CN109835867B - Etching solution and etching method - Google Patents
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- CN109835867B CN109835867B CN201711190003.6A CN201711190003A CN109835867B CN 109835867 B CN109835867 B CN 109835867B CN 201711190003 A CN201711190003 A CN 201711190003A CN 109835867 B CN109835867 B CN 109835867B
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Abstract
An etching solution and an etching method, the etching solution comprising: an etchant; an additive comprising barrier particles. The additive containing the blocking particles is added into the etching solution, after the side wall of the layer to be etched is exposed, the blocking particles enter the side wall position of the layer to be etched and are filled on the side wall of the layer to be etched, so that the purpose of inhibiting the etching agent from etching the side wall of the layer to be etched is achieved, the undercut problem is improved, the wet etching effect is improved, and the process efficiency and the etching effect are both facilitated.
Description
Technical Field
The invention relates to the field of semiconductor manufacturing, in particular to an etching solution and an etching method.
Background
Etching is a significant step in semiconductor manufacturing processes, microelectronic IC manufacturing processes, and micro-nano manufacturing processes, often in conjunction with photolithography, to achieve patterning of material films. The simplest and most commonly used etching is divided into dry etching and wet etching.
The dry etching is to etch the layer to be etched by utilizing plasma in the process cavity, and remove the layer to be etched by utilizing the reaction of the plasma and the material of the layer to be etched or the bombardment of the layer to be etched by utilizing the plasma. The dry etching has stronger directivity and better anisotropic etching performance, but only one Wafer can be accommodated in the process chamber in each dry etching process, namely, each dry etching can be carried out on one Wafer only, so that the process efficiency of the dry etching is lower, and the Wafer Per Hour (WPH) is smaller.
Wet etching is to soak the semiconductor structure to be treated in a certain chemical reagent or reagent solution after forming the resist mask layer on the semiconductor structure to be treated, so that the part of the material film layer not covered by the mask layer is chemically reacted with the reagent to be removed. Therefore, the adoption of wet etching can effectively improve the process efficiency and the hourly quantity of wafers.
However, when the wet etching is adopted in the prior art to process the layer to be etched, a serious undercut problem often occurs, so that the wet etching effect is affected, and the performance of the formed semiconductor structure is affected.
Disclosure of Invention
The invention solves the problem of providing an etching solution and an etching method to improve the undercut problem, improve the etching effect of wet etching and realize the compromise of the process efficiency and the etching effect.
In order to solve the above problems, the present invention provides an etching solution for wet etching a layer to be etched, including:
an etchant; an additive comprising barrier particles.
Optionally, the ratio of the blocking particle size to the thickness of the layer to be etched is in the range of 1/20 to 1/2.
Optionally, the blocking particles have a size in the range of 0.1 μm to 1 μm.
Optionally, in the additive, the mass percentage concentration of the blocking particles is in the range of 20% to 40%.
Optionally, the material of the blocking particles is a polymer material.
Optionally, the material of the barrier particles includes at least two of polyethylene, polypropylene, ethylene glycol, and water.
Optionally, the material of the blocking particles is a complex of polyethylene, polypropylene, ethylene glycol and water.
Optionally, the material of the layer to be etched is metal; the etchant is an acidic solution.
Optionally, the material of the layer to be etched is aluminum; the etchant comprises: one or more of phosphoric acid, nitric acid, and acetic acid.
Optionally, the etching solution temperature is in the range of 50 ℃ to 60 ℃; the vertical etching rate of the etchant to the layer to be etched is as follows
To->
Within the range.
Optionally, the additive accounts for greater than or equal to 0.5% of the etching solution by volume.
Optionally, the additive accounts for 0.8 to 1.2% of the etching solution by volume.
Correspondingly, the invention also provides an etching method, which comprises the following steps:
providing a substrate, wherein the substrate is provided with a layer to be etched; providing an etching solution of the present invention; and carrying out wet etching on the layer to be etched by adopting the etching solution, and patterning the layer to be etched to form a target pattern layer.
Optionally, the width of the target pattern layer is greater than 40 μm.
Optionally, the etching solution is adopted to carry out wet etching, and the flow of the etching agent is 8L/min to 10L/min.
Optionally, after wet etching, cleaning the target pattern layer.
Optionally, the cleaning treatment is performed on the target graphic layer by deionized water.
