CN109627825A - A kind of paper tire lacquer painting lacquer and preparation method thereof - Google Patents
A kind of paper tire lacquer painting lacquer and preparation method thereof Download PDFInfo
- Publication number
- CN109627825A CN109627825A CN201910019202.3A CN201910019202A CN109627825A CN 109627825 A CN109627825 A CN 109627825A CN 201910019202 A CN201910019202 A CN 201910019202A CN 109627825 A CN109627825 A CN 109627825A
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- Prior art keywords
- lacquer
- paper tire
- painting
- preparation
- tung oil
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- 239000004922 lacquer Substances 0.000 title claims abstract description 130
- 238000010422 painting Methods 0.000 title claims abstract description 43
- 238000002360 preparation method Methods 0.000 title claims abstract description 23
- 239000002383 tung oil Substances 0.000 claims abstract description 31
- 239000002023 wood Substances 0.000 claims description 15
- 239000003921 oil Substances 0.000 claims description 14
- DXRKLUVKXMAMOV-UHFFFAOYSA-N 3-heptadecylcatechol Chemical compound CCCCCCCCCCCCCCCCCC1=CC=CC(O)=C1O DXRKLUVKXMAMOV-UHFFFAOYSA-N 0.000 claims description 12
- 239000004615 ingredient Substances 0.000 claims description 7
- 108010029541 Laccase Proteins 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 239000012535 impurity Substances 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 4
- 102000003886 Glycoproteins Human genes 0.000 claims description 3
- 108090000288 Glycoproteins Proteins 0.000 claims description 3
- 238000013019 agitation Methods 0.000 claims 1
- 238000000527 sonication Methods 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 abstract description 6
- 238000011161 development Methods 0.000 abstract description 4
- 238000011160 research Methods 0.000 abstract description 4
- 238000002604 ultrasonography Methods 0.000 abstract description 4
- 230000004927 fusion Effects 0.000 abstract description 3
- 230000007246 mechanism Effects 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 3
- 238000010008 shearing Methods 0.000 abstract description 3
- 238000002156 mixing Methods 0.000 abstract description 2
- 238000009210 therapy by ultrasound Methods 0.000 abstract 1
- 239000003973 paint Substances 0.000 description 16
- 238000001035 drying Methods 0.000 description 11
- 238000000034 method Methods 0.000 description 10
- 241000209094 Oryza Species 0.000 description 9
- 235000007164 Oryza sativa Nutrition 0.000 description 9
- 235000009566 rice Nutrition 0.000 description 9
- 238000012360 testing method Methods 0.000 description 5
- 238000010586 diagram Methods 0.000 description 4
- 238000005259 measurement Methods 0.000 description 4
- 230000004048 modification Effects 0.000 description 4
- 238000012986 modification Methods 0.000 description 4
- 238000007792 addition Methods 0.000 description 2
- 238000009864 tensile test Methods 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- 150000005671 trienes Chemical group 0.000 description 2
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 description 1
- 241001264730 Callistemon salignus Species 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 235000010099 Fagus sylvatica Nutrition 0.000 description 1
- 240000000731 Fagus sylvatica Species 0.000 description 1
- 244000082946 Tarchonanthus camphoratus Species 0.000 description 1
- 235000005701 Tarchonanthus camphoratus Nutrition 0.000 description 1
- 244000044283 Toxicodendron succedaneum Species 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 238000006701 autoxidation reaction Methods 0.000 description 1
- 230000001680 brushing effect Effects 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 229910052602 gypsum Inorganic materials 0.000 description 1
- 239000010440 gypsum Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 239000002075 main ingredient Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 230000000659 thermocoagulation Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/06—Artists' paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D191/00—Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
- C09D191/005—Drying oils
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Printing Methods (AREA)
Abstract
The invention discloses a kind of paper tire lacquer painting lacquer and preparation method thereof, belong to lacquer painting technical field, using lacquer and ripe pure tung oil as raw material, by the ratio for coordinating the two, and combine ultrasonic treatment mixing, mechanical shearing is carried out to tung oil using the mechanism of ultrasound, promote the degrees of fusion and sophistication of tung oil and lacquer, be conducive to being impregnated on paper tire, the cavitation of ultrasound forms cavitation thermal in tung oil and lacquer mixed liquor, be conducive to the reaction of tung oil and lacquer, promote reaction efficiency, preparation process is simple, configure the lacquer for being applicable in the creation of paper tire lacquer painting, be conducive to the development of paper tire lacquer painting, new research direction is researched and proposed simultaneously for lacquer painting from now on.
