CN109810742A - A kind of biomass new energy fuel and preparation method thereof - Google Patents
A kind of biomass new energy fuel and preparation method thereof Download PDFInfo
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- CN109810742A CN109810742A CN201910231522.5A CN201910231522A CN109810742A CN 109810742 A CN109810742 A CN 109810742A CN 201910231522 A CN201910231522 A CN 201910231522A CN 109810742 A CN109810742 A CN 109810742A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel
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Abstract
The invention discloses a kind of biomass new energy fuels and preparation method thereof, belong to biomass fuel technical field.Described its material composition of biomass new energy fuel includes: stalk, and sawdust, shell skin, dehydrating agent, calcium oxide, stigmasterol, hydroxy silicon oil, epoxidized soybean oil, the preparation method includes mixing, squeeze and etc..The present invention improves the combustion heat value and physical property of biomass new energy fuel as reinforcement by using stigmasterol, hydroxy silicon oil, epoxidized soybean oil.
Description
Technical field
The invention belongs to biomass fuel technical fields, and in particular to a kind of biomass new energy fuel and its preparation side
Method.
Background technique
Biomass fuel: referring to biological material burning as fuel, generally mainly agriculture and forestry organic waste material, the main distinction
In fossil fuel.In current national policy and environmental protection standard, direct biomass burning belongs to high pollution fuel, only in rural area
Brick kitchen range in use, do not allow to use in city.The application of biomass fuel, practical is mainly biomass molding fuel, is
Various moldings are made (such as blocky, graininess by techniques such as crushing, mixing, extruding, drying using agricultural waste as raw material
Deng), a kind of Novel clean-fuel that can directly burn.
Chinese patent literature " a kind of biomass triplet-powder solid fuel and its production technology (patent No.:
ZL200910166760.9 a kind of biomass triplet-powder solid fuel and its production technology and preparation method thereof, the combustion) " are disclosed
Material presses stalk 65-75%, sawdust 15-25%, shell skin 5-15%, oxygen using stalk, sawdust, shell skin, calcium oxide as raw material
The weight proportion for changing calcium 0.5-2% is mixed；Smokeless when burning, the pernicious gases such as carbon dioxide, sulfur dioxide can reach substantially
To zero-emission, the volume of remaining ashes only has 1/10th of volume of fuel, and can make biomass fertilizers use；The fuel can replace
In generation, is coal-fired, as the main fuel of Industrial Boiler, to efficiently solve problem of environmental pollution, but its physical property and the combustion heat
Value need to be improved.
Summary of the invention
The object of the present invention is to provide a kind of biomass new energy fuels and preparation method thereof, to solve in patent document
On the basis of " a kind of biomass triplet-powder solid fuel and its production technology (patent No.: ZL200910166760.9) " is disclosed,
Optimize component, dosage, the method etc. of biomass new energy fuel, improves the physical property and the combustion heat of biomass new energy fuel
Value.
In order to solve the above technical problems, the invention adopts the following technical scheme:
A kind of biomass new energy fuel, raw material include: stalk, sawdust, shell skin, dehydrating agent, calcium oxide, beans steroid
Alcohol, hydroxy silicon oil, epoxidized soybean oil；The stigmasterol, hydroxy silicon oil, epoxidized soybean oil weight ratio are (4-6): (5-10):
(1-3)。
Further, the stigmasterol, hydroxy silicon oil, the weight ratio of epoxidized soybean oil are 5:7.5:2.
Further, the biomass new energy fuel is as unit of parts by weight, including following raw material: stalk 650-750
Part, 150-250 parts of sawdust, 50-100 parts of shell skin, 10-20 parts of calcium oxide, 4-6 parts of stigmasterol, 5-10 parts of hydroxy silicon oil, epoxy
1-3 parts of soybean oil.
Further, the biomass new energy fuel is as unit of parts by weight, including following raw material: 700 parts of stalk, wood
Consider 200 parts, 75 parts of shell skin, 15 parts of calcium oxide, 5 parts of stigmasterol, 7.5 parts of hydroxy silicon oil, 2 parts of epoxidized soybean oil to be worth doing.
Further, the stalk, sawdust, the mesh number of shell skin are 20-40 mesh.
Further, the dehydrating agent is fiber desiccant.
Further, the biomass new energy fuel is cylindrical fuel, diameter 6-20mm, length 20-60mm.
