CN109573944A - 一种连续式催化木醋液重整制氢的反应装置及方法 - Google Patents
一种连续式催化木醋液重整制氢的反应装置及方法 Download PDFInfo
- Publication number
- CN109573944A CN109573944A CN201811543644.XA CN201811543644A CN109573944A CN 109573944 A CN109573944 A CN 109573944A CN 201811543644 A CN201811543644 A CN 201811543644A CN 109573944 A CN109573944 A CN 109573944A
- Authority
- CN
- China
- Prior art keywords
- fluidized
- wood vinegar
- bed reactor
- gas
- tank
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 title claims abstract description 62
- 239000001257 hydrogen Substances 0.000 title claims abstract description 58
- 229910052739 hydrogen Inorganic materials 0.000 title claims abstract description 58
- 235000021419 vinegar Nutrition 0.000 title claims abstract description 51
- 239000000052 vinegar Substances 0.000 title claims abstract description 51
- 239000002023 wood Substances 0.000 title claims abstract description 49
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 28
- 238000000034 method Methods 0.000 title claims abstract description 25
- 238000006555 catalytic reaction Methods 0.000 title claims abstract description 24
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 24
- 239000007789 gas Substances 0.000 claims abstract description 65
- 239000003054 catalyst Substances 0.000 claims abstract description 30
- 239000012159 carrier gas Substances 0.000 claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 38
- 239000007788 liquid Substances 0.000 claims description 18
- 229910052757 nitrogen Inorganic materials 0.000 claims description 14
- 229910001873 dinitrogen Inorganic materials 0.000 claims description 10
- 150000002431 hydrogen Chemical class 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 6
- 238000001514 detection method Methods 0.000 claims description 4
- 230000008016 vaporization Effects 0.000 claims description 4
- 239000012530 fluid Substances 0.000 claims description 3
- 230000000630 rising effect Effects 0.000 claims description 3
- 238000009834 vaporization Methods 0.000 claims description 3
- 238000004458 analytical method Methods 0.000 claims description 2
- -1 is reacted Substances 0.000 claims description 2
- 238000010792 warming Methods 0.000 claims description 2
- 239000002826 coolant Substances 0.000 claims 1
- 230000002779 inactivation Effects 0.000 abstract description 9
- 238000002407 reforming Methods 0.000 abstract description 3
- 239000000047 product Substances 0.000 description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- 229910052799 carbon Inorganic materials 0.000 description 6
- 238000001833 catalytic reforming Methods 0.000 description 4
- 238000009826 distribution Methods 0.000 description 4
- 229930195733 hydrocarbon Natural products 0.000 description 3
- 150000002430 hydrocarbons Chemical class 0.000 description 3
- 238000006057 reforming reaction Methods 0.000 description 3
- 238000001816 cooling Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000000197 pyrolysis Methods 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000007233 catalytic pyrolysis Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000005243 fluidization Methods 0.000 description 1
- 238000004868 gas analysis Methods 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 238000012802 pre-warming Methods 0.000 description 1
- 230000000750 progressive effect Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
- C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
- C01B3/32—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air
- C01B3/323—Catalytic reaction of gaseous or liquid organic compounds other than hydrocarbons with gasifying agents
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
- C01B2203/02—Processes for making hydrogen or synthesis gas
- C01B2203/0205—Processes for making hydrogen or synthesis gas containing a reforming step
- C01B2203/0227—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step
- C01B2203/0233—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step the reforming step being a steam reforming step
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/141—Feedstock
- Y02P20/145—Feedstock the feedstock being materials of biological origin
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Inorganic Chemistry (AREA)
- Hydrogen, Water And Hydrids (AREA)
- Catalysts (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Abstract
Description
Claims (9)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201811543644.XA CN109573944B (zh) | 2018-12-17 | 2018-12-17 | 一种连续式催化木醋液重整制氢的反应装置及方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201811543644.XA CN109573944B (zh) | 2018-12-17 | 2018-12-17 | 一种连续式催化木醋液重整制氢的反应装置及方法 |
Publications (2)
Publication Number | Publication Date |
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CN109573944A true CN109573944A (zh) | 2019-04-05 |
CN109573944B CN109573944B (zh) | 2020-09-11 |
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CN201811543644.XA Active CN109573944B (zh) | 2018-12-17 | 2018-12-17 | 一种连续式催化木醋液重整制氢的反应装置及方法 |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111073675A (zh) * | 2019-12-24 | 2020-04-28 | 山东理工大学 | 一种连续式木质素催化热解制取富烃生物油的装置与方法 |
CN112573481A (zh) * | 2020-12-28 | 2021-03-30 | 常州市蓝博净化科技有限公司 | 一种阶梯式缓慢变温甲醇制氢生产线 |
-
2018
- 2018-12-17 CN CN201811543644.XA patent/CN109573944B/zh active Active
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111073675A (zh) * | 2019-12-24 | 2020-04-28 | 山东理工大学 | 一种连续式木质素催化热解制取富烃生物油的装置与方法 |
CN112573481A (zh) * | 2020-12-28 | 2021-03-30 | 常州市蓝博净化科技有限公司 | 一种阶梯式缓慢变温甲醇制氢生产线 |
CN112573481B (zh) * | 2020-12-28 | 2023-09-05 | 常州市蓝博氢能源科技有限公司 | 一种阶梯式缓慢变温甲醇制氢生产线 |
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CN109573944B (zh) | 2020-09-11 |
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GR01 | Patent grant | ||
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CB03 | Change of inventor or designer information | ||
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Inventor after: Li Zhihe Inventor after: Zhang Andong Inventor after: Yi Weiming Inventor after: Wei Zhenwen Inventor after: Fu Peng Inventor after: Li Yongjun Inventor after: Wang Lihong Inventor after: Li Ning Inventor after: Liang Changming Inventor before: Li Zhihe Inventor before: Zhang Andong Inventor before: Yi Weiming Inventor before: Fu Peng Inventor before: Li Yongjun Inventor before: Wang Lihong Inventor before: Li Ning Inventor before: Liang Changming |