CN109723742A - A kind of non-metallic automotive brake block and preparation method thereof - Google Patents
A kind of non-metallic automotive brake block and preparation method thereof Download PDFInfo
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- CN109723742A CN109723742A CN201910110451.3A CN201910110451A CN109723742A CN 109723742 A CN109723742 A CN 109723742A CN 201910110451 A CN201910110451 A CN 201910110451A CN 109723742 A CN109723742 A CN 109723742A
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- carbon fiber
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Abstract
The present invention provides a kind of non-metallic automotive brake block, weight percentages of components are as follows: epoxy base carbon fiber composite material waste product regenerates particle 15-20WT%;Phenolic aldehyde base carbon fiber composite material waste product regenerates particle 20-45WT%;Glass carbon dust 5-15WT%;Glass fibre 5-15WT%;Silica gray fibers 5-10WT%;Molybdenum disulphide powder 10-20WT%;Alumina fibre 5-15WT%, vermiculite power 5-10WT%.The present invention furthermore provides the preparation method of the non-metallic automotive brake block.A kind of non-metallic automotive brake block provided by the invention regenerates particle using carbon fibre composite waste product, solves waste disposal problems, reduce production cost;By the confounding effect of carbon fiber and mineral fibres, the advantage of prominent fiber respectively, performance complement, the advantages of highlighting various reinforcing materials;Inorganic non-metallic filler is selected, coefficient of friction is enhanced, reduces brake noise, has reached the requirement of braking comfort.
Description
Technical field
The invention belongs to brake system of car technical fields, and in particular to a kind of non-metallic automotive brake block and its preparation side
Method.
Background technique
Brake block directly affects car steering performance as one of link important in entire braking system, braking ability
And concerning life security, especially some heavy-duty freight cars and car are when mountain highway is run at high speed, since brake is frequent
Braking causes brake block heat fading, causes brake efficiency to weaken or fail and particularly serious traffic accident occurs, give people's life wealth
Production brings huge loss.Traditional one, two generation brake blocks are easy to happen hot ceremonial dress for royalty and move back, wear away fast, braking stationarity when forcing dynamic
The outstanding problems such as difference and noise are big, can not adapt to the new demand of the modern means of communication.It studies and is suitble to higher speed, more may be used
By stabilization, good heat resistanceheat resistant Decay Rate, more environmentally-friendly and great replicability high performance brake material, meet the friendship of China's modern times
The demand of logical tool.
The brake block of fibre reinforced is the new hot spot of domestic and international new brake investigation of materials, has heat-resist, weight
Gently, the advantages that coefficient of expansion is small, wear-resistant and good heat resistanceheat resistant Decay Rate.Fibre reinforced brake material is broadly divided into carbon fiber
Dimension enhancing two classifications of carbon/carborundum based material and carbon fiber enhancement resin base composite material.Lot of documents is to domestic and international 9
Kind C/C composite airplane brake disc thermodynamics and friction and wear behavior are tested, the results showed that carbon matrix brake disc is every
It has excellent performance.It was found that bond vitrified and deformation also do not occur for 2000 DEG C of carbon/carbon compound material disc surface temperature, absorb heat function
Can, wearability and antifading is good and wear rate is low.Brake pad material is from carbon fiber skeleton structure, thickening technology, component
Etc. C/SiC brake material studied find that its average friction coefficient reaches 0.23, friction stability reaches 0.43, linear to grind
Loss rate is 9.3 μm/secondary face, and quality wear rate is 2.6mg/ face, and coefficient of friction is to braking number and surface temperature is unwise
Sense, there is no heat fading trend;The rubbing surface of sample worn surface formation continuous-stable.Carbon fiber can reduce compound after being added
The coefficient of friction of material, carbon fiber adding manner is different, also different to the influence of coefficient of friction;Detect the examination of different resins base
The frictional behaviour of sample, the results showed that its frictional behaviour is main related with temperature, and wear rate and coefficient of friction vary with temperature and become
Change, but correspond to different matrix, degree of susceptibility is different.
In terms of application achievements, patent CN104405804A and CN105156526A etc. provide various forms of carbon fibers and increase
Strong brake pad material and preparation method thereof, the carbon fiber introduced in improves the friction and wear behavior of brake block, but brakes
Appoint in piece component and so contain a large amount of metal materials, such as copper powder and metallic fiber material, these components are to improvement brake block
Require no any effect using modern automobile industries such as low noise comforts, instead exactly the origin cause of formation of brake block brake noise because
Element.Therefore, the new demand that high-performance and low-cost brake pad material is China's Modern Traffic transportation development is prepared.
