CN109810661A - A kind of two-component water resistant color inhibition joint trimming agent and preparation method thereof - Google Patents
A kind of two-component water resistant color inhibition joint trimming agent and preparation method thereof Download PDFInfo
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- CN109810661A CN109810661A CN201910018047.3A CN201910018047A CN109810661A CN 109810661 A CN109810661 A CN 109810661A CN 201910018047 A CN201910018047 A CN 201910018047A CN 109810661 A CN109810661 A CN 109810661A
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Abstract
The present invention provides a kind of two-component water resistant color inhibition joint trimming agent and preparation method thereof, including component A and B component, the component A include: epoxy resin 90~95%, white carbon black 5~10%, dispersing agent 0~0.5%, defoaming agent 0~0.5% by mass percentage；The B component includes: modified aliphatic cyclic amine 40~50%, polyetheramine 20~30%, water resistant color inhibition agent 10~20% by mass percentage, higher boiling diluent 10~20%, pigment 3~5%, white carbon black 5~10%, dispersing agent 0~0.5%, defoaming agent 0~0.5%, levelling agent 0~0.5%.The present invention, by adding water repellent agent, makes joint trimming agent obtained be provided with excellent water-resistance, weatherability and yellowing resistance under conditions of not changing the strong original bonding force of joint trimming agent, high-low temperature resistant and funginert excellent properties.
Description
Technical field
The invention belongs to building material technical fields, and in particular to a kind of two-component water resistant color inhibition joint trimming agent and its preparation
Method.
Background technique
Today's society, various New Building Materials emerge one after another, and wherein ceramic tile is the main of ground and decorative material for wall surface
One of kind is widely used.Joint trimming agent is filled primarily with one of material as ceramic tile gap, fills ceramic tile from jointing agent is substituted
Since gap, solve the problems, such as that ceramic tile gap nigrescence mildew is inaesthetic.But in construction and use process, due to live humidity
Greatly, it is commonly present chance water to whiten the problem of changing colour, it is anti-that some joint trimming agents add nonyl phenol or low boiling point diluent etc. in formula
Aqua, though improve the water resistance of product, but there is sunlight irradiate easy xanthochromia and not environmentally the problems such as.Therefore, needle
To the above problem, it is necessary to propose further solution.
Summary of the invention
In view of this, the present invention provides a kind of two-component water resistant color inhibition joint trimming agent and preparation method thereof, do not changing beauty
Stitch that the original bonding force of agent is strong, under conditions of not mouldy and beautiful etc. excellent properties, by adding water resistant color inhibition agent and high boiling
Point diluent makes joint trimming agent obtained be provided with excellent water-resistance, yellowing resistance and weatherability.
The technical solution of the present invention is as follows: a kind of two-component water resistant color inhibition joint trimming agent, which is characterized in that including component A and B
Component, the component A include: epoxy resin 90~95% by mass percentage, white carbon black 5~10%, dispersing agent 0~0.5%,
Defoaming agent 0~0.5%；The B component includes: modified aliphatic cyclic amine 40~50% by mass percentage, and polyetheramine 20~30% resists
Water color inhibition agent 10~20%, higher boiling diluent 10~20%, pigment 3~5%, white carbon black 5~10%, dispersing agent 0~0.5% disappear
Infusion 0~0.5%, levelling agent 0~0.5%.
Further, the epoxy resin of the component A is bisphenol A-type and A Hydrogenated Bisphenol A type epoxy resin.
Further, the epoxide equivalent of the bisphenol A-type and A Hydrogenated Bisphenol A type epoxy resin is 180~250.More preferably
For epoxide equivalent is 200~240.
Further, the active hydrogen equivalent weight of the modification aliphatic cyclic amine of the B component is 90~110, (25 DEG C) of viscosity for 250~
400 mPa•s。
The molecular weight of the polyetheramine of the B component is 230~1000, the polyetheramine include one or two kinds of or two kinds with
The polyetheramine of upper different molecular weight.Preferably, the polyetheramine of the B component is any of D-230 polyetheramine, D-400 polyetheramine
Kind or two kinds of mixture.
Further, the water resistant color inhibition agent of the B component is hydrogenated bisphenol A.
Further, the water resistant color inhibition agent dosage of the B component is 10~20% by mass percentage.