Compared with the prior art, the technical scheme of the invention has the following advantages:
in the technical scheme of the invention, the etching solution comprises the blocking particles, and in the process of carrying out wet etching on the layer to be etched by adopting the etching solution, after the side wall of the layer to be etched is exposed, the blocking particles can enter the side wall position of the layer to be etched and are filled on the side wall of the layer to be etched, so that the probability of the side wall of the layer to be etched contacting with the etching agent is reduced, the etching of the side wall of the layer to be etched by the etching agent is inhibited, the etching efficiency of the etching solution on the side wall of the layer to be etched is reduced, the aim of improving the undercut problem and the wet etching effect is fulfilled, and the method is beneficial to considering both the process efficiency and the etching effect.
In an alternative embodiment of the present invention, the ratio of the size of the barrier particles to the thickness of the layer to be etched is in the range of 1/20 to 1/2. The ratio of the blocking particle size to the thickness of the layer to be etched is not too large nor too small: if the ratio of the size of the blocking particles to the thickness of the layer to be etched is too large, the blocking particles may not enter the position of the side wall of the layer to be etched; if the ratio of the size of the blocking particles to the thickness of the layer to be etched is too small, the filling effect of the blocking particles on the side wall of the layer to be etched may be affected; the blocking particles can not enter the side wall position of the layer to be etched and the poor filling effect of the blocking particles on the side wall of the layer to be etched can affect the blocking particles to reduce the contact probability of the side wall of the layer to be etched and the etching agent, so that the etching agent is not easy to inhibit the etching of the side wall of the layer to be etched, and the undercut problem is not easy to improve.
In an alternative embodiment of the present invention, the volume ratio of the additive to the etchant is greater than or equal to 0.5%. The volume ratio of the additive to the etchant is too small, and the concentration of the blocking particles in the etching solution is too small, so that the blocking particles can influence the effect of reducing the contact probability of the side wall of the layer to be etched and the etchant, thereby being unfavorable for inhibiting the etching of the side wall of the layer to be etched by the etchant and improving the undercut problem.
In an alternative embodiment of the invention, the volume ratio of the additive to the etchant is in the range of 0.8% to 1.2%. In the wet etching process, the etching solution is lost along with the progress of the etching process, so that the volume ratio of the additive in the etching solution is set within a reasonable range, the blocking particles in the etching solution can be maintained at a certain concentration, the undercut problem can be improved, the etching efficiency of the etching solution on the layer to be etched can be ensured, and the process efficiency and the etching effect can be simultaneously realized.
In an alternative scheme of the invention, the material of the blocking particles is a high polymer material, specifically, the material of the blocking particles can be a mixture of at least two of polyethylene, polypropylene, ethylene glycol and water, and can also be a complex of polyethylene, polypropylene, ethylene glycol and water. The material of the blocking particles is reasonably arranged, so that adverse effects of the addition of the blocking particles on the semiconductor structure on the substrate can be effectively prevented, and the improvement of the manufacturing yield is facilitated; and the blocking particles can be removed later by cleaning, so that the residues of the blocking particles on the surface of the formed target pattern layer are reduced as much as possible, and the method is favorable for providing a good process surface for subsequent processes.
Drawings
FIGS. 1 to 2 are schematic diagrams showing cross-sectional structures corresponding to respective steps of a method for etching by a wet method;
FIGS. 3 to 6 are schematic cross-sectional views corresponding to steps of an etching method according to an embodiment of the present invention;
FIG. 7 is a graph of the results of testing the layer to be etched after etching by the prior art etching solution;
FIG. 8 is a graph showing the results of testing after etching the layer to be etched using the etching solution (0.2% by volume of additive) according to the present invention;
fig. 9 is a graph showing the results of the test performed after etching the layer to be etched using the etching solution of the present invention (the volume ratio of the additive is 1%).
Detailed Description
As known from the background art, in the prior art, wet etching is adopted to process a layer to be etched, so that a serious undercut problem exists. The reason for serious undercut problem is analyzed by combining a wet etching process:
referring to fig. 1 and 2, schematic cross-sectional structures corresponding to respective steps of a method for etching by wet method are shown.
