CN109502189A - A kind of secure store and method - Google Patents

A kind of secure store and method Download PDF

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Publication number
CN109502189A
CN109502189A CN201811330303.4A CN201811330303A CN109502189A CN 109502189 A CN109502189 A CN 109502189A CN 201811330303 A CN201811330303 A CN 201811330303A CN 109502189 A CN109502189 A CN 109502189A
Authority
CN
China
Prior art keywords
storage
storing case
outer tank
inner canister
cooling tube
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201811330303.4A
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Chinese (zh)
Inventor
智勇
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dalian Zhuoyi Technology Co Ltd
Original Assignee
Dalian Zhuoyi Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dalian Zhuoyi Technology Co Ltd filed Critical Dalian Zhuoyi Technology Co Ltd
Priority to CN201811330303.4A priority Critical patent/CN109502189A/en
Publication of CN109502189A publication Critical patent/CN109502189A/en
Withdrawn legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B65CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65DCONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
    • B65D81/00Containers, packaging elements, or packages, for contents presenting particular transport or storage problems, or adapted to be used for non-packaging purposes after removal of contents
    • B65D81/18Containers, packaging elements, or packages, for contents presenting particular transport or storage problems, or adapted to be used for non-packaging purposes after removal of contents providing specific environment for contents, e.g. temperature above or below ambient
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/56Filters or filtering processes specially modified for separating dispersed particles from gases or vapours with multiple filtering elements, characterised by their mutual disposition
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B65CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65DCONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
    • B65D79/00Kinds or details of packages, not otherwise provided for
    • B65D79/02Arrangements or devices for indicating incorrect storage or transport
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25DREFRIGERATORS; COLD ROOMS; ICE-BOXES; COOLING OR FREEZING APPARATUS NOT OTHERWISE PROVIDED FOR
    • F25D3/00Devices using other cold materials; Devices using cold-storage bodies
    • F25D3/10Devices using other cold materials; Devices using cold-storage bodies using liquefied gases, e.g. liquid air

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Combustion & Propulsion (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Respiratory Apparatuses And Protective Means (AREA)

Abstract

The invention discloses a kind of secure store and methods, including pedestal, the base top is equipped with storage apparatus, the storage apparatus includes Storing case, the Storing case is fixedly connected with pedestal, fixed ring is equipped with inside the Storing case, fixed link is equipped at the top of the fixed ring, the fixed link side is equipped with storage outer tank, link block is equipped with inside the storage outer tank, the link block side is equipped with storage inner canister, the storage inner canister two sides are equipped with expects pipe, the expects pipe is through storage outer tank and Storing case and extends to outside, the storage outer tank two sides are equipped with cooling tube, the cooling tube is through Storing case and extends to outside.The present invention is by being equipped with storage apparatus, liquid nitrogen is delivered at the interlayer of storage outer tank and storage inner canister by cooling tube, and then low-temperature treatment is carried out to the material inside storage inner canister, ventilation inlet pipe and outlet pipe of taking a breath are conducive to keep the fixed circulation of Storing case inner air, leaked substance are avoided to spread.

