CN109692597A - A kind of polymer mother liquor is ripening device used and method - Google Patents
A kind of polymer mother liquor is ripening device used and method Download PDFInfo
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- CN109692597A CN109692597A CN201710999412.4A CN201710999412A CN109692597A CN 109692597 A CN109692597 A CN 109692597A CN 201710999412 A CN201710999412 A CN 201710999412A CN 109692597 A CN109692597 A CN 109692597A
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- Prior art keywords
- containing liquid
- liquid chamber
- mother liquor
- polymer mother
- curing
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F21/00—Dissolving
- B01F21/10—Dissolving using driven stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/05—Stirrers
- B01F27/11—Stirrers characterised by the configuration of the stirrers
- B01F27/112—Stirrers characterised by the configuration of the stirrers with arms, paddles, vanes or blades
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/05—Stirrers
- B01F27/11—Stirrers characterised by the configuration of the stirrers
- B01F27/19—Stirrers with two or more mixing elements mounted in sequence on the same axis
- B01F27/191—Stirrers with two or more mixing elements mounted in sequence on the same axis with similar elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/80—Mixing plants; Combinations of mixers
- B01F33/81—Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/80—Mixing plants; Combinations of mixers
- B01F33/81—Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles
- B01F33/811—Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles in two or more consecutive, i.e. successive, mixing receptacles or being consecutively arranged
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
- B01F2101/2805—Mixing plastics, polymer material ingredients, monomers or oligomers
Abstract
The invention discloses a kind of polymer mother liquor is ripening device used and method, belong to tertiary oil recovery field.The device includes: curing tank, blender, prizing body, and curing tank is placed on prizing body.Curing tank includes multiple containing liquid chambers, is connected between adjacent containing liquid chamber by diversion trench；The import of diversion trench is located at the bottom of preceding containing liquid chamber, and outlet is located at the top of posterior containing liquid chamber；It is provided with inlet on the containing liquid chamber of stem, liquid outlet is provided on the containing liquid chamber of tail portion, a blender is respectively arranged in each containing liquid chamber.The present invention reduces occupied area by the way that curing tank is mounted on prizing body, easy to remove, applied widely, and is connected to multiple containing liquid chambers by diversion trench and improves curing effect.
Description
Technical field
The present invention relates to tertiary oil recovery field, in particular to a kind of polymer mother liquor is ripening device used and method.
Background technique
Technique of polymer flooding is an important technology in tertiary oil recovery, when carrying out the displacement of reservoir oil using technique of polymer flooding, is needed
Polymer solution is injected into oil reservoir.In order to meet the requirement of polymer flooding, need polymer dry powder being dissolved in water
Middle formation polymer mother liquor, cures polymer mother liquor, obtains the polymer solution for meeting requirement, avoids the occurrence of fish
Eye phenomenon, and the mechanical degradation of polymer is reduced simultaneously.Therefore, it is necessary to which it is ripening device used to provide a kind of polymer mother liquor.
It is ripening device used that the prior art provides such a polymer mother liquor: installation volume is biggish ripe on wide ground
Change tank, blender is installed in the tank body of curing tank, after injection of polymer mother liquor thereto, opens blender and stir polymer
The mother liquor predetermined time completes curing.
The inventor finds that the existing technology has at least the following problems:
It is larger to cure tank volume, it is difficult to it is mobile, it takes up a large area, can not make in place finite region or offshore platform
With, and it is poor to cure effect.
Summary of the invention
It provides that a kind of polymer mother liquor is ripening device used and method, can solve the above problem.Specific technical solution is as follows:
In a first aspect, it is ripening device used to provide a kind of polymer mother liquor, comprising: curing tank, blender, described device are also wrapped
Include: prizing body, the curing tank are placed on the prizing body；
The curing tank includes multiple containing liquid chambers, is connected between the adjacent containing liquid chamber by diversion trench；
The import of the diversion trench is located at the bottom of the preceding containing liquid chamber, and outlet is located at the posterior containing liquid chamber
Top；
It is provided with inlet on the containing liquid chamber of stem, is provided with out liquid on the containing liquid chamber of tail portion
Mouthful；
The blender is respectively arranged in each containing liquid chamber.