Description
Technical field
The present invention relates to lacquer painting technical field, a kind of paper tire lacquer painting lacquer and preparation method thereof is particularly related to.
Background technique
Lacquer is also known as lacquer, is after manually extracting from lacquer tree, the natural products of processed preparation, lacquer is as unique
The artistic medium of oriental cultural characteristic has more than 8000 years history, all distributes unique artistic charm, lacquer painting from ancient times to the present
Creation be even more to add artistic color for the life of modern.
It is to hand over a kind of common mode at present that lacquer painting is made on mold, and the production method of bodiless lacquer is divided into from ancient times to the present
Tread flaking and wooden two kinds of the tire, tread flaking are the molds with soil, gypsum, wooden model etc. for product, and the wooden tire mainly uses nanmu, camphorwood, beech
The stonewoods such as wood are base, without tread flaking, are directly painted, process is identical as tread flaking cloth base, the preparation of both bodiless lacquers
In method, the requirement to lacquer performance is looser, but the lacquer painting of paper tire is not available then, due at present to paper tire lacquer painting
Study less, the requirement of related lacquer is also less, in order to promote the development of paper tire lacquer painting, grinds to the lacquer for being suitable for paper tire lacquer painting
Studying carefully is crucial factor.
Summary of the invention
In view of this, it is an object of the invention to propose a kind of paper tire lacquer painting lacquer and preparation method thereof, to fill up existing
There is the blank that paper tire lacquer painting lacquer is studied in technology.
Based on a kind of above-mentioned purpose paper tire lacquer painting lacquer provided by the invention, the lacquer includes following mass percent
Ingredient: boiled wood oil 25-35%, lacquer 65-75%.
In some optional embodiments, the lacquer includes following mass percent ingredient: boiled wood oil 30%, lacquer
70%.
In some optional embodiments, the lacquer includes following mass percent ingredient: laccol 65-75%, Qi Duo
Sugared 5-7%, glycoprotein 2-5%, laccase < 1%, surplus moisture.
In some optional embodiments, the boiled wood oil is ripe pure tung oil.
A kind of preparation method of paper tire lacquer painting lacquer, includes the following steps:
1) it takes boiled wood oil to carry out 300-400 mesh filtering and impurity removing, is then ultrasonically treated 1-5min;
2) it weighs lacquer and divides 3-5 batches to be added in the ripe pure tung oil in step (1), heating stirring 5- after being added every time
10min is ultrasonically treated 35-60min after all adding, obtains finished product.
In some optional embodiments, power ultrasonic in the step (1) is 70-180w, frequency 20-30kHz.
In some optional embodiments, the temperature of heating stirring is 28-43 DEG C in the step (2).
In some optional embodiments, the frequency being ultrasonically treated in the step (2) is 100-200kHz, temperature 17-
28℃。
From the above it can be seen that a kind of paper tire lacquer painting provided by the invention is with lacquer and ripe pure tung oil with lacquer
Raw material configures the lacquer for being applicable in the creation of paper tire lacquer painting, is conducive to the development of paper tire lacquer painting, together by coordinating the ratio of the two
When new research direction is researched and proposed for lacquer painting from now on.
