CN109518301A - A kind of easily combing antistatic wig fiber - Google Patents
A kind of easily combing antistatic wig fiber Download PDFInfo
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- CN109518301A CN109518301A CN201811415440.8A CN201811415440A CN109518301A CN 109518301 A CN109518301 A CN 109518301A CN 201811415440 A CN201811415440 A CN 201811415440A CN 109518301 A CN109518301 A CN 109518301A
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- antistatic
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/10—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one other macromolecular compound obtained by reactions only involving carbon-to-carbon unsaturated bonds as constituent
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/09—Addition of substances to the spinning solution or to the melt for making electroconductive or anti-static filaments
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/106—Radiation shielding agents, e.g. absorbing, reflecting agents
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F11/00—Chemical after-treatment of artificial filaments or the like during manufacture
- D01F11/04—Chemical after-treatment of artificial filaments or the like during manufacture of synthetic polymers
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/14—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyester as constituent
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/16—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one other macromolecular compound obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds as constituent
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- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Artificial Filaments (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention mainly relates to staple fibre processing technique fields, a kind of easily combing antistatic wig fiber is disclosed, be prepared from the following raw materials: dispersion liquid 13 ~ 15, modified beeswaxes 2.1 ~ 2.3, antistatic agent 0.7 ~ 0.9, nano silica 0.3 ~ 0.5, graphene 0.12 ~ 0.14 is concentrated in polybutylene terephthalate (PBT) 46 ~ 48, polyurethane resin 17 ~ 19, polytetrafluoroethylene (PTFE) 60%；Easy combing antistatic wig fiber provided by the invention, Rejoice silk are sliding, and really send out similar, and anti-ultraviolet ageing will not generate electrostatic, easily comb, and have preferable antibiotic property and flame retardant type, increase wig type in the market, improve the applicability of wig；Polybutylene terephthalate (PBT) and polyurethane resin are added in the concentration dispersion liquid of polytetrafluoroethylene (PTFE) 60% and are stirred heating, is sufficiently melted conducive to raw material, improves the intensity and smoothness of wig fiber.
Description
Technical field
The invention mainly relates to staple fibre processing technique fields, more particularly to a kind of easily combing antistatic wig fiber.
Background technique
Wig can play preferable decoration function, can convert different hair styles at any time, and can be avoided and often scald
Dye is damaged to caused by true hair, while can save a large amount of time and expense；Wig is all that true hair is made after treatment mostly
It is standby to form, but true hair purchase is difficult at present, and purchasing price is high, to limit the production of wig, therefore gradually uses
Staple fibre replaces true hair.
But during the wearing of wig, since friction is easy that wig is made to generate electrostatic, meeting repeatedly between wig fiber
It affects to hair style, and is easy to appear knotting after wig generation electrostatic and shows, keep combing difficult, to beating for wig
Reason brings certain adverse effect.
Summary of the invention
In order to make up the defect of prior art, the object of the present invention is to provide a kind of easily combing antistatic wig fibers.
A kind of easily combing antistatic wig fiber, is made of raw material from the following weight: polybutylene terephthalate (PBT)
46 ~ 48, dispersion liquid 13 ~ 15, modified beeswaxes 2.1 ~ 2.3, antistatic agent is concentrated in polyurethane resin 17 ~ 19, polytetrafluoroethylene (PTFE) 60%
0.7 ~ 0.9, nano silica 0.3 ~ 0.5, graphene 0.12 ~ 0.14.
Purification beeswax is heated to sufficiently melting, beeswax weight 0.3 ~ 0.5% is added into beeswax by the modified beeswaxes
Boric acid, stirring adds the tea polyphenols of beeswax weight 0.26 ~ 0.28% to full and uniform, be stirred under vacuum 20 in 45 ~ 50 DEG C ~
30min can remove the greasy feeling of beeswax, enhance the glossiness and biocidal property of beeswax, obtain modified beeswaxes.
The antistatic agent, is made of raw material from the following weight: sodium alkyl sulfonate 22 ~ 24, tartaric acid solution 5 ~ 7,
Tartaric acid solution is heated to 40 ~ 45 by cocoanut fatty acid diethanolamide 1.1 ~ 1.3, the preparation method of the antistatic agent
DEG C, sodium alkyl sulfonate and cocoanut fatty acid diethanolamide is added, stirs 15 ~ 20min in 34 ~ 36r/min, obtains antistatic
Agent.