In a kind of possible design, stirring reinforced structure is provided on the inner wall of the containing liquid chamber.
In a kind of possible design, the stirring reinforced structure by by the inner wall of containing liquid chamber be arranged to it is wavy come
It arrives.
In a kind of possible design, the spacer gap of the two neighboring containing liquid chamber is opposite, to constitute the diversion trench；
For two adjacent containing liquid chambers, the partition lower end of the preceding containing liquid chamber is provided with the diversion trench
The partition upper end of import, the posterior containing liquid chamber is provided with the outlet of the diversion trench.
In a kind of possible design, the lower end of the containing liquid chamber is provided with sewage draining exit.
In a kind of possible design, the paddle of the blender is Double-layer oblique leaf formula.
In a kind of possible design, the bottom of the prizing body is provided with universal wheel.
In a kind of possible design, the inlet is arranged in the top of the containing liquid chamber of stem；
The liquid outlet is arranged in the bottom of the containing liquid chamber of tail portion.
In a kind of possible design, air removing valve is installed on the inlet.
In a kind of possible design, it is provided with liquidometer in the containing liquid chamber of tail portion, is set on the liquid outlet
It is equipped with electrically-controlled valve；
Described device further include: the control system being electrically connected with the liquidometer and the electrically-controlled valve.
In a kind of possible design, the inlet is connect with fluid cylinder, and is set between the inlet and the fluid cylinder
It is equipped with water pump, for continuing fluid injection to the inlet.
Second aspect provides the method for carrying out polymer mother liquor curing using the device of any of the above-described, the method
Include:
Described device is moved to target area using the prizing body；
Open the blender；
By the inlet, into the curing tank, injection of polymer mother liquor, the polymer mother liquor are full of positioned at stem
The containing liquid chamber after successively flow to through the diversion trench in adjacent next containing liquid chamber, flow ultimately to be located at tail portion
The containing liquid chamber in；
In the polymer mother liquor flow process, the polymer mother liquor is cured using the blender；
After the completion of curing, the polymer mother liquor of curing is discharged from the liquid outlet.
In a kind of possible design, the method also includes:
It is located at the inside liquid level of the containing liquid chamber of tail portion using liquidometer detection, and is sent to control system；
The control system makes the instruction for whether opening the liquid outlet according to the inside liquid level, and by described instruction
It is sent to the electrically-controlled valve；
The electrically-controlled valve executes described instruction, to turn on or off the liquid outlet.
Technical solution provided in an embodiment of the present invention has the benefit that
By the way that curing tank is mounted on prizing body, reduces occupied area, be adapted to place finite region and sea is flat
The use of platform, and it is easy to remove, facilitate recycling.Meanwhile stir polymer mother liquor by the containing liquid chamber of multiple connections
Uniformly, curing effect is improved, and by the way that stirring mechanism for intensifying is arranged on containing liquid chamber inner wall, further increases curing effect.
To sum up, polymer mother liquor provided in an embodiment of the present invention is ripening device used, and curing effect can be improved, and occupied area is small is easy to
It is mobile, it is applied widely.
Detailed description of the invention
To describe the technical solutions in the embodiments of the present invention more clearly, make required in being described below to embodiment
Attached drawing is briefly described, it should be apparent that, drawings in the following description are only some embodiments of the invention, for
For those of ordinary skill in the art, without creative efforts, it can also be obtained according to these attached drawings other
Attached drawing.
Fig. 1 is the ripening device used overall schematic of polymer mother liquor provided in an embodiment of the present invention.
Appended drawing reference respectively indicates:
1- curing tank, 101- containing liquid chamber, 102- diversion trench,
2- blender,
3- prizing body,
4- inlet,
5- liquid outlet.
Specific embodiment
Unless otherwise defined, all technical terms used in the embodiment of the present invention all have usual with those skilled in the art
The identical meaning understood.To make the object, technical solutions and advantages of the present invention clearer, below in conjunction with attached drawing to this hair
Bright embodiment is described in further detail.
