CN109810579A - A kind of liquid flame-proof silicon rubber black slurry and its preparation process - Google Patents
A kind of liquid flame-proof silicon rubber black slurry and its preparation process Download PDFInfo
- Publication number
- CN109810579A CN109810579A CN201910048286.3A CN201910048286A CN109810579A CN 109810579 A CN109810579 A CN 109810579A CN 201910048286 A CN201910048286 A CN 201910048286A CN 109810579 A CN109810579 A CN 109810579A
- Authority
- CN
- China
- Prior art keywords
- carbon black
- white carbon
- dispersing agent
- silicon rubber
- blender
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 24
- 239000002002 slurry Substances 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 229920002379 silicone rubber Polymers 0.000 title claims description 23
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 49
- 239000006229 carbon black Substances 0.000 claims abstract description 49
- 239000003063 flame retardant Substances 0.000 claims abstract description 34
- 239000002270 dispersing agent Substances 0.000 claims abstract description 28
- 239000000203 mixture Substances 0.000 claims abstract description 25
- 239000012530 fluid Substances 0.000 claims abstract description 23
- 239000003921 oil Substances 0.000 claims abstract description 21
- 229920001296 polysiloxane Polymers 0.000 claims abstract description 20
- 239000000463 material Substances 0.000 claims abstract description 17
- XQSFXFQDJCDXDT-UHFFFAOYSA-N hydroxysilicon Chemical compound [Si]O XQSFXFQDJCDXDT-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000002245 particle Substances 0.000 claims abstract description 9
- 150000001875 compounds Chemical class 0.000 claims abstract description 8
- 230000001404 mediated effect Effects 0.000 claims abstract description 3
- 238000003756 stirring Methods 0.000 claims description 12
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 claims description 10
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 6
- 238000000227 grinding Methods 0.000 claims description 6
- 239000000377 silicon dioxide Substances 0.000 claims description 6
- 229920002635 polyurethane Polymers 0.000 claims description 5
- 239000004814 polyurethane Substances 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- 229920000058 polyacrylate Polymers 0.000 claims description 4
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 3
- 229910052698 phosphorus Inorganic materials 0.000 claims description 3
- 239000011574 phosphorus Substances 0.000 claims description 3
- 229920002545 silicone oil Polymers 0.000 claims description 3
- CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 claims description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 2
- 229910052710 silicon Inorganic materials 0.000 claims description 2
- 239000010703 silicon Substances 0.000 claims description 2
- QKDIBALFMZCURP-UHFFFAOYSA-N 1-methyl-1$l^{3}-silinane Chemical compound C[Si]1CCCCC1 QKDIBALFMZCURP-UHFFFAOYSA-N 0.000 claims 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims 1
- 239000005977 Ethylene Substances 0.000 claims 1
- 239000006185 dispersion Substances 0.000 abstract description 4
- 238000000034 method Methods 0.000 abstract description 4
- 239000000741 silica gel Substances 0.000 abstract description 4
- 229910002027 silica gel Inorganic materials 0.000 abstract description 4
- 230000008569 process Effects 0.000 abstract description 3
- 239000011248 coating agent Substances 0.000 abstract description 2
- 238000000576 coating method Methods 0.000 abstract description 2
- 229920000260 silastic Polymers 0.000 abstract description 2
- 239000012258 stirred mixture Substances 0.000 abstract 1
- FFUAGWLWBBFQJT-UHFFFAOYSA-N hexamethyldisilazane Chemical compound C[Si](C)(C)N[Si](C)(C)C FFUAGWLWBBFQJT-UHFFFAOYSA-N 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- 238000004040 coloring Methods 0.000 description 3
- 239000003292 glue Substances 0.000 description 3
- 229920000642 polymer Polymers 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 239000004945 silicone rubber Substances 0.000 description 3
- 238000004513 sizing Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- 238000004873 anchoring Methods 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 230000002708 enhancing effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 229920002050 silicone resin Polymers 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- OVSKIKFHRZPJSS-UHFFFAOYSA-N 2,4-D Chemical compound OC(=O)COC1=CC=C(Cl)C=C1Cl OVSKIKFHRZPJSS-UHFFFAOYSA-N 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 229920000180 alkyd Polymers 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 150000001649 bromium compounds Chemical group 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000002596 correlated effect Effects 0.000 description 1
- 230000000875 corresponding effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
- 239000012860 organic pigment Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Landscapes