The tartaric acid solution, mass concentration are 12 ~ 14%.
A kind of preparation method of easy combing antistatic wig fiber, comprising the following steps:
(1) polytetrafluoroethylene (PTFE) 60% is added in polybutylene terephthalate (PBT) and polyurethane resin to be concentrated in dispersion liquid, side stirring
While being slowly heated to melt completely, sufficiently melted conducive to raw material, improves the intensity and smoothness of wig fiber, obtain mixture A；
(2) modified beeswaxes and antistatic agent are mixed, is heated to being sufficiently mixed while stirring, add mixture A, keep the temperature vacuum
30 ~ 40min is stirred, the glossiness and flexibility of wig fiber are improved, avoids generation electrostatic and knotting that from must mixing conducive to arranging
Object B；
(3) nano silica and graphene are added in mixture B, be stirred under vacuum the intensity for uniformly improving wig fiber and
Anti-uv-ray avoids wig fiber from occurring the aging phenomenon for being broken and changing colour after long-term solar radiation, extends wig
Service life, obtain mixture C；
(4) mixture C is sent into spinning machine and carries out wet spinning, coagulating bath is alkaline ethanol solution, uses Asia after taking out spinning
Selenic acid sodium solution is rinsed well, and the intensity and silk slip of wig fiber are improved, the similarity for increasing wig and really sending out, and obtains spinning fibre
Dimension；
(5) spinning fibre is placed in baking oven, it is 4 ~ 8% that water content is dried in 30 ~ 35 DEG C, keeps wig fiber higher strong
Degree, avoids being broken in carding process, arranges, and obtains easily combing antistatic wig fiber.
The wet spinning of the step (4), spinneret 6 ~ 7m/min of speed, stretch bath temperature 52 by 12 ~ 14 DEG C of coagulation bath temperature
~ 54 DEG C, 4 ~ 5m/min of draft speed.
Sodium hydroxide is added in 56 ~ 58% alcoholic solution to volume fraction in the alkaline ethanol solution of the step (4)
Solution, the pH for being adjusted to alcoholic solution is 9.1 ~ 9.3.
The sodium selenite solution of the step (4), mass percentage concentration are 1.6 ~ 1.8%.
The easy combing antistatic wig fiber, fiber number are 40 ~ 44dtex.
The invention has the advantages that easy combing antistatic wig fiber provided by the invention, Rejoice silk is sliding, and really sends out similar,
Anti-ultraviolet ageing will not generate electrostatic, easily comb, and have preferable antibiotic property and flame retardant type, increase wig kind in the market
Class improves the applicability of wig；Polytetrafluoroethylene (PTFE) 60% is added in polybutylene terephthalate (PBT) and polyurethane resin to be concentrated
It is stirred heating in dispersion liquid, is sufficiently melted conducive to raw material, improves the intensity and smoothness of wig fiber；Add modified bee
Wax and antistatic agent, and heat preservation vacuum stirring is carried out, the glossiness and flexibility of wig fiber are improved, avoids generating electrostatic and beat
Knot, conducive to arranging；Nano silica and graphene are added, the intensity and anti-uv-ray of wig fiber is improved, avoids
There is the aging phenomenon for being broken and changing colour after long-term solar radiation in wig fiber, extends the service life of wig；It will mixing
Cleaned after raw material wet spinning by sodium selenite solution, improve wig fiber intensity and silk slip, increase wig with
The similarity really sent out；Through low temperature drying after mode, the higher intensity of wig fiber is kept, avoids breaking in carding process
It splits.
Specific embodiment
Illustrate the present invention with specific embodiment below.
Embodiment 1
A kind of easily combing antistatic wig fiber, be made of raw material from the following weight: polybutylene terephthalate (PBT) 46 gathers
Urethane resin 17, polytetrafluoroethylene (PTFE) 60% be concentrated dispersion liquid 13, modified beeswaxes 2.1, antistatic agent 0.7, nano silica 0.3,
Graphene 0.12.
Purification beeswax is heated to sufficiently melting, the boron of beeswax weight 0.3% is added into beeswax by the modified beeswaxes
Acid, stirring add the tea polyphenols of beeswax weight 0.26%, in 45 DEG C of vacuum stirring 20min, can remove bee to full and uniform
The greasy feeling of wax enhances the glossiness and biocidal property of beeswax, obtains modified beeswaxes.
