CN109793046A - Nitrogen charging low temperature electrostatic spray drying production baby matches the method for milk powder grease microcapsule - Google Patents
Nitrogen charging low temperature electrostatic spray drying production baby matches the method for milk powder grease microcapsule Download PDFInfo
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- CN109793046A CN109793046A CN201910113009.6A CN201910113009A CN109793046A CN 109793046 A CN109793046 A CN 109793046A CN 201910113009 A CN201910113009 A CN 201910113009A CN 109793046 A CN109793046 A CN 109793046A
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- milk powder
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- powder grease
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/115—Fatty acids or derivatives thereof; Fats or oils
- A23L33/12—Fatty acids or derivatives thereof
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/16—Agglomerating or granulating milk powder; Making instant milk powder; Products obtained thereby
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/30—Encapsulation of particles, e.g. foodstuff additives
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- Nutrition Science (AREA)
- Health & Medical Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Manufacturing Of Micro-Capsules (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
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Abstract
The present invention relates to a kind of nitrogen charging low temperature electrostatics to be spray-dried the method that production baby matches milk powder grease microcapsule, include the following steps: ingredient: indicating by weight, weigh 40 ~ 50 parts of lactose, 10 ~ 20 parts of lactalbumin, 0.5 ~ 4 part of skimmed milk power, water preliminarily solubilised is added to be configured to the wall material solution of solid content 20 ~ 30%;Two, wall materials dissolution: by wall material solution in 60 ~ 70 DEG C of heating water bath 15-20min;The preparation of three, core materials: 30 ~ 40 parts of miscella are weighed by weight, and composite emulsifier and emulsion adjuncts is added, in 60 DEG C of 10 ~ 15min of water-bath, is uniformly dissolved oil-soluble mixture;The pre-emulsification of four, wall materials and core material: the babies ' formula milk powder grease mixed liquor that step 3 obtains is slowly added in wall material solution, and 50 ~ 60 DEG C of 15 ~ 20min of stirring mix well it;Five, are high-pressure homogeneous;Six, spray drying.The babies ' formula milk powder grease microcapsule oil content of this method production is high, seals and is kept in dark place one month at can be reserved for 2 years or more, 63 DEG C under room temperature, product physical and chemical index meets national standard.
Description
Technical field
The present invention relates to grease processing technology fields more particularly to a kind of nitrogen charging low temperature electrostatic spray drying production baby to match milk
The method of powder grease microcapsule.
Background technique
Babies ' formula milk powder grease is to select vegetable oil to be deployed according to the characteristics of human milk fat, is formulated breast milk nutrition
All close to the content of fatty acid in breast milk, contained oil fatty acid is mainly palmitinic acid, oil by SFA, MUFA and PUFA in oil
Acid, palmitic acid content are up to 35%, and oleic acid content is up to 30%.
The breast milkization of babies ' formula milk powder is studied at this stage, is also rested on mostly in fatty acid composition and content
Breast milk, ignore the influence that fatty acid structure digests and assimilates baby.The present invention fully takes into account fatty acid composition and knot
Breast milk in terms of structure, using OPO structured lipid as primary raw material, high oleic sunflower oil, Canola Oil, purified soyabean oil
It is auxiliary material with corn oil, carries out breast milk proportion.Simultaneously, it is contemplated that the pairs of breast milk carburetion grease microcapsule of fatty acid group is stablized
The influence of property, n-3 system polyunsaturated fatty acid and arachidonic acid are aoxidized seriously during processing and storage, are carried out to it
Other technologies processing, so in breast milk carburetion grease microcapsule of the present invention and being not added with n-3 system polyunsaturated fatty acid and peanut four
Olefin(e) acid ingredient.
