotion effect.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (7)
1. a kind of high aluminum-carbon refractory material that can be improved corrosion resistance, which is characterized in that (press quality hundred including following component
Divide than meter): polystyrene resin 15~22%, organic siliconresin 8-12%, C9 Petropols 5.5-7.5%, metallic silicon power
4.8-6.4%, silicon carbide 3.2-3.8%, aluminium oxide 3.8-4.2%, organic solvent 5.65-6.12%, polyethylene wax 2.45-
3.15%, acetic acid butanol 2.24-4.58%, aluminum stearate 1.39-3.25%, auxiliary agent 5-10%, water are surplus.
2. a kind of high aluminum-carbon refractory material that can be improved corrosion resistance according to claim 1, which is characterized in that packet
It includes following component (by mass percentage): polystyrene resin 22%, organic siliconresin 8%, C9 Petropols 5.5%, gold
Belong to silicon powder 4.8%, silicon carbide 3.2%, aluminium oxide 3.8%, organic solvent 5.65%, polyethylene wax 2.45%, acetic acid butanol
2.24%, aluminum stearate 1.39%, auxiliary agent 5%, water are surplus.
3. a kind of high aluminum-carbon refractory material that can be improved corrosion resistance according to claim 1, which is characterized in that packet
It includes following component (by mass percentage): polystyrene resin 20%, organic siliconresin 11%, C9 Petropols 7%, metal
Silicon powder 6%, silicon carbide 3.6%, aluminium oxide 4.1%, organic solvent 5.95%, polyethylene wax 2.87%, acetic acid butanol 4.13%,
Aluminum stearate 2.85%, auxiliary agent 8%, water are surplus.
4. a kind of high aluminum-carbon refractory material that can be improved corrosion resistance according to claim 1, which is characterized in that packet
It includes following component (by mass percentage): polystyrene resin 17%, organic siliconresin 9%, C9 Petropols 6.5%, gold
Belong to silicon powder 5.5%, silicon carbide 3.4%, aluminium oxide 3.9%, organic solvent 5.72%, polyethylene wax 2.61%, acetic acid butanol
3.64%, aluminum stearate 1.87%, auxiliary agent 6%, water are surplus.
5. a kind of high aluminum-carbon refractory material that can be improved corrosion resistance according to claim 1, which is characterized in that packet
It includes following component (by mass percentage): polystyrene resin 15%, organic siliconresin 12%, C9 Petropols 7.5%, gold
Belong to silicon powder 6.4%, silicon carbide 3.8%, aluminium oxide 4.2%, organic solvent 6.12%, polyethylene wax 3.15%, acetic acid butanol
4.58%, aluminum stearate 3.25%, auxiliary agent 10%, water are surplus.
6. a kind of high aluminum-carbon refractory material that can be improved corrosion resistance described in -5 any one according to claim 1,
Be characterized in that: the auxiliary agent includes high-temperature-resistant adhesive, bleeding agent, defoaming agent and diluent, and high-temperature-resistant adhesive, infiltration
The ratio of agent, defoaming agent and diluent is 2:2:1:1, and the bleeding agent is Disodium sulfosuccinate solvent, and the defoaming agent is
Organosiloxane, the diluent are Vinylidene Chloride.
7. a kind of preparation of the high aluminum-carbon refractory material that can be improved corrosion resistance as claimed in any one of claims 1 to 6
Method, which comprises the following steps:
Step 1: ingredient ingredient: is carried out according to the set component of high aluminum-carbon refractory material;
Step 2: mixing: polystyrene resin and organic siliconresin are added in magnetic stirring apparatus, and the mixing of 50% water, temperature is added
Degree control at 45~65 DEG C, then use magnetic stirring apparatus with 140~170 revs/min stirring 10-20 minutes, obtain hybrid resin
Solution;
Step 3: it prepares modified maleic acid solution: acetic acid butanol and polyethylene wax being mixed and heated to 150~170 DEG C, instead
It is spare that modified acetic acid butanol is obtained after answering completely, is then heated to aluminum stearate, C9 Petropols and remaining 50% water mixing
65~80 DEG C of formation mixed solutions, then modified acetic acid butanol, maleic acid and mixed solution are mixed, pass through magnetic stirring apparatus
It is stirred 20~30 minutes with 200~300 revs/min, obtains modified maleic acid solution;
Step 4: secondary mixing: modified maleic acid solution obtained in step 3 is added in mixed resin solution, then
Metallic silicon power, silicon carbide, silicon carbide and organic solvent are sequentially added, starts to stir, mixing time 240-360r/min, stirring
When temperature setting be 35-55 DEG C, stirring 3-7 minute after auxiliary agent is added, continue stir 10-20 minutes, obtain mixed material;
Step 5: filtering: mixed material obtained in step 4 is added in filter and is filtered, fineness is obtained after filtering
For 20~40 μm of material, filtered material is high aluminum-carbon refractory material.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN113800924A (en) * | 2021-09-08 | 2021-12-17 | 青岛彩意科技集团有限公司 | Refractory material resisting aluminum liquid corrosion and preparation method thereof |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN113800924A (en) * | 2021-09-08 | 2021-12-17 | 青岛彩意科技集团有限公司 | Refractory material resisting aluminum liquid corrosion and preparation method thereof |
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Application publication date: 20190607 |