CN109609301A - A kind of down jacket cleaning agent and its preparation process - Google Patents
A kind of down jacket cleaning agent and its preparation process Download PDFInfo
- Publication number
- CN109609301A CN109609301A CN201910000339.4A CN201910000339A CN109609301A CN 109609301 A CN109609301 A CN 109609301A CN 201910000339 A CN201910000339 A CN 201910000339A CN 109609301 A CN109609301 A CN 109609301A
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- Prior art keywords
- cleaning agent
- polyoxyethylene ether
- alkyl glycosides
- down jacket
- added
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/045—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on non-ionic surface-active compounds and soap
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/008—Polymeric surface-active agents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of down jacket cleaning agents, it is characterized in that, raw material including following mass percents: alkyl glycosides 6-12%, isomerous tridecanol polyoxyethylene ether 15-20%, cocinic acid potash soap 5-10%, isomery nonylphenol polyoxyethylene ether 10-15%, ethoxylated dodecyl alcohol 5-10%, chelating titanate coupling agent 0.1-0.5%, sodium citrate 0.1-5%, triethylene glycol butyl ether 1-5%, remaining is deionized water；The alkyl glycosides used in the present invention is a kind of more comprehensive new non-ionic surfactants of performance, with high surface, good ecological security and intermiscibility, it is internationally recognized preferred " green " functional surfactant, alkyl glycosides is biodegradable, and its degradation is thorough rapidly, decontamination rear surface activating agent bring secondary pollution problem is avoided, it is environmentally friendly, realize the purpose that renewable biomass resources substitution fossil feedstock prepares environmental-friendly surfactant.
Description
Technical field
The invention belongs to daily chemical product preparation field, it is specifically related to a kind of down jacket cleaning agent and its preparation process.
Background technique
Down jacket cleaning agent is mostly that surfactant, auxiliary agent, essence etc. are formulated, although there is certain cleaning effect,
But the fat protection of current detergent (their pH value has stronger alkalinity 11 or so) destructible fiber surface
Film, and fibrous inside can be penetrated into, so that natural feather is lost original soft and moist, elastic and gloss, become to dry, harden, withered crisp, aging,
Shorten the service life of down jackets, therefore the cleaning of down jackets, without the strong down jackets scavenger specially of comprehensive performance, to natural feather
The cleaning effect of clothes is less desirable.
Summary of the invention
In order to overcome the drawbacks of the prior art, provide that one kind has decontamination and antibacterial functions, natural feather fluffy degree are good, water-soluble
Articles for washing good, the feature of environmental protection is good, the invention discloses a kind of down jacket cleaning agent and its preparation processes.
The present invention takes following technical scheme:
A kind of down jacket cleaning agent, the raw material including following mass percents: alkyl glycosides 6-12%, isomerous tridecanol polyoxy second
Alkene ether 15-20%, cocinic acid potash soap 5-10%, isomery nonylphenol polyoxyethylene ether 10-15%, ethoxylated dodecyl alcohol 5-
10%, chelating titanate coupling agent 0.1-0.5%, sodium citrate 0.1-5%, triethylene glycol butyl ether 1-5%, remaining is deionization
Water.
Further, the alkyl glycosides is in atomic number of alkyl carbon is 12, atomic number of alkyl carbon is 14 alkyl glycosides
It is any.
Further, the raw material including following mass percents: alkyl glycosides 8%, isomerous tridecanol polyoxyethylene ether 7%,
Cocinic acid potash soap 7%, isomery nonylphenol polyoxyethylene ether 8%, ethoxylated dodecyl alcohol 6%, chelating titanate coupling agent
0.3%, sodium citrate 2%, triethylene glycol butyl ether 2%, remaining is deionized water.
A kind of preparation method of the down jacket cleaning agent, comprising the following steps:
S1, according to cleaning agent formula, configured the raw material of associated weight；
S2, in a kettle, be added triethylene glycol butyl ether, isomerous tridecanol polyoxyethylene, isomery nonylphenol polyoxyethylene ether,
Ethoxylated dodecyl alcohol, be mixed 2-5min, after obtain mixed solution A；
S3, alkyl glycosides, cocinic acid potash soap are continuously added into reaction kettle, stir 5-8min, continuously add chelating type metatitanic acid
Ester coupling agent continues to stir 5-10min, sodium citrate is added, obtains mixed solution B after mixing evenly；
S4, after mixed solution B is cooled to room temperature, deionized water is added, stirs evenly, adds sodium citrate, adjust PH to
Neutrality is filtered with 200 mesh nylon screens to get the down jacket cleaning agent is arrived.