Further, the higher boiling diluent of the B component is benzyl carbinol, phenylpropanol, ethyleneglycol monophenylether and propylene glycol
One of monophenyl ether.
Further, the mass percent of the higher boiling diluent of the B component is 10~20%,
Other auxiliary agents of the present invention such as white carbon black, defoaming agent, dispersing agent, levelling agent and pigment are all not particularly limited, choosing
It is dimethicone from common classification, such as defoaming agent, dispersing agent is polyacrylic, and levelling agent is dimethyl-silicon class, pigment
It is the common pigments such as noble's gold and illusion Huang.
The present invention provides a kind of preparation method of two-component water resistant color inhibition joint trimming agent, comprising the following steps:
The component A the preparation method comprises the following steps: epoxy resin, white carbon black and dispersing agent are sequentially added in reactor, open stirring,
It is stirred 1 hour with 30~40 revs/min of speed, defoaming agent is added, speed of agitator is adjusted to 10~20 revs/min, and it is small to continue stirring 0.5
When, after system vacuumizing and defoaming, obtain component A.
The B component the preparation method comprises the following steps: higher boiling diluent and water resistant color inhibition agent are added in reactor, unlatching is stirred
Mix, stirred with 30~40 revs/min of speed, and be to slowly warm up to 70~80 DEG C, stirring it is complete it is molten after, be slowly added to modified aliphatic cyclic amine
And polyetheramine, it stirs 0.5 hour, is cooled to room temperature, sequentially add white carbon black, pigment and dispersing agent, insulated and stirred 1 hour, then
Defoaming agent is added and levelling agent, speed of agitator are adjusted to 10~20 revs/min, after continuing stirring 0.5 hour, system vacuumizing and defoaming
Afterwards, B component is obtained.
It after component A and B component are made, is respectively charged into isometric disjunctor A pipe and B pipe by bottle placer, when construction
By power-assisted glue rifle Jiao Zui mixing after squeeze into curing molding in ceramic tile gap, i.e., acquisition two-component water resistant color inhibition joint trimming agent at
Product.
The present invention provides a kind of two-component water resistant color inhibition joint trimming agent, the water resistant color inhibition agent of addition and higher boiling dilution
Agent is free of the harmful substances such as nonyl phenol and low boiling point easy volatile solvent, meets the rings such as current RoHS Directive and Reach regulation
Guaranteed request.
The preparation method of two-component water resistant color inhibition joint trimming agent provided by the invention is simple and practical, easy to industrialized production.
Specific embodiment
Technical solution of the present invention is clearly and completely described below in conjunction with embodiment, it is clear that described reality
Applying example is only a part of the embodiment of the present invention, instead of all the embodiments.
Embodiment 1
A kind of two-component water resistant color inhibition joint trimming agent, including component A and B component, the component A include 465 grams of epoxy resin
E44,33 grams of white carbon blacks, 1 gram of dispersing agent Efka PX 4701 and 1 gram of dimethicone.
The B component includes 171 grams of modified aliphatic cyclic amines, 67.5 grams of polyetheramine D230,63 grams of hydrogenated bisphenol As, 90 grams of benzene second
Alcohol, 18 grams of pigment dreamlike Huang, 36 grams of white carbon blacks, 1.8 grams of dispersing agent Efka PX, 4701,1.35 grams of dimethicones, 1.35 grams
Levelling agent BYK-323.
A kind of preparation method of two-component water resistant color inhibition joint trimming agent, include the following:
The component A the preparation method comprises the following steps: by 465 grams of epoxy resin E44,33 grams of white carbon blacks and 1 gram of dispersing agent Efka PX
4701 sequentially add in reactor, open stirring, are stirred 1 hour with 30~40 revs/min of speed, 1 gram of dimethicone is added,
Speed of agitator is adjusted to 10~20 revs/min, continues to stir 0.5 hour, after system vacuumizing and defoaming, obtains component A.
The B component the preparation method comprises the following steps: 90 grams of benzyl carbinols and 63 grams of hydrogenated bisphenol As are added in reactors, unlatching is stirred
Mix, stirred with 30~40 revs/min of speed, and be to slowly warm up to 70~80 DEG C, stirring it is complete it is molten after, be slowly added to 171 grams of modifications
Aliphatic cyclic amine and 67.5 grams of polyetheramine D230 stir 0.5 hour, are cooled to room temperature, sequentially add the illusion of 18 grams of pigment it is yellow, 36 grams it is white
Carbon black and 1.8 grams of dispersing agent Efka PX 4701 insulated and stirred 1 hour, add 1.35 grams of dimethicones and 1.35 grams of streams
Flat agent BYK-323, speed of agitator are adjusted to 10~20 revs/min, after continuing stirring 0.5 hour, after system vacuumizing and defoaming, obtain B
Component.
