CN109821922A - A kind of manufacturing process of screw wire rod - Google Patents

A kind of manufacturing process of screw wire rod Download PDF

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Publication number
CN109821922A
CN109821922A CN201910123655.0A CN201910123655A CN109821922A CN 109821922 A CN109821922 A CN 109821922A CN 201910123655 A CN201910123655 A CN 201910123655A CN 109821922 A CN109821922 A CN 109821922A
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China
Prior art keywords
wire rod
screw
manufacturing process
water
temperature
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CN201910123655.0A
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Chinese (zh)
Inventor
孙肖佳
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Sea Salt Sun Shi Builds New Standard Part Manufacturing Co Ltd
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Sea Salt Sun Shi Builds New Standard Part Manufacturing Co Ltd
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Priority to CN201910123655.0A priority Critical patent/CN109821922A/en
Publication of CN109821922A publication Critical patent/CN109821922A/en
Pending legal-status Critical Current

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Abstract

The present invention relates to a kind of manufacturing process of screw wire rod, it in turn includes the following steps: A: pickling: the coil holder for installing wire rod wire rod being hung in and carries out pickling in the slot equipped with pickling solution;B: cleaning: the wire rod wire rod after step A is rinsed, which is first hung in the slot equipped with neutralizer, to be cleaned;C: the wire rod wire rod after step B cleaning phosphatization: is hung in into phosphatization in the slot equipped with phosphating solution;D: saponification: the wire rod wire rod of step C hangs in lower saponification in the slot equipped with saponification liquor after water rinses;E: wire drawing: the wire rod wire rod in step D after saponification is fed through wire drawing machine and carries out drawing process formation screw wire rod.The present invention is superior in quality, and brightness is good, has stronger lubricity, corrosion resistance, and cold heading performance and fatigue resistance are high.