It is mixed by being simply ultrasonically treated meanwhile the present invention also provides a kind of method for preparing paper tire lacquer painting lacquer
It closes, mechanical shearing is carried out to tung oil using the mechanism of ultrasound, promotes the degrees of fusion and sophistication of tung oil and lacquer, favorably
In being impregnated on paper tire, ultrasonic cavitation forms cavitation thermal in tung oil and lacquer mixed liquor, is conducive to tung oil
With the reaction of lacquer, reaction efficiency is promoted.
Lacquer is modified using tung oil, on the one hand reduce the presence of harmful components laccol in lacquer to human body and
It is injured caused by environment, the modification of another aspect tung oil, there is long-chain flexible structure due to being added, have and improve lacquer
Flexibility, the conjugated triene structures of tung oil are conducive to the drying of lacquer, the efficiency that the promotion later period is manufactured.
Detailed description of the invention
Fig. 1 is the rice paper pictorial diagram that the embodiment of the present invention uses;
Fig. 2 is the lacquer schematic diagram of allotment of the embodiment of the present invention;
Fig. 3 is mopping of embodiment of the present invention schematic diagram;
Fig. 4 is the rice paper pictorial diagram after mopping of the embodiment of the present invention is dry;
Fig. 5 is tensile test of embodiment of the present invention figure.
Specific embodiment
To make the objectives, technical solutions, and advantages of the present invention clearer, below in conjunction with specific embodiment, and reference
Attached drawing, the present invention is described in more detail.
It discloses a kind of paper tire lacquer painting lacquer in the embodiment of the present invention, include mass percent in lacquer is respectively 25-
35% boiled wood oil and the natural paint ingredients of 65-75%.
In some optional embodiments, a kind of paper tire lacquer painting lacquer in the embodiment of the present invention includes quality hundred in lacquer
Divide than being respectively 30% boiled wood oil and 70% natural paint ingredients, wherein the content of main ingredient is laccol 65- in lacquer
75%, urushipolysaccharide 5-7%, glycoprotein 2-5%, laccase < 1%, surplus moisture, boiled wood oil are skillful tung oil.
Component content is one of the factor for determining lacquer performance, and preparation process is to determine another factor of lacquer performance, is
Research to the lacquer of paper tire lacquer painting comprehensively, therefore a kind of system of paper tire lacquer painting lacquer is disclosed in the embodiment of the present invention
Preparation Method includes the following steps:
1) it takes boiled wood oil to carry out 300-400 mesh filtering and impurity removing, is then ultrasonically treated 1-5min;
2) it weighs lacquer and divides 3-5 batches to be added in the tung oil in step (1), heating stirring 5-10min after being added every time,
It is ultrasonically treated 35-60min after all adding, obtains finished product.
In some optional embodiments, a kind of preparation method of paper tire lacquer painting lacquer is disclosed in the embodiment of the present invention,
Include the following steps:
1) ripe pure tung oil 3kg is weighed by above-mentioned formula to be placed in barrel, and carry out 400 mesh filtering and impurity removings, it then will removal of impurities
Ripe pure tung oil afterwards is 100w in power, handles 3min under the ultrasonic wave that frequency is 25kHz;
2) lacquer 7kg is weighed by above-mentioned formula, and in the ripe pure tung oil in point 5 batches of additions step (1), day is added every time
So paint after heating and thermal insulation at 35 DEG C and stirring 8min, lacquer all add after frequency be 180kHz, temperature be 25 DEG C at
It is ultrasonically treated 45min, obtains finished product.
In these cases, by changing ripe pure tung oil and the quality accounting of lacquer and respectively react item in preparation process
Part studies the obtained lacquer performance of preparation, specific as follows:
1) lacquer of preparation is evenly coated on 07 year " Red Star " board rice paper, and is carried out at a temperature of 50-120 DEG C different
Drying, then (test method is shown in Table for measurement drying time (film thickness after dry is at 100 ± 3 μm) and physical mechanical property
1).Test the results are shown in Table 2-3.
