CN109490678A - A kind of adjustable interpolar away from Ni―Ti anode reinforcing life test device - Google Patents
A kind of adjustable interpolar away from Ni―Ti anode reinforcing life test device Download PDFInfo
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- CN109490678A CN109490678A CN201811640890.7A CN201811640890A CN109490678A CN 109490678 A CN109490678 A CN 109490678A CN 201811640890 A CN201811640890 A CN 201811640890A CN 109490678 A CN109490678 A CN 109490678A
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- Prior art keywords
- anode
- away
- adjustable
- life test
- test device
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- 230000003014 reinforcing effect Effects 0.000 title claims abstract description 33
- KHYBPSFKEHXSLX-UHFFFAOYSA-N iminotitanium Chemical compound [Ti]=N KHYBPSFKEHXSLX-UHFFFAOYSA-N 0.000 title claims abstract description 26
- 229910001000 nickel titanium Inorganic materials 0.000 title claims abstract description 26
- 238000012360 testing method Methods 0.000 title claims abstract description 25
- 238000009529 body temperature measurement Methods 0.000 claims abstract description 15
- 239000003792 electrolyte Substances 0.000 claims abstract description 13
- 239000011521 glass Substances 0.000 claims description 8
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims description 6
- 239000004810 polytetrafluoroethylene Substances 0.000 claims description 6
- 239000012774 insulation material Substances 0.000 claims description 3
- -1 polytetrafluoroethylene Polymers 0.000 claims description 3
- 238000005868 electrolysis reaction Methods 0.000 abstract description 3
- 238000013461 design Methods 0.000 abstract description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000010936 titanium Substances 0.000 description 3
- 229910052719 titanium Inorganic materials 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- FLDCSPABIQBYKP-UHFFFAOYSA-N 5-chloro-1,2-dimethylbenzimidazole Chemical compound ClC1=CC=C2N(C)C(C)=NC2=C1 FLDCSPABIQBYKP-UHFFFAOYSA-N 0.000 description 1
- 239000001741 Ammonium adipate Substances 0.000 description 1
- 241000208340 Araliaceae Species 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 239000005030 aluminium foil Substances 0.000 description 1
- 235000019293 ammonium adipate Nutrition 0.000 description 1
- 239000010405 anode material Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000004210 cathodic protection Methods 0.000 description 1
- 239000011889 copper foil Substances 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 235000008434 ginseng Nutrition 0.000 description 1
- 238000003780 insertion Methods 0.000 description 1
- 230000037431 insertion Effects 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000004065 wastewater treatment Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
- G01R31/00—Arrangements for testing electric properties; Arrangements for locating electric faults; Arrangements for electrical testing characterised by what is being tested not provided for elsewhere
- G01R31/003—Environmental or reliability tests
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
- G01R1/00—Details of instruments or arrangements of the types included in groups G01R5/00 - G01R13/00 and G01R31/00
- G01R1/02—General constructional details
- G01R1/04—Housings; Supporting members; Arrangements of terminals
- G01R1/0408—Test fixtures or contact fields; Connectors or connecting adaptors; Test clips; Test sockets
- G01R1/0425—Test clips, e.g. for IC's
Landscapes
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Electrolytic Production Of Metals (AREA)
Abstract
The invention belongs to electrolysis tech field, be related to a kind of adjustable interpolar away from Ni―Ti anode reinforcing life test device, including device noumenon, the top of device noumenon be equipped with container cover;Electrolyte circular hole, temperature measurement circular hole are provided in container cover;The centre of container cover is equipped with dial, and dial is equipped with the pole plate fixture that can be moved left and right.The device is adjusted the spacing cathode-anode plate by pole plate fixture, correspond to yin-yang two-plate in parallel, it can be vertically fixed in the electrolyte in device noumenon, the interpolar of anodic-cathodic between 0-6.2cm away from can be adjusted flexibly, design is rationally, simply, the reinforcing life of Ni―Ti anode can be accurately measured, error is reduced.
Description
Technical field
The invention belongs to electrolysis tech field, it is related in laboratory research and the production quality check process of a kind of electrochemical industry
The reinforcing life test device of coating titanium anode more particularly to a kind of adjustable interpolar away from Ni―Ti anode reinforcing life test dress
It sets.
Background technique
Coating titanium anode, also known as DSA (Dimensionally Stable Anode), dimensional stability anode is 20 generation
It records a kind of novel insoluble anode material for growing up at the end of the sixties.Due to its electro catalytic activity with higher and excellent
Corrosion resistance, can be used as analysis oxygen important in acid or alkaline medium, analysis chloric pole material, be widely used to chlor-alkali work
The fields such as industry, plating, wastewater treatment, Organic electro-synthesis, cathodic protection and the manufacture of aluminium foil copper foil.