A kind of epoxy base carbon fiber composite material waste product of summary of the invention recycles granulating technique (epoxy and phenolic aldehyde)
It is multiple to solve carbon fiber using the carbon fiber in carbon fibre composite waste product or leftover pieces as main raw material(s) by the present invention
The problem of condensation material waste disposal hardly possible reduces production cost from raw material end;All select high molecular material and inorganic non-metallic
Component, optimization preparation process realize low-consumption high-efficiency preparation, and strict control cost is prepared inexpensive, highly resistance character of heat-fading energy
Nonmetallic brake pad material.
To achieve the above object, the present invention provides a kind of non-metallic automotive brake block, component content by weight percentage
As follows: epoxy base carbon fiber composite material waste product regenerates particle 15-20WT%;The regeneration of phenolic aldehyde base carbon fiber composite material waste product
Grain 30-45WT%;Glass carbon dust 5-15WT%;Glass fibre 5-15WT%;Silica gray fibers 5-10WT%;Molybdenum disulphide powder
10-20WT%;Alumina fibre 5-15WT%, vermiculite power 5-10WT%.
Specifically, the epoxy base carbon fiber composite material waste product regeneration particle and phenolic aldehyde base carbon fiber composite material are useless
Product regenerate particle, are regenerated and are processed by carbon fibre composite waste product, diameter 1-3mm, and carbon fiber content is in 60-75%, tool
There is cementability.The glass fibre length is 0.5-2mm;Alumina fibre and wollastonite fibre length are 1-2mm;Glass carbon dust
For 200-400 mesh;Molybdenum disulphide powder and vermiculite power are 600-800 mesh.
A kind of preparation method of non-metallic automotive brake block of the invention, is realized using following steps:
Step 1 weighs each component in parts by weight, and epoxy base carbon fiber composite material waste product is first regenerated particle and phenol
Aldehyde radical carbon fibre composite waste product regenerates particle and 5-8min is blended;Then 2- is stirred after glass carbon dust being added while stirring
5min;2-3min is stirred after glass fibre is added while stirring again;2-3min is stirred after molybdenum disulfide is added while stirring again;Again
2-3min is stirred after alumina fibre and silica gray fibers is added while stirring;2- is stirred after vermiculite power is added while stirring again
3min。
Blend components in step 1 are added mold, mold are put into hot press and is pressed and molded, then by step 2
Demoulding, rear processing polishing obtain non-metallic automotive brake block.
Above-mentioned mould pressing process are as follows:
1,60-80 DEG C of molding temperature, molding pressure 5-7MPA, dwell time 10-15min;
2, constant temperature, pressure relief 1-2min;
3,80-100 DEG C of molding temperature, molding pressure 10-12MPA, dwell time 30-40min;
4, constant temperature, pressure relief 2-4min;
5,110-130 DEG C of molding temperature, molding pressure 15-18MPA, dwell time 50-60min;
6, constant temperature, pressure relief 4-5min;
7,130-180 DEG C of molding temperature, molding pressure 26-29MPA, dwell time 120-180min;
8, pressure maintaining demoulds after being cooled to room temperature.
As described above, a kind of non-metallic automotive brake block and preparation method thereof of the invention, utilizes carbon fibre composite
Waste product regenerates particle, solves waste disposal problems, reduces production cost;By the confounding effect of carbon fiber and mineral fibres,
The advantage of prominent fiber respectively, performance complement, the advantages of highlighting various reinforcing materials;Select inorganic non-metallic filler, enhancing
Coefficient of friction reduces brake noise, has reached the requirement of braking comfort.
Specific embodiment
The present invention is furture elucidated combined with specific embodiments below, these embodiments are only limitted to illustrate the present invention and mend and be used for
It limits the scope of the invention.
Illustrate embodiments of the present invention below by way of specific specific example, those skilled in the art can be by this specification
Other advantages and efficacy of the present invention can be easily understood for disclosed content.The present invention can also pass through in addition different specific realities
The mode of applying is embodied or practiced, the various details in this specification can also based on different viewpoints and application, without departing from
Various modifications or alterations are carried out under spirit of the invention.
