CN109673850A - A kind of Multifunctional powder grease and preparation method thereof - Google Patents
A kind of Multifunctional powder grease and preparation method thereof Download PDFInfo
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- CN109673850A CN109673850A CN201910097598.3A CN201910097598A CN109673850A CN 109673850 A CN109673850 A CN 109673850A CN 201910097598 A CN201910097598 A CN 201910097598A CN 109673850 A CN109673850 A CN 109673850A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/158—Fatty acids; Fats; Products containing oils or fats
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/111—Aromatic compounds
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/142—Amino acids; Derivatives thereof
- A23K20/147—Polymeric derivatives, e.g. peptides or proteins
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/163—Sugars; Polysaccharides
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K40/00—Shaping or working-up of animal feeding-stuffs
- A23K40/10—Shaping or working-up of animal feeding-stuffs by agglomeration; by granulation, e.g. making powders
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Abstract
The invention belongs to field of biotechnology, propose a kind of Multifunctional powder grease, with fish oil, the compound grease and Thymol or carvacrol that vegetable oil mass ratio is 1~8:1 are as core material, using the mass ratio of hydrolyzed wheat protein and dextrin for 1:2~7 mixture as wall material, preparation method includes by hydrolyzed wheat protein, dextrin is mixed with hot water, dissolution, the temperature of hot water is 45~75 DEG C, obtain wall material solution, Thymol or carvacrol are dissolved in ethanol solution, obtain essential oil, emulsifier is added in fish oil and vegetable oil after mixing, core material solution is obtained after mixing, the essential oil that will be obtained, core material solution, it is added in wall material solution, high speed shear, it is spray-dried after homogeneous, obtain a kind of Multifunctional powder grease.The present invention solves the problems, such as that powdered oil in the prior art is unsatisfactory for the nutritional need of animal in practical breeding process.
Description
Technical field
The invention belongs to field of biotechnology, it is related to a kind of Multifunctional powder grease and preparation method thereof.
Background technique
Both polybasic unsaturated fatty acids of Ω -3 and Ω -6 are essential fatty acid, and animal body can not be synthesized voluntarily, be needed
The normal physiological function to maintain body is absorbed from food, grease is the primary energy content in animal feed, to animal
Growth, the quality of meat, eggs and milk and yield have direct relationship.To be directly appended in feed that there are digestibilities low by grease,
The defects of additive amount is limited, easy to oxidize rotten, meanwhile, it cannot achieve and meet animal to the need of Ω -3 and Ω -6 rational proportion
It asks, the presence of these defects limits promotion and application of the grease in animal feed.
Powdered oil is the evengranular powder of formation after being embedded grease with wall material appropriate using microcapsules technology
Shape product can keep the inherent characteristic of grease, can increase its compatibility, mixture, therefore powdered oil will be led in feed
Domain has broad application prospects.
Patent 201810835269.X discloses one kind using omega-fatty acid as core material, using brown sugar and maltodextrin as wall material
Powdered oil；Patent 201810313891.4 discloses a kind of preparation method of powdered oil, and wall material is formed sediment comprising Chinese chestnut resistance
Powder, soybean protein isolate, carragheen and water；The core material slurry includes polyglycerol ester, odium stearate, water and grease, after mixing
Freeze-drying；Patent 201810749306.5 discloses a kind of preparation method of stable state powdered oil.Starch is cut in this method
Stay liquid/vegetable oil mixt as core material, the existence form of oily phase are as follows: amylose/vegetable oil inclusion compound and not included
Vegetable oil greatly improves the stability of product；Patent 201810236059.9 discloses a kind of using coconut oil as the powder of core material
The preparation method of powder oil, the above patent do not consider the nutrition of the animal in practical breeding process in the selection of core material and wall material
Demand.
Summary of the invention
The present invention proposes a kind of Multifunctional powder grease and preparation method thereof, and it is discontented to solve powdered oil in the prior art
In full border breeding process the problem of the nutritional need of animal.
The technical scheme of the present invention is realized as follows:
A kind of core material, including compound grease, the mixing that the compound grease is fish oil, vegetable oil mass ratio is 1~8:1
Object, further includes Thymol or carvacrol, the additive amount of the Thymol or carvacrol be compound oil quality 0.1%~
2%.
As further technical solution, the mixture that the compound grease is fish oil, vegetable oil mass ratio is 3~5:1,
The additive amount of the Thymol or carvacrol is the 1%~2% of compound oil quality.
As further technical solution, the mixture that the compound grease is fish oil, vegetable oil mass ratio is 4:1, institute
The additive amount for stating Thymol or carvacrol is the 1.3% of compound oil quality.