For Ni―Ti anode, working life is to measure an important parameter of its performance.Due to the Ni―Ti anode real-world operation longevity
Life is very long, often all in some months or even several years or more.In Ni―Ti anode R&D process, for the rapid evaluation Ni―Ti anode service life, respectively
State scholar is tested using reinforcing life general in the world, i.e., strengthens operating in high current density, harsh electrolytic medium,
Until anode fails, it is known as reinforcing life this period.
Currently, the error of reinforcing life is mainly derived from test device, existing test device electrode interpolar is away from all comparing
It is single, the Ni―Ti anode reinforcing life under fixed pole spacing can only be tested, it is known from literature that reinforcing life test electrode interpolar away from
Can between 1.0cm-6.0cm, if to test different interpolars away from reinforcing life, need replacing test device.In addition, two
Pole plate can not be corresponded to steadily in parallel, cause surveyed reinforcing life error larger.
Summary of the invention
It is an object of the invention to overcome the above-mentioned prior art, provide a kind of adjustable interpolar away from Ni―Ti anode it is strong
Change endurance testing device, can make polar plate position is corresponding to stablize, can make that experimental result is more accurate, reduces error, to production
And experimental study has good directive significance.
To achieve the above object, the present invention provides the following technical scheme that
A kind of adjustable interpolar away from Ni―Ti anode reinforcing life test device, comprising: device noumenon, described device ontology
Top is equipped with container cover;Electrolyte circular hole, temperature measurement circular hole are provided in the container cover;The intermediate installation of the container cover
There is dial, the dial is equipped with the pole plate fixture that can be moved left and right.
Further, described device ontology further includes cathode plate and anode plate, and the cathode plate and anode plate are mounted on
The inside of device noumenon, the bottom of the anode plate are equipped with U-clamp, and the U-clamp is equipped with protrusion, and the protrusion exceeds anode plate
5-10mm guarantees that anode print and anode plate 8 are on same straight line.
Further, the pole plate fixture is fixedly connected by the second screw with dial, and the pole plate fixture passes through the
One screw is fixedly connected with the cathode-anode plate inside device noumenon.
Further, the electrolyte circular hole is located at the top of dial, and the temperature measurement circular hole is located at dial
Lower section.
Further, the scale of the dial is extended from centre to both sides, range 6.2cm, precision 1mm.
Further, settable thermometer in the temperature measurement circular hole, the thermometer go deep into along temperature measurement circular hole
The inside of device noumenon, the temperature for measuring device ontology electrolyte inside.
Further, the container cover is square, and select acid-fast alkali-proof and insulation material be made.
Further, described device ontology is glass container, and the container cover is glass container lid or polytetrafluoroethylene (PTFE) system
At container cover.
Compared with prior art, technical solution provided by the invention has the following beneficial effects: that the device is pressed from both sides by pole plate
The spacing cathode-anode plate is adjusted in tool, corresponds to yin-yang two-plate in parallel, can be vertically fixed in device noumenon
In electrolyte, for the interpolar of anodic-cathodic away from that can be adjusted flexibly between 0-6.2cm, design rationally, simply, can accurately measure titanium
The reinforcing life of anode reduces error.
Detailed description of the invention
The drawings herein are incorporated into the specification and forms part of this specification, and is used to explain this together with specification
The principle of invention.
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below
There is attached drawing needed in technical description to be briefly described, it should be apparent that, for those of ordinary skill in the art
Speech, without any creative labor, is also possible to obtain other drawings based on these drawings.
Fig. 1 be a kind of adjustable interpolar provided by the invention away from Ni―Ti anode reinforcing life test device top view;
Fig. 2 be a kind of adjustable interpolar provided by the invention away from Ni―Ti anode reinforcing life test device structural representation
Figure.
Wherein: 1 is container cover;2 be dial;3 be pole plate fixture;4 be the first screw;5 be the second screw;6 be electrolysis
Liquid circular hole;7 measure circular hole for temperature;8 be anode plate;9 be cathode plate;10 be protrusion.
Specific embodiment
Example embodiments are described in detail here, and the example is illustrated in the accompanying drawings.Following description is related to
When attached drawing, unless otherwise indicated, the same numbers in different drawings indicate the same or similar elements.Following exemplary embodiment
Described in embodiment do not represent all embodiments consistented with the present invention.On the contrary, they are only and appended power
The example of device be described in detail in sharp claim, that some aspects of the invention are consistent.
