CN109691608A - A kind of cassia seed effervescent tablet and preparation method thereof - Google Patents
A kind of cassia seed effervescent tablet and preparation method thereof Download PDFInfo
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- CN109691608A CN109691608A CN201710996131.3A CN201710996131A CN109691608A CN 109691608 A CN109691608 A CN 109691608A CN 201710996131 A CN201710996131 A CN 201710996131A CN 109691608 A CN109691608 A CN 109691608A
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- cassia seed
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- powder
- effervescent tablet
- preparation
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- 235000014489 Cinnamomum aromaticum Nutrition 0.000 title claims abstract description 121
- 244000037364 Cinnamomum aromaticum Species 0.000 title claims abstract description 120
- 239000007938 effervescent tablet Substances 0.000 title claims abstract description 37
- 238000002360 preparation method Methods 0.000 title claims abstract description 29
- 239000000843 powder Substances 0.000 claims abstract description 63
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 58
- 239000000341 volatile oil Substances 0.000 claims abstract description 32
- 239000000314 lubricant Substances 0.000 claims abstract description 28
- 238000000605 extraction Methods 0.000 claims abstract description 26
- 235000003599 food sweetener Nutrition 0.000 claims abstract description 26
- 239000003765 sweetening agent Substances 0.000 claims abstract description 26
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 30
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 30
- 238000000034 method Methods 0.000 claims description 21
- 230000008569 process Effects 0.000 claims description 20
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 18
- 238000002156 mixing Methods 0.000 claims description 13
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical group [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 12
- 239000000243 solution Substances 0.000 claims description 12
- 239000007864 aqueous solution Substances 0.000 claims description 10
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 10
- 229960004756 ethanol Drugs 0.000 claims description 10
- 239000012530 fluid Substances 0.000 claims description 9
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 9
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 9
- 108010011485 Aspartame Proteins 0.000 claims description 8
- 239000002253 acid Substances 0.000 claims description 8
- 239000000605 aspartame Substances 0.000 claims description 8
- 235000010357 aspartame Nutrition 0.000 claims description 8
- IAOZJIPTCAWIRG-QWRGUYRKSA-N aspartame Chemical compound OC(=O)C[C@H](N)C(=O)N[C@H](C(=O)OC)CC1=CC=CC=C1 IAOZJIPTCAWIRG-QWRGUYRKSA-N 0.000 claims description 8
- 229960003438 aspartame Drugs 0.000 claims description 8
- 235000012907 honey Nutrition 0.000 claims description 8
- 239000007788 liquid Substances 0.000 claims description 7
- 238000001914 filtration Methods 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 6
- 239000003826 tablet Substances 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 5
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical group OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 5
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 5
- 239000006286 aqueous extract Substances 0.000 claims description 5
- 238000005138 cryopreservation Methods 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 239000000706 filtrate Substances 0.000 claims description 5
- 238000009472 formulation Methods 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 239000004615 ingredient Substances 0.000 claims description 5
- 229960003511 macrogol Drugs 0.000 claims description 5
- 239000003595 mist Substances 0.000 claims description 5
- 238000004806 packaging method and process Methods 0.000 claims description 5
- 229940057838 polyethylene glycol 4000 Drugs 0.000 claims description 5
- 238000005057 refrigeration Methods 0.000 claims description 5
- 230000001954 sterilising effect Effects 0.000 claims description 5
- 238000004659 sterilization and disinfection Methods 0.000 claims description 5
- 239000006228 supernatant Substances 0.000 claims description 5
- 239000011975 tartaric acid Substances 0.000 claims description 5
- 235000002906 tartaric acid Nutrition 0.000 claims description 5
- TZBAVQKIEKDGFH-UHFFFAOYSA-N n-[2-(diethylamino)ethyl]-1-benzothiophene-2-carboxamide;hydrochloride Chemical compound [Cl-].C1=CC=C2SC(C(=O)NCC[NH+](CC)CC)=CC2=C1 TZBAVQKIEKDGFH-UHFFFAOYSA-N 0.000 claims description 3
- 235000008331 Pinus X rigitaeda Nutrition 0.000 claims description 2
- 235000011613 Pinus brutia Nutrition 0.000 claims description 2
- 241000018646 Pinus brutia Species 0.000 claims description 2
- 241000522254 Cassia Species 0.000 claims 1
- 239000004383 Steviol glycoside Substances 0.000 claims 1
- 238000002386 leaching Methods 0.000 claims 1
- 239000012263 liquid product Substances 0.000 claims 1