Compared with prior art, beneficial effects of the present invention are as follows:
Cleaning agent of the present invention, by Surfactants Alkyl, isomerous tridecanol polyoxyethylene ether, cocinic acid potassium
Soap, isomery nonylphenol polyoxyethylene ether, ethoxylated dodecyl alcohol and chelating titanate coupling agent, reasonable compatibility get up, shape
At compounding mixed surfactant, while triethylene glycol butyl ether is added, can be good at solubilising, improves compound surfactant
Transparency, reduce viscosity, the cleaning agent prepared effectively can remove or clean macula lutea present on clothing, pigment.
The compatibility principle of raw material of the present invention is as described below:
1, the alkyl glycosides used in the present invention is a kind of more comprehensive new non-ionic surfactants of performance, has high surface
Active, good ecological security and intermiscibility are internationally recognized preferred " green " functional surfactant, alkyl glycosides
It is biodegradable, and its degradation is thorough rapidly, avoids decontamination rear surface activating agent bring secondary pollution problem, to environment friend
It is good, realize the purpose that renewable biomass resources substitution fossil feedstock prepares environmental-friendly surfactant.
2, cocinic acid potash soap is to belong to anionic surfactant class.Cocinic acid potash soap is soluble easily in water and alcohols is organic
Solvent, stronger wetting are permeated, the ability of dispersion and decontamination.
3, isomerous tridecanol polyoxyethylene ether is easily dispersed or dissolved in water, has excellent wetability, permeability and emulsibility.
Specific embodiment
The invention will be further described combined with specific embodiments below, but does not limit the scope of the invention and apply
Range.
Embodiment 1
A kind of down jacket cleaning agent, the raw material including following mass percents: alkyl glycosides 6%, isomerous tridecanol polyoxyethylene ether
15%, cocinic acid potash soap 5%, isomery nonylphenol polyoxyethylene ether 10%, ethoxylated dodecyl alcohol 5%, chelating titanate are even
Join agent 0.1%, 0.1% triethylene glycol butyl ether 1% of sodium citrate, remaining is deionized water.
The alkyl glycosides be atomic number of alkyl carbon be 12, atomic number of alkyl carbon is any one of 14 alkyl glycosides.
A kind of preparation method of down jacket cleaning agent, comprising the following steps:
S1, according to cleaning agent formula, configured the raw material of associated weight；
S2, in a kettle, be added triethylene glycol butyl ether, isomerous tridecanol polyoxyethylene, isomery nonylphenol polyoxyethylene ether,
Ethoxylated dodecyl alcohol, be mixed 2min, after obtain mixed solution A；
S3, alkyl glycosides, cocinic acid potash soap are continuously added into reaction kettle, stir 5min, continuously add chelating titanate
Coupling agent continues to stir 5min, sodium citrate is added, obtains mixed solution B after mixing evenly；
S4, after mixed solution B is cooled to room temperature, deionized water is added, stirs evenly, adds sodium citrate, adjust PH to
Neutrality is filtered with 200 mesh nylon screens to get the down jacket cleaning agent is arrived.
Embodiment 2
A kind of down jacket cleaning agent, the raw material including following mass percents: alkyl glycosides 12%, isomerous tridecanol polyoxyethylene
Ether 20%, cocinic acid potash soap 10%, isomery nonylphenol polyoxyethylene ether 15%, ethoxylated dodecyl alcohol 10%, chelating type metatitanic acid
Ester coupling agent 0.5%, sodium citrate 5%, triethylene glycol butyl ether 5%, remaining is deionized water.
The alkyl glycosides be atomic number of alkyl carbon be 12, atomic number of alkyl carbon is any one of 14 alkyl glycosides.
