CN109486528A - A kind of device producing Fischer-Tropsch wax crude product - Google Patents
A kind of device producing Fischer-Tropsch wax crude product Download PDFInfo
- Publication number
- CN109486528A CN109486528A CN201811645575.3A CN201811645575A CN109486528A CN 109486528 A CN109486528 A CN 109486528A CN 201811645575 A CN201811645575 A CN 201811645575A CN 109486528 A CN109486528 A CN 109486528A
- Authority
- CN
- China
- Prior art keywords
- fischer
- entrance
- tropsch wax
- connect
- outlet
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G73/00—Recovery or refining of mineral waxes, e.g. montan wax
- C10G73/02—Recovery of petroleum waxes from hydrocarbon oils; Dewaxing of hydrocarbon oils
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G73/00—Recovery or refining of mineral waxes, e.g. montan wax
- C10G73/02—Recovery of petroleum waxes from hydrocarbon oils; Dewaxing of hydrocarbon oils
- C10G73/025—Recovery of petroleum waxes from hydrocarbon oils; Dewaxing of hydrocarbon oils by filtration
Abstract
The present invention relates to a kind of devices for producing Fischer-Tropsch wax crude product, belong to Fischer-Tropsch wax production technical field.Device of the present invention includes reaction kettle, filter, preheater, thin film evaporator；The outlet of the reaction kettle and the entrance of filter connect；The outlet of the filter and the entrance of preheater connect；The outlet of the preheater and the entrance of thin film evaporator connect.Fischer-Tropsch wax is slightly purified by carclazyte decoloring reaction, filtering, thin film evaporation using device of the present invention, there are simple operation and other advantages.
Description
Technical field
The present invention relates to a kind of devices for producing Fischer-Tropsch wax crude product, belong to Fischer-Tropsch wax production technical field.
Background technique
Fischer-Tropsch wax is the wax that coal gas is produced by F- T synthesis, and main component is C12-C90 alkane, normal paraffin content
Up to 80% or more, fusing point is up to 90 DEG C or more.It is made of relative molecular mass in the straight chain of 200-1200, the High-carbon alkane of saturation,
With fine crystal structure, high-melting-point, low oil content, low needle penetration, low mobility, low melting viscosity, hard, wear-resisting and steady
The advantages that qualitative high.
Fischer-Tropsch wax is mainly used for hot melt adhesive, ink and coating, plastic processing (PVC lubricant, polyene hydrocarbon lubricants and color masterbatch
Pellet dispersing agent) etc. fields.
Fischer-Tropsch wax is ideal synthetic wax used in EVA based melt adhesive, and dystectic wax can be improved the heat-resisting of adhesive
Property and quick-drying.
When Fischer-Tropsch wax with particle sprills use in ink, wearability, the wrinkle resistance of application material can be improved, apply
In coating, corrugation effect can be played, striped and water wave corrugation effect can be formed in micronised state use, powder is being added
Coating resin plays lubricating action in extrusion process, can reduce screw torque, reduces energy consumption and improves production efficiency.
Fischer-Tropsch wax is obvious with stabilizer synergy with PVC processing, can effectively extend heat-stable time, increases process warm
The amplitude of accommodation of degree, it is particularly evident in the processing of CPVC resin, since CPVC resin processing techniques parameter regulation narrow range increases
The difficulty of processing of product can be effectively improved the later period lubrication of CPVC product processing, promote the appearance and mechanical property of product.
Summary of the invention
The present invention, to black wax decoloration, filtering, thin film evaporation containing Fischer-Tropsch wax and catalyst, obtains Fischer-Tropsch using new equipment
Wax crude product is using the raw material or other purposes as high-quality Fischer-Tropsch wax product.
The present invention provides a kind of device for producing Fischer-Tropsch wax crude product, described device includes reaction kettle, filter, preheating
Device, thin film evaporator；The outlet of the reaction kettle and the entrance of filter connect；The outlet of the filter and entering for preheater
Mouth connection；The outlet of the preheater and the entrance of thin film evaporator connect.
The present invention is preferably that the filter is plate filter or frame filter.
The present invention is preferably that described device includes storage tank；The outlet of the filter and the entrance of storage tank connect；The storage
The outlet of tank and the entrance of preheater connect.
The present invention is preferably that described device includes surge tank I, surge tank II；The water of the thin film evaporator and before distillate mouth
It is connect with the entrance of surge tank I；The Fischer-Tropsch wax crude product outlet of the thin film evaporator is connect with the entrance of surge tank II.
The invention has the following beneficial effects:
Fischer-Tropsch wax is slightly purified by carclazyte decoloring reaction, filtering, thin film evaporation using device of the present invention, is had
There are simple operation and other advantages.