The antistatic agent, is made of raw material from the following weight: sodium alkyl sulfonate 22, tartaric acid solution 5, coconut oil
Tartaric acid solution is heated to 40 ~ 45 DEG C, alkyl is added by fatty diglycollic amide 1.1, the preparation method of the antistatic agent
Sodium sulfonate and cocoanut fatty acid diethanolamide stir 15min in 34r/min, obtain antistatic agent.
The tartaric acid solution, mass concentration 12%.
A kind of preparation method of easy combing antistatic wig fiber, comprising the following steps:
(1) polytetrafluoroethylene (PTFE) 60% is added in polybutylene terephthalate (PBT) and polyurethane resin to be concentrated in dispersion liquid, side stirring
While being slowly heated to melt completely, sufficiently melted conducive to raw material, improves the intensity and smoothness of wig fiber, obtain mixture A；
(2) modified beeswaxes and antistatic agent are mixed, is heated to being sufficiently mixed while stirring, add mixture A, keep the temperature vacuum
30min is stirred, the glossiness and flexibility of wig fiber are improved, generation electrostatic and knotting is avoided to obtain mixture B conducive to arranging；
(3) nano silica and graphene are added in mixture B, be stirred under vacuum the intensity for uniformly improving wig fiber and
Anti-uv-ray avoids wig fiber from occurring the aging phenomenon for being broken and changing colour after long-term solar radiation, extends wig
Service life, obtain mixture C；
(4) mixture C is sent into spinning machine and carries out wet spinning, spinneret speed 6m/min, stretches bath temperature by 12 DEG C of coagulation bath temperature
52 DEG C of degree, draft speed 4m/min, coagulating bath is alkaline ethanol solution, uses mass percentage concentration for 1.6% after taking out spinning
Sodium selenite solution is rinsed well, and the intensity and silk slip of wig fiber are improved, the similarity for increasing wig and really sending out, and fiber number is
40dtex obtains spinning fibre；Sodium hydroxide is added in 56% alcoholic solution to volume fraction in the alkaline ethanol solution
Solution, the pH for being adjusted to alcoholic solution is 9.1 ~ 9.3；
(5) spinning fibre is placed in baking oven, it is 4 ~ 8% that water content is dried in 30 DEG C, the higher intensity of wig fiber is kept,
It avoids being broken in carding process, arrange, obtain easily combing antistatic wig fiber.
Embodiment 2
A kind of easily combing antistatic wig fiber, be made of raw material from the following weight: polybutylene terephthalate (PBT) 47 gathers
Urethane resin 18, polytetrafluoroethylene (PTFE) 60% be concentrated dispersion liquid 14, modified beeswaxes 2.2, antistatic agent 0.8, nano silica 0.4,
Graphene 0.13.
Purification beeswax is heated to sufficiently melting, the boron of beeswax weight 0.4% is added into beeswax by the modified beeswaxes
Acid, stirring add the tea polyphenols of beeswax weight 0.27%, in 48 DEG C of vacuum stirring 25min, can remove bee to full and uniform
The greasy feeling of wax enhances the glossiness and biocidal property of beeswax, obtains modified beeswaxes.
The antistatic agent, is made of raw material from the following weight: sodium alkyl sulfonate 23, tartaric acid solution 6, coconut oil
Tartaric acid solution is heated to 40 ~ 45 DEG C, alkyl is added by fatty diglycollic amide 1.2, the preparation method of the antistatic agent
Sodium sulfonate and cocoanut fatty acid diethanolamide stir 18min in 35r/min, obtain antistatic agent.
The tartaric acid solution, mass concentration 13%.