With the development of microcapsules technology, being spray-dried preparation microcapsules technology using nitrogen charging low temperature electrostatic will be increasingly becoming
It is popular.The technology promotes desolventizing or the drying of water by applying electrostatic field, so that liquid emulsion be made to be converted into free-flowing
Powder.By giving electrostatic field at atomization position, the electrostatic charge for being applied to fogged emulsion, which is promoted, forms film by wall material,
And the typical required high heat of induction filming is not needed.It is spray-dried by nitrogen charging low temperature electrostatic, infant formula grease is micro-
It is encapsulated to assign the characteristics such as the better stability of product, water-disintegrable.It is not only able to retain its nutritional ingredient, and can protect
Its flavor is demonstrate,proved not change.Application No. is 201680007808.X " using the flavouring agent encapsulation of electrostatic atomization " to disclose one kind
In the method that OSAN- starch carries out microencapsulation to orange oil as wall material, although embedding rate can up to 92% or more, shelf life compared with
Other methods increase, but the microcapsules of its production are by high temperature spray-drying, and the peroxide value of product is slightly higher, micro-
Capsule structure partial size is larger and there are slight cracks.The physicochemical property of product is unstable.
Summary of the invention
The purpose of the present invention is choose soybean oil, the corn of different proportion referring to Chinese breast milk fatty acids the Nomenclature Composition and Structure of Complexes
Oil, high oleic sunflower oil, tea oil and OPO structured lipid make four kinds of battalion close to Chinese breast milk fatty acids the Nomenclature Composition and Structure of Complexes
Oil is supported, in a kind of method of the dry production babies ' formula milk powder grease microcapsule of nitrogen charging low temperature nitrogen charging electrostatic spray, is overcome existing
The deficiency of technology provides a kind of high oil content, and embedding effect is good, process degree of oxidation is low, and long shelf-life, simple process can
The preparation method of capable babies ' formula milk powder grease microcapsule.
In order to achieve the object of the present invention, the technological means that the present invention uses are as follows:
A kind of nitrogen charging low temperature electrostatic spray drying production baby matches the method for milk powder grease microcapsule, includes the following steps:
One, ingredient: indicating by weight, weighs 40 ~ 50 parts of lactose, 10 ~ 20 parts of lactalbumin, 0.5 ~ 4 part of skimmed milk power, adds water
Preliminarily solubilised is configured to the wall material solution of solid content 20 ~ 30%;
The dissolution of two, wall materials: the wall material solution that step 1 is obtained is in 60 ~ 70 DEG C of heating water bath 15-20min;
The preparation of three, core materials: 30 ~ 40 parts of miscella are weighed by weight, and composite emulsifier and emulsion adjuncts is added, in 60 DEG C
10 ~ 15min of water-bath, is uniformly dissolved oil-soluble mixture, obtains babies ' formula milk powder grease mixed liquor;
The pre-emulsification of four, wall materials and core material: it is molten that the babies ' formula milk powder grease mixed liquor that step 3 obtains is slowly added to wall material
In liquid, 50 ~ 60 DEG C of 15 ~ 20min of stirring mix well it;
Five, are high-pressure homogeneous: by emulsion that step 4 obtains using the high-pressure homogeneous place 25 ~ 35MPa after colloid mill disperses
Reason;
Six, spray drying: entering low temperature electrostatic spray drying tower through peristaltic pump for the emulsion that step 5 obtains, be filled with nitrogen,
Obtain babies ' formula milk powder grease microcapsule.
In the step 3, the composite emulsifier is by monoglyceride, citric acid fat glycerides, casein sodium, pungent
Starch alkenyl succinate sodium composition, indicates by weight, and four kinds of component compound proportions are 1:1:4:4 ~ 1:1:1:1, the compounding
The total addition level of emulsifier is 3 ~ 4 parts by weight.
In the step 3, the emulsion adjuncts are dipotassium hydrogen phosphate, and additive amount is 0.5-3 parts by weight.
In the step 5, first use milling treatment of colloid 2 ~ 3 times, then homogeneous 3 ~ 4 times at 25 ~ 35MPa.
In the step 6, spray drying condition be electrostatic ceiling voltage 15kv, minimum voltage 1kv, inlet air temperature 60 ~
100 DEG C, 40 ~ 60 DEG C of leaving air temp, and supplying nitrogen does protection gas.
Beneficial effects of the present invention:
1. the babies ' formula milk powder grease microcapsule oil content of this method production is high, mass fraction reaches 30 ~ 35%, surface oil
Mass fraction content is down to 0.82% ~ 0.85%, 0.67 ~ 0.87meq/kg of peroxide value, the mass fraction 1.99 ~ 2.29% of moisture,
It seals and is kept in dark place one month at can be reserved for 2 years or more, 63 DEG C under room temperature, product physical and chemical index all meets national standard.
