CN109627914A - Epoxy antistatic floor coatings - Google Patents
Epoxy antistatic floor coatings Download PDFInfo
- Publication number
- CN109627914A CN109627914A CN201811515380.7A CN201811515380A CN109627914A CN 109627914 A CN109627914 A CN 109627914A CN 201811515380 A CN201811515380 A CN 201811515380A CN 109627914 A CN109627914 A CN 109627914A
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- epoxy
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/24—Electrically-conducting paints
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/04—Antistatic
Abstract
The invention discloses epoxy antistatic floor coatings, including component A and B component；The component A includes: 30-40 parts of E-51 epoxy resin, 10-20 parts of alkyl glycidyl ether, 12-15 parts of organobentonite, 10-15 parts of conductive mica powder, 1-5 parts of conductive fiber, 10-15 parts of powdered whiting, 3600:0.1-0.5 parts of EFKA, 3650:0.2-0.5 parts of EFKA, 4310:0.1-0.5 parts of EFKA；The B component includes: modified aliphatic cyclic amine 10-15 parts, 10-15 parts of methyl iso-butyl ketone (MIBK), 0.8-2 parts of tertiary amine；The epoxy antistatic floor coatings have significant antistatic effect and good terrace mechanical property, and excellent structural strength and toughness are at low cost suitable for various to antistatic demanding place.
Description
Technical field
The invention belongs to building coating technical fields, and in particular to epoxy antistatic floor coatings.
Background technique
With the progress of antistatic floor coatings technology, obtained using epoxy antistatic floor coatings coating mattess
The method that must prevent electrostatic from generating increasingly is used widely, and epoxy resin antistatic floor has surfacing, beautiful, whole
The features such as body is seamless, easy to clean, easy-maintaining, and anti-static effect is long-term persistently effective, low cost, is widely portable to electronic apparatus
Manufacture, microprocessor based computer precision equipment, electrical control, print, weaving, military project etc. all need the ground of antistatic or explosion-proof place
Face coating.
Existing epoxy antistatic floor coatings the relevant technologies are also more mature, while also having many patents, such as
A kind of epoxy antistatic floor paint of CN201610412323.0 discloses a kind of epoxy antistatic floor paint, the floor paint include with
Lower parts by weight of component: 90-100 parts of aqueous epoxy resins, 15-20 parts of Lauxite, 4-10 parts of polyethylene glycol oxide fat ether, lemon
4-7 parts of lemon acid, 4.5-6.5 parts of epoxy hardener, 3-7 parts of zinc naphthenate, 10-12 parts of disodium ethylene diamine tetraacetate, paraffin wax emulsions
16-18 parts, 12-16 parts of calcite in powder, 3-5 parts of p-methyl benzenesulfonic acid, 8-12 parts of ethylene glycol, 5-9 parts of epoxy dispersing agent, poly-vinegar acid
9-15 parts of vinyl acetate, 10-14 parts of liquid rosin resin.CN201511012636.9 non-solvent epoxy antistatic floor, discloses
A kind of non-solvent epoxy antistatic floor coating is by prime coat, the screed on prime coat, on screed
Conductive copper layers of foil, the antistatic top coat layer composition set on the static conductive prime coat of conductive copper layers of foil, on static conductive prime coat.
The smooth beauty of coating surface of the invention, sheet resistance in 1 × 109 Ω hereinafter, antistatic effect it is excellent persistently, it is wear-resisting, pressure-resistant,
Impact resistance, the corrosion of acid and alkali resistance, salt, oils etc. can be widely used for requiring high level of cleanliness, beauty, dustless, sterile and antistatic
Production industries and the large-scale precision instrument factory such as electronics, microelectronics, communication product, computer, precision instrument, weaving, printing
The fields such as room and military project, space flight.
But in existing technology, anti-static material such as carbon dust is generally added in terrace, certain antistatic effect can be played
Fruit.But in some pairs of demanding places of electrostatic, the antistatic effect of this terrace cannot be met the requirements.
Summary of the invention
The present invention is intended to provide epoxy antistatic floor coatings, the epoxy antistatic floor coatings have significantly resist it is quiet
Electric energy power and good terrace mechanical property, excellent structural strength and toughness are suitable for various to antistatic demanding field
Institute, it is at low cost.