In a first aspect, the embodiment of the invention provides a kind of polymer mother liquor is ripening device used, as shown in Fig. 1, the device
It include: curing tank 1, blender 2, prizing body 3, curing tank 1 is placed on prizing body 3；
Curing tank 1 includes multiple containing liquid chambers 101, is connected between adjacent containing liquid chamber 101 by diversion trench 102；
The import of diversion trench 102 is located at the bottom of preceding containing liquid chamber 101, and outlet is located at the top of posterior containing liquid chamber 101
Portion；
It is provided with inlet 4 on the containing liquid chamber 101 of stem, is provided with liquid outlet on the containing liquid chamber 101 of tail portion
5；
A blender 2 is respectively arranged in each containing liquid chamber 101.
The working principle ripening device used to polymer mother liquor provided in an embodiment of the present invention is illustrated below:
When being cured using device provided in an embodiment of the present invention to polymer mother liquor, first with prizing body 3 by the dress
It sets and is moved to target area (that is, it needs to the region for carrying out polymer mother liquor curing), then open blender 2, pass through inlet 4
Injection of polymer mother liquor.
The import of diversion trench 102 is located at the bottom of preceding containing liquid chamber 101, and outlet is located at the top of posterior containing liquid chamber 101
Portion, that is, diversion trench 102 is connected to the bottom of preceding containing liquid chamber 101 and posterior containing liquid chamber 101 in two neighboring containing liquid chamber 101
Top.So set, on the one hand making polymer mother liquor that can just enter posterior containing liquid chamber after full of preceding containing liquid chamber 101
101, polymer mother liquor is sufficiently stirred in each containing liquid chamber 101；On the other hand, make polymer mother liquor in each storage
Bottom is all moved from top in liquid storehouse 101, the stroke of polymer mother liquor flowing is increased, further increases mixing effect.
Polymer mother liquor enters eventually into the containing liquid chamber 101 of tail portion, cures the polymer mother liquor of completion from liquid out
Mouth 5 is discharged.
As it can be seen that reduce occupied area by the way that curing tank 1 is mounted on prizing body 3, be adapted to place finite region and
The use of offshore platform, and it is easy to remove, facilitate recycling.Meanwhile polymer is made by the containing liquid chamber of multiple connections 101
Mother liquor stirs evenly, and improves curing effect.To sum up, polymer mother liquor provided in an embodiment of the present invention is ripening device used, Ke Yiti
Height curing effect, and occupied area is small is be easily moved, it is applied widely.
The ripening device used each component of polymer mother liquor provided in an embodiment of the present invention and its effect are given explained respectively below
It states:
Curing tank 1 is made of the connection of multiple containing liquid chambers 101, it is to be understood that 101 quantity of containing liquid chamber is more, polymer
The curing effect of mother liquor is better.
In the embodiment of the present invention, the quantity of containing liquid chamber 101 can be 3-7, for example, can be 3,5,6
Deng, it is defined as above by the quantity to containing liquid chamber 101, can be under the premise of meeting requirement, save the cost.
Containing liquid chamber 101 can be cylinder, and such setting can make polymer mother liquor uniformly divide the pressure of containing liquid chamber 101
Cloth, containing liquid chamber 101 are hardly damaged.
The diameter of containing liquid chamber 101 can be 2-4m, for example, can be above-mentioned straight by selecting for 2m, 3.5m, 4m etc.
The containing liquid chamber 101 of diameter, can not only improve curing efficiency, and can adapt to the use of narrow regions.
The material of containing liquid chamber 101 can be carbon steel, and can extend containing liquid chamber 101 by the way that erosion resistant coating is arranged on inner wall
Service life, the anti-corrosion layer material can be amine cured epoxy resin and Polyamide Epoxy etc..
In the embodiment of the present invention, stirring reinforced structure is provided on the inner wall of containing liquid chamber 101, to improve mixing effect.?
Under the action of blender 2, polymer mother liquor circumferential flowing in containing liquid chamber 101, setting stirring is strengthened on 101 inner wall of containing liquid chamber
Structure, can make polymer mother liquor hit stirring reinforced structure in flow process, generate reaction force to polymer mother liquor, make
The dissolution of polymer more evenly improves mixing effect.
