CN109603716A - A kind of interleaving agent continuous production device and its control system - Google Patents
A kind of interleaving agent continuous production device and its control system Download PDFInfo
- Publication number
- CN109603716A CN109603716A CN201811581269.8A CN201811581269A CN109603716A CN 109603716 A CN109603716 A CN 109603716A CN 201811581269 A CN201811581269 A CN 201811581269A CN 109603716 A CN109603716 A CN 109603716A
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- reactor
- interleaving agent
- silicone oil
- continuous production
- pure water
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/38—Polysiloxanes modified by chemical after-treatment
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00054—Controlling or regulating the heat exchange system
- B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
- B01J2219/00058—Temperature measurement
Abstract
The present invention provides a kind of interleaving agent continuous production device and its control systems, are related to interleaving agent production technical field.The present invention, reactor (1) can heat；Reactor (1) is connect with colloid mill (6) by pipeline, colloid mill (6) is connect with agitator tank (9) by pipeline, heat exchanger (10) is connect with agitator tank (9), and the pure water of heating can be passed through to agitator tank (9).Compared with prior art, the present invention, in reactor, the extent of reaction reaches 90%, in agitator tank, material specific surface area is big, reaches certain temperature, and reaction can continue to carry out to fully reacting, material does not stop in reactor, moreover, have corresponding control system, it is different according to the requirement concentration of interleaving agent produced, according to proportion, it can control stoste, the additional amount of pure water, directly dilute the interleaving agent for producing various specifications requirement, continuous production, high production efficiency, equipment is simple, easy to operate, saves manpower.
Description
Technical field
The present invention relates to interleaving agent production technical field, in particular to a kind of interleaving agent continuous production device and its control system
System.
Background technique
Interleaving agent is a kind of semipermanent tyre capsule vulcanization interleaving agent, contains active silicon polymer.It is suitable for meridian
It is isolated when line tyre capsule and bias tire bladder curing, isolation effect is excellent, not will cause starved, joint cracking, delamination, plays spot
And other issues.There is good slipping property and isolation between capsule and green tire.Generally, product be divided into 2 times be watered, 1 times
It is watered and is not watered three types.
Interleaving agent manufacturer mostly uses greatly Batch Process mode to be produced at present, i.e., into reaction kettle be added silicone oil,
The raw materials such as activating agent, are reacted under certain condition, and when reaction is completed, after being delivered to grinder grinding, then agitated tank is stirred
Mix to obtain reaction stoste, stoste directly transported into storing in finished pot, or according to product design require for stoste to be watered into
Row dilution.This production method major defect is that production efficiency is low.Batch production is mainly following reasons: being on the one hand desirable
Reaction completely in a kettle, the reaction time is long, subsequent not have reaction required temperature；It on the other hand is the arrangement of workshop appliance
Lead to the discontinuous of dilution operation.
Summary of the invention
The present invention provides a kind of interleaving agent continuous production device and its control systems, solve above-mentioned technical problem.
Specific technical solution is a kind of interleaving agent continuous production device, comprising: reactor, colloid mill, pipeline pump,
Heat exchanger, agitator tank；Wherein, reactor includes: driving motor, gear-box, shell of reactor, screw rod；Agitator tank includes: stirring
Motor and agitating paddle；Feeder, silicone oil regulating valve, silicone oil flowmeter, conduction oil regulating valve, temperature of reactor meter, pure water valve
Door, pure water ga(u)ge, stock solution flow meter, steam control valve, pure water thermometer.
Driving motor is connect by gear-box with the screw rod in reactor；Reactor discharge port and colloid mill pass through pipe
Road connection, colloid mill are connect with agitator tank by pipeline, and pipeline pump, stock solution flow meter are mounted on colloid mill and stirring
Between tank in connecting pipe.Pipeline pump is mounted on the back of colloid mill, and pipeline pump can provide power for the material in pipeline,
Guarantee that material has certain flow velocity.
