CN109744230A - A kind of fresh cut-flower antistaling agent and preparation method thereof - Google Patents

A kind of fresh cut-flower antistaling agent and preparation method thereof Download PDF

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Publication number
CN109744230A
CN109744230A CN201711102959.6A CN201711102959A CN109744230A CN 109744230 A CN109744230 A CN 109744230A CN 201711102959 A CN201711102959 A CN 201711102959A CN 109744230 A CN109744230 A CN 109744230A
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China
Prior art keywords
fresh
flower
cut
chitosan
preparation
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Pending
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CN201711102959.6A
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Chinese (zh)
Inventor
王萍
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Cixi Heroic Electric Appliance Co Ltd
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Cixi Heroic Electric Appliance Co Ltd
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Priority to CN201711102959.6A priority Critical patent/CN109744230A/en
Publication of CN109744230A publication Critical patent/CN109744230A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a kind of fresh cut-flower antistaling agents, by fresh orange peel, sucrose, zinc acetate, abscisic acid, chitosan, composite biological enzyme preparation, Glyceryl Monolaurate, Capmul MCM C8, propylene glycol, soil temperature 20, the raw materials such as food grade glacial acetic acid are made, Fresh Cutting flower fresh-keeping liquid of the present invention avoids the addition of harmful chemical component, after fresh-cut flower surface sprays film, the film of porous network structure is formed in petal surface, prevent the exchange of outside moisture, slow down moisture loss, delay to wilt caused by spray dehydration, macronutrient is rich in when using as nutrient solution, the presence of fungistatic effect also ensures the safety of cut-flower notch, bacterium infection is avoided to cause colored quality decline.