As shown in fig. 1, a substrate 11 is provided, a layer 12 to be etched is formed on the substrate, and a mask layer 13 is formed on a part of the layer 12 to be etched; as shown in fig. 2, the layer to be etched 12 (shown in fig. 1) is wet etched with an etching solution, and the layer to be etched is patterned to form a target pattern layer 14.
Since wet etching is performed by using the material of the layer to be etched and the etching solution to react with each other, most of wet etching is isotropic (i.e., there is no significant difference in etching rate in any direction of the etching contact point.
On the other hand, the layer to be etched is thick, and after the layer to be etched is etched, the side wall of the layer to be etched is exposed and is in direct contact with the etching solution, so that the side wall of the layer to be etched is corroded by the etching solution, and a lateral erosion phenomenon, namely a undercut problem, occurs.
In order to solve the technical problems, the invention provides an etching solution and an etching method, wherein an additive containing blocking particles is added into the etching solution, after the side wall of a layer to be etched is exposed, the blocking particles enter the side wall position of the layer to be etched and are filled on the side wall of the layer to be etched, so that the purpose of inhibiting the etching agent from etching the side wall of the layer to be etched is achieved, the undercut problem is improved, the wet etching effect is improved, and the effects of being beneficial to the process efficiency and the etching effect are achieved.
In order that the above objects, features and advantages of the invention will be readily understood, a more particular description of the invention will be rendered by reference to specific embodiments thereof which are illustrated in the appended drawings.
Referring to fig. 3 to 6, schematic cross-sectional structures corresponding to the steps of an etching method according to an embodiment of the present invention are shown.
It should be noted that the etching method is only an example of forming the metal interconnection structure in the mems. In other embodiments of the present invention, the etching method may be also applicable to etching other metal or non-metal materials, which is not limited in the present invention.
Referring to fig. 3, a substrate 110 is provided, the substrate 110 having a layer 130 to be etched thereon.
The substrate 110 is used to provide a handling platform for subsequent processing.
In this embodiment, the material of the substrate 110 is monocrystalline silicon. In other embodiments of the present invention, the material of the substrate may be selected from polysilicon or amorphous silicon, and may also be selected from silicon, germanium, gallium arsenide or silicon germanium compounds; the substrate may also be other semiconductor materials.
It should be noted that, the substrate 110 is further formed with an isolation layer 120 for electrically isolating the substrate 110 from the layer 130 to be etched; in addition, the isolation layer 120 is further used to protect the substrate 110 during the subsequent etching process, so as to prevent the substrate 110 from being damaged by the subsequent etching process.
Specifically, the material of the isolation layer 120 is silicon oxide, and may be formed by chemical vapor deposition, physical vapor deposition, atomic layer deposition, and film deposition such as furnace tube. In other embodiments of the present invention, the material of the isolation layer may also be other dielectric materials such as silicon nitride, silicon oxynitride, etc.
In this embodiment, the thickness of the isolation layer 120 is as follows
To->
Within the range. The thickness of the spacer layer 120 is not too large nor too small. If the thickness of the isolation layer 120 is too small, it may affect the electrical isolation performance of the isolation layer 120, affect the electrical insulation between the substrate 110 and the metal interconnection structure formed later, may also affect the protection capability of the isolation layer 120 on the substrate 110, and may increase the risk of damaging the substrate 110; if the thickness of the isolation layer 120 is too large, problems of material waste and increased process difficulty are likely to occur.
The layer to be etched 130 is etched to form a target pattern layer.
In this embodiment, an etching method of a metal interconnection structure in a Micro-Electro-mechanical system (MEMS) is described as an example. The material of the layer to be etched 130 is metal, which is used to form a metal interconnection structure in the mems. Specifically, the material of the layer to be etched 130 is aluminum.
In this embodiment, the thickness of the layer to be etched 130 is in the range of 1.5 μm to 2.5 μm. The thickness of the layer 130 to be etched is not too large nor too small. If the thickness of the layer to be etched 130 is too small, the resistance of the layer to be etched 130 will increase, which may affect the performance of the metal interconnection structure formed by the layer to be etched 130; if the thickness of the layer to be etched 130 is too large, the problems of material waste and increased process difficulty are likely to occur.
It should be noted that the layer to be etched 130 is further formed with a pattern layer 140.
The pattern layer 140 serves as an etch mask for defining the dimensions and locations of subsequently formed target pattern layers.