It after component A and B component are made, is respectively charged into isometric disjunctor A pipe and B pipe by bottle placer, when construction
Curing molding in ceramic tile gap is squeezed into after Jiao Zui mixing by power-assisted glue rifle.
Embodiment 2
A kind of two-component water resistant color inhibition joint trimming agent, including component A and B component, the component A include 455 grams of epoxy resin
E51,43 grams of white carbon blacks, 1 gram of dispersing agent Efka PX 4701 and 1 gram of dimethicone.
The B component includes 180 grams of modified aliphatic cyclic amines, 63 grams of polyetheramine D230,58.5 grams of hydrogenated bisphenol As, 90 grams of phenylpropyl alcohols
Alcohol, 18 grams of pigment dreamlike Huang, 36 grams of white carbon blacks, 1.8 grams of dispersing agent Efka PX, 4701,1.35 grams of dimethicones, 1.35 grams
Levelling agent BYK-323.
A kind of preparation method of two-component water resistant color inhibition joint trimming agent, include the following:
The component A the preparation method comprises the following steps: by 455 grams of epoxy resin E51,43 grams of white carbon blacks and 1 gram of dispersing agent Efka PX
4701 sequentially add in reactor, open stirring, are stirred 1 hour with 30~40 revs/min of speed, 1 gram of dimethicone is added,
Speed of agitator is adjusted to 10~20 revs/min, continues to stir 0.5 hour, after system vacuumizing and defoaming, obtains component A.
The B component the preparation method comprises the following steps: 90 grams of phenylpropanols and 58.5 grams of hydrogenated bisphenol As are added in reactors, open
Stirring is stirred with 30~40 revs/min of speed, and is to slowly warm up to 70~80 DEG C, stirring it is complete it is molten after, be slowly added to 180 grams and change
Property aliphatic cyclic amine and 63 grams of polyetheramine D230, stir 0.5 hour, be cooled to room temperature, sequentially add 18 grams of pigment illusions it is yellow, 36 grams it is white
Carbon black and 1.8 grams of dispersing agent Efka PX 4701 insulated and stirred 1 hour, add 1.35 grams of dimethicones and 1.35 grams of streams
Flat agent BYK-323, speed of agitator are adjusted to 10~20 revs/min, after continuing stirring 0.5 hour, after system vacuumizing and defoaming, obtain B
Component.
It after component A and B component are made, is respectively charged into isometric disjunctor A pipe and B pipe by bottle placer, when construction
Curing molding in ceramic tile gap is squeezed into after Jiao Zui mixing by power-assisted glue rifle.
Embodiment 3
A kind of two-component water resistant color inhibition joint trimming agent, including component A and B component, the component A include 465 grams of epoxy resin ST-
3000,33 grams of white carbon blacks, 1 gram of dispersing agent Efka PX 4701 and 1 gram of dimethicone.
The B component includes 171 grams of modified aliphatic cyclic amines, 67.5 grams of polyetheramine D230,58.5 grams of hydrogenated bisphenol As, 90 grams of benzene
The dreamlike Huangs of propyl alcohol, 18 grams of pigment, 40.5 grams of white carbon blacks, 1.8 grams of dispersing agent Efka PX, 4701,1.35 grams of dimethicones,
1.35 grams of levelling agent BYK-323.
A kind of preparation method of two-component water resistant color inhibition joint trimming agent, include the following:
The component A the preparation method comprises the following steps: by 465 grams of epoxy resin ST-3000,33 grams of white carbon blacks and 1 gram of dispersing agent Efka
PX 4701 is sequentially added in reactor, opens stirring, is stirred 1 hour with 30~40 revs/min of speed, 1 gram of dimethyl-silicon is added
Oil, speed of agitator are adjusted to 10~20 revs/min, continue to stir 0.5 hour, after system vacuumizing and defoaming, obtain component A.