Heat exchanger is connect with agitator tank；Shell of reactor is located at the outside of reactor, and shell of reactor is hollow structure, has
Inner and outer wall；Feeder is mounted on the inner wall of connection shell of reactor above the front end of reactor；Silicone oil regulating valve, silicone oil stream
Meter is mounted on the silicone oil inlet duct for being passed through shell of reactor inner wall；Conduction oil regulating valve, which is mounted on, is passed through shell of reactor
Heat conducting oil inlet pipeline on；Temperature of reactor meter is installed in the reactor；Agitating paddle, agitating paddle and stirring are installed in agitator tank
Motor connection；Pure water thermometer, pure penstock, pure water ga(u)ge are mounted between heat exchanger and agitator tank；Steam tune
Section valve is mounted on the valve steam inlet of heat exchanger.
The interior pars intramuralis of shell of reactor is equipped with screw rod, is equipped with silicone oil inlet duct and feeder above the front end of screw rod,
Solid material can be added in feeder；The front bottom end of reactor is equipped with heat conducting oil inlet, goes out above rear end equipped with conduction oil
Mouthful.Fluid channel is formd between the inner and outer wall of shell of reactor, is passed through conduction oil, screw rod and its interior material can be carried out
Heating.The Position Design of conduction oil entrance, lower section go out into top, can make full use of conduction oil bring heat.
Raw material has heating, is quickly reacted, degree of reaction can achieve in a short time under the stirring of reactor inner screw
90%；Storeroom will appear agglomeration, and by colloid mill, agglomeration is grated.
Pure water enters in agitator tank after being heated by heat exchanger, carries out in tank in proportion with the stoste of pipeline pump conveying
It stirs evenly；Temperature can reach reaction temperature requirement, and the material of not yet fully reacting will continue to react.According to it is produced every
Requirement concentration from agent is different, can control the additional amount of pure water, directly dilutes the interleaving agent for producing various specifications requirement.
Further, shell of reactor wall thickness 5-15cm.
It further, is 2~3mm at a distance from inner wall at the outer most edge of screw rod.It on the one hand is preferably to be heated for material,
On the other hand, guarantee that screw rod acts on the shear-mixed of material, make material fast reaction.
A kind of interleaving agent continuous production control system, the control system include a kind of above-mentioned interleaving agent continuous production dress
It sets.The control system includes: silicone oil control subsystem, feeder control subsystem, conduction oil control subsystem, automatic steam control
System, interleaving agent deploy subsystem；Specifically, silicone oil control subsystem includes: silicone oil regulating valve, silicone oil flowmeter；Feeder
Control subsystem includes: silicone oil flowmeter, feeder；Conduction oil control subsystem includes: conduction oil regulating valve, temperature of reactor
Meter composition；Steam control subsystem includes: steam control valve, pure water thermometer；It includes: pure water that interleaving agent, which deploys subsystem,
Valve, pure water ga(u)ge and stock solution flow meter.
Further, controller controls the aperture of silicone oil regulating valve according to silicone oil flowmeter.Controller is according to technique initialization
Silicone oil discharge quantity and silicone oil flowmeter value of feedback PID control is carried out to silicone oil regulating valve, the output signal of PID control controls silicon
The opening size of oily regulating valve.
Further, controller controls the discharge quantity of feeder according to the flow and proportion scale of silicone oil flowmeter.Control
Device carries out ratio control to feeder according to the actual flow that the proportion scale and silicone oil flow measurement of technique initialization obtain, control
The discharge quantity of output signal control feeder.
Further, controller controls the aperture of conduction oil regulating valve according to temperature of reactor meter.Controller is according to technique
The temperature of reactor and temperature of reactor meter value of feedback of setting carry out PID control, the output letter of PID control to conduction oil regulating valve
Number control conduction oil regulating valve opening size.
Further, controller controls the aperture of steam control valve according to pure water thermometer.Controller is set according to technique
Fixed pure coolant-temperature gage and pure water thermometer value of feedback carries out PID control, the output signal control of PID control to steam control valve
The opening size of steam control valve processed.
Further, controller controls pure penstock according to the flow of pure water ga(u)ge and stock solution flow meter.Control
Device carries out pure penstock according to the actual flow that the stoste of technique initialization and the ratio of pure water and stock solution flow measure
Ratio control, the output signal of control control the aperture of pure water regulating valve.