Description

A kind of manufacturing process of screw wire rod
Technical field
The present invention relates to a kind of manufacturing process of screw wire rod, belong to screw wire rod processing technique field.
Background technique
Currently, the technological process of production of screw wire rod be the rough drawing of wire rod → pretreatment → middle silk heat treatment line → Middle silk drawing → annealing → inspection → packaging factory.
For example, the patent of invention that patent application publication number is CN102861782B discloses a kind of drawer sliding rail and its manufacture Method, the manufacturing process of steel wire rod in a kind of metallurgical technology field, and in particular to a kind of manufacturing process of screw wire rod, technique It in turn includes the following steps: the coil holder for installing wire rod wire rod is hung in the slot equipped with pickling solution;By the wire rod line after flushing Material is hung in the slot equipped with neutralizer;Then it hangs in the slot equipped with hot lime;Scheduled semi-finished product specification is obtained after drawing Screw wire rod;Screw wire rod after drawing is placed in the heat treatment furnace, spheroidizing is carried out under methanol atmosphere protection;Weight Multiple first step acid pickling step;Screw wire rod after pickling is hung in the slot equipped with phosphating solution;It hangs in after water rinses equipped with soap In the slot for changing liquid;The steel wire of scheduled trimmed size is obtained after drawing.
The processing technology of another kind screw wire rod set forth below.
Summary of the invention
The present invention is superior in quality in view of the deficienciess of the prior art, provide a kind of manufacturing process of screw wire rod, bright It spends, there is stronger lubricity, corrosion resistance, cold heading performance and fatigue resistance are high.
The technical scheme to solve the above technical problems is that a kind of manufacturing process of screw wire rod, it is characterised in that: it It in turn includes the following steps: A: pickling: the coil holder for installing wire rod wire rod being hung in the slot equipped with pickling solution, pickling solution is heated to Pickling 5-15min under the conditions of 50 DEG C -60 DEG C;B: cleaning: the wire rod wire rod after step A is rinsed first hangs in the slot equipped with neutralizer In, 1-3min is neutralized under room temperature;Wire rod wire rod is first hung in the slot equipped with clear water liquid again, cleans 1min under room temperature;C: phosphatization: Wire rod wire rod after step B cleaning is hung in the slot equipped with phosphating solution, phosphatization 8-12min at a temperature of 75-85 DEG C;D: saponification: The wire rod wire rod of step C is hung in after water rinses in the slot equipped with saponification liquor, and 3-7min is saponified at a temperature of 75-80 DEG C;E: wire drawing: Wire rod wire rod in step D after saponification is fed through wire drawing machine and carries out drawing process formation screw wire rod;F: heat is made: will walk Screw wire rod in rapid E is placed in the heat treatment furnace, 500-600 DEG C of the environment temperature progress spheroidizing under methanol atmosphere protection Processing, obtains to be put into the screw wire rod that screw is fabricated in multifunctional nut molding machine, then carries out bending and adds Work thread;G: cold forging: the screw wire rod in step E is placed on progress cold forging processing in cold forging machine, then carries out threading processing.
The present invention is further, and in the step B, by weight percentage, neutralizer is made of following raw material: quick lime 8-12%, soap powder 0.8-1.2%, surplus are water.
The present invention is further, and the saponification liquor includes: soap powder 5-10% and water, and the pH of saponification liquor is controlled in 8.5-10.
The present invention is further, and the saponification liquor further includes odium stearate, in percentage, the soap powder and stearic acid The sum of sodium is 9:1 than the ratio of water.
The present invention is further, and the quick lime 10%, soap powder 1.0%, surplus is water.
The present invention is further, and in the step F, by weight percentage, phosphating solution is made of following raw material: di(2-ethylhexyl)phosphate Hydrogen zinc 25-40%, zinc nitrate 40-50%, water 20-30%.
The present invention is further, and the pickling solution in the step A is made of following raw material by weight percentage: salt Acid, hexamethylenetetramine, Boratex and excess water.
The present invention is further, in the step F, spheroidizing specifically comprises the processes of: under methanol atmosphere protection, 5-7h Time in the temperature in furnace risen to 600-580 DEG C, and keep the temperature 5-7h;Control cooling velocity is 15-10 DEG C/h, will be in furnace Temperature slowly cools to 515-500 DEG C;Bell is opened, control cooling velocity is 75-85 DEG C/h, by the rapid cooling of in-furnace temperature To 280-350 DEG C;It comes out of the stove, air is cooled to room temperature.
In conclusion compared with prior art, the present invention has the advantage that mainly removing wire rod by acid pickling step The oxidation film of wire surface, and under conditions of pickling 5-15min under the conditions of pickling solution is heated to 50 DEG C -60 DEG C, it can reach The effect of optimal cleaning oxidation film;With the pickling solution of wire rod wire rod in cleaning step, the hydrochloric acid of wire surface is washed Corrosion products;Phosphating step is the surface property in order to improve wire rod, and the phosphating coat of formation is by a series of of different sizes Crystal is formed, and will will form the porous of fine cracks on the tie point of crystal, the phosphating solution that the present invention uses is by following original Material composition: zinc dihydrogen phosphate 25-40%, zinc nitrate 40-50%, water 20-30% are capable of forming fine and close phosphating coat;And due to phosphoric acid The coefficient of friction of salt epithelium be not it is very low, sufficient lubricity when processing cannot be assigned, thus invention use saponification liquor packet Include: the pH of soap powder 5-10% and water, saponification liquor is controlled in 8.5-10.Furthermore saponification liquor further includes odium stearate, the soap powder It than the ratio of water is 9:1 with the sum of odium stearate, under this ratio, lubricant effect reaches best.