- 239000003921 oil Substances 0.000 claims 1
- 235000019411 steviol glycoside Nutrition 0.000 claims 1
- 229930182488 steviol glycoside Natural products 0.000 claims 1
- 150000008144 steviol glycosides Chemical class 0.000 claims 1
- 235000019202 steviosides Nutrition 0.000 claims 1
- 239000004575 stone Substances 0.000 claims 1
- 235000019605 sweet taste sensations Nutrition 0.000 claims 1
- 230000004438 eyesight Effects 0.000 abstract description 5
- 235000020965 cold beverage Nutrition 0.000 abstract description 2
- 230000013872 defecation Effects 0.000 abstract description 2
- 230000036541 health Effects 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 230000001151 other effect Effects 0.000 abstract description 2
- 239000012141 concentrate Substances 0.000 description 4
- 239000000284 extract Substances 0.000 description 3
- 244000201986 Cassia tora Species 0.000 description 2
- 235000014552 Cassia tora Nutrition 0.000 description 2
- 235000009508 confectionery Nutrition 0.000 description 2
- 210000004185 liver Anatomy 0.000 description 2
- 235000013616 tea Nutrition 0.000 description 2
- 206010010774 Constipation Diseases 0.000 description 1
- 208000031226 Hyperlipidaemia Diseases 0.000 description 1
- 206010020772 Hypertension Diseases 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- 239000003651 drinking water Substances 0.000 description 1
- 235000020188 drinking water Nutrition 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 210000000936 intestine Anatomy 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 210000002429 large intestine Anatomy 0.000 description 1
- 230000002475 laxative effect Effects 0.000 description 1
- 235000021374 legumes Nutrition 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 229940093429 polyethylene glycol 6000 Drugs 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000005070 ripening Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/34—Tea substitutes, e.g. matè; Extracts or infusions thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
- A23L2/395—Dry compositions in a particular shape or form
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/40—Effervescence-generating compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention discloses a kind of cassia seed effervescent tablets and preparation method thereof, are related to health drink manufacture field.The cassia seed effervescent tablet, in parts by mass, including powder 15-20 parts of cassia seed extraction, 0.02-0.10 parts of cassia seed volatile oil, sour 15-25 parts of agent, 20-35 parts of alkaline agent, 1-5 parts of lubricant and 4-7 parts of sweetener.Preparation method is simple for cassia seed effervescent tablet of the present invention, and prepare cassia seed effervescent tablet carry and it is easy to use, can be used as cold drink and drink, have relax bowel and defecation, lipid-loweringing improving eyesight and other effects.
Description
Technical field
The present invention relates to health drink manufacture fields, in particular to one kind is using cassia seed extract as made of primary raw material
Cassia seed effervescent tablet and preparation method thereof.
Background technique
Cassia seed is the dry mature seed of legume cassia or little cassia tora, have the function of improving eyesight with it and name it.Autumn
Ripening fruits is harvested, is dried, seed is laid, removes impurity.Cassia seed bitter, sweet, salty, cold nature enters liver, kidney, large intestine channel；Profit
Constipation and hyperlipidemia, hypertension are treated in intestines defaecation, lipid-loweringing improving eyesight.It clears liver and improve vision, sharp water defaecation has laxative action, blood pressure lowering drop
Blood lipid.The drinking way of cassia seed is more limited at present, more inconvenient in use, cannot preferably cater to the majority of consumers'
It uses.
Summary of the invention
In order to solve problems in the prior art, the present invention provides it is a kind of carrying and it is easy to use, can be used as functional guarantor
The cassia seed effervescent tablet and preparation method thereof of strong beverage.
In order to achieve the above object, the technical solution adopted by the present invention is as follows:
A kind of cassia seed effervescent tablet, in parts by mass, including cassia seed extracts powder 15-20 parts, cassia seed volatile oil 0.02-
0.10 part, sour 15-25 parts of agent, 20-35 parts of alkaline agent, 1-5 parts of lubricant and 4-7 parts of sweetener.
Further, in parts by mass, including 18 parts of powder of cassia seed extraction, 0.07 part of cassia seed volatile oil, sour 20 parts of agent,
30 parts of alkaline agent, 3 parts of lubricant and 5 parts of sweetener.
Further, the sour agent is selected from tartaric acid or citric acid；The alkaline agent is selected from sodium carbonate or sodium bicarbonate；It is described
Lubricant is Macrogol 6000 or Macrogol 4000；The sweetener is one of honey element, Aspartame or a variety of.
