CN109828088A - The device of alcohol content in a kind of quick detection food - Google Patents

The device of alcohol content in a kind of quick detection food Download PDF

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Publication number
CN109828088A
CN109828088A CN201910283453.2A CN201910283453A CN109828088A CN 109828088 A CN109828088 A CN 109828088A CN 201910283453 A CN201910283453 A CN 201910283453A CN 109828088 A CN109828088 A CN 109828088A
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China
Prior art keywords
sample
alcohol
room
sample introduction
volatilization
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CN201910283453.2A
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Chinese (zh)
Inventor
满都拉
葛根塔娜
孙子羽
万永青
李娜
崔占鑫
王瑞刚
段开红
陈忠军
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Inner Mongolia Agricultural University
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Inner Mongolia Agricultural University
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Priority to CN201910283453.2A priority Critical patent/CN109828088A/en
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Abstract

The present invention relates to a kind of devices of alcohol content in quickly detection food.The device collects what sampling system A and alcohol sensing system B was formed by alcohol;Alcohol is collected sampling system A and is made of stirring power source (1), sample volatilization room (2), blender (3), sample introduction piston (6), sample introduction piston power source (7), heating device (9) and sample introduction switch (11);Alcohol sensing system B is made of alcohol detection sensor (10), microprocessor (15) and alcohol sensing system interface (16);Apparatus of the present invention can detect the alcohol content in liquid or solid-state food in the short period, and pre-treatment is simple, and measurement is accurate, low in cost, Reusability, therefore is convenient for large-scale promotion application.

Description

The device of alcohol content in a kind of quick detection food
[technical field]
The invention belongs to technical field of food production.More particularly it relates to alcohol in a kind of quickly detection food The device of content.
[background technique]
Alcohol (ethyl alcohol) as drinks and the flavor substance of some drink and foods, content significant impact product Quality.The common detection methods of alcohol content have gas chromatography and hydrometer method in food at present.Gas chromatography detects food Middle alcohol content is accurate, but buys instrument and sample pre-treatments complexity, and professional technician is needed to carry out.Although hydrometer method is compared with gas Phase chromatography economical and convenient, but detected after being also required to distillation, and poor to the detection accuracy of alcohol micro in food.
Although CN 201310464606 and CN 201110347261 etc. develop alcohol using the principles such as colour developing and colorimetric Detection method, but they are at high cost, are suitable for hospital.And alcohol concentration signal quickly can be changed into telecommunications by alcohol sensor Number, there is high sensitivity, it is at low cost, the features such as capable of recycling, it is highly suitable for the detection of alcohol in food.
[summary of the invention]
[technical problems to be solved]
The object of the present invention is to provide a kind of devices of alcohol content in quickly detection food.
[technical solution]
The present invention is achieved through the following technical solutions.
The present invention relates to a kind of devices of alcohol content in quickly detection food.
The device collects what sampling system A and alcohol sensing system B was formed by alcohol;
Alcohol collects sampling system A by stirring power source 1, sample volatilization chamber cap 2, blender 3, sample volatilization room 4, sample introduction Piston 6, sample introduction piston power source 7, heating device 9 and sample introduction switch 11 form;
Sample volatilization room 4 is a kind of cylindrical body of jacketed;In sample volatilization 4 upper opening of room installation sample volatilization room Lid 2;Sample volatilization 2 outside hub of chamber cap is connected with stirring power source 1, sample volatilization 2 inside center of chamber cap and 3 phase of blender Even;
Sample introduction piston 6 is set in sample volatilization room 4, it is connected by sample introduction piston boit 14 with sample introduction piston power source 7; In sample volatilization 4 side wall upper part of room, sample introduction switch 11 is set;In the sample volatilization between sample introduction piston 6 and sample introduction switch 11 Temp probe 13 is arranged in 4 side wall of room;In sample volatilization 4 side of room being located between sample introduction switch 11 and sample volatilization 4 upper opening of room Injection port 12 is arranged in wall;
Alcohol sensing system B is made of alcohol detection sensor 10, microprocessor 15 and alcohol sensing system interface 16;
Sample volatilization room 4 is connected by sample introduction switch 11 with the alcohol sensing system interface 16 of alcohol sensing system B.
A preferred embodiment of the invention, the alcohol detection sensor 10 of alcohol sensing system B are fuel electricity Pond type, semi-conductor type or galvanic cell type electrochemistry type alcohol sensor.