It is of the invention under methanol atmosphere protection, the temperature in furnace is risen to 600-580 DEG C in the time of 5-7h, and keep the temperature 5- 7h;Control cooling velocity is 15-10 DEG C/h, and the temperature in furnace is slowly cooled to 515-500 DEG C;Open bell, control cooling Speed is 75-85 DEG C/h, and in-furnace temperature is quickly cooled to 280-350 DEG C;It comes out of the stove, air is cooled to room temperature, is mainly It can satisfy the two ways processing of step F and step G.
Specific embodiment
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field Art personnel every other embodiment obtained without making creative work belongs to the model that the present invention protects It encloses.
Embodiment 1, a kind of manufacturing process of screw wire rod, it in turn includes the following steps: A: pickling: will install wire rod line The coil holder of material is hung in the slot equipped with pickling solution, pickling 5-15min under the conditions of pickling solution is heated to 50 DEG C -60 DEG C, wherein pickling Liquid is made of following raw material by weight percentage: hydrochloric acid, hexamethylenetetramine, Boratex and excess water;B: it cleaning: will walk Wire rod wire rod after rapid A is rinsed first is hung in the slot equipped with neutralizer, 1-3min is neutralized under room temperature, wherein neutralizer is by following original Material composition: quick lime 8-12%, soap powder 0.8-1.2%, surplus are water, most preferably quick lime 10%, soap powder 1.0%, and surplus is Water;Wire rod wire rod is first hung in the slot equipped with clear water liquid again, cleans 1min under room temperature;C: phosphatization: by the disk after step B cleaning Wire rod is hung in the slot equipped with phosphating solution, phosphatization 8-12min at a temperature of 75-85 DEG C;Wherein by weight percentage, phosphating solution It is made of following raw material: zinc dihydrogen phosphate 25-40%, zinc nitrate 40-50%, water 20-30%;D: saponification: the wire rod wire rod of step C It is hung in after water rinses in the slot equipped with saponification liquor, 3-7min is saponified at a temperature of 75-80 DEG C, wherein saponification liquor includes: soap powder The pH of 5-10% and water, saponification liquor is controlled in 8.5-10;E: the wire rod wire rod in step D after saponification wire drawing: is fed through drawing Silk machine carries out drawing process and forms screw wire rod;F: heat is made: the screw wire rod in step E is placed in the heat treatment furnace, in first 500-600 DEG C of environment temperature progress spheroidizing processing under alcohol atmosphere protection, specially spheroidizing specifically comprises the processes of: in first Under alcohol atmosphere protection, the temperature in furnace is risen to 600-580 DEG C in the time of 5-7h, and keep the temperature 5-7h;Controlling cooling velocity is 15-10 DEG C/h, the temperature in furnace is slowly cooled to 515-500 DEG C;Bell is opened, control cooling velocity is 75-85 DEG C/h, will In-furnace temperature is quickly cooled to 280-350 DEG C;It comes out of the stove, air is cooled to room temperature;Obtain being put into multifunctional nut at The screw wire rod of screw is fabricated in type machine, then carries out bending and processes thread;G: cold forging: by the screw line in step E Material, which is placed in cold forging machine, carries out cold forging processing, then carries out threading processing.
Embodiment 2, a kind of manufacturing process of screw wire rod, compared with Example 1, saponification liquor further includes odium stearate, with Percentages, the sum of soap powder and odium stearate are 9:1 than the ratio of water.
Comparative example 1, a kind of manufacturing process of screw wire rod, compared with Example 2, saponification liquor further includes glycerol, with percentage Than meter, the sum of soap powder and glycerol are 9:1 than the ratio of water.
Comparative example 2, a kind of manufacturing process of screw wire rod, compared with Example 1, phosphating solution are zinc dihydrogen phosphate and water 20-30%。
Embodiment 3, a kind of manufacturing process of screw wire rod, compared with Example 1, phosphating solution are zinc dihydrogen phosphate 30%, nitre Sour zinc 45%, water 25%;Control Zn content 22%, phosphatase 24 0% and nitric acid 38%.
Embodiment 4, a kind of manufacturing process of screw wire rod, compared with Example 1, phosphating solution are zinc dihydrogen phosphate 30%, nitre Sour zinc 45%, water 25%;Control Zn content 10%, phosphoric acid 80% and nitric acid 10%.
Performance characterization, the intensity for testing nut material, strength grade are that embodiment 1 is that 8.8, embodiment 2 is respectively 9.8, embodiment 3 is 9.8, embodiment 4 is 9.8, comparative example 1 is 6.8, comparative example 2 is 4.8, comparative example 3 is 6.8.
The present invention is by acid pickling step, the main oxidation film for removing wire rod wire surface, and pickling solution be heated to 50 DEG C- Under the conditions of 60 DEG C under conditions of pickling 5-15min, it can achieve the effect that optimal cleaning oxidation film;In in cleaning step and The pickling solution of wire rod wire rod washes the hydrochloric acid corrosion resistance product of wire surface;Phosphating step is the surface in order to improve wire rod The phosphating coat of performance, formation is made of a series of crystal of different sizes, will will form on the tie point of crystal tiny Crackle it is porous, the phosphating solution that the present invention uses is made of following raw material: zinc dihydrogen phosphate 25-40%, zinc nitrate 40-50%, water 20-30% is capable of forming fine and close phosphating coat;And due to the coefficient of friction of phosphate coating be not it is very low, processing cannot be assigned When sufficient lubricity.So invention includes: soap powder 5-10% and water using saponification liquor, the pH of saponification liquor is controlled in 8.5- 10.Furthermore saponification liquor further includes odium stearate, and the sum of the soap powder and odium stearate are 9:1 than the ratio of water, in this ratio Under, lubricant effect reaches best.It is of the invention under methanol atmosphere protection, the temperature in furnace is risen into 600- in the time of 5-7h 580 DEG C, and keep the temperature 5-7h;Control cooling velocity is 15-10 DEG C/h, and the temperature in furnace is slowly cooled to 515-500 DEG C;It opens Bell, control cooling velocity are 75-85 DEG C/h, and in-furnace temperature is quickly cooled to 280-350 DEG C;It comes out of the stove, air is cooled to Room temperature, primarily to can satisfy the two ways processing of step F and step G.
The foregoing is merely presently preferred embodiments of the present invention, is not intended to limit the invention, all in the spirit and principles in the present invention Within, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention.