2. preparation process of the invention is simple, environment friendly and pollution-free, microcapsules yield is high, reproducible, and technological operation is simple,
With short production cycle, product cost is low, is suitble to technology large-scale production.
3. the embedding rate of production microcapsules is high (> 96%), partial size is small (200 ~ 300nm) under microstate, and stability is good.
4. the grease embedded in production process of the present invention is not oxidizable, nutrient component damages are few.
Detailed description of the invention
Fig. 1 is babies ' formula milk powder grease microcapsule powder produced by the invention breast milk under heating accelerated oxidation processing
The variation of nutrition oil microcapsule peroxide value.
Fig. 2 is babies ' formula milk powder grease microcapsule powder produced by the invention breast milk under heating accelerated oxidation processing
The variation of nutrition oil microcapsule acid value.
Specific embodiment
Embodiment 1:
A kind of method of nitrogen charging low temperature electrostatic spray drying production babies ' formula milk powder grease microcapsule, comprising the following steps:
One, ingredient: at room temperature, 48.75 grams of lactose is weighed, 13.54 grams of lactalbumin, 2.71 grams of skimmed milk power, is added at the beginning of 195 grams of water
Step dissolution is configured to the wall material solution of solid content 25%;
The dissolution of two, wall materials: at room temperature, the wall material solution that step 1 is obtained is in 65 DEG C of heating water bath 20min;
Three, core materials preparation: weigh 35 grams of compound lard, and composite emulsifier and emulsion adjuncts be added, in 60 DEG C of water-baths 10 ~
15min is uniformly dissolved oil-soluble mixture, obtains babies ' formula milk powder grease mixed liquor;The composite emulsifier is by single sweet
Rouge, citric acid fat glycerides, casein sodium, starch Sodium Octenyl Succinate composition indicate, four kinds of components are multiple by weight
It is 1:1:2:2 with ratio, the total addition level of the composite emulsifier is 3 grams;Dipotassium hydrogen phosphate is as emulsion adjuncts, additive amount
0.5 gram;
The pre-emulsification of four, wall materials and core material: it is molten that the babies ' formula milk powder grease mixed liquor that step 3 obtains is slowly added to wall material
In liquid, 60 DEG C of 15 ~ 20min of stirring mix well it;
Five, are high-pressure homogeneous: the emulsion that step 4 obtains first being used colloid mill circular treatment twice, then at 30MPa at homogeneous
Reason 3 times;
Six, spray drying: entering low temperature electrostatic spray drying tower through peristaltic pump for the emulsion that step 5 obtains, be filled with nitrogen,
Babies ' formula milk powder grease microcapsule is obtained, spray drying condition is electrostatic ceiling voltage 15kv, minimum voltage 1kv, air inlet temperature
70 DEG C of degree, obtains babies ' formula milk powder grease microcapsule powder by 50 DEG C of leaving air temp.
As a result: obtaining the peroxide value 0.68meq/kg of babies ' formula milk powder grease microcapsule powder, 0.28 mg/ of acid value
Kg, moisture content 2.06%, surface oil content 0.82%, embedding rate 96.36%, yield 94.8%.