1 paint film physical mechanical property test method of table
Project | Reference standard | Title |
Surface drying time | GB/T1728-1979 | Second method in paint film drying time measuring method |
Surface gloss | GB/T1743-1979 | Gloss of film degree measuring method |
Pencil hardness | GB/T6739-2006 | Pencil method measures hardness of paint film |
Flexibility | GB/T1731-1993 | Paint film suppleness measuring method |
Impact resistance | GB/T1732-1993 | Paint film impact resistance measuring method |
2 paint film physical mechanical property test result of table
Project | Surface drying time/min | Pencil hardness | Flexibility/mm | Impact resistance/cm | Surface gloss |
Lacquer | 175 | 5H | 10 | 30 | 70 |
Lacquer | 50 | 3H | 4 | 55 | 88 |
Modified lacquer physical mechanical property performance is more excellent than lacquer, the hardness decline of modified lacquer, flexible
The raising of property and impact resistance is the addition due to the boiled wood oil with long-chain flexible structure, destroy in lacquer laccol by
In the inierpeneirating network structure that unsaturated terminal chain is formed in the autoxidation cross-linked polymeric stage.
Paint film physical mechanical property test result under the different drying temperature states of table 3
The surface drying time of paint film is very long, be due to laccase is a kind of more copper proteins, when drying temperature is more than 60 DEG C,
Laccase protein matter can gradually by thermocoagulation and lose activity, meanwhile, the O being dissolved in water2As the raising of temperature and drop
Low solubility, and then cause enzymatic film forming speed slack-off.From the entire performance of the aggregation of data of table 3, drying temperature at 80-90 DEG C most
It is good.
2) it uses different paint uniformly to brush in dimensions as on 07 year " Red Star " board rice paper of 200 × 20mm, brushes
Amount of paint is identical, brush it is smooth after, be dried using 80 DEG C of temperature, then carry out tensile test, every group measurement 3 times, take
Average value.Measurement result is shown in Table 4, and experimentation is as shown in Fig. 1-5.
4 different component tension measurement result of table
The data of table 4 show that the tensile fracture of pure rice paper is 0.89kg, and when brushing upper lacquer, tensile fracture is
3.97kg is 4.4 times of pure rice paper intensity, and when painting the lacquer of different content component, tensile fracture is still better than pure rice paper,
And the tensile fracture of number 3 and 4 is higher than the tensile fracture of number 2, test result is consistent with the test data flexibility of table 2,
To illustrate that the combination of rice paper and lacquer can increase the intensity of rice paper, be conducive to the preservation of paper tire lacquer painting, while the paint prepared
The flexibility of film promotes paper tire lacquer painting in the operability of preparation process, as lacquer 65%-75%+ boiled wood oil 25%-35%
The lacquer overall performance of preparation is more excellent.
In the case using lacquer and ripe pure tung oil as raw material, by coordinating the ratio of the two, applicable paper tire is configured
The lacquer of lacquer painting creation is conducive to the development of paper tire lacquer painting, while researching and proposing new research direction for lacquer painting from now on.
Meanwhile by being simply ultrasonically treated mixing, mechanical shearing is carried out to tung oil using the mechanism of ultrasound, is promoted
The degrees of fusion and sophistication of tung oil and lacquer are conducive to being impregnated on paper tire, and ultrasonic cavitation is in tung oil and naturally
It paints and forms cavitation thermal in mixed liquor, be conducive to the reaction of tung oil and lacquer, promote reaction efficiency, preparation process is simple.
Lacquer is modified using tung oil, on the one hand reduce the presence of harmful components laccol in lacquer to human body and
It is injured caused by environment, the modification of another aspect tung oil, there is long-chain flexible structure due to being added, have and improve lacquer
Flexibility, the conjugated triene structures of tung oil are conducive to the drying of lacquer, the efficiency that the promotion later period is manufactured.For paper tire paint
The preparation cost of picture is low, and molding is fast, is conducive to industrialization large-scale production.