Claims (8)

1. a kind of manufacturing process of screw wire rod, it is characterised in that: it in turn includes the following steps:
A: pickling: the coil holder for installing wire rod wire rod is hung in the slot equipped with pickling solution, and pickling solution is heated to 50 DEG C of -60 DEG C of conditions Lower pickling 5-15min;
B: cleaning: the wire rod wire rod after step A is rinsed first is hung in the slot equipped with neutralizer, neutralizes 1-3min under room temperature;Again Wire rod wire rod is first hung in the slot equipped with clear water liquid, cleans 1min under room temperature;
C: phosphatization: the wire rod wire rod after step B cleaning is hung in the slot equipped with phosphating solution, phosphatization 8- at a temperature of 75-85 DEG C 12min;
D: saponification: the wire rod wire rod of step C is hung in after water rinses in the slot equipped with saponification liquor, and 3- is saponified at a temperature of 75-80 DEG C 7min;
E: wire drawing: the wire rod wire rod in step D after saponification is fed through wire drawing machine and carries out drawing process formation screw wire rod;
F: heat is made: the screw wire rod in step E being placed in the heat treatment furnace, the environment temperature 500- under methanol atmosphere protection 600 DEG C of progress spheroidizing processing obtain to be put into the screw wire rod that screw is fabricated in multifunctional nut molding machine, Then it carries out bending and processes thread;
G: cold forging: the screw wire rod in step E is placed on progress cold forging processing in cold forging machine, then carries out threading processing.
2. the manufacturing process of screw wire rod according to claim 1, which is characterized in that in the step B, with weight percent Than meter, neutralizer is made of following raw material: quick lime 8-12%, soap powder 0.8-1.2%, surplus are water.
3. the manufacturing process of screw wire rod according to claim 1, which is characterized in that the saponification liquor includes: soap powder The pH of 5-10% and water, saponification liquor is controlled in 8.5-10.
4. the manufacturing process of screw wire rod according to claim 3, which is characterized in that the saponification liquor further includes stearic acid Sodium, in percentage, the sum of the soap powder and odium stearate are 9:1 than the ratio of water.
5. the manufacturing process of screw wire rod according to claim 4, which is characterized in that the quick lime 10%, soap powder 1.0%, surplus is water.
6. the manufacturing process of screw wire rod according to claim 5, which is characterized in that in the step F, with weight percent Than meter, phosphating solution is made of following raw material: zinc dihydrogen phosphate 25-40%, zinc nitrate 40-50%, water 20-30%.
7. the manufacturing process of screw wire rod according to claim 6, which is characterized in that the pickling solution in the step A, with Weight percent meter, is made of following raw material: hydrochloric acid, hexamethylenetetramine, Boratex and excess water.
8. the manufacturing process of screw wire rod according to claim 7, which is characterized in that in the step F, spheroidizing Specifically comprises the processes of: under methanol atmosphere protection, the temperature in furnace is risen to 600-580 DEG C in the time of 5-7h, and keep the temperature 5-7h; Control cooling velocity is 15-10 DEG C/h, and the temperature in furnace is slowly cooled to 515-500 DEG C;Bell is opened, cooling velocity is controlled For 75-85 DEG C/h, in-furnace temperature is quickly cooled to 280-350 DEG C;It comes out of the stove, air is cooled to room temperature.
CN201910123655.0A 2019-02-19 2019-02-19 A kind of manufacturing process of screw wire rod Pending CN109821922A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110238231A (en) * 2019-06-11 2019-09-17 常熟市标准件厂有限公司 A kind of material reforming technology of high-strength bolt
WO2021217951A1 (en) * 2020-04-30 2021-11-04 苏州强新合金材料科技有限公司 Lime wire drawing process for steel wires
CN113649426A (en) * 2021-08-16 2021-11-16 舟山市7412工厂 Environment-friendly and energy-saving wire drawing method for stainless steel bolt
CN114318310A (en) * 2021-12-13 2022-04-12 中国建筑第二工程局有限公司 Preparation method of nuclear power saponified steel belt

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110238231A (en) * 2019-06-11 2019-09-17 常熟市标准件厂有限公司 A kind of material reforming technology of high-strength bolt
WO2021217951A1 (en) * 2020-04-30 2021-11-04 苏州强新合金材料科技有限公司 Lime wire drawing process for steel wires
CN113649426A (en) * 2021-08-16 2021-11-16 舟山市7412工厂 Environment-friendly and energy-saving wire drawing method for stainless steel bolt
CN114318310A (en) * 2021-12-13 2022-04-12 中国建筑第二工程局有限公司 Preparation method of nuclear power saponified steel belt
CN114318310B (en) * 2021-12-13 2024-03-12 中国建筑第二工程局有限公司 Preparation method of nuclear power saponification steel belt

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Application publication date: 20190531