Description

A kind of fresh cut-flower antistaling agent and preparation method thereof
Technical field
The present invention relates to Research Progress of Keeping Fresh Technology of Cut Flowers fields more particularly to a kind of fresh cut-flower antistaling agent and preparation method thereof.
Background technique
With society and economic fast development, the continuous improvement of people's living standard and the gradually improvement of environment, flower Grass demand constantly increases.China's flowers cultural and historical is long, and inside information is abundant, and the flowers of the people appreciate level also not It is disconnected to improve, this to expand flowers consumption be it is highly beneficial, wherein Fresh Cutting flower is the important flowers consumption mode of one kind again.
The fresh and alive degree of cut-flower is an important symbol of cut-flower quality.Cut-flower is adopted cut after be still lived organic Body carries out the metabolic process and physiological change of a series of complex, after cut-flower leaves plant parent, mainly by following several factors Influence: (1) lack of moisture;(2) organic nutrient, vitamin and mineral element supply are insufficient;(3) the mechanical damage of cutting trimming Wound;(4) harmful microorganism infects;(5) change of the external environments such as in vitro rear temperature, humidity, illumination, ventilation;(6) endogenous hormones It is out of control etc..These reasons result in cut-flower ratio, and to stay on maternal plant aging rotten faster.
It is generally used currently, Fresh Cutting flower in the market is fresh-keeping by nutriment, fungicide, ethylene antagonist, anti-oxidant The bottle of the compoundings such as agent and plant growth regulator inserts antistaling agent, and supplement fresh flower as far as possible is detached from the nutrition after parent, prevents Fresh Cutting flower Go bad eclipsed, but these fresh-keeping liquid ingredients all have configuration complex process, not easy to maintain, higher cost and toxic, different journeys Undesirable influence is caused on human body and environment on degree.Application No. is 200810049973.9 patent of invention disclose it is a kind of male Red, herbaceous peony cut flower antistaling agent and its application method, which describe one kind by sucrose, 8-hydroxyquinoline, citric acid, salicylic acid, two The antistaling agent for cut-flower that chlorine monoxid, silver thiosulfate and water are constituted.After cut-flower is inserted into this antistaling agent 20-30 minutes, its bottle can be made Service life extension 50-150% or more is inserted, but its chlorine dioxide used has strong corrosive, silver thiosulfate has toxicity, is not suitable for In the fresh-keeping use of conventional ornamental value Fresh Cutting flower.
The quality of Fresh Cutting flower is production of flowers and plants person, operator, consumer's questions of common interest, how from Antimicrobial preservative, It is then most important that nutritional supplementation, prevention dehydration etc. synthesis provide a kind of economic, nontoxic, convenient and fast Fresh Cutting flower fresh-keeping liquid.
Summary of the invention
The object of the invention is to remedy the disadvantages of known techniques, provides a kind of fresh cut-flower antistaling agent and its preparation side Method.
The present invention is achieved by the following technical solutions:
A kind of fresh cut-flower antistaling agent, is prepared by the following method:
(1) take fresh orange peel clean after by solid-liquid ratio 1: 8-10g/mL put into volumetric concentration be 50-60% ethyl alcohol it is molten In liquid, it is heated to 80-90 DEG C and with water-bath refluxing extraction 1-1.5 hours, by extract obtained filtering, obtained extracting solution Freeze-dried is that powder is spare;
(2) prepare raw materials of chitosan 14-15, composite biological enzyme preparation 1-2, Glyceryl Monolaurate 4-6, list by weight Glycerol caprylate 12-13, propylene glycol 18-20,20 8-10 of soil temperature, food grade glacial acetic acid 10-12, are first immersed in water for chitosan In, while composite biological enzyme preparation being added thereto, heat mixed liquor to 45-48 DEG C, refining treatment 40-45 minutes, after the completion Filter and take out chitosan, first with 60-65 DEG C hot water injection 2-3 times, it is 4-5 minutes each, then rinsed with 20-25 DEG C of water into Property, by gained chitosan drying after with Glyceryl Monolaurate, Capmul MCM C8, food grade glacial acetic acid, propylene glycol and soil The mixing jointly of temperature 20, and be stirred continuously, the fully dispersed mixing of mixed liquor is slowly added water to during stirring, adjusts pH to 6.0-6.5, It is spare to obtain emulsification chitosan;
(3) sucrose is dissolved in the water of 8-10 times of its quality, then by sucrose solution low-grade fever to 30-35 DEG C, to every liter of sugarcane 2-3g zinc acetate, 10-20mg abscisic acid, 4-5g step 1 gained powder and 10-15g are added in sugar juice and emulsifies chitosan, stirs It mixes uniformly;
(4) step 3 gained mixed liquor is poured into steam sterilization pan, persistently sterilizes 20-30 minutes, takes out nature after the completion It is cooled to room temperature, packs up to Fresh Cutting flower fresh-keeping liquid of the present invention.
The composite biological enzyme preparation be alkaline pectase and cellulase with the proportional arrangement that weight ratio is 1: 2 and At.
Fresh orange peel is first cut into fritter after cleaning or smashs to pieces in the step 1, then is extracted with ethyl alcohol, extracts effect to improve Rate.
Sterilization pressure control is controlled in 0.1-0.12MPa, sterilising temp at 120-130 DEG C in step 4 sterilization process.
The application method of the Fresh Cutting flower fresh-keeping liquid is that Fresh Cutting flower is inserted directly into fresh-keeping liquid or is watered fresh-keeping liquid Fresh-cut flower surface is sprayed at sprayer after 4-5 times of dilution.
The invention has the advantages that
Fresh Cutting flower fresh-keeping liquid of the present invention avoids the addition of harmful chemical component, takes full advantage of orange peel etc. and plants source property activity Ingredient collocation emulsification chitosan forms the film of porous network structure, flower in petal surface after fresh-cut flower surface sprays film Valve surface is capped, prevents the exchange of outside moisture, slows down moisture loss, delays to wilt caused by spray dehydration, together When emulsify chitosan molecule polar groups amino and hydroxyl presence, have very high affinity and persistence to hydrone, Cut-flower surface forms well stable humidity environment.Macronutrient is rich in when using as nutrient solution, fungistatic effect is deposited In the safety for also ensuring cut-flower notch, bacterium infection is avoided to cause colored quality decline.
Specific embodiment
A kind of fresh cut-flower antistaling agent, is prepared by the following method:
(1) it is cut into small pieces after taking fresh orange peel to clean, puts into the ethyl alcohol that volumetric concentration is 50% by solid-liquid ratio 1: 8g/mL In solution, it is heated to 80 DEG C and with water-bath refluxing extraction 1 hour, by extract obtained filtering, obtained extracting solution is through cold Being lyophilized dry is that powder is spare;
(2) it is sweet to prepare raw materials of chitosan 14, composite biological enzyme preparation 1, Glyceryl Monolaurate 4, single octanoic acid by weight Grease 12, propylene glycol 18, soil temperature 20 8, food grade glacial acetic acid 10, the composite biological enzyme preparation are alkaline pectase and fiber Plain enzyme is formed with the proportional arrangement that weight ratio is 1: 2, first chitosan is immersed in water, while compound biological enzyme being added thereto Preparation heats mixed liquor to 45 DEG C, refining treatment 40 minutes, chitosan is filtered and take out after the completion, first with 60 DEG C of hot water injections 2 It is secondary, 4 minutes every time, then rinsed with 20 DEG C of water to neutrality, it will be sweet with Glyceryl Monolaurate, single octanoic acid after the drying of gained chitosan Grease, food grade glacial acetic acid, propylene glycol and soil temperature 20 mix jointly, and are stirred continuously, and mixing is slowly added water to during stirring The fully dispersed mixing of liquid adjusts pH to 6.0, and it is spare to obtain emulsification chitosan;
(3) sucrose is dissolved in the water of 8 times of its quality, then by sucrose solution low-grade fever to 30 DEG C, to every liter of sucrose solution Middle addition 2g zinc acetate, 10mg abscisic acid, 4g step 1 gained powder and 10g emulsify chitosan, stir evenly;
(4) step 3 gained mixed liquor is poured into steam sterilization pan, sterilization pressure is controlled in 0.1MPa, sterilising temp control System persistently sterilizes 20 minutes at 120 DEG C, takes out cooled to room temperature after the completion, packs up to Fresh Cutting flower fresh-keeping liquid of the present invention.
The basic principles, main features and advantages of the present invention have been shown and described above.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and what is described in the above embodiment and the description is only the present invention Principle, various changes and improvements may be made to the invention without departing from the spirit and scope of the present invention, these variation and Improvement is both fallen in the range of claimed invention.The present invention claims protection scope by appended claims and its Equivalent defines.