Due to using above technical scheme, compared with prior art, the present invention, in reactor, the extent of reaction reaches
90%, in agitator tank, material specific surface area is big, reaches certain temperature, and reaction can continue to carry out to fully reacting, and material exists
It is not stopped in reactor, it is different according to the requirement concentration of interleaving agent produced moreover, there is corresponding control system, according to matching
Than can control stoste, the additional amount of pure water, directly diluting the interleaving agent for producing various specifications requirement, continuous production is raw
Produce high-efficient, equipment is simple, and it is easy to operate, save manpower.
Detailed description of the invention
The attached drawing constituted part of this application is used to provide further understanding of the present invention, schematic reality of the invention
It applies example and its explanation is used to explain the present invention, do not constitute improper limitations of the present invention.In the accompanying drawings:
Fig. 1 is a kind of schematic diagram of interleaving agent continuous production device of the present invention.
Fig. 2 is the schematic diagram of control system of the present invention.
Wherein: 1, reactor, 3, feeder, 6, colloid mill, 7, pipeline pump, 9, agitator tank, 10, heat exchanger, 11, control
Device processed, 101, driving motor, 102, gear-box, 103, shell of reactor, 104, screw rod, 201, silicone oil regulating valve, 202, silicone oil
Flowmeter, 401, conduction oil regulating valve, 402, temperature of reactor meter, 501, pure penstock, 502, pure water ga(u)ge, 504,
Stock solution flow meter, 801, steam control valve, 802, pure water thermometer, 901, stirring motor, 902, agitating paddle.
Specific embodiment
To make the objectives, technical solutions, and advantages of the present invention clearer, right below with reference to embodiment and attached drawing
The present invention is described in further detail.Here, exemplary embodiment and its explanation of the invention is used to explain the present invention, but simultaneously
It is not as a limitation of the invention.Here is the description carried out in conjunction with attached drawing to the present invention:
Such as attached drawing 1, a kind of interleaving agent continuous production device, comprising: reactor 1, colloid mill 6, pipeline pump 7, heat exchange
Device 10, agitator tank 9；Wherein, reactor 1 includes: driving motor 101, gear-box 102, shell of reactor 103, screw rod 104；It stirs
Mixing tank 9 includes: stirring motor 901 and agitating paddle 902；Feeder 3, silicone oil regulating valve 201, silicone oil flowmeter 202, conduction oil tune
Valve 401, temperature of reactor meter 402, pure penstock 501, pure water ga(u)ge 502, stock solution flow meter 504, steam is saved to adjust
Valve 801, pure water thermometer 802.
Driving motor 101 is connect by gear-box 102 with the screw rod 104 in reactor 1；1 discharge port of reactor and colloid
Grinder 6 is connected by pipeline, and colloid mill 6 is connect with agitator tank 9 by pipeline, and pipeline pump 7, stock solution flow meter 504 are pacified
Between colloid mill 6 and agitator tank 9 in connecting pipe；Heat exchanger 10 is connect with agitator tank 9；Shell of reactor 103 is located at
The outside of reactor 1, shell of reactor 103 are hollow structures, there is inner and outer wall；Feeder 3 is mounted on the front end of reactor 1
The inner wall of top connection shell of reactor 103；Silicone oil regulating valve 201, silicone oil flowmeter 202 are mounted on and are passed through shell of reactor
On the silicone oil inlet duct of 103 inner walls；Conduction oil regulating valve 401 is mounted on the heat conducting oil inlet pipe for being passed through shell of reactor 103
On road；Temperature of reactor meter 402 is installed in reactor 1；Agitating paddle 902, agitating paddle 902 and stirring electricity are installed in agitator tank 9
Machine 901 connects；Pure water thermometer 802, pure penstock 501, pure water ga(u)ge 502 are mounted on heat exchanger 10 and agitator tank
Between 9；Steam control valve 801 is mounted on the valve steam inlet of heat exchanger 10.
Further, 103 wall thickness 5-15cm of shell of reactor.
It further, is 2~3mm at a distance from inner wall at the outer most edge of screw rod.