Technical scheme is as follows:
Epoxy antistatic floor coatings, it is characterised in that: including component A and B component；
The component A includes: 30-40 parts of E-51 epoxy resin, 10-20 parts of alkyl glycidyl ether, organobentonite 12-
15 parts, 10-15 parts of conductive mica powder, 1-5 parts of conductive fiber, 10-15 parts of powdered whiting, 3600:0.1-0.5 parts of EFKA,
3650:0.2-0.5 parts of EFKA, 4310:0.1-0.5 parts of EFKA；
The B component includes: modified aliphatic cyclic amine 10-15 parts, 10-15 parts of methyl iso-butyl ketone (MIBK), 0.8-2 parts of tertiary amine；
Wherein, the component A further includes auxiliary agent, the auxiliary agent include 0.1-0.3 parts of BYK-320 and BYK-R605,
0.5-0.7 parts of BYK-052N.
Wherein, the B component further includes reinforcing agent, and the reinforcing agent includes 3-7 parts of Zr02, polyacrylamide 0.5-0.9
Part.
Wherein, the component A further includes 1-5 parts and Bronsted acid 0.2-0.5 parts of superfine cupper powder.
Wherein, the Bronsted acid is analytically pure hydrochloric acid.
Wherein, the epoxy antistatic floor coatings, production method include the following steps:
The preparation of S1, component A:
1. alkyl glycidyl ether, EFKA 3600, EFKA 3650, EFKA 4310 are added in a reaction container, room temperature
40-45min is stirred, mixing speed 2500-3000r/min adds organobentonite, conductive mica powder, conductive fiber, heavy
Epoxy is made in calcium carbonate, three parts of two E-51 epoxy resin, stirring at normal temperature 10-15min, mixing speed 1500-2000r/min
Anti-static composite material；
2. the E-51 epoxy resin of remaining one third is reacted chain extension under 120 ° with bisphenol-A in another reaction kettle；
Epoxy aqueous dispersion is made into using reversed conversion method；
3. mixing the substance in two reaction kettles, obtained component A is stirred evenly.
The preparation of S2, B component:
Modified aliphatic cyclic amine, methyl iso-butyl ketone (MIBK), tertiary amine are placed in container, 1~2h is mixed under room temperature, B group is made
Part；
Stirring 5min can be prepared by epoxy antistatic floor coatings after S3, construction site mix component A and B component.
The invention has the following beneficial effects:
1, the present invention has significant antistatic effect and good terrace performance, is suitable for various high to antistatic requirement
Place, it is at low cost, form uniform conductiving point in the epoxy by conductive mica powder, formed in conjunction with conductive fiber crisscross
Complexity covers comprehensive conductive network, while increasing whole imporosity and intensity, reduces because of addition Conductive mica etc.
Brittleness caused by material increases, by the way that appropriate superfine cupper powder and Bronsted acid is added, on the basis of excessively not improving cost, into one
Step improves conductive contact and distribution, to greatly improve antistatic effect.
2, the present invention can increase environmentally protective characteristic, and have oily material characteristic, at the same have it is preferable it is anti-oxidant with
And environmental protection characteristic, there is preferable one-way ventilating function, play the role of preferably preventing the Liquid Penetrants such as water, oil, by by major ingredient
E-51 epoxy resin carries out two different processing technologys, thus obtain have both it is wear-resisting, flexible, ventilative, anticorrosive and oxidation
Epoxy antistatic floor coatings.
3, the present invention prepares PART EPOXY aqueous dispersion using phase reversal, and the continuous phase in multicomponent system is in certain condition
Under mutually convert, to form firm combination, at the scene in construction, be stirred, solidified simultaneously by the way that B component is added
Make under effect two kinds of processing technologys formed epoxy resin composite material uniformly and closely combine, thus make its have both it is aqueous and
The advantages of oiliness.
Specific embodiment
The present invention is further illustrated by the following examples, but protection scope of the present invention is not limited to following reality
Apply example.
Embodiment 1
Epoxy antistatic floor coatings, it is characterised in that: including component A and B component；
The component A includes: 35 parts of E-51 epoxy resin, 15 parts of alkyl glycidyl ether, 14 parts of organobentonite, conduction
13 parts of mica powder, 3 parts of conductive fiber, 13 parts of powdered whiting, 3600:0.3 parts of EFKA, 3650:0.4 parts of EFKA, EFKA
4310:0.3 part；
The B component includes: 13 parts of modified aliphatic cyclic amine, 13 parts of methyl iso-butyl ketone (MIBK), 1.4 parts of tertiary amine；
Further, the component A further includes auxiliary agent, and the auxiliary agent includes BYK-320 and 0.2 part of BYK-R605, BYK-
0.6 part of 052N.