A kind of preparation method of down jacket cleaning agent, comprising the following steps:
S1, according to cleaning agent formula, configured the raw material of associated weight；
S2, in a kettle, be added triethylene glycol butyl ether, isomerous tridecanol polyoxyethylene, isomery nonylphenol polyoxyethylene ether,
Ethoxylated dodecyl alcohol, be mixed 5min, after obtain mixed solution A；
S3, alkyl glycosides, cocinic acid potash soap are continuously added into reaction kettle, stir 8min, continuously add chelating titanate
Coupling agent continues to stir 10min, sodium citrate is added, obtains mixed solution B after mixing evenly；
S4, after mixed solution B is cooled to room temperature, deionized water is added, stirs evenly, adds sodium citrate, adjust PH to
Neutrality is filtered with 200 mesh nylon screens to get the down jacket cleaning agent is arrived.
Embodiment 3
A kind of down jacket cleaning agent, the raw material including following mass percents: alkyl glycosides 8%, isomerous tridecanol polyoxyethylene ether
7%, cocinic acid potash soap 7%, isomery nonylphenol polyoxyethylene ether 8%, ethoxylated dodecyl alcohol 6%, chelating titanate coupling
Agent 0.3%, sodium citrate 2%, triethylene glycol butyl ether 2%, remaining is deionized water.
The alkyl glycosides be atomic number of alkyl carbon be 12, atomic number of alkyl carbon is any one of 14 alkyl glycosides.
A kind of preparation method of down jacket cleaning agent, comprising the following steps:
S1, according to cleaning agent formula, configured the raw material of associated weight；
S2, in a kettle, be added triethylene glycol butyl ether, isomerous tridecanol polyoxyethylene, isomery nonylphenol polyoxyethylene ether,
Ethoxylated dodecyl alcohol, be mixed 4min, after obtain mixed solution A；
S3, alkyl glycosides, cocinic acid potash soap are continuously added into reaction kettle, stir 6min, continuously add chelating titanate
Coupling agent continues to stir 8min, sodium citrate is added, obtains mixed solution B after mixing evenly；
S4, after mixed solution B is cooled to room temperature, deionized water is added, stirs evenly, adds sodium citrate, adjust PH to
Neutrality is filtered with 200 mesh nylon screens to get the down jacket cleaning agent is arrived.
Comparative example 1
Chelating titanate coupling agent is not added, remaining condition is consistent with embodiment 3.
Comparative example 2
Alkyl glycosides, cocinic acid potash soap, chelating titanate coupling agent are not added, remaining condition is consistent with embodiment 3.
Comparative example 3
Be not added isomerous tridecanol polyoxyethylene, isomery nonylphenol polyoxyethylene ether, ethoxylated dodecyl alcohol, remaining condition and
Embodiment 3 is consistent.
Test one: clean effect test
(1) clean effect comparative test
1, test specimen: cleaning agent, standard liquid detergent and contrast product 1 provided in an embodiment of the present invention (open a meter three times and wash king
Neutral laundry liquid).
2, test principle and method: GB/T 13174-2008 dress material detergent detergency and the survey for recycling scourability
Determine method and QB/T 1224-2012 dress material washes agent by liquid.
3, test result: it is detailed in the following table 1.Wherein, detergency experimental concentration is 0.1%, standard liquid detergent experimental concentration is
0.2%；JB-01 --- carbon black greasy dirt cloth；JB-02 --- albumen soiled cotton；JB-03 --- sebum soiled cotton.Collar detergency country mark
Quasi- parameter index requires as follows: tri- kinds of test soiled cottons of JB-01, JB-02, JB-03 are all larger than or are equal to standard liquid detergent.
Table 1
Detergency is a most important index of product quality, and general dirt-removing power is higher, and the quality of product is better.From upper table
1 test result is it is found that the detergency effect of rinse product provided in an embodiment of the present invention is good, wherein JB-01 soiled cotton decontamination
Power is up to 8.66%~8.98%；JB-02 soiled cotton detergency is up to 8.00%~8.38%；JB-03 soiled cotton detergency up to 7.12%~7.45%,
It is above contrast product and standard liquid detergent, while after lacking related component, dirt-removing power is decreased obviously.Therefore, of the invention
A variety of surfactants and chelating titanate coupling agent in the cleaning agent of embodiment offer have synergistic effect, can be effective
Ground removes the spot in clothing, and under comparable conditions, clean effect is very good.
(2) clean effect endurance life test
1, test specimen: rinse product, standard liquid detergent and contrast product provided in an embodiment of the present invention (open a meter three times to wash
King's neutral laundry liquid).
2, test method: above-mentioned test products being placed under the conditions of room temperature (20 DEG C~30 DEG C) and are stored, and was taken out every 6 months
Sample, and detergency measure of merit is carried out using the test method of above-mentioned test (one) and is recorded, off-test after 12 months.