As further technical solution, the vegetable oil is the one or more of coconut oil, palm oil, rice bran oil.
A kind of Multifunctional powder grease further includes wall material including a kind of above-mentioned core material, and the wall material is that wheat hydrolyzes egg
The mass ratio of white and dextrin mixture, the hydrolyzed wheat protein and the dextrin is 1:2~7, the wall material and the core
The mass ratio of material is 1:1~10.
As further technical solution, the mass ratio of the wall material and the core material is 1:1~5.
As further technical solution, the mass ratio of the hydrolyzed wheat protein and the dextrin is 1:3~5, described
The mass ratio of wall material and the core material is 1:2~5.
As further technical solution, the mass ratio of the hydrolyzed wheat protein and the dextrin is 1:4, the wall material
Mass ratio with the core material is 1:3.
It further include emulsifier as further technical solution, the additive amount of the emulsifier is the compound oil lipid
The 1%~10% of amount, the emulsifier are the mixture of monoglyceride and sucrose ester, the quality of the monoglyceride and the sucrose ester
Than for 0.5~2:1.
As further technical solution, the additive amount of the emulsifier is the 5% of the compound oil quality, the cream
Agent is the mixture of monoglyceride and sucrose ester, and the mass ratio of the monoglyceride and the sucrose ester is 1:1.
A kind of preparation method of Multifunctional powder grease, comprising the following steps:
S1, according to the formula of above-mentioned Multifunctional powder grease, it is spare to weigh each component；
The preparation of S2, wall material solution: hydrolyzed wheat protein, dextrin are mixed with hot water, dissolution, and the temperature of hot water is 45~
75 DEG C, obtain wall material solution；
The preparation of S3, essential oil: Thymol or carvacrol are dissolved in ethanol solution, obtain essential oil；
The preparation of S4, core material solution: emulsifier is added in fish oil and vegetable oil after mixing, obtains core after mixing
Material solution；
S5, the obtained core material solution of essential oil that step S3 is obtained, step S4 is added to the wall material solution that step S2 is obtained
In, high speed shear, the mixed solution after obtaining high speed shear；
S6, it will be spray-dried after the mixed solution homogeneous after high speed shear that step S5 is obtained, obtain a kind of multi-functional powder
Powder oil.
The present invention is using principle and has the beneficial effect that
People always search for a kind of core material, can be realized both and meet the needs of animal is to Ω -3 and Ω -6 rational proportion,
But can not solve always, the compound grease for having selected fish oil and vegetable oil of applicant's creativeness, so that the powder oil of preparation
Rouge has both Ω -3 and Ω -6, and matches rationally, meets the needs of animal is to Ω -3 and Ω -6 rational proportion, but in research process
In, it has been found that the powdered oil prepared using the compound grease of fish oil and vegetable oil as core material is in actual use
Easy to oxidize rotten, applicant has found by many experiments, and Thymol or carvacrol are added in core material, can effectively avoid
The oxidation of powdered oil in use, meanwhile, the powdered oil of preparation also has the function of antibacterial anti-inflammatory, is selecting core material
On the basis of, it selects different wall materials also to have different influences to the performance of the powdered oil of preparation, selects wheat in the present invention
Protein hydrolysate and dextrin are as wall material, so that the powdered oil of preparation is further promoted in performance, powdered oil is not oxidizable,
And antibacterial and anti-inflammatory effects are more preferable, meanwhile, glutamine peptide is rich in hydrolyzed wheat protein, so that the powdered oil of preparation also has
Play the role of promoting intestinal villi growth, improve immunity of organisms, therefore, in the present invention, wall material and core material cooperate, so that
The needs of Multifunctional powder grease of preparation not only meets in practical breeding process animal nutritionally, additionally it is possible to improve animal machine
Body immunity promotes growth of animal, therefore, good practical effect.
In the present invention, the Multifunctional powder grease of preparation is off-white powder, and appearance character is good, and crude fat content exists
34%~44%, for surface oil content 0.6%~1.3%, embedding techniques are good, and total clump count is far smaller than 10000/gram, defends
Raw degree is high, and Product Safety is good, and embedding rate is up to 98.5%~99.3%, and embedding effect is good, and preparation method of the present invention is simple,
It is good to embed effect, is suitble to industrialized production and application.
Specific embodiment
Below in conjunction in the embodiment of the present invention, technical solution in the embodiment of the present invention is clearly and completely retouched
It states, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on the present invention
In embodiment, every other implementation obtained by those of ordinary skill in the art without making creative efforts
Example, shall fall within the protection scope of the present invention.