A kind of preparation method of easy combing antistatic wig fiber, comprising the following steps:
(1) polytetrafluoroethylene (PTFE) 60% is added in polybutylene terephthalate (PBT) and polyurethane resin to be concentrated in dispersion liquid, side stirring
While being slowly heated to melt completely, sufficiently melted conducive to raw material, improves the intensity and smoothness of wig fiber, obtain mixture A；
(2) modified beeswaxes and antistatic agent are mixed, is heated to being sufficiently mixed while stirring, add mixture A, keep the temperature vacuum
30 ~ 40min is stirred, the glossiness and flexibility of wig fiber are improved, avoids generation electrostatic and knotting that from must mixing conducive to arranging
Object B；
(3) nano silica and graphene are added in mixture B, be stirred under vacuum the intensity for uniformly improving wig fiber and
Anti-uv-ray avoids wig fiber from occurring the aging phenomenon for being broken and changing colour after long-term solar radiation, extends wig
Service life, obtain mixture C；
(4) by mixture C be sent into spinning machine carry out wet spinning, spinneret speed 6.5m/min, 13 DEG C of coagulation bath temperature, stretch bath
53 DEG C of temperature, draft speed 4.5m/min, coagulating bath is alkaline ethanol solution, is using mass percentage concentration after taking-up spinning
1.7% sodium selenite solution is rinsed well, and the intensity and silk slip of wig fiber are improved, the similarity for increasing wig and really sending out,
Fiber number is 42dtex, obtains spinning fibre；Hydrogen is added in 57% alcoholic solution to volume fraction in the alkaline ethanol solution
Sodium hydroxide solution, the pH for being adjusted to alcoholic solution is 9.1 ~ 9.3；
(5) spinning fibre is placed in baking oven, it is 4 ~ 8% that water content is dried in 33 DEG C, the higher intensity of wig fiber is kept,
It avoids being broken in carding process, arrange, obtain easily combing antistatic wig fiber.
Embodiment 3
A kind of easily combing antistatic wig fiber, be made of raw material from the following weight: polybutylene terephthalate (PBT) 48 gathers
Urethane resin 19, polytetrafluoroethylene (PTFE) 60% be concentrated dispersion liquid 15, modified beeswaxes 2.3, antistatic agent 0.9, nano silica 0.5,
Graphene 0.14.
Purification beeswax is heated to sufficiently melting, the boron of beeswax weight 0.5% is added into beeswax by the modified beeswaxes
Acid, stirring add the tea polyphenols of beeswax weight 0.28%, in 50 DEG C of vacuum stirring 30min, can remove bee to full and uniform
The greasy feeling of wax enhances the glossiness and biocidal property of beeswax, obtains modified beeswaxes.
The antistatic agent, is made of raw material from the following weight: sodium alkyl sulfonate 24, tartaric acid solution 7, coconut oil
Tartaric acid solution is heated to 40 ~ 45 DEG C, alkyl is added by fatty diglycollic amide 1.3, the preparation method of the antistatic agent
Sodium sulfonate and cocoanut fatty acid diethanolamide stir 15 ~ 20min in 36r/min, obtain antistatic agent.
The tartaric acid solution, mass concentration 14%.
A kind of preparation method of easy combing antistatic wig fiber, comprising the following steps:
(1) polytetrafluoroethylene (PTFE) 60% is added in polybutylene terephthalate (PBT) and polyurethane resin to be concentrated in dispersion liquid, side stirring
While being slowly heated to melt completely, sufficiently melted conducive to raw material, improves the intensity and smoothness of wig fiber, obtain mixture A；
(2) modified beeswaxes and antistatic agent are mixed, is heated to being sufficiently mixed while stirring, add mixture A, keep the temperature vacuum
40min is stirred, the glossiness and flexibility of wig fiber are improved, generation electrostatic and knotting is avoided to obtain mixture B conducive to arranging；
(3) nano silica and graphene are added in mixture B, be stirred under vacuum the intensity for uniformly improving wig fiber and
Anti-uv-ray avoids wig fiber from occurring the aging phenomenon for being broken and changing colour after long-term solar radiation, extends wig
Service life, obtain mixture C；
(4) mixture C is sent into spinning machine and carries out wet spinning, spinneret speed 7m/min, stretches bath temperature by 14 DEG C of coagulation bath temperature
54 DEG C of degree, draft speed 5m/min, coagulating bath is alkaline ethanol solution, uses mass percentage concentration for 1.8% after taking out spinning
Sodium selenite solution is rinsed well, and the intensity and silk slip of wig fiber are improved, the similarity for increasing wig and really sending out, and fiber number is
44dtex obtains spinning fibre；Sodium hydroxide is added in 58% alcoholic solution to volume fraction in the alkaline ethanol solution
Solution, the pH for being adjusted to alcoholic solution is 9.1 ~ 9.3；
(5) spinning fibre is placed in baking oven, it is 4 ~ 8% that water content is dried in 35 DEG C, the higher intensity of wig fiber is kept,
It avoids being broken in carding process, arrange, obtain easily combing antistatic wig fiber.
Comparative example 1
Remove polyurethane resin, remaining preparation method, with embodiment 1.
Comparative example 2
Modified beeswaxes are changed to beeswax, remaining preparation method, with embodiment 1.
Comparative example 3
Remove the tartaric acid solution in antistatic agent, remaining preparation method, with embodiment 1.
Comparative example 4
Remove the cocoanut fatty acid diethanolamide in antistatic agent, remaining preparation method, with embodiment 1.
Comparative example 5
Remove nano silica, remaining preparation method, with embodiment 1.
Comparative example 6
Remove graphene, remaining preparation method, with embodiment 1.
Comparative example 7
It removes step (2) and (3), raw material is added in step (1), remaining preparation method, with embodiment 1.
Comparative example 8
Wet spinning in step (4) is changed to melt spinning, remaining preparation method, with embodiment 1.
Comparative example 9
Coagulation bath temperature in step (4) is changed to 35 DEG C, remaining preparation method, with embodiment 1.
Comparative example 10
Sodium selenite solution in step (4) is changed to water, remaining preparation method, with embodiment 1.
Comparative example 11
Temperature in step (5) is changed to 60 DEG C, remaining preparation method, with embodiment 1.
Comparative example 12
Existing commercially available Na Yisi wig.
The mechanical property of embodiment and comparative example wig fiber:
Example and the wig fiber of comparative example are appropriate respectively, according to " fibre strength detection technique and instrument, Zhu Genfeng etc. "
Method, using dry strong (CN/dtex) of YG029-I full automatic single yarn tester detection wig fiber, wet strong (CN/dtex) and
Dry to stretch (%), every group repeats detection 3 times, and results are averaged, and the mechanical property of embodiment and comparative example wig fiber is shown in Table 1.
Table 1: the mechanical property of embodiment and comparative example wig fiber
From table 1 the result shows that, the easy combing antistatic wig fiber of embodiment is done strong, wet strong and dry performance of stretching and is substantially better than
Comparative example illustrates that easy combing antistatic wig fiber provided by the invention has good mechanical property and service performance, intensity
Height, and undistorted is higher with the similarity really sent out.
The flame retardant property and anti-microbial property of embodiment and comparative example wig fiber:
Its limit oxygen index LOI(% is measured by GB/T5455-1997 " textile combustion performance test normal beam technique "), and use UL94
The flame retardant rating of standard detection each group wig fiber, and each group wig fiber 25g is taken, 80 ~ 100 mesh are crushed to, to each group wig
Fiber is inoculated with staphylococcus aureus, is cultivated according to the optimum condition of staphylococcus aureus, and each group wig fiber is detected
Bacteriostasis rate, each test is repeated 3 times, and results are averaged, the flame retardant property and antibacterial of embodiment and comparative example wig fiber
Performance is shown in Table 2.
Table 2: the flame retardant property and anti-microbial property of embodiment and comparative example wig fiber
Note: "-" indicates not fire-retardant.
From table 2 the result shows that, the easy combing antistatic wig fiber of embodiment, limit oxygen index and antibiotic rate are obviously excellent
In comparative example, flame retardant rating is significantly higher, and it is fire-retardant well to illustrate that easy combing antistatic wig fiber provided by the invention has
Performance and anti-microbial property.
The easy combing of embodiment and comparative example wig fiber and antistatic performance:
According to the method in document " the easy cardability Study on Test Method of wig, Chen Wei state ", the nylon comb pair that tooth pitch is 2mm is used
Dry wig is combed, the frictional force of test each group wig and nylon comb, according to disclosed in 108047515 A of patent CN
The method for surveying electrostatic will tie up after the cleaning of each group wig fiber, and tie surface applying conductive coatings, coating in wig after drying
Area is 200mm × 50mm, and according still further to the resistance of method detection wig fiber bundle, each test is repeated 3 times, is as a result averaged
Value, the easy combing of embodiment and comparative example wig fiber and antistatic performance are shown in Table 3.
Table 3: the easy combing of embodiment and comparative example wig fiber and antistatic performance
From table 3 the result shows that, the easy combing antistatic wig fiber of embodiment, frictional force, dry air resistance and humid air resistance are bright
It is aobvious to be better than comparative example, illustrate that easy combing antistatic wig fiber provided by the invention is easy to comb, electrostatic can be effectively prevent to produce
It is raw.
Claims (9)
1. a kind of easily combing antistatic wig fiber, which is characterized in that be made of raw material from the following weight: poly terephthalic acid
Butanediol ester 46 ~ 48, polyurethane resin 17 ~ 19, polytetrafluoroethylene (PTFE) 60% are concentrated dispersion liquid 13 ~ 15, modified beeswaxes 2.1 ~ 2.3, resist
Electrostatic agent 0.7 ~ 0.9, nano silica 0.3 ~ 0.5, graphene 0.12 ~ 0.14.