A kind of preparation method of cassia seed effervescent tablet, includes the following steps:
(1) preparation of cassia seed extraction powder and cassia seed volatile oil
Cassia seed aqueous solution is prepared after carrying out comminution pretreatment to cassia seed first, then in two times to cassia seed aqueous solution
Heating extracting, is collected the oily matter to volatilize in extractive process, obtains cassia seed volatile oil, cryo-conservation is spare, right
Aqueous extracts in extractive process filter while hot, then will twice heat extractive process in filtered fluid merge, concentration, it is to be concentrated extremely
Behind the 1/4 of filtered fluid volume, be added ethanol solution simultaneously be stirred continuously, refrigerated under low temperature, wherein the additional amount of ethanol solution with
The volume ratio of concentrate is 1:1-1:2；Finally supernatant will be taken or filtrate is spray-dried is determined after refrigeration liquid centrifugal filtration
Pine torch extracts powder, closed to save backup；
(2) mixing of ingredient
First in parts by mass, after 15-20 parts of cassia seed extraction powder being mixed with 15-25 parts of sour agent, 4-7 parts of sweet teas are added
Taste agent is uniformly mixed, and obtains powders A；Then 0.02-0.10 parts of cassia seed volatile oil are dissolved with for dehydrated alcohol, is sprayed on mist
It in the powders A, is uniformly mixed, obtains powder B, wherein the volume ratio of cassia seed volatile oil and dehydrated alcohol is 1:4-1:7；Then
After mixing by 20-35 parts of alkaline agents and the powder B, 1-5 parts of lubricants are added, mixes well, obtains powder C；
(3) it dries
Above-mentioned powder C is dried；
(4) tabletting
By the powder C direct tablet compressing after drying, cassia seed effervescent tablet is obtained；
(5) sterilization packaging
Packed after sterilized to above-mentioned cassia seed effervescent tablet to get.
Further, it is respectively 1:20-1 that the step (1) heats the volume ratio of cassia seed and water in extractive process twice:
25 and 1:10-1:15, extraction times are respectively 1.5h and 1h.
Further, refrigerated overnight is spare at 4 DEG C for step (1) the cassia seed volatile oil and cassia seed extraction powder.
Further, acid agent described in the step (2) and alkaline agent are 2-3 hours dry in 100-110 DEG C, crushed 100-
120 meshes, it is closed to save backup；The sweetener crushed 100-120 mesh, and lubricant crushed 160-200 mesh, dry
It is saved backup in device.
Further, need control formulation temperature and humidity respectively in 25 DEG C, 45% or less in preparation process.
Further, the sour agent is selected from tartaric acid or citric acid；The alkaline agent is selected from sodium carbonate or sodium bicarbonate；It is described
Lubricant is Macrogol 6000 or Macrogol 4000；The sweetener is one of honey element and Aspartame or more
Kind.
The utility model has the advantages that compared with prior art, preparation method is simple for cassia seed effervescent tablet of the present invention, and
The cassia seed effervescent tablet of preparation carries and easy to use, and investment in 250-500ml drinking water, suspends or fall into cup at room temperature
Bottom, and a large amount of bubbles are released immediately, tablet dissolves rapidly therewith, and it is molten to form the transparent cassia-tora tea of light green in a short period of time
Liquid can be used as cold drink and drink, and have relax bowel and defecation, lipid-loweringing improving eyesight and other effects.
Detailed description of the invention
Fig. 1 is preparation method flow chart provided in an embodiment of the present invention.
Specific embodiment
The present invention is further elaborated with reference to the accompanying drawings and examples.
Embodiment 1
A kind of cassia seed effervescent tablet, in parts by mass, including cassia seed extraction 15 parts of powder, 0.02 part of cassia seed volatile oil,
15 parts of sour agent, 20 parts of alkaline agent, 1 part of lubricant and 4 parts of sweetener.
Further, the sour agent is selected from tartaric acid or citric acid；The alkaline agent is selected from sodium carbonate or sodium bicarbonate；It is described
Lubricant is Macrogol 6000；The sweetener is honey element.