A kind of preparation method according to above-mentioned biomass new energy fuel, comprising the following steps: (1) first by the straw of selection
Three kinds of stalk, sawdust, shell skin raw materials crush respectively, screen out soil, grains of sand harmful components；(2) it is matched by formulation weight, by straw
Stalk, sawdust, shell skin, calcium oxide, dehydrating agent uniformly mix；(3) mixed-powder is packed into the high-order hopper of pellet press, and
Setting form is squeezed into respectively at normal temperature by multiple granulation heads of extruder.
The invention has the following advantages:
(1) as the data of embodiment 1-3 and comparative example 5 as it can be seen that the combustion of biomass new energy fuel made from embodiment 1-3
It heats value and physical property significant effect is higher than the combustion heat value and physical property of biomass new energy fuel made from comparative example 5
Effect；Simultaneously by the data of embodiment 1-3 as it can be seen that embodiment 1 is optimum embodiment.
(2) by embodiment 1 and the data of comparative example 1-4 as it can be seen that stigmasterol, hydroxy silicon oil, epoxidized soybean oil are given birth in production
Play synergistic effect in substance new energy fuel, collaboration improves the combustion heat value of biomass new energy fuel and physical
Energy；This is:
Original formulation uses the main body comburant of stalk, sawdust, shell skin as biomass combustion, and calcium oxide is as desulfuration
Agent and antichlor, but only with said components, can not achieve better combustion heat value and physical property, thus the present invention also adds
Stigmasterol, hydroxy silicon oil, epoxidized soybean oil are added.
Stigmasterol has high carbohydrate content, can increase combustion heat value, while it reduces moisture in biology with water imbibition
The content of matter promotes burning inflammability, while good film forming and ductility, has to biomass cells good affine
Property, fully dispersed each biomass components, balanced each component physical property, can enhance made of fuel whole impact strength and
Crush resistance；Hydroxy silicon oil is active hydroxyl, can further improve the Fundamental Physical Properties of material, in combustion
It is decomposed to form micro- silicon-carbon intermediate of Nano grade, the carbon black that stigmasterol is decomposed to form in combustion process can be adsorbed onto micro- silicon-carbon
On intermediate, to improve dispersibility, so as to come into full contact with promotion full combustion with air, combustion heat value is improved；Epoxy
Soybean oil has excellent water resistance, can be sufficiently mixed with each biomass components, and it is good mechanical strong to assign biomass fuel
Degree, while the terminal hydroxy group of its epoxy group and hydroxy silicon oil has hydrogen bond action, improves the dispersibility of hydroxy silicon oil, and pass through two
The combination of person further promotes the integral strength of biomass fuel in biomass fuel, and stigmasterol has certain surface-active
Agent effect can improve the viscosity of hydroxy silicon oil and epoxidized soybean oil, and flash carbonization collapses in combustion, be formed porous
Road promotes the entrance of oxygen, the decomposition rate of hydroxy silicon oil and the full combustion of stigmasterol is improved, to improve the combustion heat
Value.
(3) by the data of comparative example 6-8 as it can be seen that stigmasterol, hydroxy silicon oil, the weight ratio of epoxidized soybean oil is not at (4-6):
(5-10): when in (1-3) range, the combustion heat value and physical property effect and embodiment 1- of biomass new energy fuel obtained
3 numerical value is very different, suitable with the numerical value of the prior art (comparative example 5) much smaller than the numerical value of embodiment 1-3.Beans of the present invention
Sterol, hydroxy silicon oil, epoxidized soybean oil pass through when control produces biomass new energy fuel as reinforcement system, embodiment 1-3
Stigmasterol, hydroxy silicon oil are added, the weight ratio of epoxidized soybean oil is (4-6): (5-10): (1-3), is realized sharp in reinforcement system
There is high carbohydrate content with stigmasterol, combustion heat value, balanced each component physical property can be increased；Hydroxy silicon oil is in combustion process
In be decomposed to form micro- silicon-carbon intermediate of Nano grade, the carbon black that stigmasterol is decomposed to form in combustion process, can be adsorbed onto it is micro-
On silicon-carbon intermediate, promotion full combustion can be come into full contact with air, improve combustion heat value；Epoxidized soybean oil improves hydroxyl silicon
The dispersibility of oil, flash carbonization collapses stigmasterol in combustion, forms multi-pore channel, promotes the entrance of oxygen, improves hydroxyl
The decomposition rate of silicone oil and the full combustion of stigmasterol, so that combustion heat value is improved, to improve the combustion of biomass new energy
The combustion heat value and physical property of material.