Embodiment 2:
A kind of method of nitrogen charging low temperature electrostatic spray drying production babies ' formula milk powder grease microcapsule, comprising the following steps:
One, ingredient: at room temperature, 48.75 grams of lactose is weighed, 13.63 grams of lactalbumin, 2.80 grams of skimmed milk power, is added at the beginning of 195 grams of water
Step dissolution is configured to the wall material solution of solid content 25%;
The dissolution of two, wall materials: at room temperature, the wall material solution that step 1 is obtained is in 67 DEG C of heating water bath 20min;
Three, core materials preparation: weigh 35 grams of compound lard, and composite emulsifier and emulsion adjuncts be added, in 60 DEG C of water-baths 10 ~
15min is uniformly dissolved oil-soluble mixture, obtains babies ' formula milk powder grease mixed liquor;The composite emulsifier is by single sweet
Rouge, citric acid fat glycerides, casein sodium, starch Sodium Octenyl Succinate composition indicate, four kinds of components are multiple by weight
It is 1:1:2:2 with ratio, the total addition level of the composite emulsifier is 3 grams;Dipotassium hydrogen phosphate is as emulsion adjuncts, additive amount
It is 1 gram;
The pre-emulsification of four, wall materials and core material: it is molten that the babies ' formula milk powder grease mixed liquor that step 3 obtains is slowly added to wall material
In liquid, 65 DEG C of stirring 17min mix well it;
Five, are high-pressure homogeneous: the emulsion that step 4 obtains first being used colloid mill circular treatment twice, then at 30MPa at homogeneous
Reason 3 times;
Six, spray drying: entering low temperature electrostatic spray drying tower through peristaltic pump for the emulsion that step 5 obtains, be filled with nitrogen,
Babies ' formula milk powder grease microcapsule is obtained, spray drying condition is electrostatic ceiling voltage 15kv, minimum voltage 1kv, air inlet temperature
60 DEG C of degree, obtains babies ' formula milk powder grease microcapsule powder by 40 DEG C of leaving air temp.
As a result: obtaining the peroxide value 0.82meq/kg of babies ' formula milk powder grease microcapsule powder, 0.23 mg/ of acid value
Kg, moisture content 2.05%, surface oil content 0.78%, embedding rate 97.1%, yield 94.8%.
Embodiment 3:
A kind of method of nitrogen charging low temperature electrostatic spray drying production babies ' formula milk powder grease microcapsule, comprising the following steps:
One, ingredient: at room temperature, 43.75 grams of lactose is weighed, 16.04 grams of lactalbumin, 7.21 grams of skimmed milk power, is added at the beginning of 195 grams of water
Step dissolution is configured to the wall material solution of solid content 25%;
The dissolution of two, wall materials: at room temperature, the wall material solution that step 1 is obtained is in 62 DEG C of heating water bath 20min;
The preparation of three, core materials: 35 grams of compound lard are weighed, and composite emulsifier and emulsion adjuncts is added, in 60 DEG C of water-baths
14min is uniformly dissolved oil-soluble mixture, obtains babies ' formula milk powder grease mixed liquor;The composite emulsifier is by single sweet
Rouge, citric acid fat glycerides, casein sodium, starch Sodium Octenyl Succinate composition indicate, four kinds of components are multiple by weight
It is 1:1:3:3 with ratio, the total addition level of the composite emulsifier is 3.2 grams;Dipotassium hydrogen phosphate is as emulsion adjuncts, addition
Amount is 0.8 gram;
The pre-emulsification of four, wall materials and core material: it is molten that the babies ' formula milk powder grease mixed liquor that step 3 obtains is slowly added to wall material
In liquid, 55 DEG C of stirring 18min mix well it;
Five, are high-pressure homogeneous: the emulsion that step 4 obtains first being used colloid mill circular treatment twice, then at 32MPa at homogeneous
Reason 3 times;
Six, spray drying: entering low temperature electrostatic spray drying tower through peristaltic pump for the emulsion that step 5 obtains, be filled with nitrogen,
Babies ' formula milk powder grease microcapsule is obtained, spray drying condition is electrostatic ceiling voltage 15kv, minimum voltage 1kv, air inlet temperature
85 DEG C of degree, obtains babies ' formula milk powder grease microcapsule powder by 45 DEG C of leaving air temp.
As a result: obtaining the peroxide value 0.76meq/kg of babies ' formula milk powder grease microcapsule powder, acid value 0.35mg/
Kg, moisture content 2.34%, surface oil content 0.85%, embedding rate 97.2%, yield 94.9%.