2. easily combing antistatic wig fiber according to claim 1, which is characterized in that the modified beeswaxes will refine
Beeswax is heated to sufficiently melting, and the boric acid of beeswax weight 0.3 ~ 0.5% is added into beeswax, and stirring adds bee to full and uniform
The tea polyphenols of wax weight 0.26 ~ 0.28% can remove the greasy feeling of beeswax in 45 ~ 50 DEG C of 20 ~ 30min of vacuum stirring, enhancing
The glossiness and biocidal property of beeswax, obtain modified beeswaxes.
3. easily combing antistatic wig fiber according to claim 1, which is characterized in that the antistatic agent, by following
The raw material of parts by weight is made: sodium alkyl sulfonate 22 ~ 24, tartaric acid solution 5 ~ 7, cocoanut fatty acid diethanolamide 1.1 ~ 1.3,
Tartaric acid solution is heated to 40 ~ 45 DEG C, sodium alkyl sulfonate and coco-nut oil fatty acid is added by the preparation method of the antistatic agent
Diglycollic amide stirs 15 ~ 20min in 34 ~ 36r/min, obtains antistatic agent.
4. easily combing antistatic wig fiber according to claim 2, which is characterized in that the tartaric acid solution, quality
Concentration is 12 ~ 14%.
5. a kind of preparation method of combing antistatic wig fiber easy according to claim 1, which is characterized in that including following
Step:
(1) polytetrafluoroethylene (PTFE) 60% is added in polybutylene terephthalate (PBT) and polyurethane resin to be concentrated in dispersion liquid, side stirring
While being slowly heated to melt completely, mixture A is obtained；
(2) modified beeswaxes and antistatic agent are mixed, is heated to being sufficiently mixed while stirring, add mixture A, keep the temperature vacuum
30 ~ 40min is stirred, mixture B is obtained；
(3) nano silica and graphene are added in mixture B, are stirred under vacuum uniformly, obtain mixture C；
(4) mixture C is sent into spinning machine and carries out wet spinning, coagulating bath is alkaline ethanol solution, uses Asia after taking out spinning
Selenic acid sodium solution is rinsed well, and spinning fibre is obtained；
(5) spinning fibre is placed in baking oven, it is 4 ~ 8% that water content is dried in 30 ~ 35 DEG C, is arranged, and it is false to obtain easily combing antistatic
Send out fiber.
6. easily combing the preparation method of antistatic wig fiber according to claim 5, which is characterized in that the step (4)
Wet spinning, spinneret 6 ~ 7m/min of speed, 12 ~ 14 DEG C of coagulation bath temperature, stretch 52 ~ 54 DEG C of bath temperature, 4 ~ 5m/ of draft speed
min。
7. easily combing the preparation method of antistatic wig fiber according to claim 5, which is characterized in that the step (4)
Alkaline ethanol solution, to volume fraction be 56 ~ 58% alcoholic solution in sodium hydroxide solution is added, be adjusted to alcoholic solution
PH be 9.1 ~ 9.3.
8. easily combing the preparation method of antistatic wig fiber according to claim 5, which is characterized in that the step (4)
Sodium selenite solution, mass percentage concentration be 1.6 ~ 1.8%.
9. any one of according to claim 1 ~ 8 easy combing antistatic wig fiber, which is characterized in that fiber number for 40 ~
44dtex。
Priority Applications (1)
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| CN201811415440.8A CN109518301A (en) | 2018-11-26 | 2018-11-26 | A kind of easily combing antistatic wig fiber |
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| CN201811415440.8A CN109518301A (en) | 2018-11-26 | 2018-11-26 | A kind of easily combing antistatic wig fiber |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113512878A (en) * | 2021-05-24 | 2021-10-19 | 南通大学 | Antistatic finishing agent, antistatic wig and preparation method thereof |
| WO2024043710A1 (en) * | 2022-08-24 | 2024-02-29 | 주식회사 네오엔프라 | Composition for use in wig comprising polyester, polybutylene terephthalate, and graphene |
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| WO2024043710A1 (en) * | 2022-08-24 | 2024-02-29 | 주식회사 네오엔프라 | Composition for use in wig comprising polyester, polybutylene terephthalate, and graphene |
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