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The present invention relates to coating and its technical fields of preparation process, more particularly to a kind of liquid silica gel black slurry comprising following composition: vinyl-terminated silicone fluid 70~80%, carbon black 5~15%, white carbon black 5~15%, hydroxy silicon oil 0.5~2%, dispersing agent 0.1~3% and fire retardant 3~10；Preparation process are as follows: by the vinyl-terminated silicone fluid in formula, 5~15% white carbon black and 0.5~2% hydroxy silicon oil are mixed to join in kneader and mediate 30 minutes, and the temperature of kneader is improved and is mediated 1 hour, thick material is obtained；Thick material and remaining vinyl-terminated silicone fluid and dispersing agent, fire retardant are placed in charging basket, mixture is stirred evenly by blender；The revolving speed for reducing blender, carbon black is slowly put into charging basket, and is stirred evenly；Blender is stirred mixture uniform 30~60 minutes；Mixture is ground 3~5 times by three-roller, until compound particles partial size is less than 5um, the present invention not only stablize by simple process, performance, good dispersion, and color marks will not be left in liquid silastic, has a wide range of application.
Description
Technical field
The present invention relates to the technical fields more particularly to a kind of liquid flame-proof silicon rubber black of coating and its preparation process
Slurry and its preparation process.
Background technique
Oil pastes are to be widely used in paint, plastic processing, field of textiles, and the oil pastes of present commercial type are all
It is to use alkyd resin or synthctic fat acid resin for raw material, wetting dispersing agent is added and is formed with improving the dispersibility of toner
Product has many advantages, such as that tinting strength, tinting power is good, covering power is good.
But the drawbacks such as generally existing permeability and the transparency and dilution stability difference, it is with black oil pastes
Example, in preparation, usual organic pigment and carbon black substance oil factor are high, and prepared product content is not high in existing conventional method,
Especially black oil pastes, usually within 20%, the content more than 25% has made seen prepared product content in the market
Such compound loses free mobility, and colorant is difficult to continue to disperse in higher boiling polymer, poor compatibility, and leads to mill base
Agglomeration, trace in silicon rubber, and preparation process is complicated, it is required at high cost, early seamless colouring can not be done, it is difficult to meet market need
It asks.
Summary of the invention
In order to overcome poor fluidity in the oil pastes being currently used in liquid-state silicon gel, disperse unstable disadvantage with not
Foot, the purpose of the present invention is to provide a kind of simple process, performance is stable, compatibility is good, and dispersibility is strong, will not be in liquid-state silicon rubber
The liquid silica gel black slurry and its preparation process for leaving color marks in glue, and having a wide range of application.
To achieve the above object, the present invention is achieved by the following technical programs:
A kind of liquid flame-proof silicon rubber black slurry, the following composition including accounting for mass percent: vinyl-terminated silicone fluid 70
~80%, carbon black 5~15%, white carbon black 5~15%, hydroxy silicon oil 0.5~2%, dispersing agent 0.1~3% and fire retardant 3~
10%.
Further, the dispersing agent is high-molecular type dispersing agent, specially acrylate polymeric, polyurethane or poly- third
Olefin(e) acid ester.
Further, the fire retardant is silicon-series five-retardant or phosphorus flame retardant or nitrogenated flame retardant or bromide fire retardant.
Further, the white carbon black is the processed 300 mesh Meteorological Act silica of hexa methyl silazane.
A kind of preparation process of liquid flame-proof silicon rubber black slurry, includes the following steps:
S1, by the vinyl-terminated silicone fluid of half in formula, 5~15% white carbon black and 0.5~2% hydroxy silicon oil mixing
It is added in the kneader that temperature is 30 DEG C and mediates 30 minutes, the temperature of kneader is improved to 120 DEG C mediate 1 hour later,
Obtain the thick material of white carbon black；
S2, the thick material of the white carbon black that step S1 is obtained and remaining vinyl-terminated silicone fluid and 0.1~3% dispersing agent, 3
~10% fire retardant is placed in clean charging basket, then by blender with 600~1000 revs/min of revolving speed to being placed in charging basket
In mixture stir ten minutes, until uniformly；
S3, the revolving speed for reducing blender slowly put into 5~15% carbon black to step S2 to 150~200 revs/min
In charging basket afterwards, and stir evenly；
S4, the revolving speed for improving blender again are extremely stirred the mixture after step S3 with 600~1000 revs/min
Even 30~60 minutes；
S5, pass through three-roller again to mixture grinding 3~5 times after step S4, until compound particles partial size is less than 5um
It can.