Further, the B component further includes reinforcing agent, and the reinforcing agent includes Zr02:5 parts, polyacrylamide 0.7
Part.
Further, the component A further includes 3 parts and 0.4 part of Bronsted acid of superfine cupper powder.
Further, the Bronsted acid is analytically pure hydrochloric acid.
The epoxy antistatic floor coatings, production method include the following steps:
The preparation of S1, component A:
1. by alkyl glycidyl ether, EFKA 3600, EFKA 3650, EFKA 4310, acrylate glycidol ether,
BYK-320, BYK-R605, BYK-052N, purifying hydrochloric acid be added in a reaction container, stirring at normal temperature 42min, mixing speed
2800r/min adds organobentonite, conductive mica powder, conductive fiber, superfine cupper powder, three parts of two E-51 epoxy resin,
Epoxy anti-static composite material is made in stirring at normal temperature 13min, mixing speed 1700r/min；
2. the E-51 epoxy resin of remaining one third is reacted chain extension under 120 ° with bisphenol-A in another reaction kettle；
Epoxy aqueous dispersion is made into using reversed conversion method；
3. mixing the substance in two reaction kettles, obtained component A is stirred evenly.
The preparation of S2, B component:
Modified aliphatic cyclic amine, methyl iso-butyl ketone (MIBK), tertiary amine, Zr02, polyacrylamide are placed in container, mixing is stirred under room temperature
It mixes 1.5h and B component is made；
Stirring 5min can be prepared by epoxy antistatic floor coatings after S3, construction site mix component A and B component.
Embodiment 2
Epoxy antistatic floor coatings, it is characterised in that: including component A and B component；
The component A includes: 30 parts of E-51 epoxy resin, 10 parts of alkyl glycidyl ether, 12 parts of organobentonite, conduction
10 parts of mica powder, 1 part of conductive fiber, 10 parts of powdered whiting, 3600:0.1 parts of EFKA, 3650:0.2 parts of EFKA, EFKA
4310:0.1 part；
The B component includes: 10 parts of modified aliphatic cyclic amine, 10 parts of methyl iso-butyl ketone (MIBK), 0.8 part of tertiary amine；
Further, the component A further includes auxiliary agent, and the auxiliary agent includes BYK-320 and 0.1 part of BYK-R605, BYK-
0.5 part of 052N.
Further, the B component further includes reinforcing agent, and the reinforcing agent includes 3 parts of Zr02, polyacrylamide 0.5
Part.
Further, the component A further includes 1 part and 0.2 part of Bronsted acid of superfine cupper powder.
Further, the Bronsted acid is analytically pure hydrochloric acid.
The epoxy antistatic floor coatings, production method include the following steps:
The preparation of S1, component A:
1. by alkyl glycidyl ether, EFKA 3600, EFKA 3650, EFKA 4310, acrylate glycidol ether,
BYK-320, BYK-R605, BYK-052N, purifying hydrochloric acid be added in a reaction container, stirring at normal temperature 4min, mixing speed
2500r/min adds organobentonite, conductive mica powder, conductive fiber, superfine cupper powder, three parts of two E-51 epoxy resin,
Epoxy anti-static composite material is made in stirring at normal temperature 10min, mixing speed 1500r/min；
2. the E-51 epoxy resin of remaining one third is reacted chain extension under 120 ° with bisphenol-A in another reaction kettle；
Epoxy aqueous dispersion is made into using reversed conversion method；
3. mixing the substance in two reaction kettles, obtained component A is stirred evenly.
The preparation of S2, B component:
Modified aliphatic cyclic amine, methyl iso-butyl ketone (MIBK), tertiary amine, Zr02, polyacrylamide are placed in container, mixing is stirred under room temperature
It mixes 1h and B component is made；
Stirring 5min can be prepared by epoxy antistatic floor coatings after S3, construction site mix component A and B component.
Embodiment 3
Epoxy antistatic floor coatings, it is characterised in that: including component A and B component；
The component A includes: 40 parts of E-51 epoxy resin, 20 parts of alkyl glycidyl ether, 15 parts of organobentonite, conduction
15 parts of mica powder, 5 parts of conductive fiber, 15 parts of powdered whiting, 3600:0.5 parts of EFKA, 3650:0.5 parts of EFKA,
EFKA4310:0.5 parts；
The B component includes: 15 parts of modified aliphatic cyclic amine, 15 parts of methyl iso-butyl ketone (MIBK), 2 parts of tertiary amine；
Further, the component A further includes auxiliary agent, and the auxiliary agent includes BYK-320 and 0.3 part of BYK-R605, BYK-
0.7 part of 052N.