For stirring mechanism for intensifying how is arranged, a kind of example is given below:
As shown in Fig. 1, stirring reinforced structure by by the inner wall of containing liquid chamber 101 be arranged to it is wavy obtain, improve
Mixing effect.
Specifically, wavy inner wall is obtained by the way that the spherical protrusion of equally distributed semicircle is arranged on 101 inner wall of containing liquid chamber
, setting in this way can make the inner wall of containing liquid chamber 101 that can form continuous Wave curved on sectional elevation and horizontal profile,
Under the effect of blender 2 when circumferential flowing, the circulation around vertical axes and the circulation around trunnion axis can be hit polymer mother liquor
Reinforced structure is stirred, mixing effect is improved.
Polymer mother liquor is circulated in curing tank 1 by diversion trench 102, provides a kind of example with regard to its set-up mode below；
As shown in Fig. 1, the spacer gap of two neighboring containing liquid chamber 101 is opposite, to constitute diversion trench 102；
For two adjacent containing liquid chambers 101, the partition lower end of preceding containing liquid chamber 101 be provided with diversion trench 102 into
Mouthful, the partition upper end of posterior containing liquid chamber 101 is provided with the outlet of diversion trench 102.
So set, diversion trench 102 is made to be close to the side wall of two neighboring containing liquid chamber 101, shorten the length of diversion trench 102,
The stroke for flowing polymer mother liquor in diversion trench 102 shortens, and improves curing efficiency.
It is understood that the time that polymer mother liquor flows in diversion trench 102 belongs to the time without curing, contracting
Curing efficiency can be improved in the stroke that short polymer mother liquor flows in diversion trench 102.
In the embodiment of the present invention, the lower end of containing liquid chamber 101 is provided with sewage draining exit, convenient for clearing up containing liquid chamber 101.
Sewage draining exit is in close state when carrying out polymer mother liquor curing, when being cleared up, closes liquid outlet 5,
The injected clear water out of inlet 4, and detergent is added, after standing a period of time, sewage draining exit is opened, since sewage draining exit is located at liquid storage
The lower section in storehouse 101, sewage is flowed out from sewage draining exit under the effect of gravity, reaches cleaning effect.It, can be right in order to improve cleaning effect
Containing liquid chamber 101 is repeatedly rinsed, until can not observe obvious impurity in the sewage of discharge.
Detergent is that this field is common, for example, the village minister profession of Xinghua Heng Yi commerce and trade Co., Ltd sale is with entirely
Energy detergent can be adapted for the embodiment of the present invention.
Blender 2 is that this field is common, and a kind of example is given below:
Blender 2 includes motor, retarder, top braces, agitating shaft and paddle.Top braces fix motor
In the upper end of containing liquid chamber 101, agitating shaft is vertically arranged in 101 inner hub location of containing liquid chamber, and agitating shaft passes through retarder and electricity
Motivation main shaft is connected, and paddle is connected on agitating shaft, after motor start-up, drives agitating shaft rotation, paddle is around agitating shaft
Rotation, plays stirring action.
Further, the paddle of blender 2 is Double-layer oblique leaf formula, can make polymer mother liquor stirring more evenly, improve
Cure effect.
Specifically, Double-layer oblique leaf formula paddle refers to paddle point upper and lower two layers of arrangement on agitating shaft, and each stirs
Leaf is mixed to be in tilted layout.In the embodiment of the present invention, agitating shaft is vertically arranged, the folder between plane and agitating shaft where paddle
Angle can be 30 ° -50 °, for example, can be 30 °, 40 °, 50 ° etc..
Rebuilding can expand the range of paddle influence, and paddle inclination arrangement can be such that polymer mother liquor is stirring
Machine 2 acts on the existing circulation around vertical axes when lower circumferential direction flows to, and has the circulation around trunnion axis, keeps polymer mother liquor stirring equal
It is even, improve curing effect.