Embodiment 4:
A kind of method of nitrogen charging low temperature electrostatic spray drying production babies ' formula milk powder grease microcapsule, comprising the following steps:
One, ingredient: at room temperature, 47.25 grams of lactose is weighed, 14.34 grams of lactalbumin, 3.41 grams of skimmed milk power, adds 195 grams grams of water
Preliminarily solubilised is configured to the wall material solution of solid content 25%;
The dissolution of two, wall materials: at room temperature, the wall material solution that step 1 is obtained is in 67 DEG C of heating water bath 20min;
The preparation of three, core materials: 35 grams of compound lard are weighed, and composite emulsifier and emulsion adjuncts is added, in 60 DEG C of water-baths
12min is uniformly dissolved oil-soluble mixture, obtains babies ' formula milk powder grease mixed liquor;The composite emulsifier is by single sweet
Rouge, citric acid fat glycerides, casein sodium, starch Sodium Octenyl Succinate composition indicate, four kinds of components are multiple by weight
It is 1:1:4:2 with ratio, the total addition level of the composite emulsifier is 3.7 grams;Dipotassium hydrogen phosphate is as emulsion adjuncts, addition
Amount is 0.7 gram;
The pre-emulsification of four, wall materials and core material: it is molten that the babies ' formula milk powder grease mixed liquor that step 3 obtains is slowly added to wall material
In liquid, 66 DEG C of stirring 18min mix well it;
Five, are high-pressure homogeneous: the emulsion that step 4 obtains first being used colloid mill circular treatment twice, then at 29MPa at homogeneous
Reason 4 times;
Six, spray drying: entering low temperature electrostatic spray drying tower through peristaltic pump for the emulsion that step 5 obtains, be filled with nitrogen,
Babies ' formula milk powder grease microcapsule is obtained, spray drying condition is electrostatic ceiling voltage 15kv, minimum voltage 1kv, air inlet temperature
58 DEG C of degree, obtains babies ' formula milk powder grease microcapsule powder by 77 DEG C of leaving air temp.
As a result: obtaining the peroxide value 0.77meq/kg of babies ' formula milk powder grease microcapsule powder, 0.23 mg/ of acid value
Kg, moisture content 2.34%, surface oil content 0.83%, embedding rate 96.7%, yield 95.2%.
The above description is only an embodiment of the present invention, is not intended to limit the scope of the invention, all to utilize this hair
Equivalents made by bright specification and accompanying drawing content are applied directly or indirectly in relevant technical field, are similarly included in
In scope of patent protection of the invention.
Claims (5)
1. a kind of nitrogen charging low temperature electrostatic spray drying production baby matches the method for milk powder grease microcapsule, which is characterized in that including such as
Lower step:
One, ingredient: indicating by weight, weighs 40 ~ 50 parts of lactose, 10 ~ 20 parts of lactalbumin, 0.5 ~ 4 part of skimmed milk power, adds water
Preliminarily solubilised is configured to the wall material solution of solid content 20 ~ 30%;
The dissolution of two, wall materials: the wall material solution that step 1 is obtained is in 60 ~ 70 DEG C of heating water bath 15-20min;
The preparation of three, core materials: 30 ~ 40 parts of miscella are weighed by weight, and composite emulsifier and emulsion adjuncts is added, in 60 DEG C
10 ~ 15min of water-bath, is uniformly dissolved oil-soluble mixture, obtains babies ' formula milk powder grease mixed liquor;
The pre-emulsification of four, wall materials and core material: it is molten that the babies ' formula milk powder grease mixed liquor that step 3 obtains is slowly added to wall material
In liquid, 50 ~ 60 DEG C of 15 ~ 20min of stirring mix well it;
Five, are high-pressure homogeneous: by emulsion that step 4 obtains using the high-pressure homogeneous place 25 ~ 35MPa after colloid mill disperses
Reason;
Six, spray drying: entering low temperature electrostatic spray drying tower through peristaltic pump for the emulsion that step 5 obtains, be filled with nitrogen,
Obtain babies ' formula milk powder grease microcapsule.
2. nitrogen charging low temperature electrostatic spray drying production baby according to claim 1 matches the method for milk powder grease microcapsule,
Be characterized in that: in the step 3, the composite emulsifier is by monoglyceride, citric acid fat glycerides, casein sodium, pungent
Starch alkenyl succinate sodium composition, indicates by weight, and four kinds of component compound proportions are 1:1:4:4 ~ 1:1:1:1, the compounding
The total addition level of emulsifier is 3 ~ 4 parts by weight.
3. nitrogen charging low temperature electrostatic spray drying production baby according to claim 1 matches the method for milk powder grease microcapsule,
Be characterized in that: in the step 3, the emulsion adjuncts are dipotassium hydrogen phosphate, and additive amount is 0.5-3 parts by weight.
