CN109550349A - A kind of gas complexing agent and preparation method thereof - Google Patents
A kind of gas complexing agent and preparation method thereof Download PDFInfo
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- CN109550349A CN109550349A CN201811448889.4A CN201811448889A CN109550349A CN 109550349 A CN109550349 A CN 109550349A CN 201811448889 A CN201811448889 A CN 201811448889A CN 109550349 A CN109550349 A CN 109550349A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2257/00—Components to be removed
- B01D2257/70—Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
- B01D2257/702—Hydrocarbons
- B01D2257/7022—Aliphatic hydrocarbons
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2257/00—Components to be removed
- B01D2257/70—Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
- B01D2257/702—Hydrocarbons
- B01D2257/7022—Aliphatic hydrocarbons
- B01D2257/7025—Methane
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02C—CAPTURE, STORAGE, SEQUESTRATION OR DISPOSAL OF GREENHOUSE GASES [GHG]
- Y02C20/00—Capture or disposal of greenhouse gases
- Y02C20/20—Capture or disposal of greenhouse gases of methane
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- Oil, Petroleum & Natural Gas (AREA)
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- Medicines Containing Plant Substances (AREA)
Abstract
The present invention relates to gas, and technical field is complexed, specifically a kind of gas complexing agent, is characterized in that: including below according to the raw material of parts by weight: 20-30 parts of aloe, 20-25 parts of gleditsia sinensis, 10-20 parts of the fleece-flower root, 10-18 parts of pine and cypress, 10-15 parts of cacumen biotae, 10-15 parts of Chinese toon leaf, 5-15 parts of Radix Angelicae Sinensis, 5-12 parts of tea seed cake, 5-10 parts of rosin.The invention also discloses the preparation methods of the gas complexing agent.Gas complexing agent prepared by the present invention has excellent mash gas effect, can be used for eliminating the methane gas in mine, has a vast market foreground.
Description
Technical field
The present invention relates to gas, and technical field, specifically a kind of gas complexing agent and preparation method thereof is complexed.
Background technique
Gas is initial stage of the archaeophyte in accumulation coal-forming, and cellulose and organic matter are decomposed through the effect of anaerobic bacteria.
High temperature, high pressure environment in, while coal-forming, due to physics and chemical action, continue to generate gas.Gas be it is colourless,
Tasteless gas, but the fragrance of similar apple can be smelt sometimes, this is because aromatic hydrocarbon gas gushes simultaneously with gas
Reason out.Gas is 0.554 to the relative density of air, and the density of gas is 0.716kg/m in normal conditions3, gas
Penetrating power be 1.6 times of air, be insoluble in water, it is not combustion-supporting to maintain to breathe, when reaching a certain concentration, can make one because
Anoxic and suffocate, and can occur burn or explode.Gas is existing for free state and sorption state in coal body or country rock.
Under coal mine, gas can threaten the safety of personnel the moment.In order to effectively prevent Gas Outburst and explosion,
The invention proposes a kind of gas complexing agents, have splendid gas that effect is complexed.
Summary of the invention
The purpose of the present invention is to provide a kind of gas complexing agents and preparation method thereof, to solve to mention in above-mentioned background technique
Out the problem of.
To achieve the above object, the invention provides the following technical scheme:
A kind of gas complexing agent, including below according to the raw material of parts by weight: 20-30 parts of aloe, 20-25 parts of gleditsia sinensis, He Shou
10-20 parts black, 10-18 parts of pine and cypress, 10-15 parts of cacumen biotae, 10-15 parts of Chinese toon leaf, 5-15 parts of Radix Angelicae Sinensis, 5-12 parts of tea seed cake, rosin
5-10 parts.
As a further solution of the present invention: including below according to the raw material of parts by weight: 25-30 parts of aloe, gleditsia sinensis 20-23
Part, 10-16 parts of the fleece-flower root, 12-18 parts of pine and cypress, 12-15 parts of cacumen biotae, 10-13 parts of Chinese toon leaf, 5-10 parts of Radix Angelicae Sinensis, tea seed cake 5-10
Part, 5-8 parts of rosin.
As the present invention further scheme: including below according to the raw material of parts by weight: 28 parts of aloe, 22 parts of gleditsia sinensis,
14 parts of the fleece-flower root, 15 parts of pine and cypress, 13 parts of cacumen biotae, 12 parts of Chinese toon leaf, 7 parts of Radix Angelicae Sinensis, 8 parts of tea seed cake, 6 parts of rosin.