In this embodiment, the material of the pattern layer 140 is photoresist, and a coating process and a photolithography process are used to form the pattern layer. In other embodiments of the present invention, the pattern layer may also be a mask layer formed by using a multiple patterning mask process. Specifically, in this embodiment, the thickness of the pattern layer 140 is in the range of 40 μm to 50 μm.
Referring to fig. 4 to 6, after the substrate 110 is provided, an etching solution is provided; and carrying out wet etching on the layer 130 to be etched by adopting the etching solution, and patterning the layer 130 to be etched to form a target pattern layer.
The etching solution is used for wet etching the layer 130 to be etched, and the etching solution includes: an etchant 151; an additive comprising barrier particles 152.
The pattern layer 140 has an opening therein, and a portion of the surface of the layer to be etched 130 is exposed at the bottom of the opening, and the exposed surface of the layer to be etched 130 is subsequently reacted with the etchant 151 in the etching solution to be removed, thereby implementing etching.
In the process of wet etching the layer 130 to be etched by adopting the etching solution, after the side wall of the layer 130 to be etched is exposed, the blocking particles 152 in the etching solution can enter the side wall position of the layer 130 to be etched (as shown in a circle 153 in fig. 4 to 6) and are filled on the side wall of the layer 130 to be etched, so that the probability that the side wall of the layer 130 to be etched contacts with the etching agent 151 is reduced, the etching agent 151 is inhibited from etching the side wall of the layer 130 to be etched, and the etching efficiency of the etching solution on the side wall of the layer 130 to be etched is reduced, thereby achieving the purposes of improving the undercut problem and the wet etching effect, and being beneficial to considering the process efficiency and the etching effect.
In this embodiment, in order to enable the barrier particles 152 to fill the sidewall of the layer to be etched 130, the ratio of the size of the barrier particles 152 to the thickness of the layer to be etched 130 is in the range of 1/20 to 1/2.
The ratio of the size of the barrier particles 152 to the thickness of the layer 130 to be etched should not be too large or too small: if the ratio of the size of the barrier particles 152 to the thickness of the layer 130 to be etched is too large, the barrier particles 152 may not enter the position of the sidewall of the layer 130 to be etched; if the ratio of the size of the barrier particles 152 to the thickness of the layer 130 to be etched is too small, the filling effect of the barrier particles 152 on the sidewall of the layer 130 to be etched may be affected; the failure of the blocking particles 152 to enter the position of the side wall of the layer to be etched 130 and the poor filling effect of the blocking particles 152 on the side wall of the layer to be etched 130 affect the effect of the blocking particles 152 in reducing the contact probability between the side wall of the layer to be etched 130 and the etching agent 151, which is not beneficial to inhibiting the etching of the side wall of the layer to be etched 130 by the etching agent 151 and improving the undercut problem.
Specifically, the thickness of the layer to be etched 130 is in the range of 1.5 μm to 2.5 μm, so the size of the barrier particles 152 is in the range of 0.1 μm to 1 μm.
The material of the blocking particles 152 may be a polymer material. Specifically, the material of the barrier particles 152 includes at least two of polyethylene, polypropylene, ethylene glycol, and water. In this embodiment, the material of the blocking particles 152 is a complex of polyethylene, polypropylene, ethylene glycol, and water.
The material of the blocking particles 152 is a polymer material, specifically, the material of the blocking particles 152 may be a mixture of at least two of polyethylene, polypropylene, ethylene glycol and water, and in this embodiment, the material of the blocking particles 152 is a complex of polyethylene, polypropylene, ethylene glycol and water. The material of the blocking particles 152 is reasonably arranged, so that adverse effects of the addition of the blocking particles 152 on the semiconductor structure on the substrate 110 can be effectively prevented, and the improvement of the manufacturing yield is facilitated; moreover, the material of the barrier particles 152 is arranged in this way, so that the barrier particles 152 can be removed later by cleaning, thereby minimizing the residual of the barrier particles 152 on the surface of the formed target pattern layer, and being beneficial to providing a good process surface for subsequent processes.
On the other hand, since the material of the layer to be etched 130 is metal, the etchant 151 is an acidic solution. In this embodiment, the material of the layer to be etched 130 is aluminum; the etchant 151 includes: one or more of phosphoric acid, nitric acid, and acetic acid. Specifically, in the etchant 151, the etchant 151 includes: the volume ratio of phosphoric acid is 75% to 85%, and the volume ratio of nitric acid is 5% to 15%; the volume ratio of acetic acid is in the range of 5% to 15%.