4. nitrogen charging low temperature electrostatic spray drying production baby according to claim 1 matches the method for milk powder grease microcapsule,
It is characterized in that: in the step 5, first using milling treatment of colloid 2 ~ 3 times, then homogeneous 3 ~ 4 times at 25 ~ 35MPa.
5. nitrogen charging low temperature electrostatic spray drying production baby according to claim 1 matches the method for milk powder grease microcapsule,
Be characterized in that: in the step 6, spray drying condition is electrostatic ceiling voltage 15kv, minimum voltage 1kv, inlet air temperature 60
~ 100 DEG C, 40 ~ 60 DEG C of leaving air temp, and supplying nitrogen does protection gas.
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CN201910113009.6A CN109793046A (en) | 2019-02-13 | 2019-02-13 | Nitrogen charging low temperature electrostatic spray drying production baby matches the method for milk powder grease microcapsule |
CN202010053108.2A CN111387291A (en) | 2019-02-13 | 2020-01-17 | Method for producing grease microcapsule by low-temperature electrostatic spray drying |
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CN201910113009.6A CN109793046A (en) | 2019-02-13 | 2019-02-13 | Nitrogen charging low temperature electrostatic spray drying production baby matches the method for milk powder grease microcapsule |
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CN201910113009.6A Pending CN109793046A (en) | 2019-02-13 | 2019-02-13 | Nitrogen charging low temperature electrostatic spray drying production baby matches the method for milk powder grease microcapsule |
CN202010053108.2A Pending CN111387291A (en) | 2019-02-13 | 2020-01-17 | Method for producing grease microcapsule by low-temperature electrostatic spray drying |
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WO2021102231A1 (en) * | 2019-11-21 | 2021-05-27 | Spraying Systems Co. | Electrostatic spray dried milk product and production method thereof |
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CN113558242B (en) * | 2021-07-28 | 2023-08-25 | 安徽乐氏食品有限公司 | High-stability grease particle product and preparation method thereof |
WO2023129587A1 (en) * | 2022-01-03 | 2023-07-06 | Spraying Systems Co. | Electrostatic spray dried oil powders and production method thereof |
WO2023192594A1 (en) * | 2022-03-31 | 2023-10-05 | Sppraying Systems Co. | Electrostatic spray dried active compound powders and production method thereof |
CN115530251B (en) * | 2022-09-20 | 2024-01-30 | 湖北工业大学 | Oil phase semi-solidified grease microcapsule powder and preparation method and application thereof |
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CN1465264A (en) * | 2002-06-19 | 2004-01-07 | 西藏圣岗实业有限公司 | Method for preparing microcapsule powder of instant buttered tea |
CN103160490B (en) * | 2011-12-13 | 2016-02-10 | 北京大北农科技集团股份有限公司 | The preparation method of Lactobacillus johnsonii microcapsule and the application of its microcapsule and additive |
CN102726470B (en) * | 2012-07-13 | 2016-09-07 | 河南正通食品科技有限公司 | The preparation method of one class microcapsule emulsifier |
CN103564065B (en) * | 2013-10-30 | 2014-12-17 | 广州绿萃生物科技有限公司 | Preparation method of purple perilla seed oil microcapsule |
PL3628398T3 (en) * | 2015-01-28 | 2021-12-20 | Fona Technologies, Llc | Method for preparing an encapsulated product and encapsulated product |
CN106974267A (en) * | 2017-04-10 | 2017-07-25 | 南昌大学 | A kind of breast milk nutrition oil microcapsule powder preparation method |
US9861945B1 (en) * | 2017-08-04 | 2018-01-09 | ZoomEssence, Inc. | Ultrahigh efficiency spray drying apparatus and process |
CN108902676A (en) * | 2018-05-31 | 2018-11-30 | 山东渠风食品科技有限公司 | Wheat-based polypeptide and modified starch compounding wheat analogies and preparation method thereof |
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WO2021102231A1 (en) * | 2019-11-21 | 2021-05-27 | Spraying Systems Co. | Electrostatic spray dried milk product and production method thereof |
CN115003162A (en) * | 2019-11-21 | 2022-09-02 | 喷雾系统公司 | Electrostatic spray dried dairy products and methods of making the same |
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