According to another preferred method of implementation of the present invention, sample volatilization room 4 is that the volume made of stainless steel material is The cavity of 100~500mL.
According to another preferred method of implementation of the present invention, heating device 9 is the electric heating in sample volatilization 4 collet of room Silk or water vapor system, they can make the temperature of sample volatilization room 4 reach 40~80 DEG C.
According to another preferred method of implementation of the present invention, stirring power source 1 is manual or motor driven.
According to another preferred method of implementation of the present invention, sample introduction piston power source 7 is manual or motor driven.
According to another preferred method of implementation of the present invention, sample volatilization chamber cap 2 and sample volatilization room 4 be with ring flange or Screw thread loose joint mode realizes sealed connection.
According to another preferred method of implementation of the present invention, bracket 8 connects sample volatilization room 4 with pedestal 17 in a vertical manner Integrally.
According to another preferred method of implementation of the present invention, sample introduction piston boit 14 has instruction sample volatilization 4 volume of room Scale.
According to another preferred method of implementation of the present invention, alcohol detection sensor 10 is feulcell prototype, semi-conductor type Or original battery electrochemistry type sensor.
The present invention is described in more detail below.
The present invention relates to a kind of devices of alcohol content in quickly detection food.
The device collects what sampling system A and alcohol sensing system B was formed by alcohol;
Alcohol collects sampling system A by stirring power source 1, sample volatilization chamber cap 2, blender 3, sample volatilization room 4, sample introduction Piston 6, sample introduction piston power source 7, heating device 9 and sample introduction switch 11 form;
Sample volatilization room 4 is a kind of cylindrical body of jacketed;In sample volatilization 4 upper opening of room installation sample volatilization room Lid 2;
Sample volatilization room 4 is the staving made of stainless steel material, its volume is 100~500mL.Sample volatilization chamber cap 2 be the lid made of stainless steel material, and sample volatilization chamber cap 2 and sample volatilization room 4 are the ring flange or screw thread to generally use Loose joint mode realizes sealed connection.It is of course also possible to be contacted in 2 the inside of sample volatilization chamber cap at the top of sample volatilization room 4 Part seal groove is set, sealing element is placed in the seal groove to guarantee that sample and its volatile matter are not let out in sample volatilization room 4 Dew.The sealing element is, for example, to use made of silica gel or rubber material.
Heating device 9 is placed in sample volatilization 4 collet of room, heating device 9 is heating wire or water vapor system, their energy The temperature of sample volatilization room 4 is enough set to reach 40~80 DEG C.
Sample volatilization 2 outside hub of chamber cap is connected with stirring power source 1, sample volatilization 2 inside center of chamber cap and blender 3 It is connected;
Stirring power source 1 is manual or motor driven, and the motor that the present invention uses is alternating current generator, its power is usually 150~200W;It is current market sales of product, such as by shield mound precision drive equipment (Shanghai) Co., Ltd. with commodity Name soar motor sale product.It can guarantee that equipment also can be used normally in no power supply using manual actuation.Stirring Device 3 is agitation means usually used in the art.
Sample introduction piston 6 is set in sample volatilization room 4, it is connected by sample introduction piston boit 14 with sample introduction piston power source 7;
Sample introduction piston 6 and sample introduction piston boit 14 are all made of stainless steel material.Sample introduction piston 6 and sample volatilization room 4 It is that sealing is realized in a manner of sealing ring using silica gel or rubber material between inner wall;Sample introduction piston boit 14 marks energy on its column The scale of enough display volatilization 4 volumes of room, such people are easy to read the volume of sample volatilization room 4 by its scale.
Sample introduction piston power source 7 is manual or motor driven, and the motor that the present invention uses is alternating current generator, its power is logical It is often 150~200W;It is current market sales of product, for example, by shield mound precision drive equipment (Shanghai) Co., Ltd. with Trade name soar motor sale product.It can guarantee that equipment also can be used in no power supply using manual actuation.
In sample volatilization 4 side wall upper part of room, sample introduction switch 11 is set;Between sample introduction piston 6 and sample introduction switch 11 Temp probe 13 is arranged in sample volatilization 4 side wall of room;
The sample introduction switch 11 that the present invention uses is a kind of ball valve switch, it is current market sales of product, such as by The product that Funing Zhong Xiang hydraulic valve factory is sold with trade name high pressure American Standard ball valve.The temp probe 13 that the present invention uses is platinum Resistance temperature detector, it is current market sales of product, such as by gold dollar Xiang Electronics Co., Ltd., Huizhou City with commodity The product of name temp probe sale.