3, the following table 2, table 3 and table 4 test result: are detailed in.
2 detergency comparison result of table (initial storage)
3 detergency comparison result of table (after storage 6 months)
4 detergency comparison result of table (after storage 12 months)
It is found that cleaning agent provided in an embodiment of the present invention places 6 at room temperature from the test result of upper table 2,3,4
Month, after 12 months, decontamination force value (JB-01, JB-02, JB-03) amplitude of variation is little, and the persistence of clean effect is good, because
This, cleaning agent provided in an embodiment of the present invention constructs decontamination body using a variety of surfactants and chelating titanate coupling agent
System, not only clean effect is good, and clean effect influenced by the resting period it is small.
Test five: antiredeposition performance test
1, test specimen: rinse product, standard liquid detergent and contrast product provided in an embodiment of the present invention (open a meter three times and wash king
Neutral laundry liquid).
Cotton fabric and polyester textile (white fabrics)；Human society soil greasy dirt mixing soiling solution :+20% standard human society of 75% deionized water
Native+5% Oil stain mixture (75%+No. 25%26 mineral oil of commercially available ready-mixed oil).
2, test method: preparing 9 washing tanks, and number 1~9, weighs 10g human society soil greasy dirt mixing soiling solution (essence respectively
It really to 0.01g), puts into washing tank, is provided respectively toward the embodiment of the present invention 1~4 that equivalent is added in 1~No. 9 washing tank clear
The cleaning agent that the embodiment of the present invention 1 provides is added in lotion (2g/L), i.e. No. 1 washing tank, and the embodiment of the present invention is added in No. 2 washing tanks
The cleaning agent that comparative example 2 of the present invention provides is added in 2 cleaning agents ... and so on provided, No. 6 washing tanks；No. 8 washing tanks add
Enter standard liquid detergent (2g/L)；No. 9 washing tank additions open a meter three times and wash king's neutral laundry liquid (2g/L).Respectively toward each washing tank
1000mL hard water is added, is packed into spotter, stirs evenly, and under stirring, 7cm × 7cm is added into washing tank respectively
Cotton fabric and polyester textile each 3,20min is then washed under conditions of 30 DEG C, 20min, 120r/min, washing terminates
Afterwards, the test fabric in washing tank is taken out, after clear water rinsed clean, hang airing at room temperature is placed on, visually observes test fabric
The amount of upper deposition soil layer, and evaluated by the way of " ★ " quantity, " ★ " quantity is more, and it is weaker to represent antiredeposition performance.
3, test result: it is detailed in the following table 5.
Table 5
| Test specimen | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 |
| Test result | ★ | ★ | ★ | ★★★★ | ★★★ |
| Test specimen | Comparative example 3 | Open rice | Standard liquid detergent | / | / |
| Test result | ★★★ | ★★★★★★ | ★★★★★★★ | / | / |
In washing process, the spot washed away on clothing is also possible to redeposited on clothing, these, which remain, to make
At clothing jaundice, wear.Antiredeposition is an important indicator for reflecting detergent performance.From the test result of upper table 5
As can be seen that compare Kai meter and standard liquid detergent, the cleaning agent that the embodiment of the present invention 1~4 provides has more preferably to resist to sink again
Product performance is conducive to the pure and fresh cleaning for keeping clothing.
Test six: skin irritation test
1, test specimen: rinse product provided in an embodiment of the present invention.
2, test method: (for age level 18~55, health is non-by 30 volunteers in a certain area of random selection
Constitution sensitive subjects) cleaning agent of the invention is used, daily using once, it is used continuously 3 months, observes and records volunteer daily
Using the skin irritation reaction after cleaning agent hand wash laundry, (skin irritation reaction refers to that during the test subject's connects
There is redness, itch, decortication symptom using the partial skin (such as hand skin) of this product in touching.) and subject wearing make
After the clothing cleaned with cleaning agent of the invention, the irritative response of skin.
3, test result: using excitement percentage value come the effect of evaluation test, wherein excitement index percent value is got over
Greatly, illustrate that the product is big to the irritation of skin；Excitement percent value is smaller, illustrates that the product gets over the irritation of skin
It is small；Specific test result is detailed in the following table 6.