In conclusion compared with prior art, the present invention has the advantages that following substantive distinguishing features outstanding and significant:
(1) present invention is mainly finely combined to using silicone oil polymer with toner, can be used for LSR liquid silica gel, silicone resin,
And the coloring of functionality A/B glue, be applied to 3C Electronic Protection set, medical instruments, wearing ornaments, kitchen utensils, sports goods,
The fields such as cable accessory, automobile parts, have a wide range of application；
(2) dispersing agent is high-molecular type dispersing agent, specially acrylate polymeric, polyurethane or polyacrylate, by
Anchoring group one in them adsorbs with Resin Wound, and other end is again attached with pigment particles packet.Therefore storage stability is high, point
It is good to dissipate property, and color marks will not be left in fluid silicone rubber；
(3) white carbon black, after using the mill base for enhancing, the tensile strength and tear strength of sizing material, and fire retardant
Addition, can increase its flame retardant property；
(4) manufacture craft of the invention is simple, low manufacture cost, can meet the market demand.
Specific embodiment
Invention is further described With reference to embodiment:
Embodiment one:
A kind of liquid flame-proof silicon rubber black slurry, the following composition including accounting for mass percent: vinyl-terminated silicone fluid
80%, carbon black 5%, white carbon black 5%, hydroxy silicon oil 0.5%, dispersing agent 0.5% and fire retardant 9%.
Wherein, the dispersing agent is high-molecular type dispersing agent, specially acrylate polymeric.
Wherein, the fire retardant is silicon-series five-retardant.
Wherein, the white carbon black is the processed 300 mesh Meteorological Act silica of hexa methyl silazane.
A kind of preparation process of liquid flame-proof silicon rubber black slurry, includes the following steps:
S1, in formula 40% vinyl-terminated silicone fluid, 5% white carbon black and 0.5% hydroxy silicon oil are mixed to join
It is mediated in the kneader that temperature is 30 DEG C 30 minutes, the temperature of kneader is improved to 120 DEG C mediate 1 hour later, obtained white
The thick material of carbon black；
S2, the thick material of the white carbon black that step S1 is obtained and remaining 40% vinyl-terminated silicone fluid and 0.5% dispersing agent,
9% fire retardant is placed in clean charging basket, then passes through mixing of the blender with 600 revs/min of revolving speed to being placed in charging basket
Object stirs ten minutes, until uniformly；
S3, the revolving speed for reducing blender slowly put into 5% carbon black to the charging basket after step S2 to 150 revs/min
In, and stir evenly；
S4, the revolving speed for improving blender again are extremely stirred uniform 60 points to the mixture after step S3 with 600 revs/min
Clock；
S5, pass through three-roller again to mixture grinding 5 times after step S4, until compound particles partial size is less than 5um.
Embodiment two:
A kind of liquid flame-proof silicon rubber black slurry, the following composition including accounting for mass percent: vinyl-terminated silicone fluid
76%, carbon black 10%, white carbon black 10%, hydroxy silicon oil 0.5%, dispersing agent 0.5% and fire retardant 3%.
Wherein, the dispersing agent is high-molecular type dispersing agent, specially polyurethane.
Wherein, the fire retardant is phosphorus flame retardant.
Wherein, the white carbon black is the processed 300 mesh Meteorological Act silica of hexa methyl silazane.