Claims (5)

1. a kind of fresh cut-flower antistaling agent, it is characterised in that be prepared by the following method:
(1) it is put into the ethanol solution that volumetric concentration is 50-60% after taking fresh orange peel to clean by solid-liquid ratio 1: 8-10g/mL, It is heated to 80-90 DEG C and with water-bath refluxing extraction 1-1.5 hours, by extract obtained filtering, obtained extracting solution is through cold Being lyophilized dry is that powder is spare;
(2) prepare raw materials of chitosan 14-15, composite biological enzyme preparation 1-2, Glyceryl Monolaurate 4-6, single octanoic acid by weight Chitosan, is first immersed in water, together by glyceride 12-13, propylene glycol 18-20, soil temperature 208-10, food grade glacial acetic acid 10-12 When be added composite biological enzyme preparation thereto, heat mixed liquor to 45-48 DEG C, refining treatment 40-45 minutes, filter after the completion simultaneously Take out chitosan, first with 60-65 DEG C hot water injection 2-3 times, it is 4-5 minutes each, then rinsed with 20-25 DEG C of water to neutrality, by institute It obtains common with Glyceryl Monolaurate, Capmul MCM C8, food grade glacial acetic acid, propylene glycol and soil temperature 20 after chitosan is dried Mixing, and be stirred continuously, the fully dispersed mixing of mixed liquor is slowly added water to during stirring, is adjusted pH to 6.0-6.5, is emulsified Chitosan is spare;
(3) sucrose is dissolved in the water of 8-10 times of its quality, then by sucrose solution low-grade fever to 30-35 DEG C, it is molten to every liter of sucrose 2-3g zinc acetate, 10-20mg abscisic acid, 4-5g step 1 gained powder and 10-15g are added in liquid and emulsifies chitosan, stirring is equal It is even;
(4) step 3 gained mixed liquor is poured into steam sterilization pan, persistently sterilizes 20-30 minutes, takes out natural cooling after the completion To room temperature, pack up to Fresh Cutting flower fresh-keeping liquid of the present invention.
2. a kind of preparation method of Fresh Cutting flower fresh-keeping liquid according to claim 1, which is characterized in that the compound bio Enzyme preparation is that alkaline pectase and cellulase are formed with the proportional arrangement that weight ratio is 1: 2.
3. a kind of preparation method of Fresh Cutting flower fresh-keeping liquid according to claim 1, which is characterized in that fresh tangerine in step 1 Skin is first cut into fritter after cleaning or smashs to pieces, then is extracted with ethyl alcohol, to improve extraction efficiency.
4. a kind of preparation method of Fresh Cutting flower fresh-keeping liquid according to claim 1, which is characterized in that step 4 sterilization process In 0.1-0.12MPa, sterilising temp is controlled at 120-130 DEG C for middle sterilization pressure control.
5. the application method of the described in any item Fresh Cutting flower fresh-keeping liquids of claim 1-4, which is characterized in that directly insert Fresh Cutting flower Enter in fresh-keeping liquid or fresh-keeping liquid is watered after 4-5 times of dilution and is sprayed at fresh-cut flower surface with sprayer.
CN201711102959.6A 2017-11-06 2017-11-06 A kind of fresh cut-flower antistaling agent and preparation method thereof Pending CN109744230A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711102959.6A CN109744230A (en) 2017-11-06 2017-11-06 A kind of fresh cut-flower antistaling agent and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711102959.6A CN109744230A (en) 2017-11-06 2017-11-06 A kind of fresh cut-flower antistaling agent and preparation method thereof

Publications (1)

Publication Number Publication Date
CN109744230A true CN109744230A (en) 2019-05-14

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711102959.6A Pending CN109744230A (en) 2017-11-06 2017-11-06 A kind of fresh cut-flower antistaling agent and preparation method thereof

Country Status (1)

Country Link
CN (1) CN109744230A (en)

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