CN109704564A - A kind of preparation method of high strength slim glass - Google Patents

A kind of preparation method of high strength slim glass Download PDF

Info

Publication number
CN109704564A
CN109704564A CN201910215719.XA CN201910215719A CN109704564A CN 109704564 A CN109704564 A CN 109704564A CN 201910215719 A CN201910215719 A CN 201910215719A CN 109704564 A CN109704564 A CN 109704564A
Authority
CN
China
Prior art keywords
glass
weight
parts
glass metal
metal
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910215719.XA
Other languages
Chinese (zh)
Inventor
刘仁玉
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NANTONG XIANGYANG OPTICAL ELEMENT CO Ltd
Original Assignee
NANTONG XIANGYANG OPTICAL ELEMENT CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NANTONG XIANGYANG OPTICAL ELEMENT CO Ltd filed Critical NANTONG XIANGYANG OPTICAL ELEMENT CO Ltd
Priority to CN201910215719.XA priority Critical patent/CN109704564A/en
Publication of CN109704564A publication Critical patent/CN109704564A/en
Pending legal-status Critical Current

Links

Abstract

The present invention provides a kind of preparation methods of high strength slim glass, and raw material includes following component according to weight percent: silica 60-65 parts by weight, aluminium oxide 10-17 parts by weight, sodium oxide molybdena 11-15 parts by weight, magnesia 3-13 parts by weight, zirconium oxide 0-3 parts by weight;The preparation method of the high strength slim glass, includes the following steps: 1) melting sources: above-mentioned raw materials being added directly into the melting furnaces of 1300 degrees centigrades, forms glass metal;2) glass metal is clarified: temperature being increased to 1400-1500 degrees Celsius, glass metal is formed, visible bubble in bubble and dissolved gas therein is discharged;3) glass metal is homogenized: glass being chronically under high temperature, the striped in glass metal is eliminated, forms the glass metal of homogenizing.The present invention improves the tensile strength of glass by reasonably adjusting glass formula and preparation process, and the strain point of glass, annealing point, softening point, the coefficient of expansion, density mechanical strength, photoelectric information performance is made to meet the requirement of ultra-thin cover-plate glass.

Description

A kind of preparation method of high strength slim glass
Technical field
The present invention relates to a kind of preparation methods of high strength slim glass, belong to optical element field.
Background technique
With the fast development of touch screen display industry, the thickness requirement of touched panel glass surface protection glass is got in market Come thinner, the ultrathin of glass has become one of important trend of glass.Touched panel glass surface protection thickness of glass It is required that being less than 1mm, super-thin electronic glass product has been widely used in smart phone, tablet computer, AG glass, protection glass In equal display terminals.
However ultrathin also brings apparent drawback, that is exactly the reduction of mechanical strength.It reducing weight, reducing While volume, impurity, defect and any negative factor for reducing strength of glass can be all amplified.Such as: it is one slight Crackle or defect are an inappreciable flaw on surface for the glass of general thickness, but relative to ultra-thin glass For, an equal amount of crackle may but go deep into inside glass, and the destruction that can not ignore is caused to its intensity.This directly makes Common plate glass is lagged significantly behind on the mechanical performance indexs such as flexural strength, surface hardness at ultra-thin glass, this gives The practical application of ultra-thin glass brings huge obstruction.
Summary of the invention
The purpose of the present invention is to overcome the deficiencies of the prior art, provides a kind of preparation side of high strength slim glass Method.
The preparation method of high strength slim glass of the invention, raw material include following component according to weight percent: oxidation Silicon 60-65 parts by weight, aluminium oxide 10-17 parts by weight, sodium oxide molybdena 11-15 parts by weight, magnesia 3-13 parts by weight, zirconium oxide 0-3 Parts by weight;
The preparation method of the high strength slim glass, includes the following steps:
1) melting sources: above-mentioned raw materials being added directly into the melting furnaces of 1300 degrees centigrades, forms glass metal;
2) glass metal is clarified: temperature is increased to 1400-1500 degrees Celsius, forms glass metal, be discharged visible bubble in bubble therein and Dissolved gas;
3) glass metal is homogenized: glass being chronically under high temperature, the striped in glass metal is eliminated, forms the glass metal of homogenizing;
4) glass metal is cooling: by the glass metal uniform decrease in temperature after clarification and homogenization, glass molding;
5) tempering processing is carried out to high strength slim glass made of step 4) using ion-exchange, specific processing step is such as Under: after glass is carried out ultrasonic cleaning, scrub, through 200 ~ 300 degrees Celsius of the pre-heat treatments, it is then immersed in 450 degrees Celsius of meltings Ion-exchange treatment is carried out in KNO3.
The present invention improves the tensile strength of glass, makes answering for glass by reasonably adjusting glass formula and preparation process Height, annealing point, softening point, the coefficient of expansion, density mechanical strength, photoelectric information performance meet the requirement of ultra-thin cover-plate glass.
Specific embodiment
Embodiment 1
The preparation method of high strength slim glass of the invention, raw material includes following component according to weight percent: silica 60 Parts by weight, 10 parts by weight of aluminium oxide, 11 parts by weight of sodium oxide molybdena, 3 parts by weight of magnesia;
The preparation method of the high strength slim glass, includes the following steps:
1) melting sources: above-mentioned raw materials being added directly into the melting furnaces of 1300 degrees centigrades, forms glass metal;
2) glass metal is clarified: temperature is increased to 1400-1500 degrees Celsius, forms glass metal, be discharged visible bubble in bubble therein and Dissolved gas;
3) glass metal is homogenized: glass being chronically under high temperature, the striped in glass metal is eliminated, forms the glass metal of homogenizing;
4) glass metal is cooling: by the glass metal uniform decrease in temperature after clarification and homogenization, glass molding;
5) tempering processing is carried out to high strength slim glass made of step 4) using ion-exchange, specific processing step is such as Under: after glass is carried out ultrasonic cleaning, scrub, through 200 ~ 300 degrees Celsius of the pre-heat treatments, it is then immersed in 450 degrees Celsius of meltings Ion-exchange treatment is carried out in KNO3.
Embodiment 2
The preparation method of high strength slim glass of the invention, raw material includes following component according to weight percent: silica 65 Parts by weight, 17 parts by weight of aluminium oxide, 15 parts by weight of sodium oxide molybdena, 13 parts by weight of magnesia, 3 parts by weight of zirconium oxide.
The preparation method is the same as that of Example 1 for embodiment 2.
Embodiment 3
The preparation method of high strength slim glass of the invention, raw material includes following component according to weight percent: silica 62 Parts by weight, 15 parts by weight of aluminium oxide, 13 parts by weight of sodium oxide molybdena, 10 parts by weight of magnesia, 2 parts by weight of zirconium oxide.
The preparation method is the same as that of Example 1 for embodiment 3.