Therefore, the etching solution temperature is in the range of 50 ℃ to 60 ℃; the vertical etching rate of the etchant 151 to the layer 130 to be etched is as follows
To->
Within the range. The vertical etching rate refers to an etching rate of the layer 130 to be etched by the etchant in a direction perpendicular to the surface of the layer 130 to be etched.
In this embodiment, the mass percentage concentration of the blocking particles 152 in the additive is in the range of 20% to 40%.
The concentration of the barrier particles 152 in the additive should not be too high nor too low. If the concentration of the blocking particles 152 in the additive is too low, the filling effect of the blocking particles 152 on the side wall of the layer to be etched 130 is affected, so that the effect of the blocking particles 152 on reducing the contact probability between the side wall of the layer to be etched 130 and the etchant 151 is affected, and the undercut problem is not improved; if the concentration of the blocking particles 152 in the additive is too high, the etching efficiency of the etching solution on the layer 130 to be etched may be affected, which is not beneficial to ensuring the process efficiency and not beneficial to achieving both the process efficiency and the etching effect.
And the additive accounts for 0.5% or more of the volume of the etching solution.
The volume ratio of the additive to the etchant is not too large nor too small. The volume ratio of the additive to the etchant is too small, and the concentration of the blocking particles 152 in the etching solution is too small, which may affect the effect of the blocking particles 152 in reducing the contact probability between the side wall of the layer to be etched 130 and the etchant 151, so that the etching of the side wall of the layer to be etched 130 by the etchant 151 is not inhibited, and the undercut problem is not improved.
Specifically, the additive accounts for 0.8 to 1.2% of the etching solution by volume. In the wet etching process, the etching solution is lost along with the progress of the etching process, so that the volume ratio of the additive in the etching solution is set within a reasonable range, the blocking particles 152 in the etching solution can be maintained at a certain concentration, the undercut problem can be improved, the etching efficiency of the etching solution on the layer to be etched can be ensured, and the process efficiency and the etching effect can be simultaneously realized.
Specifically, in this embodiment, in the wet etching process of the etching solution with the etching solution, the flow of the etchant is 8L/min to 10L/min, and the addition amount of the additive is set according to the flow of the etchant, so as to achieve the purposes of improving the undercut problem and ensuring the etching efficiency.
In this embodiment, the width of the target pattern layer is greater than 40 μm. The width of the target pattern layer cannot be too small due to process limitations. The width of the target pattern layer is too small, so that the target pattern layer meeting the technological requirements cannot be formed by wet etching, and the product yield and the device performance are not guaranteed.
In this embodiment, after wet etching, the target pattern layer is cleaned. Specifically, the cleaning treatment is performed on the target graphic layer through deionized water.
Since the material of the blocking particles 152 is a polymer material, specifically a complex of polyethylene, polypropylene, ethylene glycol and water, the cleaning of the target pattern layer with deionized water can remove the additive remaining on the surface of the target pattern layer, thereby removing the residue of the blocking particles 152 and providing a clean operation surface for the subsequent process.
Referring to fig. 7 to 9 in combination, fig. 7 is a graph showing the result of testing after etching the layer to be etched by the conventional etching solution; FIG. 8 is a graph showing the results of testing after etching the layer to be etched using the etching solution (0.2% by volume of additive) according to the present invention; fig. 9 is a graph showing the results of the test performed after etching the layer to be etched using the etching solution of the present invention (the volume ratio of the additive is 1%).
As can be seen from fig. 7 to 9, after the layer to be etched is etched, the sidewalls of the layer to be etched are exposed, so that an undercut problem occurs.
However, as shown in fig. 7, since no blocking particles are added to the etching solution in the prior art, the probability that the etchant contacts the sidewall of the layer to be etched is high, the sidewall of the layer to be etched is severely etched, and the length d1 of the gap formed between the pattern layer and the substrate is about 8 μm.
As shown in fig. 8 and 9, after etching with the etching solution of the present invention, the probability of the etchant contacting the sidewall of the layer to be etched is reduced due to the addition of the blocking particles, the etching phenomenon of the sidewall of the layer to be etched is alleviated, and the undercut problem is improved, so that the lengths d2 and d3 of the gaps formed between the pattern layer and the substrate are reduced.