The B component the preparation method comprises the following steps: 90 grams of phenylpropanols and 18 grams of hydrogenated bisphenol As are added in reactors, unlatching is stirred
Mix, stirred with 30~40 revs/min of speed, and be to slowly warm up to 70~80 DEG C, stirring it is complete it is molten after, be slowly added to 171 grams of modifications
Aliphatic cyclic amine and 67.5 grams of polyetheramine D230 stir 0.5 hour, are cooled to room temperature, sequentially add the illusion of 18 grams of pigment it is yellow, 36 grams it is white
Carbon black and 1.8 grams of dispersing agent Efka PX 4701 insulated and stirred 1 hour, add 1.35 grams of dimethicones and 1.35 grams of streams
Flat agent BYK-323, speed of agitator are adjusted to 10~20 revs/min, after continuing stirring 0.5 hour, after system vacuumizing and defoaming, obtain B
Component.
It after component A and B component are made, is respectively charged into isometric disjunctor A pipe and B pipe by bottle placer, when construction
Curing molding in ceramic tile gap is squeezed into after Jiao Zui mixing by power-assisted glue rifle.
Embodiment 4
A kind of two-component water resistant color inhibition joint trimming agent, including component A and B component, the component A include 455 grams of epoxy resin
E44,43 grams of white carbon blacks, 1 gram of dispersing agent Efka PX 4701 and 1 gram of dimethicone.
The B component includes 171 grams of modified aliphatic cyclic amines, 63 grams of polyetheramine D400,67.5 grams of hydrogenated bisphenol As, 90 grams of second two
The dreamlike Huangs of alcohol monophenyl ether, 18 grams of pigment, 36 grams of white carbon blacks, 1.8 grams of dispersing agent Efka PX, 4701,1.35 grams of dimethicones,
1.35 grams of levelling agent BYK-323.
A kind of preparation method of two-component water resistant color inhibition joint trimming agent, include the following:
The component A the preparation method comprises the following steps: by 455 grams of epoxy resin E44,43 grams of white carbon blacks and 1 gram of dispersing agent Efka PX
4701 sequentially add in reactor, open stirring, are stirred 1 hour with 30~40 revs/min of speed, 1 gram of dimethicone is added,
Speed of agitator is adjusted to 10~20 revs/min, continues to stir 0.5 hour, after system vacuumizing and defoaming, obtains component A.
The B component the preparation method comprises the following steps: reactors are added in 90 grams of ethyleneglycol monophenylethers and 67.5 grams of hydrogenated bisphenol As
In, open stirring, stirred with 30~40 revs/min of speed, and be to slowly warm up to 70~80 DEG C, stirring it is complete it is molten after, be slowly added to
171 grams of modified aliphatic cyclic amines and 63 grams of polyetheramine D400 are stirred 0.5 hour, are cooled to room temperature, sequentially add 18 grams of pigment illusions
Yellow, 36 grams of white carbon blacks and 1.8 grams of dispersing agent Efka PX 4701, insulated and stirred 1 hour, add 1.35 grams of dimethicones and
1.35 grams of levelling agent BYK-323, speed of agitator are adjusted to 10~20 revs/min, after continuing stirring 0.5 hour, system vacuumizing and defoaming
Afterwards, B component is obtained.
It after component A and B component are made, is respectively charged into isometric disjunctor A pipe and B pipe by bottle placer, when construction
Curing molding in ceramic tile gap is squeezed into after Jiao Zui mixing by power-assisted glue rifle.
Embodiment 5
A kind of two-component water resistant color inhibition joint trimming agent, including component A and B component, the component A include 450 grams of epoxy resin
E51,48 grams of white carbon blacks, 1 gram of dispersing agent Efka PX 4701 and 1 gram of dimethicone.
The B component includes 193.5 grams of modified aliphatic cyclic amines, 67.5 grams of polyetheramine D400,54 grams of hydrogenated bisphenol As, 90 grams of second
Glycol monophenyl ether, 18 grams of pigment dreamlike Huang, 22.5 grams of white carbon blacks, 1.8 grams of dispersing agent Efka PX, 4701,1.35 grams of dimethyl-silicons
Oil, 1.35 grams of levelling agent BYK-323.
A kind of preparation method of two-component water resistant color inhibition joint trimming agent, include the following:
The component A the preparation method comprises the following steps: by 450 grams of epoxy resin E51,48 grams of white carbon blacks and 1 gram of dispersing agent Efka PX
4701 sequentially add in reactor, open stirring, are stirred 1 hour with 30~40 revs/min of speed, 1 gram of dimethicone is added,
Speed of agitator is adjusted to 10~20 revs/min, continues to stir 0.5 hour, after system vacuumizing and defoaming, obtains component A.
The B component the preparation method comprises the following steps: 90 grams of ethyleneglycol monophenylethers and 54 grams of hydrogenated bisphenol As are added in reactors,
Open stirring, stirred with 30~40 revs/min of speed, and be to slowly warm up to 70~80 DEG C, stirring it is complete it is molten after, be slowly added to
193.5 grams of modified aliphatic cyclic amines and 67.5 grams of polyetheramine D400 are stirred 0.5 hour, are cooled to room temperature, sequentially add 18 grams of pigment dreams
Unreal yellow, 22.5 grams of white carbon blacks and 1.8 grams of dispersing agent Efka PX 4701, insulated and stirred 1 hour, add 1.35 grams of dimethyl-silicons
Oil and 1.35 grams of levelling agent BYK-323, speed of agitator are adjusted to 10~20 revs/min, and after continuing stirring 0.5 hour, system is vacuumized
After deaeration, B component is obtained.
It after component A and B component are made, is respectively charged into isometric disjunctor A pipe and B pipe by bottle placer, when construction
Curing molding in ceramic tile gap is squeezed into after Jiao Zui mixing by power-assisted glue rifle.
Embodiment 6
A kind of two-component water resistant color inhibition joint trimming agent, including component A and B component, the component A include 450 grams of epoxy resin ST-
3000,48 grams of white carbon blacks, 1 gram of dispersing agent Efka PX 4701 and 1 gram of dimethicone.
The B component includes 171 grams of modified aliphatic cyclic amines, 67.5 grams of polyetheramine D400,58.5 grams of hydrogenated bisphenol As, 90 gram third
Glycol monophenyl ether, 18 grams of pigment dreamlike Huang, 40.5 grams of white carbon blacks, 1.8 grams of dispersing agent Efka PX, 4701,1.35 grams of dimethyl-silicons
Oil, 1.35 grams of levelling agent BYK-323.
A kind of preparation method of two-component water resistant color inhibition joint trimming agent, include the following:
The component A the preparation method comprises the following steps: by 450 grams of epoxy resin ST-3000,48 grams of white carbon blacks and 1 gram of dispersing agent Efka PX
4701 sequentially add in reactor, open stirring, are stirred 1 hour with 30~40 revs/min of speed, 1 gram of dimethicone is added,
Speed of agitator is adjusted to 10~20 revs/min, continues to stir 0.5 hour, after system vacuumizing and defoaming, obtains component A.
The B component the preparation method comprises the following steps: reactors are added in 90 grams of propylene glycol monophenyl ethers and 58.5 grams of hydrogenated bisphenol As
In, open stirring, stirred with 30~40 revs/min of speed, and be to slowly warm up to 70~80 DEG C, stirring it is complete it is molten after, be slowly added to
171 grams of modified aliphatic cyclic amines and 67.5 grams of polyetheramine D400 are stirred 0.5 hour, are cooled to room temperature, sequentially add 18 grams of pigment illusions
Yellow, 40.5 grams of white carbon blacks and 1.8 grams of dispersing agent Efka PX 4701, insulated and stirred 1 hour, add 1.35 grams of dimethicones
With 1.35 grams of levelling agent BYK-323, speed of agitator is adjusted to 10~20 revs/min, and after continuing stirring 0.5 hour, system vacuumizes de-
After bubble, B component is obtained.
It after component A and B component are made, is respectively charged into isometric disjunctor A pipe and B pipe by bottle placer, when construction
Curing molding in ceramic tile gap is squeezed into after Jiao Zui mixing by power-assisted glue rifle.
In addition, it should be understood that although this specification is described in terms of embodiments, but not for those skilled in the art
For member, it is clear that invention is not limited to the details of the above exemplary embodiments, and without departing substantially from spirit of the invention or substantially
In the case where feature, the present invention can be realized in other specific forms.Therefore, in all respects, should all will implement
Example regards exemplary as, and is non-limiting, and the scope of the present invention is by appended claims rather than above description limits
It is fixed, it is intended that including all changes that fall within the meaning and scope of the equivalent elements of the claims in the present invention.
Each embodiment only contains an independent technical solution, this narrating mode of specification be only be clear
For the sake of, the skilled in the art should refer to the specification as a whole, and the technical solutions in the embodiments can also be through appropriate
Combination, forms other embodiments that can be understood by those skilled in the art.It is noted that being not described in detail in the present invention
Technical characteristic, can be realized by this field any prior art.
Claims (8)
1. a kind of two-component water resistant color inhibition joint trimming agent, which is characterized in that including component A and B component, the component A presses quality
Percentages include: epoxy resin 90~95%, white carbon black 5~10%, dispersing agent 0~0.5%, defoaming agent 0~0.5%；The B group
Divide includes: modified aliphatic cyclic amine 40~50% by mass percentage, polyetheramine 20~30%, and water resistant color inhibition agent 10~20% is high boiling
Point diluent 10~20%, pigment 3~5%, white carbon black 5~10%, dispersing agent 0~0.5%, defoaming agent 0~0.5%, levelling agent 0~
0.5%。
2. two-component water resistant color inhibition joint trimming agent according to claim 1, which is characterized in that the asphalt mixtures modified by epoxy resin of the component A
Rouge is bisphenol A-type and A Hydrogenated Bisphenol A type epoxy resin.
3. two-component water resistant color inhibition joint trimming agent according to claim 2, which is characterized in that the bisphenol A-type and hydrogenation
The epoxide equivalent of bisphenol-type epoxy resin is 180~250.
4. two-component water resistant color inhibition joint trimming agent according to claim 1, which is characterized in that the modification rouge of the B component
The active hydrogen equivalent weight of cyclammonium is 90~110, and viscosity is 250~400 mPa s.
5. two-component water resistant color inhibition joint trimming agent according to claim 1, which is characterized in that the polyetheramine of the B component
Molecular weight be 230~1000, the polyetheramine includes the polyetheramine of one or two kinds of or two or more different molecular weights.
6. two-component water resistant color inhibition joint trimming agent according to claim 1, which is characterized in that the water resistant of the B component is resistance to
Xanthochromia agent is hydrogenated bisphenol A, and the water resistant color inhibition agent dosage is 10~20% by mass percentage.
7. two-component water resistant color inhibition joint trimming agent according to claim 1, which is characterized in that the higher boiling of the B component
Diluent is one of benzyl carbinol, phenylpropanol, ethyleneglycol monophenylether and propylene glycol monophenyl ether, and the higher boiling of the B component is dilute
Release agent dosage by by mass percentage be 10~20%.
8. a kind of preparation method of such as described in any item two-component water resistant color inhibition joint trimming agents of claim 1-7, feature exist
In, comprising the following steps:
S1. epoxy resin, white carbon black and dispersing agent are sequentially added in reactor, stirring is opened, with 30~40 revs/min of speed
Defoaming agent is added in stirring 1 hour, and speed of agitator is adjusted to 10~20 revs/min, continues stirring 0.5 hour, system vacuumizing and defoaming
Afterwards, component A is obtained；
S2. higher boiling diluent and water resistant color inhibition agent are added in reactor, stirring are opened, with 30~40 revs/min of speed
Stirring, and is to slowly warm up to 70~80 DEG C, stirring it is complete it is molten after, be slowly added to modified aliphatic cyclic amine and polyetheramine, stir 0.5 hour,
It is cooled to room temperature, white carbon black, pigment and dispersing agent is sequentially added, insulated and stirred 1 hour, adds defoaming agent and levelling agent, stir
It mixes revolving speed and is adjusted to 10~20 revs/min, after continuing stirring 0.5 hour, after system vacuumizing and defoaming, obtain B component；
S3. it after component A and B component being made, is respectively charged into isometric disjunctor A pipe and B pipe by bottle placer, when construction is logical
Cross power-assisted glue rifle Jiao Zui mixing after squeeze into curing molding in ceramic tile gap, i.e., acquisition two-component water resistant color inhibition joint trimming agent at
Product.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115093772A (en) * | 2022-08-16 | 2022-09-23 | 北京吉时吉兴贸易有限公司 | Bi-component crack sealer and construction process thereof |
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| US5008308A (en) * | 1987-08-19 | 1991-04-16 | Kawasaki Steel Corp. | Thermal adhesive coating composition based on epoxy resin, high Tg polymer, amine curing agent and film forming agent |
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Application publication date: 20190528 |