Claims (1)

1. a kind of preparation method of high strength slim glass, which is characterized in that the raw material according to weight percent include with Lower ingredient: silica 60-65 parts by weight, aluminium oxide 10-17 parts by weight, sodium oxide molybdena 11-15 parts by weight, magnesia 3-13 weight Part, zirconium oxide 0-3 parts by weight;
The preparation method of the high strength slim glass, includes the following steps:
1) melting sources: above-mentioned raw materials being added directly into the melting furnaces of 1300 degrees centigrades, forms glass metal;
2) glass metal is clarified: temperature is increased to 1400-1500 degrees Celsius, forms glass metal, be discharged visible bubble in bubble therein and Dissolved gas;
3) glass metal is homogenized: glass being chronically under high temperature, the striped in glass metal is eliminated, forms the glass metal of homogenizing;
4) glass metal is cooling: by the glass metal uniform decrease in temperature after clarification and homogenization, glass molding;
5) tempering processing is carried out to high strength slim glass made of step 4) using ion-exchange, specific processing step is such as Under: after glass is carried out ultrasonic cleaning, scrub, through 200 ~ 300 degrees Celsius of the pre-heat treatments, it is then immersed in 450 degrees Celsius of meltings Ion-exchange treatment is carried out in KNO3.
CN201910215719.XA 2019-03-21 2019-03-21 A kind of preparation method of high strength slim glass Pending CN109704564A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910215719.XA CN109704564A (en) 2019-03-21 2019-03-21 A kind of preparation method of high strength slim glass

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910215719.XA CN109704564A (en) 2019-03-21 2019-03-21 A kind of preparation method of high strength slim glass

Publications (1)

Publication Number Publication Date
CN109704564A true CN109704564A (en) 2019-05-03

Family

ID=66266962

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910215719.XA Pending CN109704564A (en) 2019-03-21 2019-03-21 A kind of preparation method of high strength slim glass

Country Status (1)

Country Link
CN (1) CN109704564A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110204195A (en) * 2019-06-28 2019-09-06 凯茂科技(深圳)有限公司 A kind of ultra-thin glass and preparation method thereof
CN111976485A (en) * 2020-08-17 2020-11-24 宿州竹梦光学科技有限公司 Accuse touch screen AG glass in car