A kind of interleaving agent continuous production control system, the control system include a kind of above-mentioned interleaving agent continuous production dress
It sets.The control system includes: silicone oil control subsystem, feeder control subsystem, conduction oil control subsystem, automatic steam control
System, interleaving agent deploy subsystem；Specifically, silicone oil control subsystem includes: silicone oil regulating valve 201, silicone oil flowmeter 202；
Feeder control subsystem includes: silicone oil flowmeter 202, feeder 3；Conduction oil control subsystem includes: conduction oil regulating valve
401, temperature of reactor meter 402 forms；Steam control subsystem includes: steam control valve 801, pure water thermometer 802；Isolation
It includes: pure penstock 501, pure water ga(u)ge 502 and stock solution flow meter 504 that subsystem is deployed in agent.
Specifically, controller 11 controls the aperture of silicone oil regulating valve 201 according to silicone oil flowmeter 202.11 basis of controller
The discharge quantity of flow and proportion scale the control feeder 3 of silicone oil flowmeter 202.Controller 11 is according to temperature of reactor meter 402
Control the aperture of conduction oil regulating valve 401.Controller 11 controls the aperture of steam control valve 801 according to pure water thermometer 802.
Controller 11 controls pure penstock 501 according to the flow of pure water ga(u)ge 502 and stock solution flow meter 504.
Embodiment 1: production is not watered the interleaving agent of type, first sets each material amounts according to formula, and set temperature is 80 DEG C；
Conduction oil regulating valve 401 is first opened, conduction oil, which enters, preheats screw rod 104；Silicone oil regulating valve 201, feeder 3, original are opened again
Flow meters 504, steam control valve 801, pure penstock 501, raw material are added to reactor 1, open motor 101 and pass through gear
Case 102 drives the rotation of screw rod 104, and raw material starts to react under stiring, has heating, quickly reacted, degree of reaction is in short-term
It is interior to can achieve 90%；Storeroom will appear agglomeration, and material is delivered to colloid mill 6 by reactor 1, grind agglomeration object
Material, increases the specific surface area of material；Material is pumped into agitator tank 9 by pipeline pump 7, under the effect of agitating paddle 902, there is certain temperature
Degree, reaction continue to complete reaction；It exports and stores.It is not watered in the interleaving agent production of type and needs to add suitable quantity of water, this is anti-
It should be able to be carried out continuously.
Embodiment 2: production W-1620D4 D5 (2 times are watered type) interleaving agent, output is identical, on the basis of embodiment 1
On, controller 11 carries out PID control to silicone oil regulating valve 201 according to silicon oil dosage and 202 value of feedback of silicone oil flowmeter, appropriate to adjust
The aperture of small silicone oil regulating valve 201；The reality that controller 11 is measured according to the proportion scale and silicone oil flowmeter 202 of technique initialization
Flow carries out ratio control, the discharge quantity of the output signal control feeder 3 of control to feeder 3；Controller 11 is according to technique
80 DEG C of the temperature of reactor of setting and 402 value of feedback of temperature of reactor meter carry out PID control, PID control to conduction oil regulating valve 401
The opening size of the output signal control conduction oil regulating valve 401 of system, make 402 test temperature of temperature of reactor meter maintain 80 ±
5℃；Controller 11 is according to 80 DEG C of the pure coolant-temperature gage and 802 value of feedback of pure water thermometer of technique initialization to steam control valve
801 carry out PID control, and the opening size of the output signal control steam control valve 801 of PID control makes pure water thermometer 802
Test temperature maintains 80 ± 5 DEG C；Controller 11 is according to the stoste of technique initialization and the ratio of pure water and stock solution flow meter 504
The actual flow measured controls pure penstock 501.Wherein, the increment of pure water is larger, reaches 80 DEG C of water temperature, steams
The aperture of steam control valve 801 can also increase accordingly.