Embodiment 1
A kind of non-metallic automotive brake block and preparation method thereof chooses epoxy base carbon fiber composite material waste product by its component
Regenerate particle 15g;Phenolic aldehyde base carbon fiber composite material waste product regenerates particle 30g;Glass carbon dust 10g;Glass fibre 5g;Wollastonite
Fiber 5g;Molybdenum disulphide powder 15g;Alumina fibre 10g, vermiculite power 10g.
Specifically, the epoxy base carbon fiber composite material waste product regeneration particle and phenolic aldehyde base carbon fiber composite material are useless
Product regenerate particle, are regenerated and are processed by carbon fibre composite waste product, and carbon fiber content has cementability 65%.The glass
Glass fibre length is 0.5-2mm;Alumina fibre and wollastonite fibre length are 1-2mm;Glass carbon dust is 200 mesh;Curing
Molybdenum powder and vermiculite power are 600 mesh.
It is realized using following steps:
Step 1 weighs each component in parts by weight, and epoxy base carbon fiber composite material waste product is first regenerated particle and phenol
Aldehyde radical carbon fibre composite waste product regenerates particle and 5min is blended;Then 2min is stirred after glass carbon dust being added while stirring;Again
2min is stirred after glass fibre is added while stirring;2min is stirred after molybdenum disulfide is added while stirring again;Add while stirring again
2min is stirred after entering alumina fibre and silica gray fibers;2min is stirred after vermiculite power is added while stirring again.
Blend components in step 1 are added mold, mold are put into hot press and is pressed and molded, then by step 2
Demoulding, rear processing polishing obtain non-metallic automotive brake block.
Above-mentioned mould pressing process are as follows:
1,60 DEG C of molding temperature, molding pressure 5MPA, dwell time 10min;
2, constant temperature, pressure relief 1min;
3,90 DEG C of molding temperature, molding pressure 10MPA, dwell time 30min;
4, constant temperature, pressure relief 2-4min;
5,120 DEG C of molding temperature, molding pressure 18MPA, dwell time 60min;
6, constant temperature, pressure relief 4min;
7,1130 DEG C of molding temperature, molding pressure 29MPA, dwell time 120min;
8, pressure maintaining demoulds after being cooled to room temperature.
Embodiment 2
A kind of non-metallic automotive brake block and preparation method thereof, it is as follows by its component content by weight percentage: epoxy group
Carbon fibre composite waste product regenerates particle 20g;Phenolic aldehyde base carbon fiber composite material waste product regenerates particle 30g;Glass carbon dust
10g;Glass fibre 10g;Silica gray fibers 5g;Molybdenum disulphide powder 15g;Alumina fibre 5g, vermiculite power 5g.
Specifically, the epoxy base carbon fiber composite material waste product regeneration particle and phenolic aldehyde base carbon fiber composite material are useless
Product regenerate particle, are regenerated and are processed by carbon fibre composite waste product, and carbon fiber content has cementability 75%.The glass
Glass fibre length is 0.5-2mm;Alumina fibre and wollastonite fibre length are 1-2mm;Glass carbon dust is 400 mesh;Curing
Molybdenum powder and vermiculite power are 800 mesh.
A kind of preparation method of non-metallic automotive brake block of the invention, is realized using following steps:
Step 1 weighs each component in parts by weight, and epoxy base carbon fiber composite material waste product is first regenerated particle and phenol
Aldehyde radical carbon fibre composite waste product regenerates particle and 8min is blended;Then 5min is stirred after glass carbon dust being added while stirring;Again
3min is stirred after glass fibre is added while stirring;3min is stirred after molybdenum disulfide is added while stirring again;Add while stirring again
3min is stirred after entering alumina fibre and silica gray fibers;3min is stirred after vermiculite power is added while stirring again.
Blend components in step 1 are added mold, mold are put into hot press and is pressed and molded, then by step 2
Demoulding, rear processing polishing obtain non-metallic automotive brake block.
Above-mentioned mould pressing process are as follows:
1,80 DEG C of molding temperature, molding pressure 5MPA, dwell time 15min;
2, constant temperature, pressure relief 1min;
3,100 DEG C of molding temperature, molding pressure 12MPA, dwell time 40min;
4, constant temperature, pressure relief 3min;
5,130 DEG C of molding temperature, molding pressure 18MPA, dwell time 50min;
6, constant temperature, pressure relief 4-5min;
7,160 DEG C of molding temperature, molding pressure 29MPA, dwell time 180min;
8, pressure maintaining demoulds after being cooled to room temperature.