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101508524A (en) * 2009-03-31 2009-08-19 成都光明光电股份有限公司 Glass suitable for chemically tempering and chemical tempered glass
CN102092940A (en) * 2009-12-11 2011-06-15 肖特公开股份有限公司 Aluminum silicate glass for touch screen
CN102167509A (en) * 2010-02-26 2011-08-31 肖特玻璃科技(苏州)有限公司 Chemical toughened glass capable of carrying out subsequent cutting
CN102363567A (en) * 2010-06-18 2012-02-29 旭硝子株式会社 Glass for display device and glass plate
CN102745896A (en) * 2011-04-18 2012-10-24 旭硝子株式会社 Method for producing chemically tempered glass, and glass for chemical tempering
CN102811963A (en) * 2010-03-24 2012-12-05 Hoya株式会社 Display cover glass and display
CN102892722A (en) * 2010-05-19 2013-01-23 旭硝子株式会社 Glass for chemical strengthening and glass plate for display device
CN105924010A (en) * 2016-04-21 2016-09-07 东莞市银泰玻璃有限公司 Ultra-thin crystal glass and preparation method thereof
CN108863051A (en) * 2018-07-13 2018-11-23 河北省沙河玻璃技术研究院 A kind of devitrified glass floating preparation process applied to 5G communication mobile terminal

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101508524A (en) * 2009-03-31 2009-08-19 成都光明光电股份有限公司 Glass suitable for chemically tempering and chemical tempered glass
CN102092940A (en) * 2009-12-11 2011-06-15 肖特公开股份有限公司 Aluminum silicate glass for touch screen
CN102167509A (en) * 2010-02-26 2011-08-31 肖特玻璃科技(苏州)有限公司 Chemical toughened glass capable of carrying out subsequent cutting
CN102811963A (en) * 2010-03-24 2012-12-05 Hoya株式会社 Display cover glass and display
CN102892722A (en) * 2010-05-19 2013-01-23 旭硝子株式会社 Glass for chemical strengthening and glass plate for display device
CN102363567A (en) * 2010-06-18 2012-02-29 旭硝子株式会社 Glass for display device and glass plate
CN102745896A (en) * 2011-04-18 2012-10-24 旭硝子株式会社 Method for producing chemically tempered glass, and glass for chemical tempering
CN105924010A (en) * 2016-04-21 2016-09-07 东莞市银泰玻璃有限公司 Ultra-thin crystal glass and preparation method thereof
CN108863051A (en) * 2018-07-13 2018-11-23 河北省沙河玻璃技术研究院 A kind of devitrified glass floating preparation process applied to 5G communication mobile terminal

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110204195A (en) * 2019-06-28 2019-09-06 凯茂科技(深圳)有限公司 A kind of ultra-thin glass and preparation method thereof
CN111976485A (en) * 2020-08-17 2020-11-24 宿州竹梦光学科技有限公司 Accuse touch screen AG glass in car

Similar Documents

Publication Publication Date Title
TWI679184B (en) Alkali-doped and alkali-free boroaluminosilicate glass
CN105859129B (en) A kind of glass composition and glass and its preparation method and application
JP6027016B2 (en) Alkaline earth aluminoborosilicate crack resistant glass
CN109704564A (en) A kind of preparation method of high strength slim glass
KR20140141601A (en) High CTE Potassium Borosilicate Core Glasses and Glass Articles Comprising the Same
WO2020239048A1 (en) Alkali aluminosilicate glass, product thereof, strengthening method therefor, and application thereof
WO2019225918A1 (en) Curved laminated glass manufacturing method and curved laminated glass manufactured thereby
CN107056046B (en) Toughened sheet glass and preparation method thereof
CN102092940A (en) Aluminum silicate glass for touch screen
TW200909373A (en) Alkali free glass and alkali free glass substrate
JP4898792B2 (en) High-deformation point glass composition for substrates
US9789665B2 (en) Alkali-aluminosilicate glass
KR20200003274A (en) Alkali-free glass and alkali-free glass plate using same
CN105731791B (en) Composition for glass, high-transmittance glass, and preparation method and application thereof
JP2013043783A (en) Method for manufacturing tempered glass plate
CN112441746A (en) Low surface pressure stress strengthened glass ceramic and original glass
JPH09301732A (en) Glass composition for substrate
JPH09301733A (en) Glass composition for substrate
JP4169013B2 (en) Substrate glass composition
JP2020510948A (en) Glass to protect capacitive touch systems
TW201704161A (en) Strengthened glass plate producing method, glass plate for strengthening, and strengthened glass plate
JP2005255521A (en) Glass composition for substrate
JP7339605B2 (en) aluminosilicate glass
CN107337346A (en) A kind of low fragility, the glass of high index of refraction, composition and preparation method thereof and its application
KR102133339B1 (en) Non-alkali glass

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20190503