A kind of preparation process of liquid flame-proof silicon rubber black slurry, includes the following steps:
S1, the vinyl-terminated silicone fluid (38%) by half in formula, 10% white carbon black and 0.5% hydroxy silicon oil mixing
It is added in the kneader that temperature is 30 DEG C and mediates 30 minutes, the temperature of kneader is improved to 120 DEG C mediate 1 hour later,
Obtain the thick material of white carbon black；
S2, the thick material of the white carbon black that step S1 is obtained and remaining vinyl-terminated silicone fluid (38%) and 0.5% dispersion
Agent, 3% fire retardant be placed in clean charging basket, then it is mixed in charging basket to being placed in 800 revs/min of revolving speed by blender
It closes object to stir ten minutes, until uniformly；
S3, the revolving speed for reducing blender slowly put into 10% carbon black to the charging basket after step S2 to 170 revs/min
In, and stir evenly；
S4, the revolving speed for improving blender again are extremely stirred uniform 40 points to the mixture after step S3 with 800 revs/min
Clock；
S5, pass through three-roller again to mixture grinding 3~5 times after step S4, until compound particles partial size is less than 5um
It can.
Embodiment three:
A kind of liquid flame-proof silicon rubber black slurry, the following composition including accounting for mass percent: vinyl-terminated silicone fluid
71%, carbon black 8%, white carbon black 8%, hydroxy silicon oil 1%, dispersing agent 2% and fire retardant 10%.
Wherein, the dispersing agent is high-molecular type dispersing agent, specially polyacrylate.
Wherein, the fire retardant is nitrogenated flame retardant.
Wherein, the white carbon black is the processed 300 mesh Meteorological Act silica of hexa methyl silazane.
A kind of preparation process of liquid flame-proof silicon rubber black slurry, includes the following steps:
S1, the vinyl-terminated silicone fluid (35.5%) by half in formula, 8% white carbon black and 1% hydroxy silicon oil mixing
It is added in the kneader that temperature is 30 DEG C and mediates 30 minutes, the temperature of kneader is improved to 120 DEG C mediate 1 hour later,
Obtain the thick material of white carbon black；
S2, the thick material of the white carbon black that step S1 is obtained and remaining vinyl-terminated silicone fluid (35.5%) and 2% dispersion
Agent, 10% fire retardant be placed in clean charging basket, then by blender with 900 revs/min of revolving speed to being placed in charging basket
Mixture stirs ten minutes, until uniformly；
S3, the revolving speed for reducing blender slowly put into 8% carbon black to the charging basket after step S2 to 190 revs/min
In, and stir evenly；
S4, the revolving speed for improving blender again are extremely stirred uniform 50 points to the mixture after step S3 with 900 revs/min
Clock；
S5, pass through three-roller again to mixture grinding 4 times after step S4, until compound particles partial size is less than 5um.
Example IV:
A kind of liquid flame-proof silicon rubber black slurry, the following composition including accounting for mass percent: vinyl-terminated silicone fluid
75%, carbon black 7%, white carbon black 7%, hydroxy silicon oil 2%, dispersing agent 3% and fire retardant 6%.
Wherein, the dispersing agent is high-molecular type dispersing agent, specially acrylate polymeric.
Wherein, the fire retardant is bromide fire retardant.
Wherein, the white carbon black is the processed 300 mesh Meteorological Act silica of hexa methyl silazane.
A kind of preparation process of liquid flame-proof silicon rubber black slurry, includes the following steps:
S1, the vinyl-terminated silicone fluid (37.5%) by half in formula, 7% white carbon black and 2% hydroxy silicon oil mixing
It is added in the kneader that temperature is 30 DEG C and mediates 30 minutes, the temperature of kneader is improved to 120 DEG C mediate 1 hour later,
Obtain the thick material of white carbon black；
S2, the thick material of the white carbon black that step S1 is obtained and remaining vinyl-terminated silicone fluid (37.5%) and 3% dispersion
Agent, 6% fire retardant be placed in clean charging basket, then by blender with 1000 revs/min of revolving speed to being placed in charging basket
Mixture stirs ten minutes, until uniformly；
S3, the revolving speed for reducing blender slowly put into 7% carbon black to the charging basket after step S2 to 200 revs/min
In, and stir evenly；
S4, the revolving speed for improving blender again are extremely stirred uniform 60 to the mixture after step S3 with 1000 revs/min
Minute；
S5, pass through three-roller again to mixture grinding 5 times after step S4, until compound particles partial size is less than 5um.