The preparation method of the gas complexing agent, steps are as follows:
1) aloe, gleditsia sinensis, the fleece-flower root, pine and cypress, cacumen biotae, Chinese toon leaf, Radix Angelicae Sinensis, tea seed cake and pine are successively weighed according to parts by weight
Rouge is cleaned, is dried, spare；
2) all raw materials taken in step 1) are uniformly mixed, obtain material A；
3) material A is crushed, crosses 500 meshes, obtains material B；
4) material B is impregnated by bath raio 1:12 with deionized water, filtering removal residue obtains filtrate A；
5) filtrate A is concentrated in vacuo to get the gas complexing agent.
As further scheme of the invention: in step 4), the soaking temperature is 50 DEG C.
As further scheme of the invention: in step 4), the soaking time is 30-50 hours.
The purposes of gas complexing agent gas in eliminating mine.
A kind of gas elimination equipment based on the gas complexing agent.
Compared with prior art, the beneficial effects of the present invention are:
Gas complexing agent prepared by the present invention has excellent mash gas effect, can be used for eliminating the device in Gas in mine
Body has a vast market foreground.
Specific embodiment
The technical solution of the patent is explained in further detail With reference to embodiment.
Embodiment 1
A kind of gas complexing agent, including below according to the raw material of parts by weight: 20 parts of aloe, 20 parts of gleditsia sinensis, 10 parts of the fleece-flower root,
10 parts of pine and cypress, 10 parts of cacumen biotae, 10 parts of Chinese toon leaf, 5 parts of Radix Angelicae Sinensis, 5 parts of tea seed cake, 5 parts of rosin.
In the present embodiment, the preparation method of the gas complexing agent, steps are as follows:
1) aloe, gleditsia sinensis, the fleece-flower root, pine and cypress, cacumen biotae, Chinese toon leaf, Radix Angelicae Sinensis, tea seed cake and pine are successively weighed according to parts by weight
Rouge is cleaned, is dried, spare；
2) all raw materials taken in step 1) are uniformly mixed, obtain material A；
3) material A is crushed, crosses 500 meshes, obtains material B；
4) material B is impregnated by bath raio 1:12 with deionized water, filtering removal residue obtains filtrate A；
5) filtrate A is concentrated in vacuo to get the gas complexing agent.
Wherein, in step 4), the soaking temperature is 50 DEG C, and the soaking time is 30 hours.
The purposes of gas complexing agent gas in eliminating mine.
A kind of gas elimination equipment based on the gas complexing agent.
Embodiment 2
A kind of gas complexing agent, including below according to the raw material of parts by weight: 25 parts of aloe, 20 parts of gleditsia sinensis, 10 parts of the fleece-flower root,
12 parts of pine and cypress, 12 parts of cacumen biotae, 10 parts of Chinese toon leaf, 5 parts of Radix Angelicae Sinensis, 5 parts of tea seed cake, 5 parts of rosin.
In the present embodiment, the preparation method of the gas complexing agent, steps are as follows:
1) aloe, gleditsia sinensis, the fleece-flower root, pine and cypress, cacumen biotae, Chinese toon leaf, Radix Angelicae Sinensis, tea seed cake and pine are successively weighed according to parts by weight
Rouge is cleaned, is dried, spare；
2) all raw materials taken in step 1) are uniformly mixed, obtain material A；
3) material A is crushed, crosses 500 meshes, obtains material B；
4) material B is impregnated by bath raio 1:12 with deionized water, filtering removal residue obtains filtrate A；
5) filtrate A is concentrated in vacuo to get the gas complexing agent.
Wherein, in step 4), the soaking temperature is 50 DEG C, and the soaking time is 35 hours.
The purposes of gas complexing agent gas in eliminating mine.
A kind of gas elimination equipment based on the gas complexing agent.
Embodiment 3
A kind of gas complexing agent, including below according to the raw material of parts by weight: 28 parts of aloe, 22 parts of gleditsia sinensis, 14 parts of the fleece-flower root,
15 parts of pine and cypress, 13 parts of cacumen biotae, 12 parts of Chinese toon leaf, 7 parts of Radix Angelicae Sinensis, 8 parts of tea seed cake, 6 parts of rosin.