Embodiment 3
A kind of non-metallic automotive brake block and preparation method thereof, it is as follows by its component content by weight percentage: epoxy group
Carbon fibre composite waste product regenerates particle 15g;Phenolic aldehyde base carbon fiber composite material waste product regenerates particle 35g;Glass carbon dust 5g;
Glass fibre 5g;Silica gray fibers 10g;Molybdenum disulphide powder 15g;Alumina fibre 10g, vermiculite power 5g.
Specifically, the epoxy base carbon fiber composite material waste product regeneration particle and phenolic aldehyde base carbon fiber composite material are useless
Product regenerate particle, are regenerated and are processed by carbon fibre composite waste product, and carbon fiber content has cementability in 60-75%.It is described
Glass fibre length is 0.5-2mm;Alumina fibre and wollastonite fibre length are 1-2mm;Glass carbon dust is 200 mesh;Two sulphur
Change molybdenum powder and vermiculite power is 800 mesh.
A kind of preparation method of non-metallic automotive brake block of the invention, is realized using following steps:
Step 1 weighs each component in parts by weight, and epoxy base carbon fiber composite material waste product is first regenerated particle and phenol
Aldehyde radical carbon fibre composite waste product regenerates particle and 6min is blended;Then 3min is stirred after glass carbon dust being added while stirring;Again
3min is stirred after glass fibre is added while stirring;3min is stirred after molybdenum disulfide is added while stirring again;Add while stirring again
2min is stirred after entering alumina fibre and silica gray fibers;2min is stirred after vermiculite power is added while stirring again.
Blend components in step 1 are added mold, mold are put into hot press and is pressed and molded, then by step 2
Demoulding, rear processing polishing obtain non-metallic automotive brake block.
Above-mentioned mould pressing process are as follows:
1,60 DEG C of molding temperature, molding pressure 5MPA, dwell time 10min;
2, constant temperature, pressure relief 1min;
3,100 DEG C of molding temperature, molding pressure 10MPA, dwell time 30min;
4, constant temperature, pressure relief 3min;
5,130 DEG C of molding temperature, molding pressure 18MPA, dwell time 50min;
6, constant temperature, pressure relief 5min;
7,180 DEG C of molding temperature, molding pressure 29MPA, dwell time 180min;
8, pressure maintaining demoulds after being cooled to room temperature.
Embodiment 4
A kind of non-metallic automotive brake block and preparation method thereof, it is as follows by its component content by weight percentage: epoxy group
Carbon fibre composite waste product regenerates particle 15g;Phenolic aldehyde base carbon fiber composite material waste product regenerates particle 40g;Glass carbon dust 5g;
Glass fibre 10g;Silica gray fibers 10g;Molybdenum disulphide powder 5g;Alumina fibre 5g, vermiculite power 10g.
Specifically, the epoxy base carbon fiber composite material waste product regeneration particle and phenolic aldehyde base carbon fiber composite material are useless
Product regenerate particle, are regenerated and are processed by carbon fibre composite waste product, and carbon fiber content has cementability in 60-75%.It is described
Glass fibre length is 0.5-2mm;Alumina fibre and wollastonite fibre length are 1-2mm;Glass carbon dust is 400 mesh;Two sulphur
Change molybdenum powder and vermiculite power is 600 mesh.
A kind of preparation method of non-metallic automotive brake block of the invention, is realized using following steps:
Step 1 weighs each component in parts by weight, and epoxy base carbon fiber composite material waste product is first regenerated particle and phenol
Aldehyde radical carbon fibre composite waste product regenerates particle and 6min is blended;Then 3min is stirred after glass carbon dust being added while stirring;Again
3min is stirred after glass fibre is added while stirring;3min is stirred after molybdenum disulfide is added while stirring again;Add while stirring again
2min is stirred after entering alumina fibre and silica gray fibers;2min is stirred after vermiculite power is added while stirring again.
Blend components in step 1 are added mold, mold are put into hot press and is pressed and molded, then by step 2
Demoulding, rear processing polishing obtain non-metallic automotive brake block.