In the embodiment shown in fig. 8, the volume of the additive is relatively low, the etching phenomenon of the side wall of the layer to be etched is relieved, and the length d2 of the gap formed between the pattern layer and the substrate is relatively large and is about 5 μm; whereas in the embodiment of fig. 9, the additive volume is relatively high, the side wall of the layer to be etched is more significantly relieved, and the length d3 of the gap formed between the pattern layer and the substrate is smaller, which is about 3 μm. Therefore, the addition of the additive containing the blocking particles can effectively relieve the etching suffered by the side wall of the layer to be etched, thereby improving the undercut problem.
Although the present invention is disclosed above, the present invention is not limited thereto. Various changes and modifications may be made by one skilled in the art without departing from the spirit and scope of the invention, and the scope of the invention should be assessed accordingly to that of the appended claims.
Claims (16)
1. An etching solution for wet etching a layer to be etched, comprising:
an etchant;
and the additive comprises blocking particles to enter the side wall position of the layer to be etched and is filled on the side wall of the layer to be etched, and the volume ratio of the additive to the etching solution is in the range of 0.8-1.2%.
2. The etching solution of claim 1, wherein the ratio of the barrier particle size to the thickness of the layer to be etched is in the range of 1/20 to 1/2.
3. The etching solution of claim 1 or 2, wherein the barrier particles have a size in the range of 0.1 μm to 1 μm.
4. The etching solution of claim 1, wherein the additive has a concentration of the barrier particles in the range of 20% to 40% by mass.
5. The etching solution of claim 1, wherein the material of the barrier particles is a polymeric material.
6. The etching solution of claim 1 or 5, wherein the material of the barrier particles comprises at least two of polyethylene, polypropylene, ethylene glycol, and water.
7. The etching solution of claim 6, wherein the material of the barrier particles is a complex of polyethylene, polypropylene, ethylene glycol, and water.
8. The etching solution according to claim 1 or 5, wherein the material of the layer to be etched is a metal;
the etchant is an acidic solution.
9. The etching solution according to claim 8, wherein the material of the layer to be etched is aluminum; the etchant comprises: one or more of phosphoric acid, nitric acid, and acetic acid.
10. The etching solution of claim 9, wherein the etching solution is at a temperature in the range of 50 ℃ to 60 ℃; the vertical etching rate of the etchant to the layer to be etched is as follows
To->
Within the range.
11. The etching solution of claim 1, wherein the additive is greater than or equal to 0.5% by volume of the etching solution.
12. An etching method, comprising:
providing a substrate, wherein the substrate is provided with a layer to be etched;
providing an etching solution according to any one of claims 1 to 11;
and carrying out wet etching on the layer to be etched by adopting the etching solution, and patterning the layer to be etched to form a target pattern layer.
13. The etching method of claim 12, wherein the width of the target pattern layer is greater than 40 μm.
14. The etching method according to claim 12, wherein the etching solution is used for wet etching the layer to be etched, and the flow rate of the etchant is 8L/min to 10L/min.
15. The etching method according to claim 12, wherein after wet etching, the target pattern layer is subjected to a cleaning process.
16. The etching method according to claim 15, wherein the cleaning treatment is performed on the target pattern layer by deionized water.
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| CN103118805A (en) * | 2010-05-21 | 2013-05-22 | 纳诺特拉公司 | Stencils for high-throughput micron-scale etching of substrates and processes of making and using the same |
| KR20120040466A (en) * | 2010-10-19 | 2012-04-27 | 주식회사 엔에스티 | Wet etching apparatus and wet etching method using the same |
| CN103492947A (en) * | 2011-04-28 | 2014-01-01 | 默克专利股份有限公司 | Selectively etching of a polymer matrix on pet |
| CN103582942A (en) * | 2011-05-23 | 2014-02-12 | 阿西莫公司 | Method for forming vertical conductive connections in layered semiconductor structures |
| CN103703547A (en) * | 2011-07-14 | 2014-04-02 | 3M创新有限公司 | Etching method and devices produced using etching method |
| CN103907216A (en) * | 2011-10-27 | 2014-07-02 | 默克专利股份有限公司 | Selective etching of a matrix comprising silver nano wires |
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