In the present embodiment, the preparation method of the gas complexing agent, steps are as follows:
1) aloe, gleditsia sinensis, the fleece-flower root, pine and cypress, cacumen biotae, Chinese toon leaf, Radix Angelicae Sinensis, tea seed cake and pine are successively weighed according to parts by weight
Rouge is cleaned, is dried, spare；
2) all raw materials taken in step 1) are uniformly mixed, obtain material A；
3) material A is crushed, crosses 500 meshes, obtains material B；
4) material B is impregnated by bath raio 1:12 with deionized water, filtering removal residue obtains filtrate A；
5) filtrate A is concentrated in vacuo to get the gas complexing agent.
Wherein, in step 4), the soaking temperature is 50 DEG C, and the soaking time is 40 hours.
The purposes of gas complexing agent gas in eliminating mine.
A kind of gas elimination equipment based on the gas complexing agent.
Embodiment 4
A kind of gas complexing agent, including below according to the raw material of parts by weight: 30 parts of aloe, 23 parts of gleditsia sinensis, 16 parts of the fleece-flower root,
18 parts of pine and cypress, 15 parts of cacumen biotae, 13 parts of Chinese toon leaf, 10 parts of Radix Angelicae Sinensis, 10 parts of tea seed cake, 8 parts of rosin.
In the present embodiment, the preparation method of the gas complexing agent, steps are as follows:
1) aloe, gleditsia sinensis, the fleece-flower root, pine and cypress, cacumen biotae, Chinese toon leaf, Radix Angelicae Sinensis, tea seed cake and pine are successively weighed according to parts by weight
Rouge is cleaned, is dried, spare；
2) all raw materials taken in step 1) are uniformly mixed, obtain material A；
3) material A is crushed, crosses 500 meshes, obtains material B；
4) material B is impregnated by bath raio 1:12 with deionized water, filtering removal residue obtains filtrate A；
5) filtrate A is concentrated in vacuo to get the gas complexing agent.
Wherein, in step 4), the soaking temperature is 50 DEG C, and the soaking time is 45 hours.
The purposes of gas complexing agent gas in eliminating mine.
A kind of gas elimination equipment based on the gas complexing agent.
Embodiment 5
A kind of gas complexing agent, including below according to the raw material of parts by weight: 30 parts of aloe, 25 parts of gleditsia sinensis, 20 parts of the fleece-flower root,
18 parts of pine and cypress, 15 parts of cacumen biotae, 15 parts of Chinese toon leaf, 15 parts of Radix Angelicae Sinensis, 12 parts of tea seed cake, 10 parts of rosin.
In the present embodiment, the preparation method of the gas complexing agent, steps are as follows:
1) aloe, gleditsia sinensis, the fleece-flower root, pine and cypress, cacumen biotae, Chinese toon leaf, Radix Angelicae Sinensis, tea seed cake and pine are successively weighed according to parts by weight
Rouge is cleaned, is dried, spare；
2) all raw materials taken in step 1) are uniformly mixed, obtain material A；
3) material A is crushed, crosses 500 meshes, obtains material B；
4) material B is impregnated by bath raio 1:12 with deionized water, filtering removal residue obtains filtrate A；
5) filtrate A is concentrated in vacuo to get the gas complexing agent.
Wherein, in step 4), the soaking temperature is 50 DEG C, and the soaking time is 50 hours.
The purposes of gas complexing agent gas in eliminating mine.
A kind of gas elimination equipment based on the gas complexing agent.
Comparative example 1
Compared with Example 3, cacumen biotae is free of, other are same as Example 3.
Comparative example 2
Compared with Example 3, Chinese toon leaf is free of, other are same as Example 3.
Comparative example 3
Compared with Example 3, cacumen biotae and Chinese toon leaf are free of, other are same as Example 3.
Comparative example 4
A kind of plant source compound methane (gas) complexing agent disclosed in Chinese invention patent CN102698565B.
To plant source compound methane described in gas complexing agent prepared by embodiment 3, comparative example 1-3 and comparative example 4 (watt
This) complexing agent carries out eliminating gas performance test, and test result is as shown in table 1.
1 gas of table eliminates performance test
As can be seen that gas complexing agent prepared by the present invention has excellent mash gas effect from result above, can use
In eliminating the methane gas in mine, have a vast market foreground.
In addition, from the data comparison of embodiment 3 and comparative example 1-3 as can be seen that the present invention by be added cacumen biotae and
Chinese toon leaf, cacumen biotae and Chinese toon leaf cooperate, and are conducive to the mash gas effect for improving gas complexing agent.