In embodiments of the present invention, prizing body 3 can be the chassis suitable for skid mounted equipment, by the way that curing tank 1 to be mounted on
On prizing body 3, it need to only use lifting equipment (for example, crane, crowbar etc.) mobile prizing body 3 that the movement to curing tank 1 can be realized,
Allow to be not easy to mobile curing tank 1 to be moved to target area according to use demand.
Further, the bottom of prizing body 3 is provided with universal wheel, firmly smaller to push prizing body 3 by the way that universal wheel is arranged
Movement, polymer mother liquor provided in an embodiment of the present invention easy to remove is ripening device used.
Universal wheel is that this field is common, for example, Zhejiang EDL Casters Co., Ltd. produces and sells
Medium-sized 5 cun 150Kg mouths brake high-strength polyurethane (TPU) high speed castor of 5045L-86A model can be adapted for the present invention
Embodiment.
Prizing body 3 can be the hardened structure of cuboid, and the length and width of prizing body 3 is determined by the size for the curing tank 1 installed thereon
Fixed, the length and width of prizing body 3 can have more 10-20cm than the size of curing tank 1, for example, can for 10cm, 15cm,
20cm etc. so that curing tank 1 is all mounted on prizing body 3, and facilitates the movement of prizing body 3.The thickness of prizing body 3 can be 10-
20cm, for example, it can be 10cm, 15m, 20cm etc., so set, will not both make prizing body 3 because too thick without easy to remove,
It will not bearing capacity be lower produces fracture or deform due to too thin.
Prizing body 3 can be various material, as long as can guarantee will not be ripened 1 pressure break of tank or deformation when prizing body 3 is mobile.
As an example, prizing body 3 can be carbon steel plate.
In the embodiment of the present invention, polymer mother liquor passes through inlet 4 and the injection of liquid outlet 5 and discharge respectively, such as 1 institute of attached drawing
Show, inlet 4 is arranged in the top of the containing liquid chamber 101 of stem, and liquid outlet 5 is arranged in the containing liquid chamber 101 of tail portion
Bottom.So set, not only can increase the stroke that polymer mother liquor flows in containing liquid chamber 101, but also polymer mother liquor can be made to inject
When do not influenced by the pressure for having polymer mother liquor in containing liquid chamber 101, when discharge, can be discharged more thoroughly under pressure action.
Inlet 4 and liquid outlet 5 can be round hole, be not only convenient for being arranged, and injection and row convenient for polymer mother liquor
Out.
When by 4 injection of polymer mother liquor of inlet, in order to remove the gas in polymer mother liquor, pacify on inlet 4
Fill air removing valve.There are when gas in polymer mother liquor, foam can be generated in whipping process, influences mixing effect, by into
Gas in air removing valve removal polymer mother liquor is installed on liquid mouth 4, can be improved mixing effect.
Air removing valve is that this field is common, and a kind of example is given below:
Air removing valve is the solid cylinder for being mounted on inlet 4 and blocking inlet 4, opens helicla flute inside cylindrical body,
The helicla flute is in communication with the outside at top, bottom closing, has the sieve pore being connected to helicla flute, polymer mother liquor in cylindrical sidewall
It in injection, is flowed downward by helicla flute, is entered in curing tank 1 in flow process by the sieve pore exudation on side wall,
Gas during exudation in removal polymer mother liquor.
Curing tank 1 is discharged from liquid outlet 5 in polymer mother liquor, is provided with liquidometer in the containing liquid chamber 101 of tail portion, described
It is provided with electrically-controlled valve, liquidometer and electrically-controlled valve on liquid outlet 5 and control system is electrically connected.Liquidometer collects the storage for being located at tail portion
The liquid level information of 101 interpolymer mother liquor of liquid storehouse, and it is transmitted to control system, control system receives and processes liquid level information, hair
The instruction whether electrically-controlled valve is opened out controls the automatic open-close of liquid outlet 5, saves manpower.