In sample volatilization 4 side wall of room being located between sample introduction switch 11 and sample volatilization 4 upper opening of room, injection port 12 is set; Injection port 12 is feed inlet food to be detected being added in sample volatilization room 4.The diameter of injection port 12 be 100~ 150mm, it is sealed using engagement thread.
Alcohol sensing system B is made of alcohol detection sensor 10, microprocessor 15 and alcohol sensing system interface 16;
The alcohol detection sensor 10 that the present invention uses is current market sales of feulcell prototype, semi-conductor type or original Cell type electrochemistry type alcohol sensor, these alcohol sensors are all configured with corresponding microprocessor 15.Feulcell prototype wine Smart sensor is a kind of fuel cell type alcohol sensor that detection sensitivity is 115 ± 85mg/L, it is to sell currently on the market The product sold, such as the production sold by Zhengzhou Wei Sheng Electronic Technology Co., Ltd with trade name fuel cell type alcohol sensor Product.Semi-conductor type alcohol sensor is a kind of semi-conductor type alcohol sensor that detection sensitivity is 25~500ppm, it is mesh Preceding product available on the market, such as by Zhengzhou Wei Sheng Electronic Technology Co., Ltd with trade name semi-conductor type alcohol sensor pin The product sold.Galvanic cell type alcohol sensor is a kind of alcohol sensor that detection sensitivity is 0~1.0mg/L, it is current Product available on the market, the production that example Zhengzhou Wei Sheng Electronic Technology Co., Ltd is sold with trade name galvanic cell type alcohol sensor Product.
Sample volatilization room 4 is connected by sample introduction switch 11 with the alcohol sensing system interface 16 of alcohol sensing system B.This hair The bright sample introduction switch 11 used is a kind of ball valve switch, it is current market sales of product, such as Xiang is hydraulic in Funing The product that valve plant is sold with trade name high pressure American Standard ball valve.
According to the present invention, sample volatilization room 4 is connected with pedestal 17 by bracket 8 in a vertical manner.Bracket 8 is using not It becomes rusty made of steel, plastics or wood materials.
The step of detecting alcohol content method using alcohol content detection device of the present invention is as follows:
By 100~1000mg sample to be tested by injection port 12 be added to sample volatilization room 5, close sample volatilization chamber cap 2 with into Sample mouth 12 is stirred sample to be tested by heating device 9 and is heated to 30~90 DEG C, sample to be tested is made to volatilize, and detection is passed through The method detection confirmation that sample volatilization room temperature reaches set temperature is no longer volatilized, then opens sample introduction switch 11, starts sample introduction Piston power source 7, it drives sample introduction piston 6 to detect sample feeding alcohol sensing system B, is calculated by its testing result Alcohol content into sample to be tested.
[beneficial effect]
The beneficial effects of the present invention are:
Firstly, the present invention has pre-treatment simple using the middle alcohol content of sensor technology detection food, measurement is accurate The advantages of.
Secondly, sample volatilization of the present invention room 2 can guarantee ethyl alcohol volatilization sufficiently, and pass through sampling device for second of all volatilizing Alcohol is all sent to alcohol sensing system B, to guarantee the accuracy of detection.
Third, all component structures of the present invention are simple, low in cost, therefore the installation cost is low and can make repeatedly With, therefore it is convenient for large-scale promotion application.
[Detailed description of the invention]
Fig. 1 is alcohol content apparatus structure schematic diagram in quickly detection food of the invention;
In figure:
1- stirring power source;2- sample volatilization chamber cap;3- blender;4- sample volatilization room;5- interlayer;6- sample introduction piston; 7- sample introduction piston power source;8- bracket;9- heating device;10- alcohol detection sensor;11- sample introduction switch;12- sample holes; 13- temp probe;14- sample introduction piston boit;15- microprocessor, 16- alcohol sensing system interface;Pedestal 17.
[specific embodiment]
It will be better understood that the present invention by following embodiments.