A kind of preparation method of cassia seed effervescent tablet includes the following steps: with reference to Fig. 1
(1) preparation of cassia seed extraction powder and cassia seed volatile oil
Cassia seed aqueous solution is prepared after carrying out comminution pretreatment to cassia seed first, then in two times to cassia seed aqueous solution
Heating extracting, is collected the oily matter to volatilize in extractive process, obtains cassia seed volatile oil, cryo-conservation is spare, right
Aqueous extracts in extractive process filter while hot, then will twice heat extractive process in filtered fluid merge, concentration, it is to be concentrated extremely
Behind the 1/4 of filtered fluid volume, be added ethanol solution simultaneously be stirred continuously, refrigerated under low temperature, wherein the additional amount of ethanol solution with
The volume ratio of concentrate is 1:1；Finally supernatant will be taken or filtrate is spray-dried obtains cassia seed after refrigeration liquid centrifugal filtration
Powder is extracted, it is closed to save backup；
(2) mixing of ingredient
First in parts by mass, after 15 parts of cassia seed extraction powder being mixed with 15 parts of sour agent, 4 parts of sweetener mixing are added
Uniformly, powders A is obtained；Then 0.02 part of cassia seed volatile oil is dissolved with for dehydrated alcohol, is sprayed in the powders A with mist,
It is uniformly mixed, obtains powder B, wherein the volume ratio of cassia seed volatile oil and dehydrated alcohol is 1:4；Then by 20 parts of alkaline agents with it is described
Powder B after mixing, is added 1 part of lubricant, mixes well, obtain powder C；
(3) it dries
Above-mentioned powder C is dried；
(4) tabletting
By the powder C direct tablet compressing after drying, cassia seed effervescent tablet is obtained；
(5) sterilization packaging
Packed after sterilized to above-mentioned cassia seed effervescent tablet to get.
Further, the step (1) heat twice the volume ratio of cassia seed and water in extractive process be respectively 1:20 and
1:10, extraction times are respectively 1.5h and 1h.
Further, refrigerated overnight is spare at 4 DEG C for step (1) the cassia seed volatile oil and cassia seed extraction powder.
Further, acid agent described in the step (2) and alkaline agent are 3 hours dry in 100 DEG C, and crushing sieves with 100 mesh sieve, close
It closes and saves backup；The sweetener crushing sieves with 100 mesh sieve, and lubricant crushed 160 meshes, save backup in drier.
Further, need control formulation temperature and humidity respectively in 25 DEG C, 45% or less in preparation process.
Further, the sour agent is selected from tartaric acid or citric acid；The alkaline agent is selected from sodium carbonate；The lubricant is poly-
Ethylene glycol 6000；The sweetener is honey element.
Embodiment 2
A kind of cassia seed effervescent tablet, in parts by mass, including cassia seed extraction 18 parts of powder, 0.07 part of cassia seed volatile oil,
20 parts of sour agent, 30 parts of alkaline agent, 3 parts of lubricant and 5 parts of sweetener.
Further, the sour agent is selected from citric acid；The alkaline agent is selected from sodium bicarbonate；The lubricant is polyethylene glycol
4000；The sweetener is honey element and Aspartame.
A kind of preparation method of cassia seed effervescent tablet includes the following steps: with reference to Fig. 1
(1) preparation of cassia seed extraction powder and cassia seed volatile oil
Cassia seed aqueous solution is prepared after carrying out comminution pretreatment to cassia seed first, then in two times to cassia seed aqueous solution
Heating extracting, is collected the oily matter to volatilize in extractive process, obtains cassia seed volatile oil, cryo-conservation is spare, right
Aqueous extracts in extractive process filter while hot, then will twice heat extractive process in filtered fluid merge, concentration, it is to be concentrated extremely
Behind the 1/4 of filtered fluid volume, be added ethanol solution simultaneously be stirred continuously, refrigerated under low temperature, wherein the additional amount of ethanol solution with
The volume ratio of concentrate is 1:2；Finally supernatant will be taken or filtrate is spray-dried obtains cassia seed after refrigeration liquid centrifugal filtration
Powder is extracted, it is closed to save backup；
(2) mixing of ingredient
First in parts by mass, after 18 parts of cassia seed extraction powder being mixed with 20 parts of sour agent, 5 parts of sweetener mixing are added
Uniformly, powders A is obtained；Then 0.07 part of cassia seed volatile oil is dissolved with for dehydrated alcohol, is sprayed in the powders A with mist,
It is uniformly mixed, obtains powder B, wherein the volume ratio of cassia seed volatile oil and dehydrated alcohol is 1:5；Then by 30 parts of alkaline agents with it is described
Powder B after mixing, is added 3 parts of lubricants, mixes well, obtain powder C；
(3) it dries
Above-mentioned powder C is dried；
(4) tabletting
By the powder C direct tablet compressing after drying, cassia seed effervescent tablet is obtained；
(5) sterilization packaging
Packed after sterilized to above-mentioned cassia seed effervescent tablet to get.