Specific embodiment
To facilitate a better understanding of the present invention, it is illustrated by the following examples, these examples belong to protection of the invention
Range, but do not limit the scope of the invention.
In embodiment, a kind of biomass new energy fuel, as unit of parts by weight, including following raw material: stalk 650-
750 parts, 150-250 parts of sawdust, 50-100 parts of shell skin, 10-20 parts of calcium oxide, 4-6 parts of stigmasterol, 5-10 parts of hydroxy silicon oil,
1-3 parts of epoxidized soybean oil.
The stalk, sawdust, the mesh number of shell skin are 20-40 mesh.The dehydrating agent is fiber desiccant.It is new to state biomass
Energy fuel is cylindrical fuel, diameter 6-20mm, length 20-60mm.
A kind of preparation method according to above-mentioned biomass new energy fuel, comprising the following steps: (1) first by the straw of selection
Three kinds of stalk, sawdust, shell skin raw materials crush respectively, screen out soil, grains of sand harmful components；(2) it is matched by formulation weight, by straw
Stalk, sawdust, shell skin, calcium oxide, dehydrating agent uniformly mix；(3) mixed-powder is packed into the high-order hopper of pellet press, and
Setting form is squeezed into respectively at normal temperature by multiple granulation heads of extruder.
Embodiment 1
A kind of biomass new energy fuel, as unit of parts by weight, including following raw material: 700 parts of stalk, 200 parts of sawdust,
75 parts of shell skin, 15 parts of calcium oxide, 5 parts of stigmasterol, 7.5 parts of hydroxy silicon oil, 2 parts of epoxidized soybean oil.
The stalk, sawdust, the mesh number of shell skin are 30 mesh.The dehydrating agent is fiber desiccant.State the new energy of biomass
Source fuel is cylindrical fuel, diameter 13mm, length 40mm.
A kind of preparation method according to above-mentioned biomass new energy fuel, which comprises the following steps: (1)
Three kinds of stalk of selection, sawdust, shell skin raw materials are crushed respectively first, screen out soil, grains of sand harmful components；(2) by formula weight
Amount proportion, by stalk, sawdust, shell skin, calcium oxide, dehydrating agent is uniformly mixed；(3) mixed-powder is packed into pellet press
High-order hopper, and setting form is squeezed into respectively at normal temperature by multiple granulation heads of extruder.
Embodiment 2
A kind of biomass new energy fuel, as unit of parts by weight, including following raw material: 650 parts of stalk, 250 parts of sawdust,
50 parts of shell skin, 20 parts of calcium oxide, 4 parts of stigmasterol, 10 parts of hydroxy silicon oil, 1 part of epoxidized soybean oil.
The stalk, sawdust, the mesh number of shell skin are 20 mesh.The dehydrating agent is fiber desiccant.State the new energy of biomass
Source fuel is cylindrical fuel, diameter 20mm, length 20mm.
A kind of preparation method according to above-mentioned biomass new energy fuel, comprising the following steps: (1) first by the straw of selection
Three kinds of stalk, sawdust, shell skin raw materials crush respectively, screen out soil, grains of sand harmful components；(2) it is matched by formulation weight, by straw
Stalk, sawdust, shell skin, calcium oxide, dehydrating agent uniformly mix；(3) mixed-powder is packed into the high-order hopper of pellet press, and
Setting form is squeezed into respectively at normal temperature by multiple granulation heads of extruder.
Embodiment 3
A kind of biomass new energy fuel, as unit of parts by weight, including following raw material: 750 parts of stalk, 150 parts of sawdust,
100 parts of shell skin, 10 parts of calcium oxide, 6 parts of stigmasterol, 5 parts of hydroxy silicon oil, 3 parts of epoxidized soybean oil.
The stalk, sawdust, the mesh number of shell skin are 40 mesh.The dehydrating agent is fiber desiccant.State the new energy of biomass
Source fuel is cylindrical fuel, diameter 6mm, length 60mm.
A kind of preparation method according to above-mentioned biomass new energy fuel, comprising the following steps: (1) first by the straw of selection
Three kinds of stalk, sawdust, shell skin raw materials crush respectively, screen out soil, grains of sand harmful components；(2) it is matched by formulation weight, by straw
Stalk, sawdust, shell skin, calcium oxide, dehydrating agent uniformly mix；(3) mixed-powder is packed into the high-order hopper of pellet press, and
Setting form is squeezed into respectively at normal temperature by multiple granulation heads of extruder.