Above-mentioned mould pressing process are as follows:
1,70 DEG C of molding temperature, molding pressure 5MPA, dwell time 12min;
2, constant temperature, pressure relief 1min;
3,110 DEG C of molding temperature, molding pressure 10MPA, dwell time 30min;
4, constant temperature, pressure relief 3min;
5,120 DEG C of molding temperature, molding pressure 17MPA, dwell time 50min;
6, constant temperature, pressure relief 4min;
7,160 DEG C of molding temperature, molding pressure 26MPA, dwell time 160min;
8, pressure maintaining demoulds after being cooled to room temperature.
9, sample obtained by embodiment 1-4 is tested for the property, mainly tests shear strength;Friction and wear behavior, antithesis
Part is No. 45 steel.
Claims (3)
1. a kind of non-metallic automotive brake block, component is by weight percentage are as follows: the regeneration of epoxy base carbon fiber composite material waste product
Particle 15-20WT%;Phenolic aldehyde base carbon fiber composite material waste product regenerates particle 20-45WT%;Glass carbon dust 5-15WT%;Glass
Fiber 5-15WT%;Silica gray fibers 5-10WT%;Molybdenum disulphide powder 10-20WT%;Alumina fibre 5-15WT%, vermiculite power
5-10WT%.
2. a kind of non-metallic automotive brake block according to claim 1, it is characterised in that the epoxy base carbon fibre is compound
Material waste product regenerates particle and phenolic aldehyde base carbon fiber composite material waste product regenerates particle, and for carbon fiber content in 60-75%, diameter is small
In 1-3mm, there is cementability;The glass fibre length is 0.5-2mm;Alumina fibre and wollastonite fibre length are 1-
2mm;Glass carbon dust is 200-400 mesh;Molybdenum disulphide powder and vermiculite power are 600-800 mesh.
3. a kind of preparation method of non-metallic automotive brake block according to claim 1-2, is realized using following steps:
1) epoxy base carbon fiber composite material waste product is first regenerated into particle and phenolic aldehyde base carbon fiber composite material waste product regenerates particle
5-8min is blended;Then 2-5min is stirred after glass carbon dust being added while stirring;It is stirred after glass fibre is added while stirring again
2-3min;2-3min is stirred after molybdenum disulfide is added while stirring again;Alumina fibre is added while stirring again and wollastonite is fine
2-3min is stirred after dimension;2-3min is stirred after vermiculite power is added while stirring again.
2) mould pressing process are as follows:
A. 60-80 DEG C of molding temperature, molding pressure 5-7MPA, dwell time 10-15min;
B. constant temperature, pressure relief 1-2min;
C. 80-100 DEG C of molding temperature, molding pressure 10-12MPA, dwell time 30-40min;
D. constant temperature, pressure relief 2-4min;
E. 110-130 DEG C of molding temperature, molding pressure 15-18MPA, dwell time 50-60min;
F. constant temperature, pressure relief 4-5min;
G. 130-180 DEG C of molding temperature, molding pressure 26-29MPA, dwell time 120-180min;After pressure maintaining is cooled to room temperature
Demoulding.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112178091A (en) * | 2020-09-30 | 2021-01-05 | 兰州城市学院 | Carbon/carbon fiber friction material and preparation method and application thereof |
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CN205202333U (en) * | 2015-11-04 | 2016-05-04 | 宜兴市中碳科技有限公司 | Direct plastic combines epoxy base carbon fiber board |
CN106402217A (en) * | 2016-11-13 | 2017-02-15 | 徐州乐泰机电科技有限公司 | Nanoscale compound wear-resisting brake pad |
CN106907414A (en) * | 2017-02-27 | 2017-06-30 | 李通 | Automotive disc brake non-metallic friction materials and its preparation method and application |
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CN1109830A (en) * | 1994-01-24 | 1995-10-11 | 纽摩爱伯克斯公司 | Hybrid brake assembly |
EP0987461A1 (en) * | 1997-05-09 | 2000-03-22 | DaimlerChrysler AG | Brake unit with a non-metallic ceramic brake disc and a hub made from a different material |
CN1628015A (en) * | 2002-05-20 | 2005-06-15 | 杜邦-东丽株式会社 | Shreds for reinforcement, fiber-reinforced product using shreds, and method of mfg. shreds and product |
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Application publication date: 20190507 |