In order to make those skilled in the art more fully understand technical solution of the present invention, with reference to the accompanying drawings and embodiments
Present invention is further described in detail.
Embodiment 1:
Referring to shown in Fig. 1-2, the present invention provides a kind of adjustable interpolar away from Ni―Ti anode reinforcing life test device, packet
Include: the top of device noumenon, the device noumenon is equipped with container cover 1;Electrolyte circular hole 6, temperature measurement circle are provided in container cover 1
Hole 7;The centre of container cover 1 is equipped with dial 2, and dial 2 is equipped with the pole plate fixture 3 that can be moved left and right.
Further, which further includes cathode plate 9 and anode plate 8, and cathode plate 9 and anode plate 8 are mounted on dress
The inside of ontology is set, the bottom of anode plate 8 is equipped with U-clamp, and U-clamp is equipped with protrusion 10, and length of the protrusion 10 beyond anode plate 8 is
5-10mm guarantees that anode print and anode plate 8 are on same straight line.
Further, pole plate fixture 3 is fixedly connected by the second screw 5 with dial 2, and pole plate fixture 3 passes through the first spiral shell
Silk 4 is fixedly connected with the cathode-anode plate inside device noumenon.
Further, electrolyte circular hole 6 is located at the top of dial 2, and temperature measurement circular hole 7 is located at the lower section of dial 2.
Further, the scale of dial 2 is extended from centre to both sides, range 6.2cm, precision 1mm.
Further, settable thermometer in temperature measurement circular hole 7, thermometer go deep into device noumenon along temperature measurement circular hole
Inside.
Further, container cover 1 is square, and select acid-fast alkali-proof and insulation material be made.
Further, device noumenon is glass container, and container cover 1 is container made of glass container lid or polytetrafluoroethylene (PTFE)
Lid.
The device, specific working principle are as follows: preparing electrolyte in proportion and pour into glass container, in the U of anode plate 8
Anode print having a size of 10mm × 20mm on clevis opening folder, is in anode print and anode plate 8 on same straight line;Ginseng
Stir pole plate fixture 3 according to the scale in dial 2, reach experiment interpolar away from;The first screw 4 and the second screw 5 are tightened, really
It protects cathode-anode plate to correspond in parallel, and is vertically fixed in electrolyte;Insertion thermometer records temperature in temperature measurement circular hole 7;
Finally, yin-yang two-plate connects the positive and negative anodes of power supply as required, it is powered and records the time, measure its reinforcing life time.
Embodiment 2:
The ammonium adipate solution for preparing 10% pours into glass container 11, successively on the U-clamp opening folder of anode plate 8
Anode print A, B, C of the different batches of size 10mm × 20mm are in anode print and anode plate on same straight line;Reference
Scale in dial 2 stirs pole plate fixture 3, makes interpolar away from remaining 2.0cm, 4.0cm, 6.0cm respectively;Tighten the first screw
4 and second screw 5, it is ensured that cathode-anode plate corresponds in parallel, and is vertically fixed in electrolyte;It is inserted into temperature measurement circular hole 7
Thermometer records temperature;Finally, yin-yang two-plate meets the positive and negative anodes of power supply, electrical current density 4000A/m as required2, record
Time, the reinforcing life time of anode print A, B, C are measured, specific experiment the results are shown in Table 1.
1 electrode interpolar of table is away from the influence to reinforcing life
As can be seen from the above table, to Mr. Yu's anode print, in the case where temperature is certain, when the interpolar between cathode-anode plate away from
When changing, the reinforcing life time of Ni―Ti anode can change, and when interpolar is away from for 2cm, the time of reinforcing life exists
8.3% is improved on the basis of originally.
The above is only a specific embodiment of the invention, is made skilled artisans appreciate that or realizing this hair
It is bright.The general principles defined herein can without departing from the spirit or scope of the present invention, in other embodiments
Middle realization.
It should be understood that the invention is not limited to the above-mentioned contents having been described, and carrying out without departing from the scope
Various modifications and change.The scope of the present invention is limited only by the attached claims.
Claims (10)
1. a kind of adjustable interpolar away from Ni―Ti anode reinforcing life test device characterized by comprising device noumenon, it is described
The top of device noumenon is equipped with container cover (1);Electrolyte circular hole (6), temperature measurement circular hole are provided on the container cover (1)
(7);The centre of the container cover (1) is equipped with dial (2), and the dial (2) is equipped with the pole plate folder that can be moved left and right
Have (3).