Comparative example 1
It is essentially identical with the production technology of embodiment 1, it has only the difference is that in the raw material of preparation biomass new energy fuel
Lack stigmasterol, hydroxy silicon oil, epoxidized soybean oil.
Comparative example 2
It is essentially identical with the production technology of embodiment 1, it has only the difference is that in the raw material of preparation biomass new energy fuel
Lack stigmasterol.
Comparative example 3
It is essentially identical with the production technology of embodiment 1, it has only the difference is that in the raw material of preparation biomass new energy fuel
Lack hydroxy silicon oil.
Comparative example 4
It is essentially identical with the production technology of embodiment 1, it has only the difference is that in the raw material of preparation biomass new energy fuel
Lack epoxidized soybean oil.
Comparative example 5
Using Chinese patent literature " a kind of biomass triplet-powder solid fuel and its production technology (patent No.:
ZL200910166760.9 method described in specific embodiment 1 produces thermoplastic elastic material in) ".
Comparative example 6
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that in the raw material of preparation biomass new energy fuel
8 parts of stigmasterol, 4 parts of hydroxy silicon oil, 4 parts of epoxidized soybean oil.
Comparative example 7
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that in the raw material of preparation biomass new energy fuel
3 parts of stigmasterol, 12 parts of hydroxy silicon oil, 0.5 part of epoxidized soybean oil.
Comparative example 8
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that in the raw material of preparation biomass new energy fuel
3 parts of stigmasterol, 4 parts of hydroxy silicon oil, 4 parts of epoxidized soybean oil.
Biomass new energy fuel is produced according to the technique of embodiment 1-3 and comparative example 1-8, tests Polodyakonov coefficient coefficient,
And combustion heat value is tested according to GBT 14402-2007, as a result as shown in the table.
As seen from the above table: (1) as the data of embodiment 1-3 and comparative example 5 as it can be seen that biomass made from embodiment 1-3 is new
The combustion heat value and physical property significant effect of energy fuel are higher than the combustion heat of biomass new energy fuel made from comparative example 5
Value and physical property effect；Simultaneously by the data of embodiment 1-3 as it can be seen that embodiment 1 is optimum embodiment.
(2) by embodiment 1 and the data of comparative example 1-4 as it can be seen that stigmasterol, hydroxy silicon oil, epoxidized soybean oil are given birth in production
Play synergistic effect in substance new energy fuel, collaboration improves the combustion heat value of biomass new energy fuel and physical
Energy；This is:
Original formulation uses the main body comburant of stalk, sawdust, shell skin as biomass combustion, and calcium oxide is as desulfuration
Agent and antichlor, but only with said components, can not achieve better combustion heat value and physical property, thus the present invention also adds
Stigmasterol, hydroxy silicon oil, epoxidized soybean oil are added.
Stigmasterol has high carbohydrate content, can increase combustion heat value, while it reduces moisture in biology with water imbibition
The content of matter promotes burning inflammability, while good film forming and ductility, has to biomass cells good affine
Property, fully dispersed each biomass components, balanced each component physical property, can enhance made of fuel whole impact strength and
Crush resistance；Hydroxy silicon oil is active hydroxyl, can further improve the Fundamental Physical Properties of material, in combustion
Be decomposed to form micro- silicon-carbon intermediate of Nano grade, the carbon black that stigmasterol is decomposed to form in combustion process, can be adsorbed onto micro- silicon
On intermediate carbon, to improve dispersibility, so as to come into full contact with promotion full combustion with air, combustion heat value is improved；Ring
Oxygen soybean oil has excellent water resistance, can be sufficiently mixed with each biomass components, assigns the good machinery of biomass fuel
Intensity, while the terminal hydroxy group of its epoxy group and hydroxy silicon oil has hydrogen bond action, improves the dispersibility of hydroxy silicon oil, and pass through
The combination of the two further promotes the integral strength of biomass fuel in biomass fuel, and stigmasterol has certain surface living
Property agent effect, the viscosity of hydroxy silicon oil and epoxidized soybean oil can be improved, in combustion flash carbonization collapse, formed it is more
Duct promotes the entrance of oxygen, improves the decomposition rate of hydroxy silicon oil and the full combustion of stigmasterol, to improve burning
Calorific value.