The present invention mainly uses silicone oil polymer to be finely combined to toner, can be used for LSR liquid silica gel, silicone resin, with
And the coloring of functionality A/B glue, it is applied to 3C Electronic Protection set, medical instruments, wearing ornaments, kitchen utensils, sports goods, electricity
The fields such as cable fittings, automobile parts, have a wide range of application.
Dispersing agent is high-molecular type dispersing agent, specially acrylate polymeric, polyurethane or polyacrylate, due to it
Anchoring group one adsorbed with Resin Wound, other end is again attached with pigment particles packet.Therefore storage stability is high, dispersibility
It is good, and color marks will not be left in liquid silastic.
White carbon black, for enhancing using after the mill base, the tensile strength and tear strength of sizing material, and fire retardant adds
Add, its flame retardant property can be increased.
It is special to produce the existing sizing material prepared by fluid silicone rubber black slurry on the market in order to confirm above-mentioned correlated performance
Product and the present embodiment carry out dependence test, and test data is as shown in the table:
| Category of test | The prior art | Embodiment one | Embodiment two | Embodiment three | Example IV |
| Tensile strength (MPa) | 6.82 | 7.53 | 7.55 | 7.54 | 7.55 |
| Tear strength (KN/m) | 35.73 | 38.52 | 38.75 | 38.56 | 38.78 |
| Elongation (%) | 552 | 479 | 482 | 475 | 777 |
| Flame retardant rating | It is flammable | UL94 V-0 | UL94 V-0 | UL94 V-0 | UL94 V-0 |
In conclusion poor fluidity in oil pastes of the invention, disperses unstable disadvantage and deficiency, it is of the invention
It is designed to provide that a kind of simple process, performance is stable, compatibility is good, dispersibility is strong, and color will not be left in fluid silicone rubber
Trace, and have a wide range of application.
For those skilled in the art, it is various corresponding that other can be made according to above technical scheme and design
Change and deformation, and all these change and modification all should belong within the scope of protection of the claims of the present invention.
Claims (5)
1. a kind of liquid flame-proof silicon rubber black slurry, which is characterized in that the following composition including accounting for mass percent: end ethylene
Base silicone oil 70~80%, carbon black 5~15%, white carbon black 5~15%, hydroxy silicon oil 0.5~2%, dispersing agent 0.1~3% and resistance
Fire agent 3~10%.
2. a kind of liquid flame-proof silicon rubber black slurry according to claim 1, which is characterized in that the dispersing agent is height
Molecule-type dispersing agent, specially acrylate polymeric, polyurethane or polyacrylate.
3. a kind of liquid flame-proof silicon rubber black slurry according to claim 1, which is characterized in that the fire retardant is silicon
Flame retardant or phosphorus flame retardant or nitrogenated flame retardant or bromide fire retardant.
4. a kind of liquid flame-proof silicon rubber black slurry according to claim 1, which is characterized in that the white carbon black is six
The processed 300 mesh Meteorological Act silica of methylsilazane.