It should be understood by those ordinary skilled in the art that: the discussion of any of the above embodiment is exemplary only, not
It is intended to imply that the scope of the present disclosure (including claim) is limited to these examples;Under thinking of the invention, above embodiments
Or can also be combined between the technical characteristic in different embodiments, step can be realized with random order, and be existed such as
Many other variations of the upper different aspect of the invention, for simplicity, they are not provided in details.
The embodiment of the present invention be intended to cover fall into all such replacements within the broad range of appended claims,
Modifications and variations.Therefore, all within the spirits and principles of the present invention, any omission, modification, equivalent replacement, the improvement made
Deng should all be included in the protection scope of the present invention.
Claims (8)
1. a kind of paper tire lacquer painting lacquer, which is characterized in that the lacquer includes following mass percent ingredient: boiled wood oil 25-
35%, lacquer 65-75%.
2. paper tire lacquer painting lacquer according to claim 1, which is characterized in that the lacquer include following mass percent at
Point: boiled wood oil 30%, lacquer 70%.
3. paper tire lacquer painting lacquer according to claim 1, which is characterized in that the lacquer includes following quality percentage
Than ingredient: laccol 65-75%, urushipolysaccharide 5-7%, glycoprotein 2-5%, laccase < 1%, surplus moisture.
4. paper tire lacquer painting lacquer according to claim 1, which is characterized in that the boiled wood oil is ripe pure tung oil.
5. a kind of preparation method of paper tire lacquer painting lacquer, which comprises the steps of:
1) it takes boiled wood oil to carry out 300-400 mesh filtering and impurity removing, is then ultrasonically treated 1-5min;
2) it weighs lacquer and divides 3-5 batches to be added in the ripe pure tung oil in step (1), heating stirring 5-10min after being added every time,
It is ultrasonically treated 35-60min after all adding, obtains finished product.
6. the preparation method of paper tire lacquer painting lacquer according to claim 1, which is characterized in that surpass in the step (1)
The power of sound is 70-180w, frequency 20-30kHz.
7. the preparation method of paper tire lacquer painting lacquer according to claim 1, which is characterized in that add in the step (2)
The temperature of thermal agitation is 28-43 DEG C.
8. the preparation method of paper tire lacquer painting lacquer according to claim 1, which is characterized in that surpass in the step (2)
The frequency of sonication is 100-200kHz, and temperature is 17-28 DEG C.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201910019202.3A CN109627825A (en) | 2019-01-09 | 2019-01-09 | A kind of paper tire lacquer painting lacquer and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201910019202.3A CN109627825A (en) | 2019-01-09 | 2019-01-09 | A kind of paper tire lacquer painting lacquer and preparation method thereof |
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Publication Number | Publication Date |
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CN109627825A true CN109627825A (en) | 2019-04-16 |
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CN201910019202.3A Withdrawn CN109627825A (en) | 2019-01-09 | 2019-01-09 | A kind of paper tire lacquer painting lacquer and preparation method thereof |
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Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108129989A (en) * | 2017-12-25 | 2018-06-08 | 中山市得高行知识产权中心(有限合伙) | A kind of colour wear resistant raw lacquer coating and preparation method thereof |
-
2019
- 2019-01-09 CN CN201910019202.3A patent/CN109627825A/en not_active Withdrawn
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108129989A (en) * | 2017-12-25 | 2018-06-08 | 中山市得高行知识产权中心(有限合伙) | A kind of colour wear resistant raw lacquer coating and preparation method thereof |
Non-Patent Citations (2)
Title |
---|
段久芳: "《天然高分子材料》", 30 September 2016, 华中科技大学出版社 * |
雷骏志等: "《大漆涂装技术》", 31 August 1988, 北京航空学院出版社 * |
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Application publication date: 20190416 |