Embodiment 1
A kind of preparation method of Multifunctional powder grease, comprising the following steps:
The preparation of S1, wall material solution: 6 kilograms of hydrolyzed wheat protein, 45 kilograms of dextrin are mixed with 300 liters of 45 DEG C of hot water,
Dissolution, obtains wall material solution；
The preparation of S2, essential oil: 0.05 kilogram of Thymol is dissolved in 0.15 liter of ethanol solution, essential oil is obtained；
The preparation of S3, core material solution: 25 liters of fish oil and 26 liters of coconut oil are added 0.17 kilogram of monoglyceride after mixing
With 0.34 kilogram of sucrose ester, obtain core material solution after mixing；
S4, the obtained core material solution of essential oil that step S2 is obtained, step S3 is added to the wall material solution that step S1 is obtained
In, high speed shear, the mixed solution after obtaining high speed shear；
S5, the mixed solution pressure homogenizer after high speed shear that step S4 is obtained is done by spraying after homogeneous under 100MPa
Dry, 190 DEG C of inlet temperature when spray drying, outlet temperature is 80 DEG C, obtains a kind of Multifunctional powder grease.
Embodiment 2
A kind of preparation method of Multifunctional powder grease, comprising the following steps:
The preparation of S1, wall material solution: 5 kilograms of hydrolyzed wheat protein, 35 kilograms of dextrin are mixed with 300 liters of 45 DEG C of hot water,
Dissolution, obtains wall material solution；
The preparation of S2, essential oil: 8 kilograms of Thymol are dissolved in 24 liters of ethanol solutions, essential oil is obtained；
The preparation of S3, core material solution: by 350 liters of fish oil and 50 liters of palm oils be added after mixing 27 kilograms of monoglyceride with
13 kilograms of sucrose ester, core material solution is obtained after mixing；
S4, the obtained core material solution of essential oil that step S2 is obtained, step S3 is added to the wall material solution that step S1 is obtained
In, high speed shear, the mixed solution after obtaining high speed shear；
S5, the mixed solution pressure homogenizer after high speed shear that step S4 is obtained is done by spraying after homogeneous under 100MPa
Dry, 190 DEG C of inlet temperature when spray drying, outlet temperature is 80 DEG C, obtains a kind of Multifunctional powder grease.
Embodiment 3
A kind of preparation method of Multifunctional powder grease, comprising the following steps:
The preparation of S1, wall material solution: 10 kilograms of hydrolyzed wheat protein, 50 kilograms of dextrin are mixed with 300 liters of 45 DEG C of hot water,
Dissolution, obtains wall material solution；
The preparation of S2, essential oil: 4.5 kilograms of Thymol are dissolved in 13 liters of ethanol solutions, essential oil is obtained；
The preparation of S3, core material solution: by 250 liters of fish oil and 50 liters of rice bran oils be added after mixing 11 kilograms of monoglyceride with
10 kilograms of sucrose ester, core material solution is obtained after mixing；
S4, the obtained core material solution of essential oil that step S2 is obtained, step S3 is added to the wall material solution that step S1 is obtained
In, high speed shear, the mixed solution after obtaining high speed shear；
S5, the mixed solution pressure homogenizer after high speed shear that step S4 is obtained is done by spraying after homogeneous under 100MPa
Dry, 190 DEG C of inlet temperature when spray drying, outlet temperature is 80 DEG C, obtains a kind of Multifunctional powder grease.
Embodiment 4
A kind of preparation method of Multifunctional powder grease, comprising the following steps:
The preparation of S1, wall material solution: 10 kilograms of hydrolyzed wheat protein, 30 kilograms of dextrin are mixed with 300 liters of 45 DEG C of hot water,
Dissolution, obtains wall material solution；
The preparation of S2, essential oil: 0.8 kilogram of Thymol is dissolved in 2 liters of ethanol solutions, essential oil is obtained；
The preparation of S3, core material solution: by 60 liters of fish oil and 20 liters of coconut oil be added after mixing 0.8 kilogram of monoglyceride with
1.6 kilograms of sucrose ester, core material solution is obtained after mixing；
S4, the obtained core material solution of essential oil that step S2 is obtained, step S3 is added to the wall material solution that step S1 is obtained
In, high speed shear, the mixed solution after obtaining high speed shear；
S5, the mixed solution pressure homogenizer after high speed shear that step S4 is obtained is done by spraying after homogeneous under 100MPa
Dry, 190 DEG C of inlet temperature when spray drying, outlet temperature is 80 DEG C, obtains a kind of Multifunctional powder grease.