5. a kind of preparation process of liquid flame-proof silicon rubber black slurry according to any one of claims 1 to 4, special
Sign is, includes the following steps:
S1, by the vinyl-terminated silicone fluid of half in formula, 5~15% white carbon black and 0.5~2% hydroxy silicon oil are mixed and are added
It is mediated in the kneader for being 30 DEG C to temperature 30 minutes, the temperature of kneader is improved to 120 DEG C mediate 1 hour later, obtained
The thick material of white carbon black；
S2, the thick material of the white carbon black that step S1 is obtained and remaining vinyl-terminated silicone fluid and 0.1~3% dispersing agent, 3~
10% fire retardant is placed in clean charging basket, then by blender with 600~1000 revs/min of revolving speed to being placed in charging basket
Mixture stir ten minutes, until uniformly；
S3, the revolving speed for reducing blender slowly put into 5~15% carbon black to step S2 to 150~200 revs/min
In charging basket, and stir evenly；
S4, the revolving speed for improving blender again are extremely stirred uniform 30 to the mixture after step S3 with 600~1000 revs/min
~60 minutes；
S5, pass through three-roller again to mixture grinding 3~5 times after step S4, until compound particles partial size is less than 5um.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910048286.3A CN109810579A (en) | 2019-01-18 | 2019-01-18 | A kind of liquid flame-proof silicon rubber black slurry and its preparation process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910048286.3A CN109810579A (en) | 2019-01-18 | 2019-01-18 | A kind of liquid flame-proof silicon rubber black slurry and its preparation process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109810579A true CN109810579A (en) | 2019-05-28 |
Family
ID=66604580
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910048286.3A Pending CN109810579A (en) | 2019-01-18 | 2019-01-18 | A kind of liquid flame-proof silicon rubber black slurry and its preparation process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109810579A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113861697A (en) * | 2021-10-15 | 2021-12-31 | 东莞天绘新材料有限公司 | Liquid silica gel with excellent dispersibility and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103555070A (en) * | 2013-10-25 | 2014-02-05 | 上海韩基化工科技有限公司 | Method for processing super-concentrated oil-based colour paste |
| CN107254177A (en) * | 2017-07-01 | 2017-10-17 | 东莞市良展有机硅科技有限公司 | A kind of use for synthetic leather flame retardant silica gel and preparation method thereof |
-
2019
- 2019-01-18 CN CN201910048286.3A patent/CN109810579A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103555070A (en) * | 2013-10-25 | 2014-02-05 | 上海韩基化工科技有限公司 | Method for processing super-concentrated oil-based colour paste |
| CN107254177A (en) * | 2017-07-01 | 2017-10-17 | 东莞市良展有机硅科技有限公司 | A kind of use for synthetic leather flame retardant silica gel and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 朱万强: "涂料与颜料标准应用手册 下", vol. 1, 西南交通大学出版社, pages: 1089 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113861697A (en) * | 2021-10-15 | 2021-12-31 | 东莞天绘新材料有限公司 | Liquid silica gel with excellent dispersibility and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102617916A (en) | Composition of color high-concentration mono-color master batch for polyolefin | |
| CN106753132A (en) | A kind of halogen-free flame-resistant high-temperature-resistant tough epoxy adhesive and preparation method thereof | |
| CN101250358A (en) | Flame-proof nitrocellulose lacquer prepared by halogen-free flame retardant and preparation method thereof | |
| CN105153847A (en) | Water-based glass high-temperature baking varnish and preparation method thereof | |
| CN109810579A (en) | A kind of liquid flame-proof silicon rubber black slurry and its preparation process | |
| CN107841234A (en) | A kind of silicon-modified epoxy acrylic acid allochroic paint and preparation method thereof | |
| CN107761393A (en) | A kind of flame-retardant coating fabric and its preparation technology | |
| CN109913080A (en) | A kind of novel solvent-free electrostatic conductive anticorrosion paint | |
| JP2002025338A (en) | Coloring conductive paste and conductive laminate using the same, and manufacturing method of the same | |
| CN101921513B (en) | Polyvinyl chloride (PVC) pigment color paste | |
| CN109111836A (en) | A kind of production method of modified internal and external wall coating | |
| CN112694653B (en) | Environment-friendly high-molecular pre-dispersed pigment and preparation method and application thereof | |
| CN104861827A (en) | Solvent-free epoxy self-leveling floor coating suitable for low-temperature environment | |
| CN109054463A (en) | A kind of preparation method of the polymolecularity pigment for PVC film structural material | |
| CN105348916B (en) | A kind of polymolecularity high thixotropic Neutral writing ink and preparation method thereof | |
| CN107286743A (en) | A kind of boiling water resistance water-based ink printed applied to PVC | |
| CN109897423A (en) | A kind of cavity flooding material and preparation method thereof | |
| KR20110131869A (en) | A method of manufacturing printing ink and ink composition manufactured by the method | |
| CN104861470A (en) | PBT filling color master batch | |
| CN104356690A (en) | Modified calcium carbonate with flame-retardant effect and preparation method thereof | |
| CN115975287B (en) | Enhanced high-weather-resistance color master batch and preparation method thereof | |
| CN103694586A (en) | PVC black master batch | |
| CN108641241A (en) | A kind of modified fluorubber and preparation method thereof | |
| CN110016240B (en) | Cationic black dye composition and preparation method and application thereof | |
| CN109504119B (en) | Black pigment and preparation method and application thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |