CN109554105A - A kind of environment-friendly type aqueous paint and its production technology - Google Patents
A kind of environment-friendly type aqueous paint and its production technology Download PDFInfo
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- CN109554105A CN109554105A CN201811396829.2A CN201811396829A CN109554105A CN 109554105 A CN109554105 A CN 109554105A CN 201811396829 A CN201811396829 A CN 201811396829A CN 109554105 A CN109554105 A CN 109554105A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/14—Polyurethanes having carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
- C08K2003/3045—Sulfates
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses a kind of environment-friendly type aqueous paint and its production technologies.It is characterized in that being made of the raw material that following weight matches: waterborne polyurethane modified acrylic emulsion 45-50%, defoaming agent 0.1-0.2%, dimethylethanolamine 0.1-0.2%, dispersing agent 0.5-2%, fungicide 0.1-0.2%, titanium dioxide 22%, filler 5-10%, aqueous epoxy emulsion 5%, wetting agent 0.2-0.5%, film forming agent 3-5.5%, thickener 0.5-1%, deionized water 10-15%.The present invention also provides the production technology of above-mentioned water paint.The present invention, as solvent, has many advantages, such as environmental protection, low irritant smell, simple and safe operation using deionized water, is suitble to large-scale production.The present invention is not necessarily to crosslinking agent, and prepared water paint property is stable, can save for a long time, have good heat resistance, wearability, anticorrosive property.Water paint disclosed in this invention must paint adhesive force with stronger, provide a kind of high-intensitive, high rigidity and strong water resistance novel environment-friendly water paint.
Description
Technical field
The present invention relates to paint fields, and in particular to a kind of environment-friendly type aqueous paint and its production technology.The water paint is applicable in
In substrates such as most of common iron, timber, macromolecule resins.
Background technique
A large amount of organic solvent is added based on nitrate paint, Polyester Paint in oil paint in manufacture and dilution, these
If solvent prolonged stay can cause great damage to human health in interior.Therefore, oil paint is also assigned that " stealth is killed
The title of hand ".Presence in view of the above problems, research and use are harmless, and free from environmental pollution, paint film is plentiful, sparkling and crystal-clear
It is bright, flexibility is good and has the characteristics that water-fast, wear-resisting, ageing-resistant, color inhibition, fast drying, water paint easy to use obtain
Concern and development.
Water paint has apparent advantage in the following aspects: (1) environmentally friendly.Water paint is then using clear water as uniquely
It is minimum to have brushed dry rear harm to the human body for diluent.(2) energy saving.Water paint needs to provide from fossil in addition to resin and part of auxiliary
Outside refining in source, solvent is water, has saved a large amount of valuable petroleum resources.(3) it does not burn.Using clear water as the Waterborne wood of diluent
Device paint fundamentally solves this hidden danger.(4) performance is stable and flexibility is good.However, restricting asking for water paint development at present
Topic is that its adhesive force, wearability and chemical resistance are poor.
To solve the above-mentioned problems, the invention discloses a kind of environment-friendly type aqueous paint and its production technologies.With it is similar specially
Benefit (application number: 201711412689.9) different places is, the present invention be one-component system, without add isocyanates or
Coupling agent solidification.With same domain patent (application number: compared with 201810007580.5), the present invention without adding aqueous drier,
Also it can achieve the effect that quick surface drying.
Summary of the invention
The present invention provide a kind of property is stable, can save for a long time, have good heat resistance, wearability, anticorrosive property,
High-intensitive, high rigidity and strong water resistance novel environment-friendly water paint, can effectively improve paint adhesive force.
The technical solution that the application takes is as follows: a kind of environment-friendly type aqueous paint, the water paint are matched by following weight
Raw material is made: waterborne polyurethane modified acrylic emulsion 45-50%, defoaming agent 0.1-0.2%, dispersing agent 0.5-2%, fungicide
0.1-0.2%, titanium dioxide 22%, filler 5-10%, aqueous epoxy emulsion 5%, wetting agent 0.2-0.5%, film forming agent 3-5.5% increase
Thick dose of 0.5-1%, deionized water 10-15%；The water paint is one-component system, solid without adding isocyanates or coupling agent
Change, without the aqueous drier of addition.Wherein, the specific ingredient of the water paint is,
(1) main component of waterborne polyurethane modified acrylic emulsion used in is 1515 resins (Ang Gao company).
(2) defoaming agent used in is the one or two of polyether siloxane copolymer or dimethyl silicone polymer.
(3) dispersing agent used in is the one or two of polycarboxylate sodium or lauryl sodium sulfate.
(4) fungicide used in is KBS fungicide (Clariant Corporation).
(5) filler used in be nano barium sulfate or talcum powder one of which or two kinds.
(6) aqueous epoxy emulsion used in is anion epoxy emulsion.