Description

A kind of secure store and method
Technical field
The present invention relates to hazardous chemical production and storing and transporting security safeguards technique field, in particular to a kind of safe storage dress It sets and method.
Background technique
Anhydrous hydrogen fluoride for industrial use is a kind of widely used chemical products, and appearance is 99% or more of colourless fuming liquids Hydrofluoric acid easily gasifies under decompression or high temperature.It is mainly used as producing villiaumite, fluorohaloparaffin, fluorine refrigerant, etching glass, dipping Timber, electrolysis element fluorine etc..Its chemical property is extremely active, there is very strong water imbibition, strong corrosive, can be with alkali, metal, oxygen The reaction such as compound and silicate (energy etching glass and other silicon-containing materials of destruction), can freely mix under certain condition with water At hydrofluoric acid (extreme heat emission forms hydrofluoric acid when being dissolved in water).
Big portion's anhydrous hydrogen fluoride safety when being stored domestic at present is relatively low, and protection effect is bad, when part nothing Water hydrogen fluoride cannot be prompted timely when revealing.
Therefore, it invents a kind of secure store and method is necessary to solve the above problems.
Summary of the invention
The purpose of the present invention is to provide a kind of secure store and methods, and liquid nitrogen is delivered to storage by cooling tube Outer tank and storage inner canister interlayer at, and then to storage inner canister inside material carry out low-temperature treatment, open exhaust fan, take a breath into Pipe and ventilation outlet pipe keep the fixed circulation of Storing case inner air, avoid leaked substance from spreading, while air humidity detector Hydrogen fluoride alarm auto-alarm-signal keying device when the humidity inside detection Storing case and hydrogen fluoride are more than preset value in real time, promotes prompt effect Fruit increases safety, to solve the problems mentioned in the above background technology.
To achieve the above object, the invention provides the following technical scheme: a kind of secure store, including pedestal, it is described Base top is equipped with storage apparatus, and the storage apparatus includes Storing case, and the Storing case is fixedly connected with pedestal, the storage It is equipped with fixed ring inside case, fixed link is equipped at the top of the fixed ring, the fixed link side is equipped with storage outer tank, the storage Link block is equipped with inside outer tank, the link block side is equipped with storage inner canister, and the storage inner canister two sides are equipped with expects pipe, described Expects pipe is through storage outer tank and Storing case and extends to outside, and the storage outer tank two sides are equipped with cooling tube, the cooling tube Through Storing case and outside is extended to, the storage chamber interior wall is equipped with air humidity detector, and the Storing case side is equipped with fluorine Change hydrogen alarm, the Storing case other side is equipped with ventilation inlet pipe, be equipped with ventilation outlet pipe at the top of the Storing case, the expects pipe and Solenoid valve is equipped with inside cooling tube.
Preferably, it is equipped with filter device inside the ventilation outlet pipe, the filter device includes Rose Box, the filtering dress It sets inside and is equipped with cartridge filter, be equipped with the first filter layer inside the cartridge filter, first filter layer is made of absorbent charcoal material.
Preferably, first filter layer bottom is equipped with the second filter layer, and second filter layer is by PP cotton material system.
Preferably, the cartridge filter side is equipped with snap-gauge, and the snap-gauge side is equipped with pull ring, and the pull ring is fixed with snap-gauge Connection.
Preferably, it is equipped with first exhaust fan inside the ventilation inlet pipe, is equipped with second exhaust fan inside the ventilation outlet pipe, The second exhaust fan is arranged at the top of Rose Box.
A kind of safe storage method, including the secure store, including following methods:
S1: material is delivered to inside storage inner canister by expects pipe;
S2: the solenoid valve of expects pipe is closed;
S3: and then be delivered to liquid nitrogen at the interlayer of storage outer tank and storage inner canister by cooling tube, and then in storage Material inside tank carries out low-temperature treatment;
S4: exhaust fan is opened;
S5: the fixed circulation of ventilation inlet pipe and outlet pipe holding Storing case inner air of taking a breath, while air humidity detector Hydrogen fluoride alarm auto-alarm-signal keying device when the humidity inside detection Storing case and hydrogen fluoride are more than preset value in real time.
Technical effect and advantage of the invention:
1, by being equipped with storage apparatus, liquid nitrogen is delivered at the interlayer of storage outer tank and storage inner canister by cooling tube, And then low-temperature treatment is carried out to the material inside storage inner canister, ventilation inlet pipe and ventilation outlet pipe are conducive to keep empty inside Storing case The fixed circulation of gas, avoids leaked substance from spreading, at the same air humidity detector detect in real time humidity inside Storing case and Hydrogen fluoride alarm auto-alarm-signal keying device when hydrogen fluoride is more than preset value is conducive to promote prompt effect, increases safety;
2, by being equipped with filter device, the ventilating air of discharge is filtered by the first filter layer and second inside cartridge filter It is discharged safely after layer filtering, is polluted when being beneficial to prevent material minor leakage, while pulling pull ring that cartridge filter is driven to remove Rose Box can be replaced the first filter layer and the second filter layer, advantageously ensure that filter effect.
Detailed description of the invention
Fig. 1 is overall structure diagram of the invention.
Fig. 2 is top view of the invention.
Fig. 3 is filter apparatus configuration schematic diagram of the invention.
In figure: 1 pedestal, 2 storage apparatus, 3 Storing cases, 4 fixed rings, 5 fixed links, 6 storage outer tanks, 7 link blocks, 8 storages Inner canister, 9 expects pipes, 10 cooling tubes, 11 air humidity detectors, 12 hydrogen fluoride alarms, 13 take a breath into, 14 ventilation outlet pipes, 15 mistakes Filter device, 16 Rose Boxes, 17 cartridge filters, 18 first filter layers, 19 second filter layers, 20 snap-gauges, 21 pull rings, 22 first exhausts Fan, 23 second exhaust fan, 24 solenoid valves.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