The preferred embodiment of the patent is described in detail above, but this patent is not limited to above-mentioned embodiment party
Formula within the knowledge of one of ordinary skill in the art can also be under the premise of not departing from this patent objective
It makes a variety of changes.
Claims (8)
1. a kind of gas complexing agent, which is characterized in that including below according to the raw material of parts by weight: 20-30 parts of aloe, gleditsia sinensis 20-
25 parts, 10-20 parts of the fleece-flower root, 10-18 parts of pine and cypress, 10-15 parts of cacumen biotae, 10-15 parts of Chinese toon leaf, 5-15 parts of Radix Angelicae Sinensis, tea seed cake 5-
12 parts, 5-10 parts of rosin.
2. gas complexing agent according to claim 1, which is characterized in that including below according to the raw material of parts by weight: aloe
25-30 parts, 20-23 parts of gleditsia sinensis, 10-16 parts of the fleece-flower root, 12-18 parts of pine and cypress, 12-15 parts of cacumen biotae, 10-13 parts of Chinese toon leaf, when
Return 5-10 parts, 5-10 parts of tea seed cake, 5-8 parts of rosin.
3. gas complexing agent according to claim 2, which is characterized in that including below according to the raw material of parts by weight: aloe
28 parts, 22 parts of gleditsia sinensis, 14 parts of the fleece-flower root, 15 parts of pine and cypress, 13 parts of cacumen biotae, 12 parts of Chinese toon leaf, 7 parts of Radix Angelicae Sinensis, 8 parts of tea seed cake, rosin 6
Part.
4. a kind of preparation method of gas complexing agent a method according to any one of claims 1-3, which is characterized in that steps are as follows:
1) aloe, gleditsia sinensis, the fleece-flower root, pine and cypress, cacumen biotae, Chinese toon leaf, Radix Angelicae Sinensis, tea seed cake and rosin are successively weighed according to parts by weight,
It cleans, dries, it is spare；
2) all raw materials taken in step 1) are uniformly mixed, obtain material A；
3) material A is crushed, crosses 500 meshes, obtains material B；
4) material B is impregnated by bath raio 1:12 with deionized water, filtering removal residue obtains filtrate A；
5) filtrate A is concentrated in vacuo to get the gas complexing agent.
5. the preparation method of gas complexing agent according to claim 4, which is characterized in that in step 4), the immersion temperature
Degree is 50 DEG C.
6. the preparation method of gas complexing agent according to claim 4, which is characterized in that in step 4), when the immersion
Between be 30-50 hours.
7. the purposes of gas complexing agent a method according to any one of claims 1-3 gas in eliminating mine.
8. a kind of gas based on gas complexing agent a method according to any one of claims 1-3 eliminates equipment.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811448889.4A CN109550349A (en) | 2018-11-28 | 2018-11-28 | A kind of gas complexing agent and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811448889.4A CN109550349A (en) | 2018-11-28 | 2018-11-28 | A kind of gas complexing agent and preparation method thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101939077A (en) * | 2007-10-16 | 2011-01-05 | 黑炭公司 | A method and an apparatus for absorbing methane and a method of determining an emission credit |
| CN102698565A (en) * | 2012-05-25 | 2012-10-03 | 上海复振科技有限公司 | Plant source compound methane (gas) complexing agent and preparation method and application thereof |
| CN103554894A (en) * | 2013-10-25 | 2014-02-05 | 安徽文峰电子科技集团有限公司 | Environment-friendly type flame-retardant polyurethane rubber cable material |
| WO2017073518A1 (en) * | 2015-10-29 | 2017-05-04 | 千代田化工建設株式会社 | Carbon dioxide separation method |
-
2018
- 2018-11-28 CN CN201811448889.4A patent/CN109550349A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101939077A (en) * | 2007-10-16 | 2011-01-05 | 黑炭公司 | A method and an apparatus for absorbing methane and a method of determining an emission credit |
| CN102698565A (en) * | 2012-05-25 | 2012-10-03 | 上海复振科技有限公司 | Plant source compound methane (gas) complexing agent and preparation method and application thereof |
| CN103554894A (en) * | 2013-10-25 | 2014-02-05 | 安徽文峰电子科技集团有限公司 | Environment-friendly type flame-retardant polyurethane rubber cable material |
| WO2017073518A1 (en) * | 2015-10-29 | 2017-05-04 | 千代田化工建設株式会社 | Carbon dioxide separation method |
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Application publication date: 20190402 |