Further, the B component further includes reinforcing agent, and the reinforcing agent includes 7 parts of Zr02, polyacrylamide 0.9
Part.
Further, the component A further includes 5 parts and 0.5 part of Bronsted acid of superfine cupper powder.
Further, the Bronsted acid is analytically pure hydrochloric acid.
The epoxy antistatic floor coatings, production method include the following steps:
The preparation of S1, component A:
1. by alkyl glycidyl ether, EFKA3600, EFKA3650, EFKA 4310, acrylate glycidol ether,
BYK-320, BYK-R605, BYK-052N, purifying hydrochloric acid, be added in a reaction container, stirring at normal temperature 45min, mixing speed
3000r/min adds organobentonite, conductive mica powder, conductive fiber, superfine cupper powder, three parts of two E-51 epoxy resin,
Epoxy anti-static composite material is made in stirring at normal temperature 15min, mixing speed 2000r/min；
2. the E-51 epoxy resin of remaining one third is reacted chain extension under 120 ° with bisphenol-A in another reaction kettle；
Epoxy aqueous dispersion is made into using reversed conversion method；
3. mixing the substance in two reaction kettles, obtained component A is stirred evenly.
The preparation of S2, B component:
Modified aliphatic cyclic amine, methyl iso-butyl ketone (MIBK), tertiary amine, Zr02, polyacrylamide are placed in container, mixing is stirred under room temperature
It mixes 2h and B component is made；
Stirring 5min can be prepared by epoxy antistatic floor coatings after S3, construction site mix component A and B component.
Comparative example 1
A kind of epoxy antistatic floor paint discloses a kind of epoxy antistatic floor paint, which includes following parts by weight
Component: 90-100 parts of aqueous epoxy resins, 15-20 parts of Lauxite, 4-10 parts of polyethylene glycol oxide fat ether, citric acid 4-7
Part, 4.5-6.5 parts of epoxy hardener, 3-7 parts of zinc naphthenate, 10-12 parts of disodium ethylene diamine tetraacetate, 16-18 parts of paraffin wax emulsions,
12-16 parts of calcite in powder, 3-5 parts of p-methyl benzenesulfonic acid, 8-12 parts of ethylene glycol, 5-9 parts of epoxy dispersing agent, polyvinyl acetate 9-15
Part, 10-14 parts of liquid rosin resin.
Comparative example 2
Non-solvent epoxy antistatic floor, the antistatic backing are made of following components by weight: epoxy
30-35 parts of resin E-54,20-40 parts of n-butyl glycidyl ether, polyamide curing agent are 10-15 parts, powdered whiting 2-5
Part, 20-25 parts of electroconductive glass fibre, 0.8-1.2 parts of dispersing agent, 0.8-1.2 parts of levelling agent, 0.8-1.2 parts of defoaming agent and anti-zoned
Hurt 0.5-1.0 parts of agent；The dispersing agent is BYK-110；The levelling agent is in BYK-323 and CERAFLOUR 996
It is a kind of；The defoaming agent is BYK-A530；The scratching resistant is NANOBYK-3601.
The following are above-described embodiments to carry out detection performance, Its Relevant Technology Standards GB/ by corresponding national standard
T22374-2008 technical indicator, test result see the table below:
As seen from the above table, be made epoxy antistatic floor coatings have preferable adhesive force, toughness, wearability, water resistance,
Ageing-resistant and high-antistatic performance, better than the floor coatings of comparative example.
The above embodiment is a preferred embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment
Limitation, other any changes, modifications, substitutions, combinations, simplifications made without departing from the spirit and principles of the present invention,
It should be equivalent substitute mode, be included in protection scope of the present invention.
Claims (6)
1. epoxy antistatic floor coatings, it is characterised in that: including component A and B component；
The component A includes: 30-40 parts of E-51 epoxy resin, 10-20 parts of alkyl glycidyl ether, organobentonite 12-15
Part, 10-15 parts of conductive mica powder, 1-5 parts of conductive fiber, 10-15 parts of powdered whiting, 3600:0.1-0.5 parts of EFKA, EFKA
3650:0.2-0.5 parts, 4310:0.1-0.5 parts of EFKA；
The B component includes: modified aliphatic cyclic amine 10-15 parts, 10-15 parts of methyl iso-butyl ketone (MIBK), 0.8-2 parts of tertiary amine.