Further, the step (1) heat twice the volume ratio of cassia seed and water in extractive process be respectively 1:22 and
1:13, extraction times are respectively 1.5h and 1h.
Further, refrigerated overnight is spare at 4 DEG C for step (1) the cassia seed volatile oil and cassia seed extraction powder.
Further, acid agent described in the step (2) and alkaline agent are 3 hours dry in 100 DEG C, and crushing sieves with 100 mesh sieve, close
It closes and saves backup；The sweetener crushing sieves with 100 mesh sieve, and lubricant crushed 160 meshes, save backup in drier.
Further, need control formulation temperature and humidity respectively in 25 DEG C, 45% or less in preparation process.
Further, the sour agent is selected from citric acid；The alkaline agent is selected from sodium bicarbonate；The lubricant is polyethylene glycol
4000；The sweetener is honey element and Aspartame.
Embodiment 3
A kind of cassia seed effervescent tablet, in parts by mass, including cassia seed extraction 20 parts of powder, 0.10 part of cassia seed volatile oil,
25 parts of sour agent, 35 parts of alkaline agent, 5 parts of lubricant and 7 parts of sweetener.
Further, the sour agent is selected from citric acid；The alkaline agent is selected from sodium bicarbonate；The lubricant is polyethylene glycol
4000；The sweetener is Aspartame.
A kind of preparation method of cassia seed effervescent tablet includes the following steps: with reference to Fig. 1
(1) preparation of cassia seed extraction powder and cassia seed volatile oil
Cassia seed aqueous solution is prepared after carrying out comminution pretreatment to cassia seed first, then in two times to cassia seed aqueous solution
Heating extracting, is collected the oily matter to volatilize in extractive process, obtains cassia seed volatile oil, cryo-conservation is spare, right
Aqueous extracts in extractive process filter while hot, then will twice heat extractive process in filtered fluid merge, concentration, it is to be concentrated extremely
Behind the 1/4 of filtered fluid volume, be added ethanol solution simultaneously be stirred continuously, refrigerated under low temperature, wherein the additional amount of ethanol solution with
The volume ratio of concentrate is 1:2；Finally supernatant will be taken or filtrate is spray-dried obtains cassia seed after refrigeration liquid centrifugal filtration
Powder is extracted, it is closed to save backup；
(2) mixing of ingredient
First in parts by mass, after 20 parts of cassia seed extraction powder being mixed with 25 parts of sour agent, 7 parts of sweetener mixing are added
Uniformly, powders A is obtained；Then 0.10 part of cassia seed volatile oil is dissolved with for dehydrated alcohol, is sprayed in the powders A with mist,
It is uniformly mixed, obtains powder B, wherein the volume ratio of cassia seed volatile oil and dehydrated alcohol is 1:7；Then by 35 parts of alkaline agents with it is described
Powder B after mixing, is added 5 parts of lubricants, mixes well, obtain powder C；
(3) it dries
Above-mentioned powder C is dried；
(4) tabletting
By the powder C direct tablet compressing after drying, cassia seed effervescent tablet is obtained；
(5) sterilization packaging
Packed after sterilized to above-mentioned cassia seed effervescent tablet to get.
Further, the step (1) heat twice the volume ratio of cassia seed and water in extractive process be respectively 1:25 and
1:15, extraction times are respectively 1.5h and 1h.
Further, refrigerated overnight is spare at 4 DEG C for step (1) the cassia seed volatile oil and cassia seed extraction powder.
Further, acid agent described in the step (2) and alkaline agent are 2 hours dry in 110 DEG C, crushed 120 meshes, close
It closes and saves backup；The sweetener crushed 120 meshes, and lubricant crushed 200 meshes, save backup in drier.
Further, need control formulation temperature and humidity respectively in 25 DEG C, 45% or less in preparation process.
Further, the sour agent is selected from citric acid；The alkaline agent is selected from sodium bicarbonate；The lubricant is polyethylene glycol
4000；The sweetener is Aspartame.
The above is only the preferable specific embodiment of the present invention.It should be pointed out that for the common skill of the art
For art personnel, the present invention is not limited only to this, under the premise of not departing from technical solution of the present invention, can also make several improvement
And retouching, these modifications and embellishments should also be considered as the scope of protection of the present invention.
Claims (9)
1. a kind of cassia seed effervescent tablet, it is characterised in that: in parts by mass, including powder 15-20 parts of cassia seed extraction, cassia seed are waved
0.02-0.10 parts of hair oil, sour 15-25 parts of agent, 20-35 parts of alkaline agent, 1-5 parts of lubricant and 4-7 parts of sweetener.