Claims (9)
1. a kind of interleaving agent continuous production device, comprising: reactor (1), colloid mill (6), pipeline pump (7), heat exchanger
(10), agitator tank (9)；Wherein, reactor (1) include: driving motor (101), gear-box (102), shell of reactor (103),
Screw rod (104)；Agitator tank (9) includes: stirring motor (901) and agitating paddle (902)；It is characterized in that,
Further include: feeder (3), silicone oil regulating valve (201), silicone oil flowmeter (202), conduction oil regulating valve (401), reactor
Thermometer (402), pure penstock (501), pure water ga(u)ge (502), stock solution flow meter (504), steam control valve
(801), pure water thermometer (802)；
Driving motor (101) is connect by gear-box (102) with the screw rod (104) in reactor (1)；Reactor (1) discharge port
It is connect with colloid mill (6) by pipeline, colloid mill (6) is connect with agitator tank (9) by pipeline, pipeline pump (7), original
Flow meters (504) are mounted between colloid mill (6) and agitator tank (9) in connecting pipe；Heat exchanger (10) and agitator tank (9)
Connection；
Shell of reactor (103) is located at the outside of reactor (1), and shell of reactor (103) is hollow structure, there is inner wall and outer
Wall；Feeder (3) is mounted on the inner wall of connection shell of reactor (103) above the front end of reactor (1)；Silicone oil regulating valve
(201), silicone oil flowmeter (202) is mounted on the silicone oil inlet duct for being passed through shell of reactor (103) inner wall；Conduction oil is adjusted
Valve (401) is mounted on the heat conducting oil inlet pipeline for being passed through shell of reactor (103)；Temperature of reactor meter (402) is mounted on instead
It answers in device (1)；Agitating paddle (902) are installed in agitator tank (9), agitating paddle (902) is connect with stirring motor (901)；Pure water temperature
Degree meter (802), pure penstock (501), pure water ga(u)ge (502) are mounted between heat exchanger (10) and agitator tank (9)；It steams
Steam control valve (801) is mounted on the valve steam inlet of heat exchanger (10).
2. a kind of interleaving agent continuous production device according to claim 1, which is characterized in that shell of reactor (103) wall
Thick 5-15cm.
3. a kind of interleaving agent continuous production device according to claim 1, which is characterized in that at the outer most edge of screw rod with it is interior
The distance of wall is 2~3mm.
4. a kind of interleaving agent continuous production control system, which is characterized in that the control system includes any institute of claims 1 to 3
A kind of interleaving agent continuous production device stated；
The control system includes: silicone oil control subsystem, feeder control subsystem, conduction oil control subsystem, automatic steam control
Subsystem, interleaving agent deploy subsystem；
Silicone oil control subsystem includes: silicone oil regulating valve (201), silicone oil flowmeter (202)；
Feeder control subsystem includes: silicone oil flowmeter (202), feeder (3)；
Conduction oil control subsystem includes: conduction oil regulating valve (401), temperature of reactor meter (402) composition；
Steam control subsystem includes: steam control valve (801), pure water thermometer (802)；
It includes: pure penstock (501), pure water ga(u)ge (502) and stock solution flow meter (504) that interleaving agent, which deploys subsystem,.
5. a kind of interleaving agent continuous production control system according to claim 4, which is characterized in that controller (11) basis
Silicone oil flowmeter (202) controls the aperture of silicone oil regulating valve (201).
6. a kind of interleaving agent continuous production control system according to claim 4, which is characterized in that controller (11) basis
The discharge quantity of flow and the proportion scale control feeder (3) of silicone oil flowmeter (202).
7. a kind of interleaving agent continuous production control system according to claim 4, which is characterized in that controller (11) basis
Temperature of reactor meter (402) controls the aperture of conduction oil regulating valve (401).
8. a kind of interleaving agent continuous production control system according to claim 4, which is characterized in that controller (11) basis
Pure water thermometer (802) controls the aperture of steam control valve (801).
9. a kind of interleaving agent continuous production control system according to claim 4, which is characterized in that controller (11) basis
The flow of pure water ga(u)ge (502) and stock solution flow meter (504), controls pure penstock (501).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811581269.8A CN109603716B (en) | 2018-12-24 | 2018-12-24 | Continuous production device for separant and control system thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811581269.8A CN109603716B (en) | 2018-12-24 | 2018-12-24 | Continuous production device for separant and control system thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109603716A true CN109603716A (en) | 2019-04-12 |
| CN109603716B CN109603716B (en) | 2020-09-04 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201811581269.8A Active CN109603716B (en) | 2018-12-24 | 2018-12-24 | Continuous production device for separant and control system thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2020132910A1 (en) * | 2018-12-26 | 2020-07-02 | 山东万圣博化工有限公司 | Device for continuously producing separant and control system therefor |
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| US3130070A (en) * | 1960-08-10 | 1964-04-21 | Potters Robert | Coating method and apparatus |
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| CN109603716B (en) | 2020-09-04 |
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