(7) wetting agent used in is polyether silicones.
(8) used film forming agent is one or both of alcohol ester-12 or butyl glycol ether.
(9) thickener used in is one or both of polyurethane or propylene acid & alkali liquid.
A kind of environment-friendly type aqueous paint disclosed in this invention, preparation method are as follows:
Step S1: film forming agent, wetting agent and the deionized water that predetermined weight is matched stir at low speed speed with 600 revs/min
Rate is mixed 10-15 minutes, obtains uniformly mixed mixed liquor；
Step S2: successively by predetermined weight proportion aqueous polyurethane acrylic resin, defoaming agent, dispersing agent, fungicide and
Filler is added in the mixed liquor in above-mentioned steps S1, with ultrasonic high speed dispersion 30 minutes of 1000-1500 revs/min, is divided
Dispersion liquid；
Step S3: the obtained mixed liquor of step S1 is slowly added in the dispersion liquid that step S2 is obtained, low with 600 revs/min
Fast stirring rate is stirred, and mixing time is not less than 10 minutes, until stirring evenly；
Step S4: successively the aqueous epoxy emulsion, film forming agent, thickener of predetermined weight proportion are added in step S3, with 600
Rev/min the rate that stirs at low speed be stirred, until stirring evenly, so that the environment-friendly type aqueous paint be made.
The beneficial effects of the present invention are:
The water paint of the invention is one-component system, solidifies without adding isocyanates or coupling agent, is not necessarily to crosslinking agent,
Without adding aqueous drier, prepared water paint property is stable, can save for a long time, have good heat resistance, is wear-resisting
Property, anticorrosive property.Meanwhile also having many advantages, such as environmental protection, low irritant smell, simple and safe operation, it is suitble to large-scale production.This
The disclosed water paint of invention have it is stronger must paint adhesive force, provide the novel of a kind of high intensity, high rigidity and strong water resistance
Environment-friendly type aqueous paint.
Specific embodiment:
The progress such as technical solution of this name of a young woman are described in detail and completely below in conjunction with specific embodiment.It is following described
Embodiment be a part of the embodiments of the present invention, ask the embodiment being not all of, be merely to illustrate the present invention, rather than limit
The scope of the present invention processed.Based on the embodiments of the present invention, those skilled in the art are without making creative work
It is obtained all for his embodiment, it shall fall within the protection scope of the present invention.Agents useful for same and instrument are can be by commercially available
Channel purchase.
The invention discloses a kind of environment-friendly type aqueous paint, the water paint is made of the raw material that following weight matches: aqueous
Polyurethane-modified acrylic acid lotion 45-50%, defoaming agent 0.1-0.2%, dispersing agent 0.5-2%, fungicide 0.1-0.2%, titanium dioxide
Titanium 22%, filler 5-10%, aqueous epoxy emulsion 5%, wetting agent 0.2-0.5%, film forming agent 3-5.5%, thickener 0.5-1%, go from
Sub- water 10-15%；The water paint is one-component system, aqueous without adding without adding isocyanates or coupling agent solidification
Drier.Wherein, the specific ingredient of the water paint is,
The main component of waterborne polyurethane modified acrylic emulsion used is 1515 resins (Ang Gao company)；
Defoaming agent used is the one or two of polyether siloxane copolymer or dimethyl silicone polymer；
Dispersing agent used is the one or two of polycarboxylate sodium or lauryl sodium sulfate；
Fungicide used is KBS fungicide (Clariant Corporation)；
Filler used be nano barium sulfate or talcum powder one of which or two kinds；
Aqueous epoxy emulsion used is anion epoxy emulsion；
Wetting agent used is polyether silicones；
Used film forming agent is one or both of alcohol ester-12 or butyl glycol ether；
Thickener used is one or both of polyurethane or propylene acid & alkali liquid.
A kind of environment-friendly type aqueous paint disclosed in this invention, preparation method are as follows:
Step S1: film forming agent, wetting agent and the deionized water that predetermined weight is matched stir at low speed speed with 600 revs/min
Rate is mixed 10-15 minutes, obtains uniformly mixed mixed liquor；
Step S2: successively by predetermined weight proportion aqueous polyurethane acrylic resin, defoaming agent, dispersing agent, fungicide and
Filler is added in the mixed liquor in above-mentioned steps S1, with ultrasonic high speed dispersion 30 minutes of 1000-1500 revs/min, is divided
Dispersion liquid；
Step S3: the obtained mixed liquor of step S1 is slowly added in the dispersion liquid that step S2 is obtained, low with 600 revs/min
Fast stirring rate is stirred, and mixing time is not less than 10 minutes, until stirring evenly；
Step S4: successively the aqueous epoxy emulsion, film forming agent, thickener of predetermined weight proportion are added in step S3, with 600
Rev/min the rate that stirs at low speed be stirred, until stirring evenly, so that the environment-friendly type aqueous paint be made.