Detailed description of the invention
3 width of attached drawing of the present invention,
Fig. 1 is the structural schematic diagram that Fischer-Tropsch wax crude product device is produced described in embodiment 1；
Fig. 2 is the structural schematic diagram that Fischer-Tropsch wax crude product device is produced described in embodiment 2；
Fig. 3 is the structural schematic diagram that Fischer-Tropsch wax crude product device is produced described in embodiment 3；
Wherein, 1, reaction kettle, 2, filter, 3, preheater, 4, thin film evaporator, 5, storage tank, 6, surge tank I, 7, buffering
Tank II.
Specific embodiment
Following non-limiting embodiments can with a person of ordinary skill in the art will more fully understand the present invention, but not with
Any mode limits the present invention.
Embodiment 1
A kind of device producing Fischer-Tropsch wax crude product, described device include reaction kettle 1, filter 2, preheater 3, film steaming
Send out device 4；
The filter 2 is plate filter 2；
The outlet of the reaction kettle 1 is connect with the entrance of plate filter 2；
The outlet of the plate filter 2 is connect with the entrance of preheater 3；
The outlet of the preheater 3 is connect with the entrance of thin film evaporator 4.
Embodiment 2
A kind of device producing Fischer-Tropsch wax crude product, described device include reaction kettle 1, filter 2, storage tank 5, preheater 3,
Thin film evaporator 4；
The filter 2 is frame filter 2；
The outlet of the reaction kettle 1 is connect with the entrance of frame filter 2；
The outlet of the frame filter 2 is connect with the entrance of storage tank 5；
The outlet of the storage tank 5 is connect with the entrance of preheater 3；
The outlet of the preheater 3 is connect with the entrance of thin film evaporator 4.
Embodiment 3
A kind of device producing Fischer-Tropsch wax crude product, described device include reaction kettle 1, filter 2, storage tank 5, preheater 3,
Thin film evaporator 4, surge tank I 6, surge tank II 7；
The filter 2 is plate filter 2；
The outlet of the reaction kettle 1 is connect with the entrance of plate filter 2；
The outlet of the plate filter 2 is connect with the entrance of storage tank 5；
The outlet of the storage tank 5 is connect with the entrance of preheater 3；
The outlet of the preheater 3 is connect with the entrance of thin film evaporator 4；
The water of the thin film evaporator 4 and before distillate mouth and connect with the entrance of surge tank I 6；
The Fischer-Tropsch wax crude product outlet of the thin film evaporator 4 is connect with the entrance of surge tank II 7.
Application examples 1
A method of Fischer-Tropsch wax crude product being prepared using 3 described device of embodiment, the preparation method includes following step
It is rapid:
1. black wax is added in reaction kettle 1, melted at 130 DEG C, the carclazyte stirring for adding black wax weight 8% is de-
Color is filtered using plate filter 2, obtains the Fischer-Tropsch wax that fusing point is 90-105 DEG C；
2. step Fischer-Tropsch wax 110 DEG C of fusings in storage tank 5 that 1. gained fusing point is 90-105 DEG C are obtained liquid Fischer-Tropsch
Wax；
3. 2. step is added in thin film evaporator 4 after gained liquid Fischer-Tropsch wax improves temperature by preheater 3, film
The condition of evaporation are as follows: temperature is 180 DEG C, vacuum degree 50Pa, knifing rotating speed 120rpm, and condensation temperature is 70 DEG C, Leng Jingwen
Degree is 20 DEG C, and the water sloughed and before evaporating is temporarily stored in surge tank I 6, obtains Fischer-Tropsch wax crude product and is temporarily stored in surge tank II 7.
Claims (4)
1. a kind of device for producing Fischer-Tropsch wax crude product, it is characterised in that: described device include reaction kettle, filter, preheater,
Thin film evaporator；
The outlet of the reaction kettle and the entrance of filter connect；
The outlet of the filter and the entrance of preheater connect；
The outlet of the preheater and the entrance of thin film evaporator connect.
2. producing the device of Fischer-Tropsch wax crude product according to claim 1, it is characterised in that: the filter is plate-type filtering
Machine or frame filter.
3. producing the device of Fischer-Tropsch wax crude product according to claim 2, it is characterised in that: described device includes storage tank；
The outlet of the filter and the entrance of storage tank connect；
The outlet of the storage tank and the entrance of preheater connect.