Embodiment 1
The present invention provides a kind of secure store as shown in Figs. 1-3, including pedestal 1, it is equipped at the top of the pedestal 1 Storage apparatus 2, the storage apparatus 2 include Storing case 3, and the Storing case 3 is fixedly connected with pedestal 1, inside the Storing case 3 Equipped with fixed ring 4, fixed link 5 is equipped at the top of the fixed ring 4,5 side of fixed link is equipped with storage outer tank 6, the storage Link block 7 is equipped with inside outer tank 6,7 side of link block is equipped with storage inner canister 8, and 8 two sides of storage inner canister are equipped with expects pipe 9, the expects pipe 9 is through storage outer tank 6 and Storing case 3 and extends to outside, and 6 two sides of storage outer tank are equipped with cooling tube 10, the cooling tube 10 is through Storing case 3 and extends to outside, and 3 inner wall of Storing case is equipped with air humidity detector 11, institute 3 side of Storing case is stated equipped with hydrogen fluoride alarm 12,3 other side of Storing case is equipped with ventilation inlet pipe 13, and the Storing case 3 pushes up Portion is equipped with ventilation outlet pipe 14, and by being equipped with storage apparatus 2, liquid nitrogen is delivered in storage outer tank 6 and storage by cooling tube 10 At the interlayer of tank 8, and then low-temperature treatment is carried out to the material inside storage inner canister 8, ventilation inlet pipe 13 and ventilation outlet pipe 14 are advantageous In the fixed circulation for keeping 3 inner air of Storing case, leaked substance is avoided to spread, while air humidity detector 11 is examined in real time 12 auto-alarm-signal keying device of hydrogen fluoride alarm, is conducive to promote prompt when the humidity and hydrogen fluoride surveyed inside Storing case 3 are more than preset value Effect increases safety.
Further, in the above-mentioned technical solutions, filter device 15, the filtering dress are equipped with inside the ventilation outlet pipe 14 Setting 15 includes Rose Box 16, and cartridge filter 17 is equipped with inside the filter device 15, the first filtering is equipped with inside the cartridge filter 17 Layer 18, first filter layer 18 is made of absorbent charcoal material, and the ventilating air by being equipped with filter device 15, discharge passed through It is discharged safely after the first filter layer 18 and the filtering of the second filter layer 19 inside filter cylinder 17, when being beneficial to prevent material minor leakage It pollutes, while pulling pull ring 21 that cartridge filter 17 is driven to remove Rose Box 16, it can be to the first filter layer 18 and the second filtering Layer 19 is replaced, and advantageously ensures that filter effect;
Further, in the above-mentioned technical solutions, 18 bottom of the first filter layer is equipped with the second filter layer 19, and described the Two filter layers 19 are made of PP cotton material;
Further, in the above-mentioned technical solutions, 17 side of cartridge filter is equipped with snap-gauge 20, and 20 side of snap-gauge is set Have pull ring 21, the pull ring 21 is fixedly connected with snap-gauge 20, by setting snap-gauge 20 and pull ring 21, be conducive to cartridge filter 17 into Row movement;
Further, in the above-mentioned technical solutions, first exhaust fan 22, the ventilation are equipped with inside the ventilation inlet pipe 13 Second exhaust fan 23 is equipped with inside outlet pipe 14, the setting of second exhaust fan 23 is at 16 top of Rose Box, by the way that first row is arranged Gas fan 22 and second exhaust fan 23 guarantee the circulation of 3 inner air of Storing case;
Further, in the above-mentioned technical solutions, solenoid valve 24 is equipped with inside the expects pipe 9 and cooling tube 10.
Working method of the present invention:
Referring to Figure of description 1 and 2, material is delivered to inside storage inner canister 8 by expects pipe 9, closes the electromagnetism of expects pipe 9 Then liquid nitrogen is delivered at the interlayer of storage outer tank 6 and storage inner canister 8 by valve 24 by cooling tube 10, and then to storage inner canister 8 Internal material carries out low-temperature treatment, opens exhaust fan, and ventilation inlet pipe 13 and outlet pipe 14 of taking a breath keep 3 inner air of Storing case Fixed circulation, avoids leaked substance from spreading, while air humidity detector 11 detects the humidity and fluorine inside Storing case 3 in real time Change 12 auto-alarm-signal keying device of hydrogen fluoride alarm when hydrogen is more than preset value, promotes prompt effect, increase safety;
Referring to Figure of description 3, while the ventilating air being discharged is by the first filter layer 18 and the inside cartridge filter 17 It is discharged safely after the filtering of two filter layers 19, prevents from polluting when material minor leakage, while pull ring 21 being pulled to drive cartridge filter 17 remove Rose Box 16, can be replaced to the first filter layer 18 and the second filter layer 19, guarantee filter effect.
Embodiment 2
A kind of safe storage method, including the secure store, including following methods:
S1: material is delivered to inside storage inner canister 8 by expects pipe 9;
S2: the solenoid valve 24 of expects pipe 9 is closed;
S3: and then be delivered to liquid nitrogen at the interlayer of storage outer tank 6 and storage inner canister 8 by cooling tube 10, and then to storage It deposits the material inside inner canister 8 and carries out low-temperature treatment;
S4: exhaust fan is opened;
S5: the fixed circulation of ventilation inlet pipe 13 and holding 3 inner air of Storing case of outlet pipe 14 of taking a breath, while air humidity is examined 12 auto-alarm-signal keying device of hydrogen fluoride alarm when the humidity and hydrogen fluoride surveyed inside the real-time detection Storing case 3 of instrument 11 are more than preset value.
Finally, it should be noted that the foregoing is only a preferred embodiment of the present invention, it is not intended to restrict the invention, Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features, All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in of the invention Within protection scope.