Embodiment 1
Configure following raw materials according to the weight percent of setting: waterborne polyurethane modified acrylic emulsion (1515 resin) 47% disappears
Infusion polyether siloxane copolymer 0.2%, dispersing agent polycarboxylate sodium 1.0%, fungicide KBS fungicide 0.1%, titanium dioxide
22%, filler talcum powder 5.5%, anion epoxy emulsion 5%, wetting agent polyether silicones 0.2%, film forming agent (alcohol ester-12) 3%, increasing
Thick dose of polyurethane 0.5%, deionized water 15%.
Above-mentioned substance is configured into mixed solution as steps described below, obtains product.
Step S1: film forming agent, wetting agent and the deionized water that above-mentioned predetermined weight is matched, with 600 revs/min of low speed
Stirring rate is mixed 10-15 minutes, obtains uniformly mixed mixed liquor；
Step S2: successively by predetermined weight proportion aqueous polyurethane acrylic resin, defoaming agent, dispersing agent, fungicide and
Filler is added in the mixed liquor in above-mentioned steps S1, with ultrasonic high speed dispersion 30 minutes of 1000-1500 revs/min, is divided
Dispersion liquid；
Step S3: the obtained mixed liquor of step S1 is slowly added in the dispersion liquid that step S2 is obtained, low with 600 revs/min
Fast stirring rate is stirred, and mixing time is not less than 10 minutes, until stirring evenly；
Step S4: successively the aqueous epoxy emulsion, film forming agent, thickener of predetermined weight proportion are added in step S3, with 600
Rev/min the rate that stirs at low speed be stirred, until stirring evenly, so that the environment-friendly type aqueous paint be made.
Embodiment 2
Configure following raw materials according to the weight percent of setting: waterborne polyurethane modified acrylic emulsion (1515 resin) 45% disappears
Infusion polyether siloxane copolymer 0.2%, dispersing agent polycarboxylate sodium 1.7%, fungicide KBS fungicide 0.1%, titanium dioxide
22%, filler nanometer barium sulfate 10%, anion epoxy emulsion 5%, wetting agent polyether silicones 0.5%, film forming agent (alcohol ester-12)
5%, thickener polyurethane 0.5%, deionized water 10%.
Above-mentioned substance is configured into mixed solution according to 1 step of embodiment, obtains product.
Embodiment 3
Configure following raw materials according to the weight percent of setting: waterborne polyurethane modified acrylic emulsion (1515 resin) 50% disappears
Infusion polyether siloxane copolymer 0.1%, dispersing agent lauryl sodium sulfate 1.0%, fungicide KBS fungicide 0.1%, titanium dioxide
Titanium 22%, filler nanometer barium sulfate 7%, anion epoxy emulsion 5%, wetting agent polyether silicones 0.2%, film forming agent (ethylene glycol fourth
Ether) 4%, thickener polyurethane 0.6%, deionized water 10%.
Above-mentioned substance is configured into mixed solution according to 1 step of embodiment, obtains product.
Embodiment 4
Configure following raw materials according to the weight percent of setting: waterborne polyurethane modified acrylic emulsion (1515 resin) 46% disappears
Infusion dimethyl silicone polymer 0.2%, dispersing agent polycarboxylate sodium 1.5%, fungicide KBS fungicide 0.2%, titanium dioxide 22%,
Filler talcum powder 7%, anion epoxy emulsion 5%, wetting agent polyether silicones 0.4%, film forming agent (alcohol ester-12) 5.5%, thickener
Polyurethane 1.0%, deionized water 11.2%.
Above-mentioned substance is configured into mixed solution according to 1 step of embodiment, obtains product.
Embodiment 5
Configure following raw materials according to the weight percent of setting: waterborne polyurethane modified acrylic emulsion (1515 resin) 48% disappears
Infusion polyether siloxane copolymer 0.2%, dispersing agent polycarboxylate sodium 0.9%, fungicide KBS fungicide 0.1%, titanium dioxide
22%, filler nanometer barium sulfate 6%, anion epoxy emulsion 5%, wetting agent polyether silicones 0.2%, film forming agent (alcohol ester-12) 3%,
Thickener polyurethane 1.0%, deionized water 14.6%.
Above-mentioned substance is configured into mixed solution according to 1 step of embodiment, obtains product.
Embodiment 6
Configure following raw materials according to the weight percent of setting: waterborne polyurethane modified acrylic emulsion (1515 resin) 49% disappears
Infusion polyether siloxane copolymer 0.1%, dispersing agent lauryl sodium sulfate 1.0%, fungicide KBS fungicide 0.1%, titanium dioxide
Titanium 22%, filler nanometer barium sulfate 5%, anion epoxy emulsion 5%, wetting agent polyether silicones 0.2%, film forming agent (alcohol ester-12)
4%, thickener polyurethane 0.6%, deionized water 13%.