Embodiment 5
A kind of preparation method of Multifunctional powder grease, comprising the following steps:
The preparation of S1, wall material solution: 10 kilograms of hydrolyzed wheat protein, dextrin 40 kilogram are mixed with 300 liters of 45 DEG C of hot water,
Dissolution, obtains wall material solution；
The preparation of S2, essential oil: 2 kilograms of Thymol are dissolved in 5 liters of ethanol solutions, essential oil is obtained；
The preparation of S3, core material solution: 120 liters of fish oil and 30 liters of coconut oil are added 3.75 kilograms of monoglyceride after mixing
With 3.75 kilograms of sucrose ester, obtain core material solution after mixing；
S4, the obtained core material solution of essential oil that step S2 is obtained, step S3 is added to the wall material solution that step S1 is obtained
In, high speed shear, the mixed solution after obtaining high speed shear；
S5, the mixed solution pressure homogenizer after high speed shear that step S4 is obtained is done by spraying after homogeneous under 100MPa
Dry, 190 DEG C of inlet temperature when spray drying, outlet temperature is 80 DEG C, obtains a kind of Multifunctional powder grease.
Embodiment 6
A kind of preparation method of Multifunctional powder grease, comprising the following steps:
The preparation of S1, wall material solution: 10 kilograms of hydrolyzed wheat protein, dextrin 40 kilogram are mixed with 300 liters of 45 DEG C of hot water,
Dissolution, obtains wall material solution；
The preparation of S2, essential oil: 2 kilograms of carvacrol are dissolved in 5 liters of ethanol solutions, essential oil is obtained；
The preparation of S3, core material solution: 120 liters of fish oil and 30 liters of coconut oil are added 3.75 kilograms of monoglyceride after mixing
With 3.75 kilograms of sucrose ester, obtain core material solution after mixing；
S4, the obtained core material solution of essential oil that step S2 is obtained, step S3 is added to the wall material solution that step S1 is obtained
In, high speed shear, the mixed solution after obtaining high speed shear；
S5, the mixed solution pressure homogenizer after high speed shear that step S4 is obtained is done by spraying after homogeneous under 100MPa
Dry, 190 DEG C of inlet temperature when spray drying, outlet temperature is 80 DEG C, obtains a kind of Multifunctional powder grease.
The Multifunctional powder grease of Examples 1 to 6 preparation is performed the following performance tests:
1, appearance: according to GB/T 15682-2008 " grain and oil detection paddy, rice cooking edible quality sensory evaluation method "
Specified in test method, the appearance of test sample；
2, crude fat content: according to rule in GB/T 5512-2018 " crude fat content measures standard in grain and oil detection grain "
Fixed test mode measures the crude fat content in sample；
3, surface oil content: accurately weighing quality (m) is the sample of 2~3g in triangular flask, with 40mL30~60 DEG C
Petroleum ether accurately extracts 1min under gentle agitation, is filtered immediately with G3 sand core funnel, with 25mL petroleum ether filter residue
40s is filtered immediately, and filtrate is transferred to the conical flask (m of constant weight1) in, after recycling petroleum ether, at 65 DEG C, it is dried to perseverance
Weight (m2), surface oil content=(m2-m1)/m × 100%)；
4, total clump count: according to GB 4789.2-2016, " national food safety standard food microbiological examination bacterium colony is total
Number measurement " specified in test method, total clump count in test sample；
5, total carbohydrates: using the total carbohydrates content in anthrone colorimetry measurement sample；
6, embedding rate: embedding efficiency=(oil content-surface oil content)/oil content × 100%, oil content use chloroform-
Methanol extraction measurement；
Test result see the table below:
The Multifunctional powder grease the performance test results of 1 Examples 1 to 6 of table preparation
It can be seen from the data in Table 1 that Multifunctional powder grease prepared by the embodiment of the present invention 1~6 is off-white powder,
Appearance character is good, and crude fat content is 34%~44%, and for surface oil content 0.6%~1.3%, embedding techniques are good, total bacterium
It falls number and is far smaller than 10000/gram, sanitation degree is high, and Product Safety is good, and embedding rate is up to 98.5%~99.3%, embedding
Effect is good.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of core material, which is characterized in that including compound grease, the compound grease is fish oil, vegetable oil mass ratio is 1~8:
1 mixture, further includes Thymol or carvacrol, and the additive amount of the Thymol or carvacrol is compound oil quality
0.1%~2%.
2. a kind of core material according to claim 1, which is characterized in that the compound grease is fish oil, vegetable oil mass ratio
For the mixture of 3~5:1, the additive amount of the Thymol or carvacrol is the 1%~2% of compound oil quality.