Claims (6)

1. a kind of secure store, including pedestal (1), it is characterised in that: storage apparatus (2) are equipped at the top of the pedestal (1), The storage apparatus (2) includes Storing case (3), and the Storing case (3) is fixedly connected with pedestal (1), and the Storing case (3) is internal Equipped with fixed ring (4), fixed link (5) are equipped at the top of the fixed ring (4), fixed link (5) side is equipped with storage outer tank (6), link block (7) are equipped with inside the storage outer tank (6), link block (7) side is equipped with storage inner canister (8), the storage Inner canister (8) two sides to be deposited to be equipped with expects pipe (9), the expects pipe (9) is through storage outer tank (6) and Storing case (3) and extends to outside, Storage outer tank (6) two sides are equipped with cooling tube (10), and the cooling tube (10) is through Storing case (3) and extends to outside, Storing case (3) inner wall is equipped with air humidity detector (11), and Storing case (3) side is equipped with hydrogen fluoride alarm (12), Storing case (3) other side is equipped with ventilation inlet pipe (13), is equipped with ventilation outlet pipe (14), institute at the top of the Storing case (3) It states and is equipped with solenoid valve (24) inside expects pipe (9) and cooling tube (10).
2. a kind of secure store according to claim 1, it is characterised in that: be equipped with inside the ventilation outlet pipe (14) Filter device (15), the filter device (15) include Rose Box (16), and cartridge filter is equipped with inside the filter device (15) (17), the first filter layer (18) are equipped with inside the cartridge filter (17), first filter layer (18) is made of absorbent charcoal material.
3. a kind of secure store according to claim 2, it is characterised in that: the first filter layer (18) bottom is set Have the second filter layer (19), second filter layer (19) is made of PP cotton material.
4. a kind of secure store according to claim 2, it is characterised in that: cartridge filter (17) side is equipped with card Plate (20), snap-gauge (20) side are equipped with pull ring (21), and the pull ring (21) is fixedly connected with snap-gauge (20).
5. a kind of secure store according to claim 1, it is characterised in that: be equipped with inside the ventilation inlet pipe (13) First exhaust fan (22), the ventilation outlet pipe (14) is internal to be equipped with second exhaust fan (23), second exhaust fan (23) setting At the top of Rose Box (16).
6. a kind of safe storage method, it is characterised in that: including secure store as described in claim 1, including it is following Method:
S1: material is delivered to by storage inner canister (8) inside by expects pipe (9);
S2: the solenoid valve (24) of expects pipe (9) is closed;
S3: and then be delivered to liquid nitrogen at the interlayer of storage outer tank (6) and storage inner canister (8) by cooling tube (10), and then right It stores inner canister (8) internal material and carries out low-temperature treatment;
S4: exhaust fan is opened;
S5: the fixed circulation of ventilation inlet pipe (13) and outlet pipe (14) holding Storing case (3) inner air of taking a breath, while air humidity Detector (11) detect the internal humidity of Storing case (3) in real time and when hydrogen fluoride is more than preset value hydrogen fluoride alarm (12) from Dynamic alarm.
CN201811330303.4A 2018-11-09 2018-11-09 A kind of secure store and method Withdrawn CN109502189A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811330303.4A CN109502189A (en) 2018-11-09 2018-11-09 A kind of secure store and method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811330303.4A CN109502189A (en) 2018-11-09 2018-11-09 A kind of secure store and method