Embodiment 1: the present invention quickly detects alcohol content device in food
The embodiment of the embodiment is as follows:
The device collects what sampling system A and alcohol sensing system B was formed by alcohol;
Alcohol collects sampling system A by stirring power source 1, sample volatilization chamber cap 2, blender 3, sample volatilization room 4, sample introduction Piston 6, sample introduction piston power source 7, heating device 9 and sample introduction switch 11 form;
Sample volatilization room 4 is a kind of jacketed cylindrical body made of stainless steel material, its volume is 240mL, Electric-heating-wire-heating device 9 is placed in this jacket, and the temperature of sample volatilization room 4 is made to reach 40 DEG C;In sample volatilization 4 upper opening of room The volatilization of sample made of the installation stainless steel material chamber cap 2 in a manner of ring flange loose joint;Sample volatilize 2 outside hub of chamber cap with by Shield mound precision drive equipment (Shanghai) Co., Ltd. with trade name soar motor sale power for 150W motor driven stir Power source 1 is connected, and sample volatilization 2 inside center of chamber cap is connected with blender 3;Blender 3 by shield mound precision drive equipment (on Sea) Co., Ltd with trade name soar motor sale power 150W motor driven stirring power source 1 drive blender 3 carry out Stirring;
The sample introduction piston 6 made of setting stainless steel material in sample volatilization room 4, it by sample introduction piston boit 14 with by Shield mound precision drive equipment (Shanghai) Co., Ltd. with trade name soar motor sale power 150W motor sample introduction piston it is dynamic Power source 7 is connected;In sample volatilization 4 side wall upper part of room, sample introduction switch 11 is set;Between sample introduction piston 6 and sample introduction switch 11 Sample volatilization 4 side wall of room setting by gold dollar Xiang Electronics Co., Ltd., Huizhou City with trade name platinum resistance temperature probe 13;In place Injection port 12 is arranged in sample volatilization 4 side wall of room between sample introduction switch 11 and sample volatilization 4 upper opening of room;
Alcohol sensing system B by it is a kind of by Zhengzhou Wei Sheng Electronic Technology Co., Ltd production measurement range be 0~ Fuel cell type alcohol sensor 10, microprocessor 15 and the alcohol sensing system interface 16 of 1.0mg/L forms;
Sample volatilization room 4 is connected by sample introduction switch 11 with the alcohol sensing system interface 16 of alcohol sensing system B.
The alcohol content detection method described using this specification, detects the alcohol content in beer wine with dregs.It is logical The standard curve established with alcoholic solution is crossed, while obtaining 10mL beer wine with dregs from beer enterprise, has carried out wine according to same method Essence detection, is obtained by its testing result by standard curve, the alcohol content of the beer wine with dregs is 1.5%.
Embodiment 2: the present invention quickly detects alcohol content device in food
The embodiment of the embodiment is identical as the embodiment of embodiment 1, and only blender 3 is by hand operated mixing power source 1 driving is stirred;Sample introduction piston 6 is driven by hand sampling piston power source 7 and is carried out;Sample volatilization room 4 volume be 400mL places water vapor system heating device 9 in the collet of sample volatilization room 4;In sample volatilization 4 upper opening of room with screw thread Loose joint mode installs sample volatilization chamber cap 2;Alcohol sensing system B uses the inspection produced by Zhengzhou Wei Sheng Electronic Technology Co., Ltd Surveying concentration is the semi-conductor type alcohol sensor 10 that range is 25~500ppm;
It is carried out using the alcohol content detection method of this specification description to by covering the sorghum fermented grain that strong wind chateau in continent obtains Detection.By establishing standard curve, 20g fermented grain and 10mL water are prepared into solution and carried out alcohol detection according to same method, It is 1.2% by the alcohol content that standard curve obtains the fermented grain.
Embodiment 3: the present invention quickly detects alcohol content device in food
The embodiment of the embodiment is identical as the embodiment of embodiment 1, and only blender 3 is by by shield mound precision drive Equipment (Shanghai) Co., Ltd. with trade name soar motor sale power 200W motor stirring power source 1 driving stirred It mixes;Sample introduction piston 6 is soared the power 200W of motor sale by shield mound precision drive equipment (Shanghai) Co., Ltd. with trade name The driving of motor sample introduction piston power source 7 carries out;Sample volatilization room 4 is a kind of jacketed column barrel made of stainless steel material Body, its volume are 500mL, place electric-heating-wire-heating device 9 in the collet of sample volatilization room 4;It is opened on sample volatilization room 4 Mouth installs sample volatilization chamber cap 2 in a manner of ring flange;Alcohol sensing system B is produced using Zhengzhou Wei Sheng Electronic Technology Co., Ltd Measurement range be 0~1.0mg/L fuel cell type alcohol sensor 10;
It is carried out using the alcohol content detection method that this specification describes to by the vinegar fermented grain Huang sample for acquisition of voluntarily fermenting Detection.As a result it is obtained by standard curve, the alcohol content of the vinegar fermented grain is 2.5%.