2. a kind of adjustable interpolar according to claim 1 away from Ni―Ti anode reinforcing life test device, which is characterized in that
Described device ontology further includes cathode plate (9) and anode plate (8), and the cathode plate (9) and anode plate (8) are mounted on device sheet
The bottom of the inside of body, the anode plate (8) is equipped with U-clamp.
3. a kind of adjustable interpolar according to claim 2 away from Ni―Ti anode reinforcing life test device, which is characterized in that
The U-clamp is equipped with protrusion (10).
4. a kind of adjustable interpolar according to claim 3 away from Ni―Ti anode reinforcing life test device, which is characterized in that
The protrusion (10) exceeds anode plate (8) 5-10mm.
5. a kind of adjustable interpolar according to claim 1 away from Ni―Ti anode reinforcing life test device, which is characterized in that
The pole plate fixture (3) is fixedly connected by the second screw (5) with dial (2), and the pole plate fixture (3) passes through the first screw
(4) it is fixedly connected with the cathode-anode plate inside device noumenon.
6. a kind of adjustable interpolar according to claim 1 away from Ni―Ti anode reinforcing life test device, which is characterized in that
The electrolyte circular hole (6) is located at the top of dial (2), and temperature measurement circular hole (7) is located at the lower section of dial (2).
7. a kind of adjustable interpolar according to claim 1 away from Ni―Ti anode reinforcing life test device, which is characterized in that
The scale of the dial (2) is extended from centre to both sides, range 6.2cm, precision 1mm.
8. a kind of adjustable interpolar according to claim 1-7 away from Ni―Ti anode reinforcing life test device,
It is characterized in that, settable thermometer in temperature measurement circular hole (7), the thermometer gos deep into device sheet along temperature measurement circular hole
The inside of body.
9. a kind of adjustable interpolar according to claim 1-7 away from Ni―Ti anode reinforcing life test device,
Be characterized in that, the container cover (1) is square, and select acid-fast alkali-proof and insulation material be made.
10. a kind of adjustable interpolar according to claim 1-7 away from Ni―Ti anode reinforcing life test device,
It is characterized in that, described device ontology is glass container, and the container cover (1) is to hold made of glass container lid or polytetrafluoroethylene (PTFE)
Device lid.
Priority Applications (1)
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CN201811640890.7A CN109490678A (en) | 2018-12-29 | 2018-12-29 | A kind of adjustable interpolar away from Ni―Ti anode reinforcing life test device |
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CN105002541A (en) * | 2015-08-07 | 2015-10-28 | 上海海事大学 | Automated electrolytic tank |
CN205317871U (en) * | 2016-01-10 | 2016-06-15 | 国网电网公司 | Apart from adjustable discharge electrode device |
CN105954613A (en) * | 2016-04-29 | 2016-09-21 | 中国船舶重工集团公司第七二五研究所 | Titanium electrode acceleration life testing device |
CN206244475U (en) * | 2016-10-20 | 2017-06-13 | 中国石油大学(华东) | A kind of two-dimensional/three-dimensional electrode reactor device of adjusting plate spacing |
CN207727169U (en) * | 2017-12-31 | 2018-08-14 | 浙江大学 | A kind of adjustable pitch electrophoretic deposition teaching aid |
CN209728068U (en) * | 2018-12-29 | 2019-12-03 | 西安泰金工业电化学技术有限公司 | A kind of adjustable interpolar away from Ni―Ti anode reinforcing life test device |
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2018
- 2018-12-29 CN CN201811640890.7A patent/CN109490678A/en active Pending
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JP2001347270A (en) * | 2000-06-06 | 2001-12-18 | Omega:Kk | Electrolytic apparatus |
CN202758002U (en) * | 2012-08-17 | 2013-02-27 | 中国科学院宁波材料技术与工程研究所 | Resistivity testing device |
CN202814909U (en) * | 2012-10-29 | 2013-03-20 | 黑龙江八一农垦大学 | Inter-electrode distance adjustable electrolytic bath |
CN202886546U (en) * | 2012-11-15 | 2013-04-17 | 云南电力试验研究院(集团)有限公司电力研究院 | High-voltage testing apparatus |
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CN104313657A (en) * | 2014-11-10 | 2015-01-28 | 临安振有电子有限公司 | Electro-deposition device of through hole of HDI printed circuit board |
CN105002541A (en) * | 2015-08-07 | 2015-10-28 | 上海海事大学 | Automated electrolytic tank |
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CN206244475U (en) * | 2016-10-20 | 2017-06-13 | 中国石油大学(华东) | A kind of two-dimensional/three-dimensional electrode reactor device of adjusting plate spacing |
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