Based on the automatic open-close of above-mentioned liquid outlet 5, following improvement is made to fluid injection mode:
It connect inlet 4 with fluid cylinder, and is provided with water pump between inlet 4 and fluid cylinder, for persistently being infused to inlet 4
Liquid.Continue fluid injection into inlet 4 by opening water pump, replaces artificial fluid injection, can be realized polymer mother liquor maturing process
Automatic to carry out, staff only needs that polymer mother liquor is periodically added into fluid cylinder, the polymerization after being cured from liquid outlet
Object solution saves manpower.
For ripening device used for a certain polymer mother liquor, curing speed can be obtained by measurement, and scene makes
Used time selects the water pump of appropriate power according to curing speed, fluid injection speed adaption is made to cure speed, can not influence curing effect
Under the premise of fruit, make to cure continual progress.
Second aspect, the embodiment of the invention provides the sides that the device using any of the above-described carries out polymer mother liquor curing
Method, this method comprises:
Device provided in an embodiment of the present invention is moved to target area using prizing body 3, then opens blender 2.
By inlet 4, into curing tank 1, injection of polymer mother liquor, polymer mother liquor are full of the containing liquid chamber positioned at stem
It is successively flow in adjacent next containing liquid chamber 101 after 101 through diversion trench 102, flows ultimately to the containing liquid chamber 101 positioned at tail portion
It is interior.
In polymer mother liquor flow process, polymer mother liquor is cured using blender 2.
After the completion of curing, liquid outlet 5 is opened, the polymer mother liquor of curing is discharged.
When being cured using method provided in an embodiment of the present invention, the embodiment of the present invention is provided first with prizing body 3
Device be moved to target area (that is, it needs to the region for carrying out polymer mother liquor curing), then open blender 2, by into
4 injection of polymer mother liquor of liquid mouth.
The input end of diversion trench 102 is in the bottom of containing liquid chamber 101, and outlet end is at the top of containing liquid chamber 101, that is, diversion trench
The bottom of preceding containing liquid chamber 101 and the top of posterior containing liquid chamber 101 in the 102 two neighboring containing liquid chambers 101 of connection.So set
It sets, on the one hand makes polymer mother liquor that can just enter latter containing liquid chamber 101 after full of previous containing liquid chamber 101, make polymer mother liquor
It is all sufficiently stirred in each containing liquid chamber 101；On the other hand, make polymer mother liquor in each containing liquid chamber 101 from top
Portion is moved to bottom, increases the stroke of polymer mother liquor flowing, further increases mixing effect.
Polymer mother liquor enters eventually into the containing liquid chamber 101 of tail portion, cures the polymer mother liquor of completion from liquid out
Mouth 5 is discharged.
As it can be seen that reduce occupied area by the way that curing tank 1 is mounted on prizing body 3, be adapted to place finite region and
The use of offshore platform, and it is easy to remove, facilitate recycling, meanwhile, polymer is made by the containing liquid chamber 101 of multiple connections
Mother liquor stirs evenly, and improves curing effect.To sum up, polymer mother liquor ageing method provided in an embodiment of the present invention, Ke Yiti
Height curing effect, and occupied area is small is be easily moved, it is applied widely.
Further, this method further include: it is located at the inside liquid level of the containing liquid chamber 101 of tail portion using liquidometer detection, and
It is sent to control system；Control system makes the instruction for whether opening liquid outlet 5 according to inside liquid level, and sends instructions to electricity
Control valve；Electrically-controlled valve executes instruction, and to turn on or off liquid outlet 5, realizes the automatic control of polymer mother liquor discharge process, section
Human-saving.
It is common that liquid level is calculated as this field, for example, the integral type that Beijing Shen Pu finite instrument company produces and sells
Ultrasonic level gage can be adapted for the embodiment of the present invention, which can measure liquid level information, have display screen can be with thereon
It shows liquid level information, and liquid level information can be transported in the form of electric current to middle control platform.
Control system can be computer, PLC etc., receive and process liquid level information according to pre-set programs, and according to processing
As a result instruction is issued, the folding of liquid outlet 5 is controlled by electrically-controlled valve, realizes the automatic control of polymer mother liquor discharge process.
The foregoing is merely presently preferred embodiments of the present invention, the protection scope being not intended to limit the invention, all in this hair
Within bright spirit and principle, any modification, equivalent replacement, improvement and so on should be included in protection scope of the present invention
Within.