Publications (1)

Publication Number Publication Date
CN109502189A true CN109502189A (en) 2019-03-22

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CN201811330303.4A Withdrawn CN109502189A (en) 2018-11-09 2018-11-09 A kind of secure store and method

Country Status (1)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112389884A (en) * 2020-11-18 2021-02-23 太仓市茜泾化工有限公司 Preparation of diisopropyl phosphite is with depositing equipment

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2834187A (en) * 1954-09-10 1958-05-13 Union Carbide Corp Refrigerated container for liquefied gases
CN103697321A (en) * 2013-12-24 2014-04-02 衢州市鼎盛化工科技有限公司 Equipment for storing and transporting liquid and application thereof
JP2016030611A (en) * 2014-07-28 2016-03-07 ビーエム工業株式会社 Heat insulation container
CN206417426U (en) * 2016-12-08 2017-08-18 广州市同源化工科技有限公司 A kind of chemical material holding vessel with temperature adjustment function
CN206704955U (en) * 2017-05-16 2017-12-05 新昌县镜岭镇康柳电子元件厂 A kind of industrial chemicals storage tank
CN207060879U (en) * 2017-06-09 2018-03-02 新昌县大市聚镇洪聚机械厂 A kind of industrial chemicals storage device
CN207242549U (en) * 2017-09-08 2018-04-17 湖南斯派克科技股份有限公司 A kind of hydrofluoric acid storage tank
CN207395300U (en) * 2017-08-08 2018-05-22 江山市华伟化工科技有限公司 A kind of phosphorus pentoxide stored dry device

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2834187A (en) * 1954-09-10 1958-05-13 Union Carbide Corp Refrigerated container for liquefied gases
CN103697321A (en) * 2013-12-24 2014-04-02 衢州市鼎盛化工科技有限公司 Equipment for storing and transporting liquid and application thereof
JP2016030611A (en) * 2014-07-28 2016-03-07 ビーエム工業株式会社 Heat insulation container
CN206417426U (en) * 2016-12-08 2017-08-18 广州市同源化工科技有限公司 A kind of chemical material holding vessel with temperature adjustment function
CN206704955U (en) * 2017-05-16 2017-12-05 新昌县镜岭镇康柳电子元件厂 A kind of industrial chemicals storage tank
CN207060879U (en) * 2017-06-09 2018-03-02 新昌县大市聚镇洪聚机械厂 A kind of industrial chemicals storage device
CN207395300U (en) * 2017-08-08 2018-05-22 江山市华伟化工科技有限公司 A kind of phosphorus pentoxide stored dry device
CN207242549U (en) * 2017-09-08 2018-04-17 湖南斯派克科技股份有限公司 A kind of hydrofluoric acid storage tank

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112389884A (en) * 2020-11-18 2021-02-23 太仓市茜泾化工有限公司 Preparation of diisopropyl phosphite is with depositing equipment

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Application publication date: 20190322