2. a kind of cassia seed effervescent tablet according to claim 1, it is characterised in that: in parts by mass, including cassia seed leaching
Mention 18 parts of powder, 0.07 part of cassia seed volatile oil, sour 20 parts of agent, 30 parts of alkaline agent, 3 parts of lubricant and 5 parts of sweetener.
3. a kind of cassia seed effervescent tablet according to claim 1 or 2, it is characterised in that: it is described acid agent be selected from tartaric acid or
Citric acid；The alkaline agent is selected from sodium carbonate or sodium bicarbonate；The lubricant is Macrogol 6000 or Macrogol 4000；Institute
Stating sweetener is one of honey element, steviol glycoside, Aspartame or a variety of.
4. a kind of preparation method of cassia seed effervescent tablet as described in claim 1, characterized by the following steps:
(1) preparation of cassia seed extraction powder and cassia seed volatile oil
Cassia seed aqueous solution is prepared after carrying out comminution pretreatment to cassia seed first, then cassia seed aqueous solution is heated in two times
Extracting, is collected the oily matter to volatilize in extractive process, obtains cassia seed volatile oil, cryo-conservation is spare, to extracting
Aqueous extracts in the process filter while hot, then merge the filtered fluid heated in extractive process twice, concentration, to be concentrated to filtering
Behind the 1/4 of liquid product, ethanol solution is added and is stirred continuously, is refrigerated under low temperature, wherein the additional amount and concentration of ethanol solution
The volume ratio of liquid is 1:1-1:2；Finally supernatant will be taken or filtrate is spray-dried obtains cassia seed after refrigeration liquid centrifugal filtration
Powder is extracted, it is closed to save backup；
(2) mixing of ingredient
First in parts by mass, after 15-20 parts of cassia seed extraction powder being mixed with 15-25 parts of sour agent, 4-7 parts of sweeteners are added
It is uniformly mixed, obtains powders A；Then 0.02-0.10 parts of cassia seed volatile oil are dissolved with for dehydrated alcohol, is sprayed on mist described
It in powders A, is uniformly mixed, obtains powder B, wherein the volume ratio of cassia seed volatile oil and dehydrated alcohol is 1:4-1:7；Then will
20-35 parts of alkaline agents and the powder B after mixing, are added 1-5 parts of lubricants, mix well, obtain powder C；
(3) it dries
Above-mentioned powder C is dried；
(4) tabletting
By the powder C direct tablet compressing after drying, cassia seed effervescent tablet is obtained；
(5) sterilization packaging
Packed after sterilized to above-mentioned cassia seed effervescent tablet to get.
5. a kind of preparation method of cassia seed effervescent tablet according to claim 4, it is characterised in that: the step (1) two
The volume ratio of cassia seed and water is respectively 1:20-1:25 and 1:10-1:15 in secondary heating extractive process, and extraction times are respectively
1.5h and 1h.
6. a kind of preparation method of cassia seed effervescent tablet according to claim 4, it is characterised in that: the step (1) is certainly
Refrigerated overnight is spare at 4 DEG C for pine torch volatile oil and cassia seed extraction powder.
7. a kind of preparation method of cassia seed effervescent tablet according to claim 4, it is characterised in that: in the step (2)
The acid agent and alkaline agent are 2-3 hours dry in 100-110 DEG C, crushed 100-120 mesh, closed to save backup；The sweet taste
Agent crushed 100-120 mesh, and lubricant crushed 160-200 mesh, save backup in drier.
8. a kind of preparation method of cassia seed effervescent tablet according to claim 4, it is characterised in that: need to control in preparation process
Formulation temperature processed and humidity are respectively in 25 DEG C, 45% or less.
9. a kind of preparation method of cassia seed effervescent tablet according to claim 4, it is characterised in that: the acid agent is selected from wine
Stone acid or citric acid；The alkaline agent is selected from sodium carbonate or sodium bicarbonate；The lubricant is Macrogol 6000 or polyethylene glycol
4000；The sweetener is one of honey element and Aspartame or a variety of.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113712097A (en) * | 2021-09-13 | 2021-11-30 | 江苏医药职业学院 | Method for preparing dark plum tea beverage effervescent tablets |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113712097A (en) * | 2021-09-13 | 2021-11-30 | 江苏医药职业学院 | Method for preparing dark plum tea beverage effervescent tablets |
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