3. a kind of core material according to claim 2, which is characterized in that the compound grease is fish oil, vegetable oil mass ratio
For the mixture of 4:1, the additive amount of the Thymol or carvacrol is the 1.3% of compound oil quality.
4. a kind of core material according to any one of claims 1 to 3, which is characterized in that the vegetable oil is coconut oil, palm fibre
The one or more of palmitic acid oil, rice bran oil.
5. a kind of Multifunctional powder grease, which is characterized in that including a kind of core material described in Claims 1 to 4 any one, also
Including wall material, the wall material is the mixture of hydrolyzed wheat protein and dextrin, the matter of the hydrolyzed wheat protein and the dextrin
Ratio is measured as 1:2~7, the mass ratio of the wall material and the core material is 1:1~10.
6. a kind of Multifunctional powder grease according to claim 5, which is characterized in that the hydrolyzed wheat protein and described
The mass ratio of dextrin is 1:3~5, and the mass ratio of the wall material and the core material is 1:2~5.
7. a kind of Multifunctional powder grease according to claim 6, which is characterized in that the hydrolyzed wheat protein and described
The mass ratio of dextrin is 1:4, and the mass ratio of the wall material and the core material is 1:3.
8. a kind of Multifunctional powder grease according to claim 5~7 any one, which is characterized in that further include emulsification
Agent, the additive amount of the emulsifier are the 1%~10% of the compound oil quality, and the emulsifier is monoglyceride and sucrose ester
Mixture, the mass ratio of the monoglyceride and the sucrose ester is 0.5~2:1.
9. a kind of Multifunctional powder grease according to claim 8, which is characterized in that the additive amount of the emulsifier is institute
The 5% of compound oil quality is stated, the emulsifier is the mixture of monoglyceride and sucrose ester, the monoglyceride and the sucrose ester
Mass ratio be 1:1.
10. a kind of preparation method of Multifunctional powder grease, which comprises the following steps:
The formula of S1, the Multifunctional powder grease according to claim 5~9 any one, it is spare to weigh each component；
The preparation of S2, wall material solution: hydrolyzed wheat protein, dextrin are mixed with hot water, dissolution, and the temperature of hot water is 45~75
DEG C, obtain wall material solution；
The preparation of S3, essential oil: Thymol or carvacrol are dissolved in ethanol solution, obtain essential oil；
The preparation of S4, core material solution: emulsifier is added in fish oil and vegetable oil after mixing, it is molten to obtain core material after mixing
Liquid；
S5, the obtained core material solution of essential oil that step S3 is obtained, step S4 is added in the wall material solution that step S2 is obtained, it is high
Speed shearing, the mixed solution after obtaining high speed shear；
S6, it will be spray-dried after the mixed solution homogeneous after high speed shear that step S5 is obtained, obtain a kind of Multifunctional powder oil
Rouge.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112753905A (en) * | 2019-10-21 | 2021-05-07 | 内蒙古蒙牛乳业（集团）股份有限公司 | Functional beverage and preparation method thereof |
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| JP2007289116A (en) * | 2006-04-27 | 2007-11-08 | Miyoshi Oil & Fat Co Ltd | Powdered oil and fat |
| US20110189315A1 (en) * | 2008-06-10 | 2011-08-04 | Regina Goralczyk | Plant extract and pufa combinations |
| CN103082033A (en) * | 2013-02-06 | 2013-05-08 | 浙江中同科技有限公司 | Instant powdery grease treating starch sodium octenylsuccinate as wall material, and its preparation method |
| CN107518436A (en) * | 2017-08-29 | 2017-12-29 | 湖北欣和生物科技有限公司 | A kind of DHA grease microscapsule powder containing polypeptide and preparation method thereof |
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2019
- 2019-01-31 CN CN201910097598.3A patent/CN109673850A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2007289116A (en) * | 2006-04-27 | 2007-11-08 | Miyoshi Oil & Fat Co Ltd | Powdered oil and fat |
| US20110189315A1 (en) * | 2008-06-10 | 2011-08-04 | Regina Goralczyk | Plant extract and pufa combinations |
| CN103082033A (en) * | 2013-02-06 | 2013-05-08 | 浙江中同科技有限公司 | Instant powdery grease treating starch sodium octenylsuccinate as wall material, and its preparation method |
| CN107518436A (en) * | 2017-08-29 | 2017-12-29 | 湖北欣和生物科技有限公司 | A kind of DHA grease microscapsule powder containing polypeptide and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112753905A (en) * | 2019-10-21 | 2021-05-07 | 内蒙古蒙牛乳业（集团）股份有限公司 | Functional beverage and preparation method thereof |
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Application publication date: 20190426 |