6 use feeling of table (irritation) evaluation result
As can be seen that in actual use, subject is using 1-3 of the embodiment of the present invention from the test result of upper table 6
When the cleaning agent provided with comparative example 1-3, the allergic stimulated of skin is 0, while dressing the clothing after cleaning using this product
Object is still non-stimulated to skin.Therefore, cleaning agent provided in an embodiment of the present invention is mildly non-stimulated to skin, highly-safe.
Cleaning agent of the invention can be removed fast and effeciently various in clothing under the synergistic effect of Surfactant sum
Stain, washing effect are good；In addition, formula is neutral low foam formulations, it is easy to rinsing and noresidue, and mildly stingless to skin
Swash, while not damaging laundry.
It is counted as example embodiment of the invention although having been described and describing, it will be apparent to those skilled in the art that
It can be variously modified and is replaced, without departing from spirit of the invention.Furthermore it is possible to make many modifications with will be special
Condition of pledging love is fitted to religious doctrine of the invention, without departing from invention described herein central concept.So the present invention is unrestricted
In specific embodiment disclosed herein, but the present invention may further include belonging to all embodiments of the scope of the invention and its being equal
Object.
Claims (4)
1. a kind of down jacket cleaning agent, which is characterized in that the raw material including following mass percents: alkyl glycosides 6-12%, isomery
Tridecanol polyoxyethylene ether 15-20%, cocinic acid potash soap 5-10%, isomery nonylphenol polyoxyethylene ether 10-15%, laruyl alcohol are poly-
Ethylene oxide ether 5-10%, chelating titanate coupling agent 0.1-0.5%, sodium citrate 0.1-5%, triethylene glycol butyl ether 1-5%,
Remaining is deionized water.
2. down jacket cleaning agent according to claim 1, which is characterized in that the alkyl glycosides is that atomic number of alkyl carbon is
12, any one of the alkyl glycosides that atomic number of alkyl carbon is 14.
3. down jacket cleaning agent according to claim 1, which is characterized in that the raw material including following mass percents: alkane
Base glucosides 8%, isomerous tridecanol polyoxyethylene ether 7%, cocinic acid potash soap 7%, isomery nonylphenol polyoxyethylene ether 8%, laruyl alcohol
Polyoxyethylene ether 6%, chelating titanate coupling agent 0.3%, sodium citrate 2%, triethylene glycol butyl ether 2%, remaining is deionization
Water.
4. a kind of preparation method of down jacket cleaning agent as described in claim 1, which comprises the following steps:
S1, according to cleaning agent formula, configured the raw material of associated weight；
S2, in a kettle, be added triethylene glycol butyl ether, isomerous tridecanol polyoxyethylene, isomery nonylphenol polyoxyethylene ether,
Ethoxylated dodecyl alcohol, be mixed 2-5min, after obtain mixed solution A；
S3, alkyl glycosides, cocinic acid potash soap are continuously added into reaction kettle, stir 5-8min, continuously add chelating type metatitanic acid
Ester coupling agent continues to stir 5-10min, sodium citrate is added, obtains mixed solution B after mixing evenly；
S4, after mixed solution B is cooled to room temperature, deionized water is added, stirs evenly, adds sodium citrate, adjust PH to
Neutrality is filtered with 200 mesh nylon screens to get the down jacket cleaning agent is arrived.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910000339.4A CN109609301A (en) | 2019-01-02 | 2019-01-02 | A kind of down jacket cleaning agent and its preparation process |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910000339.4A CN109609301A (en) | 2019-01-02 | 2019-01-02 | A kind of down jacket cleaning agent and its preparation process |
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| Publication Number | Publication Date |
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| CN109609301A true CN109609301A (en) | 2019-04-12 |
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| CN201910000339.4A Pending CN109609301A (en) | 2019-01-02 | 2019-01-02 | A kind of down jacket cleaning agent and its preparation process |
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Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105754736A (en) * | 2014-12-16 | 2016-07-13 | 刘方旭 | Down jacket cleaning agent composition |
-
2019
- 2019-01-02 CN CN201910000339.4A patent/CN109609301A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105754736A (en) * | 2014-12-16 | 2016-07-13 | 刘方旭 | Down jacket cleaning agent composition |
Non-Patent Citations (1)
| Title |
|---|
| 廖文胜编: "《液体洗涤剂-新原料•新配方（第2版）》", 31 January 2005, 化学工业出版社 * |
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