Claims (13)
1. a kind of polymer mother liquor is ripening device used, comprising: curing tank (1), blender (2), which is characterized in that described device is also wrapped
Include: prizing body (3), the curing tank (1) are placed on the prizing body (3)；
The curing tank (1) includes multiple containing liquid chambers (101), between the adjacent containing liquid chamber (101) even by diversion trench (102)
It is logical；
The import of the diversion trench (102) is located at the bottom of the preceding containing liquid chamber (101), and outlet is located at the posterior storage
The top in liquid storehouse (101)；
Inlet (4) are provided on the containing liquid chamber (101) of stem, are set on the containing liquid chamber (101) of tail portion
It is equipped with liquid outlet (5)；
The blender (2) is respectively arranged in each containing liquid chamber (101).
2. the apparatus according to claim 1, which is characterized in that it is strong to be provided with stirring on the inner wall of the containing liquid chamber (101)
Change structure.
3. the apparatus of claim 2, which is characterized in that the stirring reinforced structure is by by containing liquid chamber (101)
Inner wall is arranged to wavy obtain.
4. the apparatus according to claim 1, which is characterized in that the spacer gap phase of the two neighboring containing liquid chamber (101)
It is right, to constitute the diversion trench (102)；
For two adjacent containing liquid chambers (101), the partition lower end of the preceding containing liquid chamber (101) is provided with described lead
The partition upper end of the import of chute (102), the posterior containing liquid chamber (101) is provided with the outlet of the diversion trench (102).
5. the apparatus according to claim 1, which is characterized in that the lower end of the containing liquid chamber (101) is provided with sewage draining exit.
6. the apparatus according to claim 1, which is characterized in that the paddle of the blender (2) is Double-layer oblique leaf formula.
7. the apparatus according to claim 1, which is characterized in that the bottom of the prizing body (3) is provided with universal wheel.
8. the apparatus according to claim 1, which is characterized in that the inlet (4) is arranged in the storage of stem
The top in liquid storehouse (101)；
The liquid outlet (5) is arranged in the bottom of the containing liquid chamber (101) of tail portion.
9. device according to claim 8, which is characterized in that be equipped with air removing valve on the inlet (4).
10. device according to claim 8, which is characterized in that be provided with liquid in the containing liquid chamber (101) of tail portion
Position is counted, and is provided with electrically-controlled valve on the liquid outlet (5)；
Described device further include: the control system being electrically connected with the liquidometer and the electrically-controlled valve.
11. device according to claim 8, which is characterized in that the inlet (4) connect with fluid cylinder, and the feed liquor
It is provided with water pump between mouth (4) and the fluid cylinder, for continuing fluid injection to the inlet (4).
12. the method for carrying out polymer mother liquor curing using device described in claim 1-11, which is characterized in that the method
Include:
Described device is moved to target area using the prizing body (3)；
Open the blender (2)；
By the interior injection of polymer mother liquor of the inlet (4) Xiang Suoshu curing tank (1), the polymer mother liquor, which is full of, is located at head
The containing liquid chamber (101) in portion is successively flow in adjacent next containing liquid chamber (101) by the diversion trench (102),
It flows ultimately in the containing liquid chamber (101) of tail portion；
In the polymer mother liquor flow process, the polymer mother liquor is cured using the blender (2)；
After the completion of curing, the polymer mother liquor of curing is discharged from the liquid outlet (5).
13. according to the method for claim 12, which is characterized in that the method also includes:
It is located at the inside liquid level of the containing liquid chamber (101) of tail portion using liquidometer detection, and is sent to control system；
The control system makes the instruction for whether opening the liquid outlet (5) according to the inside liquid level, and by described instruction
It is sent to the electrically-controlled valve；
The electrically-controlled valve executes described instruction, to turn on or off the liquid outlet (5).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
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| CN112516834A (en) * | 2020-11-13 | 2021-03-19 | 湖北宇浩高科新材料有限公司 | Preparation system and preparation process of carbon nanotube slurry with electric and heat conduction functions |
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Application publication date: 20190430 |