2. epoxy antistatic floor coatings as described in claim 1, it is characterised in that: the component A further includes auxiliary agent, described
Auxiliary agent includes 0.1-0.3 parts of BYK-320 and BYK-R605,0.5-0.7 parts of BYK-052N.
3. epoxy antistatic floor coatings as described in claim 1, it is characterised in that: the B component further includes reinforcing agent, institute
Stating reinforcing agent includes 3-7 parts of Zr02,0.5-0.9 parts of polyacrylamide.
4. epoxy antistatic floor coatings as described in claim 1, it is characterised in that: the component A further includes superfine cupper powder
1-5 parts and Bronsted acid 0.2-0.5 parts.
5. epoxy antistatic floor coatings as claimed in claim 4, it is characterised in that: the Bronsted acid is analytically pure salt
Acid.
6. epoxy antistatic floor coatings as described in claim 1, production method include the following steps:
The preparation of S1, component A:
1. alkyl glycidyl ether, EFKA 3600, EFKA 3650, EFKA 4310 are added in a reaction container, stirring at normal temperature
40-45min, mixing speed 2500-3000r/min add organobentonite, conductive mica powder, conductive fiber, heavy carbonic acid
Calcium, three parts of two E-51 epoxy resin, stirring at normal temperature 10-15min, mixing speed 1500-2000r/min, obtained epoxy resists quiet
Composite；
2. the E-51 epoxy resin of remaining one third is reacted chain extension under 120 ° with bisphenol-A in another reaction kettle；It utilizes
Reversed conversion method is made into epoxy aqueous dispersion；
3. mixing the substance in two reaction kettles, obtained component A is stirred evenly；
The preparation of S2, B component:
Modified aliphatic cyclic amine, methyl iso-butyl ketone (MIBK), tertiary amine are placed in container, 1 ~ 2h is mixed under room temperature, B component is made；
Stirring 5min can be prepared by epoxy antistatic floor coatings after S3, construction site mix component A and B component.
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| CN201811515380.7A CN109627914A (en) | 2018-12-12 | 2018-12-12 | Epoxy antistatic floor coatings |
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|---|---|---|---|
| CN201811515380.7A CN109627914A (en) | 2018-12-12 | 2018-12-12 | Epoxy antistatic floor coatings |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109608982A (en) * | 2018-11-28 | 2019-04-12 | 河北晨阳工贸集团有限公司 | A kind of novel solvent-free epoxy antistatic floor |
| CN110591492A (en) * | 2019-10-09 | 2019-12-20 | 厦门珉瑶贸易有限公司 | Antistatic epoxy ester modified styrene-acrylic resin anticorrosive paint |
| CN110652100A (en) * | 2019-09-05 | 2020-01-07 | 安徽名扬刷业有限公司 | Prevent variable brush roller of static |
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| CN101818015A (en) * | 2010-05-24 | 2010-09-01 | 广州飞宇建材科技有限公司 | Aqueous antistatic epoxy floor paint and preparation method and application thereof |
| CN108047874A (en) * | 2017-11-24 | 2018-05-18 | 鹤山市信兴化工有限公司 | Solvent-free antistatic epoxy floor paint and preparation method thereof |
| CN108753108A (en) * | 2018-06-20 | 2018-11-06 | 上海维度化工科技有限公司 | A kind of non-solvent epoxy super abrasive anti-corrosion antistatic floor coatings and preparation method thereof |
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| CN101397473A (en) * | 2007-09-26 | 2009-04-01 | 洛阳七维防腐工程材料有限公司 | Novel additive type solvent-free epoxy self-leveling antistatic floor coatings |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109608982A (en) * | 2018-11-28 | 2019-04-12 | 河北晨阳工贸集团有限公司 | A kind of novel solvent-free epoxy antistatic floor |
| CN110652100A (en) * | 2019-09-05 | 2020-01-07 | 安徽名扬刷业有限公司 | Prevent variable brush roller of static |
| CN110591492A (en) * | 2019-10-09 | 2019-12-20 | 厦门珉瑶贸易有限公司 | Antistatic epoxy ester modified styrene-acrylic resin anticorrosive paint |
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Application publication date: 20190416 |