(3) by the data of comparative example 6-8 as it can be seen that stigmasterol, hydroxy silicon oil, the weight ratio of epoxidized soybean oil is not at (4-6):
(5-10): when in (1-3) range, the combustion heat value and physical property effect and embodiment 1- of biomass new energy fuel obtained
3 numerical value is very different, suitable with the numerical value of the prior art (comparative example 5) much smaller than the numerical value of embodiment 1-3.Beans of the present invention
Sterol, hydroxy silicon oil, epoxidized soybean oil pass through when control produces biomass new energy fuel as reinforcement system, embodiment 1-3
Stigmasterol, hydroxy silicon oil are added, the weight ratio of epoxidized soybean oil is (4-6): (5-10): (1-3), is realized sharp in reinforcement system
There is high carbohydrate content with stigmasterol, combustion heat value, balanced each component physical property can be increased；Hydroxy silicon oil is in combustion process
In be decomposed to form micro- silicon-carbon intermediate of Nano grade, the carbon black that stigmasterol is decomposed to form in combustion process, can be adsorbed onto it is micro-
On silicon-carbon intermediate, promotion full combustion can be come into full contact with air, improve combustion heat value；Epoxidized soybean oil improves hydroxyl silicon
The dispersibility of oil, flash carbonization collapses stigmasterol in combustion, forms multi-pore channel, promotes the entrance of oxygen, improves hydroxyl
The decomposition rate of silicone oil and the full combustion of stigmasterol, so that combustion heat value is improved, to improve the combustion of biomass new energy
The combustion heat value and physical property of material.
The above content is it cannot be assumed that present invention specific implementation is only limited to these instructions, for the technical field of the invention
Those of ordinary skill for, under the premise of not departing from present inventive concept, a number of simple deductions or replacements can also be made, all answers
When being considered as belonging to present invention scope of patent protection determined by the appended claims.
Claims (8)
1. a kind of biomass new energy fuel, which is characterized in that its raw material includes: stalk, sawdust, shell skin, dehydrating agent, oxidation
Calcium, stigmasterol, hydroxy silicon oil, epoxidized soybean oil；The stigmasterol, hydroxy silicon oil, epoxidized soybean oil weight ratio are (4-6):
(5-10):(1-3)。
2. biomass new energy fuel according to claim 1, which is characterized in that the stigmasterol, hydroxy silicon oil, epoxy
The weight ratio of soybean oil is 5:7.5:2.
3. biomass new energy fuel according to claim 1, which is characterized in that the biomass new energy fuel is with weight
Amount part is unit, including following raw material: 650-750 parts of stalk, 150-250 parts of sawdust, 50-100 parts of shell skin, calcium oxide 10-
20 parts, 4-6 parts of stigmasterol, 5-10 parts of hydroxy silicon oil, 1-3 parts of epoxidized soybean oil.
4. biomass new energy fuel according to claim 1, which is characterized in that the biomass new energy fuel is with weight
Amount part is unit, including following raw material: 700 parts of stalk, 200 parts of sawdust, 75 parts of shell skin, 15 parts of calcium oxide, 5 parts of stigmasterol,
7.5 parts of hydroxy silicon oil, 2 parts of epoxidized soybean oil.
5. biomass new energy fuel according to claim 1, which is characterized in that the stalk, sawdust, the mesh of shell skin
Number is 20-40 mesh.
6. biomass new energy fuel according to claim 1, which is characterized in that the dehydrating agent is fiber desiccant.
7. biomass new energy fuel according to claim 1, which is characterized in that the biomass new energy fuel is circle
Cylindricality fuel, diameter 6-20mm, length 20-60mm.
8. a kind of preparation method of biomass new energy fuel according to claim 1-7, which is characterized in that packet
Include following steps: (1) first crushing three kinds of stalk of selection, sawdust, shell skin raw materials respectively, screen out soil, grains of sand nocuousness at
Point；(2) it is matched by formulation weight, by stalk, sawdust, shell skin, calcium oxide, dehydrating agent is uniformly mixed；(3) mixed-powder is filled
Enter the high-order hopper of pellet press, and is squeezed into setting form respectively at normal temperature by multiple granulation heads of extruder.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110208276A (en) * | 2019-07-02 | 2019-09-06 | 长沙而道新能源科技有限公司 | A kind of Concrete In Structures visual defects analyzer and its detection device |
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