Embodiment 4: the present invention quickly detects alcohol content device in food
The embodiment of the embodiment is identical as the embodiment of embodiment 1, and only blender 3 is set by shield mound precision drive Standby (Shanghai) Co., Ltd. is stirred with the soar driving of motor stirring power source 1 of power 150W of motor sale of trade name; Sample introduction piston 6 by shield mound precision drive equipment (Shanghai) Co., Ltd. with trade name soar motor sale power 150W motor The driving of sample introduction piston power source 7 carries out;Sample volatilization room 4 is a kind of jacketed cylindrical body made of stainless steel material, Its volume is 500mL, places electric-heating-wire-heating device 9 in the collet of sample volatilization room 4;In sample volatilization 4 upper opening of room Sample volatilization chamber cap 2 is installed in a manner of screw thread loose joint;Alcohol sensing system B use is given birth to by Zhengzhou Wei Sheng Electronic Technology Co., Ltd The measurement range of production is the galvanic cell type electrochemistry type alcohol sensor 10 of 0~1.0mg/L;
The Wine Sample obtained by market purchase is examined using the alcohol content detection method of this specification description It surveys.After taking 0.010ml Wine Sample that 50ml water is added, after this method detection, as a result obtained by standard curve, the white wine Alcohol content is 51.3%.

Claims (10)

1. the device of alcohol content in a kind of quickly detection food, it is characterised in that the device is to collect sampling system by alcohol (A) it is formed with alcohol sensing system (B);
Alcohol collects sampling system (A) by stirring power source (1), sample volatilization chamber cap (2), blender (3), sample volatilization room (4), sample introduction piston (6), sample introduction piston power source (7), heating device (9) and sample introduction switch (11) composition;
Sample volatilization room (4) is a kind of cylindrical body of jacketed;In sample volatilization room (4) upper opening installation sample volatilization room It covers (2);Sample volatilization chamber cap (2) outside hub be connected with stirring power source (1), sample volatilization chamber cap (2) inside center with stir Device (3) are mixed to be connected;
Sample introduction piston (6) are set in sample volatilization room (4), it passes through sample introduction piston boit (14) and sample introduction piston power source (7) It is connected;(11) are switched in sample volatilization room (4) side wall upper part setting sample introduction;It is being located at sample introduction piston (6) and sample introduction switch (11) Between sample volatilization room (4) side wall setting temp probe (13);It is opened on being located at sample introduction switch (11) and sample volatilization room (4) Sample volatilization room (4) side wall setting injection port (12) between mouthful;
Alcohol sensing system (B) is by alcohol detection sensor (10), microprocessor (15) and alcohol sensing system interface (16) group At;
Sample volatilization room (4) is connected by sample introduction switch (11) with the alcohol sensing system interface (16) of alcohol sensing system (B).
2. the apparatus according to claim 1, it is characterised in that the alcohol detection sensor (10) of alcohol sensing system (B) is Feulcell prototype, semi-conductor type or galvanic cell type electrochemistry type alcohol sensor.
3. the apparatus according to claim 1, it is characterised in that sample volatilization room (4) is the volume made of stainless steel material The cavity of 100~500mL.
4. the apparatus according to claim 1, it is characterised in that heating device (9) is located in sample volatilization room (4) collet Heating wire or water vapor system, they can make sample volatilization room (4) temperature reach 30~80 DEG C.
5. the apparatus according to claim 1, it is characterised in that stirring power source (1) is manual or motor driven.
6. the apparatus according to claim 1, it is characterised in that sample introduction piston power source (7) is manual or motor driven.
7. the apparatus according to claim 1, it is characterised in that be that sample volatilization chamber cap (2) is with sample volatilization room (4) Sealed connection is realized in a manner of ring flange or screw thread loose joint.
8. device according to claim 3, it is characterised in that bracket (8) by sample volatilization room (4) in a vertical manner with bottom Seat (17) is connected.
9. the apparatus according to claim 1, it is characterised in that there is sample introduction piston boit (14) instruction sample volatilization room (4) to hold Long-pending scale.
10. the apparatus according to claim 1, it is characterised in that alcohol detection sensor (10) is feulcell prototype, partly leads Figure or original battery electrochemistry type alcohol sensor.
CN201910283453.2A 2019-04-10 2019-04-10 The device of alcohol content in a kind of quick detection food Pending CN109828088A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112858313A (en) * 2021-01-14 2021-05-28 内蒙古农业大学 Sheep milk adulteration detection device

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