4. according to claim 3 produce Fischer-Tropsch wax crude product device, it is characterised in that: described device include surge tank I,
Surge tank II；
The water of the thin film evaporator and before distillate mouth and connect with the entrance of surge tank I；
The Fischer-Tropsch wax crude product outlet of the thin film evaporator is connect with the entrance of surge tank II.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811645575.3A CN109486528A (en) | 2018-12-29 | 2018-12-29 | A kind of device producing Fischer-Tropsch wax crude product |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811645575.3A CN109486528A (en) | 2018-12-29 | 2018-12-29 | A kind of device producing Fischer-Tropsch wax crude product |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109486528A true CN109486528A (en) | 2019-03-19 |
Family
ID=65712106
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811645575.3A Pending CN109486528A (en) | 2018-12-29 | 2018-12-29 | A kind of device producing Fischer-Tropsch wax crude product |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109486528A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2005121280A1 (en) * | 2004-06-08 | 2005-12-22 | Shell Internationale Research Maatschappij B.V. | Process to make a base oil |
| CN101892073A (en) * | 2010-07-28 | 2010-11-24 | 广州市浩立生物科技有限公司 | Method for extracting base oil from cutting line oil |
| CN205953958U (en) * | 2016-07-19 | 2017-02-15 | 广州市海珥玛植物油脂有限公司 | Oil treatment system of one -level film second grade molecular distillation device |
| CN207143182U (en) * | 2017-05-05 | 2018-03-27 | 山西潞安精蜡化学品有限公司 | A kind of wax cutting device using three-stage distillation |
-
2018
- 2018-12-29 CN CN201811645575.3A patent/CN109486528A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2005121280A1 (en) * | 2004-06-08 | 2005-12-22 | Shell Internationale Research Maatschappij B.V. | Process to make a base oil |
| CN101892073A (en) * | 2010-07-28 | 2010-11-24 | 广州市浩立生物科技有限公司 | Method for extracting base oil from cutting line oil |
| CN205953958U (en) * | 2016-07-19 | 2017-02-15 | 广州市海珥玛植物油脂有限公司 | Oil treatment system of one -level film second grade molecular distillation device |
| CN207143182U (en) * | 2017-05-05 | 2018-03-27 | 山西潞安精蜡化学品有限公司 | A kind of wax cutting device using three-stage distillation |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN110506930B (en) | Starch-based high-stability Pickering emulsion and preparation method thereof | |
| CN102382552B (en) | Low temperature cured solvent-free epoxy anticorrosion paint and its preparation method | |
| CN105175962B (en) | A kind of chliorinated polyvinyl chloride is material modified | |
| Francis et al. | Hybrid hydrogel dispersed low fat and heat resistant chocolate | |
| CN109517626A (en) | A kind of preparation method of high-quality Fischer-Tropsch wax | |
| CN106750454A (en) | A kind of insulation one-way heat conduction polyimide film high and preparation method thereof | |
| CN109486528A (en) | A kind of device producing Fischer-Tropsch wax crude product | |
| CN109486525A (en) | A kind of preparation method of Fischer-Tropsch wax crude product | |
| CN103865194A (en) | Application of environment-friendly calcium-zinc stabilizer on heavy-caliber PVC tubular product and PVC tubular product prepared by using stabilizer | |
| CN102061139A (en) | Automobile hot-melt lamp adhesive | |
| CN109486524A (en) | A kind of device producing high-quality Fischer-Tropsch wax | |
| Agi et al. | Influence of ultrasonic on the flow behavior and disperse phase of cellulose nano-particles at fluid–fluid interface | |
| CN109294032B (en) | Multi-element composite filling particle modified heat-conducting PE composite material and preparation method thereof | |
| CN102382555A (en) | Solvent-free low-temperature solidified phenolic epoxy anticorrosive paint and preparation method thereof | |
| CN106833514B (en) | A kind of hot melt adhesive and preparation method thereof | |
| CN102206474A (en) | Solvent-based adhesive for CPVC (Chlorinated Polyvinyl Chloride) material | |
| CN110002959A (en) | Preparation method of L-menthol spherical crystal | |
| CN104194657B (en) | A kind of notebook glue of heatproof oil resistant is ordered and is used hot melt adhesive | |
| CN106085562A (en) | A kind of injection molding machine lubricating oil | |
| CN109735384A (en) | A kind of lamps and lanterns lubricating oil and preparation method thereof | |
| CN111534041B (en) | Modified POM material and preparation method thereof | |
| CN103421409A (en) | Polyaniline anti-corrosion paint and preparation method thereof | |
| CN103540260B (en) | A kind of Natural environment-friendlytung tung oil composite paint with antibacterial and preparation method thereof | |
| DE913846C (en) | Container closure sealing compound and container closures equipped with such as well as methods for introducing such mass into container closures | |
| CN108772534B (en) | Precoated sand and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190319 |
|
| RJ01 | Rejection of invention patent application after publication |