Above-mentioned substance is configured into mixed solution according to 1 step of embodiment, obtains product.
Be shown in table 1 to above-described embodiment 1-6 preparation environment-friendly type aqueous paint carry out drying time (surface drying/min),
Adhesive force, gloss, hardness, water resistance (h), freeze-thawing resistant stability and performance test comparison in placement 1 year etc. naturally.
The performance comparison of the environment-friendly type aqueous paint of 1 above-described embodiment 1-6 of table preparation
The surface drying speed that can be seen that environment-friendly type aqueous paint produced by the present invention from the test result of above-mentioned watch 1 is fast, 25-30 table
Dry/minute；Have it is stronger must paint adhesive force, 1-2 grades；Glossiness is good, in 25-35；Hardness is high, in H or HB；With good water-fast
Property, room temperature soaked 48 hours or more are without exception；And good freeze-thawing resistant stability, it is placed naturally with 1 year, above-mentioned various performances
Normally, bubble-free, without the tank phenomenon that rises.
Finally, it should be noted that the foregoing is only a preferred embodiment of the present invention, it is not intended to restrict the invention,
Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used
To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features,
All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in of the invention
Within protection scope.
Claims (10)
1. a kind of environment-friendly type aqueous paint, it is characterised in that:
The water paint is made of the raw material that following weight matches: waterborne polyurethane modified acrylic emulsion 45-50%, defoaming agent
0.1-0.2%, dispersing agent 0.5-2%, fungicide 0.1-0.2%, titanium dioxide 22%, filler 5-10%, aqueous epoxy emulsion 5%, profit
Humectant 0.2-0.5%, film forming agent 3-5.5%, thickener 0.5-1%, deionized water 10-15%；
The water paint is one-component system, without adding isocyanates or coupling agent solidification, without the aqueous drier of addition.
2. a kind of environment-friendly type aqueous paint according to claim 1, which is characterized in that the waterborne polyurethane modified propylene
The main component of yogurt liquid is 1515 resins.
3. a kind of environment-friendly type aqueous paint according to claim 1, which is characterized in that the defoaming agent is polyether silicone
The one or two of copolymer or dimethyl silicone polymer.
4. a kind of environment-friendly type aqueous paint according to claim 1, which is characterized in that the dispersing agent is polycarboxylate sodium
Or the one or two of lauryl sodium sulfate.
5. a kind of environment-friendly type aqueous paint according to claim 1, which is characterized in that the fungicide is KBS fungicide；
The wetting agent is polyether silicones.
6. a kind of environment-friendly type aqueous paint according to claim 1, which is characterized in that the filler be nano barium sulfate or
The one of which of talcum powder or two kinds.
7. a kind of environment-friendly type aqueous paint according to claim 1, which is characterized in that the aqueous epoxy emulsion be yin from
Sub- epoxy emulsion.
8. a kind of environment-friendly type aqueous paint according to claim 1, which is characterized in that the film forming agent be alcohol ester-12 or
One or both of butyl glycol ether.
9. a kind of environment-friendly type aqueous paint according to claim 1, which is characterized in that the thickener is polyurethane or third
One or both of olefin(e) acid lye.
10. for according to a kind of described in any item preparation methods of environment-friendly type aqueous paint of claims 1-10, feature to exist
In, the preparation process the following steps are included:
Step S1: film forming agent, wetting agent and the deionized water that predetermined weight is matched stir at low speed speed with 600 revs/min
Rate is mixed 10-15 minutes, obtains uniformly mixed mixed liquor；
Step S2: successively by predetermined weight proportion aqueous polyurethane acrylic resin, defoaming agent, dispersing agent, fungicide and
Filler is added in the mixed liquor in above-mentioned steps S1, with ultrasonic high speed dispersion 30 minutes of 1000-1500 revs/min, is divided
Dispersion liquid；
Step S3: the obtained mixed liquor of step S1 is slowly added in the dispersion liquid that step S2 is obtained, low with 600 revs/min
Fast stirring rate is stirred, and mixing time is not less than 10 minutes, until stirring evenly；
Step S4: successively the aqueous epoxy emulsion, film forming agent, thickener of predetermined weight proportion are added in step S3, with 600
Rev/min the rate that stirs at low speed be stirred, until stirring evenly, so that the environment-friendly type aqueous paint be made.
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| CN201811396829.2A CN109554105A (en) | 2018-11-22 | 2018-11-22 | A kind of environment-friendly type aqueous paint and its production technology |
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| CN201811396829.2A CN109554105A (en) | 2018-11-22 | 2018-11-22 | A kind of environment-friendly type aqueous paint and its production technology |
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Application publication date: 20190402 |